data_global _audit_creation_date 2018-06-25 _audit_creation_method ; Olex2 1.2-beta (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _shelxl_version_number 2013-4 _publ_requested_journal ; European Journal of Chemistry ; _publ_contact_author_name ; Ilkay Gumus ; _publ_contact_author_address ; Department of Chemistry, Faculty of Arts and Science, Mersin University, Mersin, TR 33343, Turkey ; _publ_contact_author_email ; ilkay.gumus@mersin.edu.tr ; _publ_contact_author_fax ; +903243610047 ; _publ_contact_author_phone ; +905385589656 ; _publ_section_title ; Synthesis, characterization and crystal structure of platinum(II) complexes with thiourea derivative ligands ; _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; data_cu_18_046_4brprpt3_0m_a _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C28 H36 Br2 N4 O2 Pt S2' _chemical_formula_sum 'C28 H36 Br2 N4 O2 Pt S2' _chemical_formula_weight 879.64 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pt' 'Pt' -4.5932 6.9264 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 15.7174(6) _cell_length_b 17.5696(6) _cell_length_c 25.3974(9) _cell_angle_alpha 80.253(2) _cell_angle_beta 85.604(2) _cell_angle_gamma 63.8880(10) _cell_volume 6206.7(4) _cell_formula_units_Z 8 _cell_measurement_reflns_used 9339 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 72.493 _cell_measurement_theta_min 3.103 _shelx_estimated_absorpt_T_max 0.305 _shelx_estimated_absorpt_T_min 0.203 _exptl_absorpt_coefficient_mu 12.990 _exptl_absorpt_correction_T_max 0.7536 _exptl_absorpt_correction_T_min 0.5047 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0953 before and 0.0670 after correction. The Ratio of minimum to maximum transmission is 0.6697. The \l/2 correction factor is Not present.' _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.883 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 3424 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.12 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0527 _diffrn_reflns_av_unetI/netI 0.0235 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 257871 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 73.243 _diffrn_reflns_theta_min 2.833 _diffrn_ambient_temperature 99.99 _diffrn_detector 'CMOS Area Detector' _diffrn_detector_area_resol_mean 10.24 _diffrn_detector_type 'Bruker PHOTON 100 CMOS' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device 'Bruker D8 VENTURE' _diffrn_measurement_device_type 'Bruker D8 VENTURE PHOTON 100 CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation.monochromator 'Multilayer mirror' _diffrn_radiation_probe X-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source ? _diffrn_source.source 'Microfocus sealed tube' _diffrn_source.type 'INCOATEC microfocus sealed tube' _diffrn_source_target Cu _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 18197 _reflns_number_total 24579 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT V8.38A (17, 2016)' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'SAINT V8.38A (17, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2015)' _refine_diff_density_max 1.558 _refine_diff_density_min -2.362 _refine_diff_density_rms 0.182 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1421 _refine_ls_number_reflns 24579 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0483 _refine_ls_R_factor_gt 0.0322 _refine_ls_restrained_S_all 1.053 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0364P)^2^+16.9215P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0743 _refine_ls_wR_factor_ref 0.0817 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C9(H9A,H9B), C10(H10A,H10B), C12(H12A,H12B), C13(H13A,H13B), C23(H23A,H23B), C24(H24A,H24B), C26(H26A,H26B), C27(H27A,H27B), C9B(H9BA,H9BB), C10B(H10G, H10H), C12B(H12G,H12H), C13B(H13G,H13H), C23B(H23G,H23H), C24B(H24G,H24H), C26B(H26G,H26H), C27B(H27G,H27H), C9A(H9AA,H9AB), C10A(H10E,H10F), C12A(H12E, H12F), C13A(H13E,H13F), C23A(H23E,H23F), C24A(H24E,H24F), C26A(H26E,H26F), C27A(H27E,H27F), C9C(H9CA,H9CB), C10C(H10C,H10D), C12C(H12C,H12D), C13C(H13C, H13D), C23C(H23C,H23D), C24C(H24C,H24D), C26C(H26C,H26D), C27C(H27C,H27D) 2.b Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C6(H6), C7(H7), C17(H17), C18(H18), C20(H20), C21(H21), C3B(H3B), C4B(H4B), C6B(H6B), C7B(H7B), C17B(H17B), C18B(H18B), C20B(H20B), C21B(H21B), C3A(H3A), C4A(H4A), C6A(H6A), C7A(H7A), C17A(H17A), C18A(H18A), C20A(H20A), C21A(H21A), C3C(H3C), C4C(H4C), C6C(H6C), C7C(H7C), C17C(H17C), C18C(H18C), C20C(H20C), C21C(H21C) 2.c Idealised Me refined as rotating group: C11(H11A,H11B,H11C), C14(H14A,H14B,H14C), C25(H25A,H25B,H25C), C28(H28A,H28B, H28C), C11B(H11J,H11K,H11L), C14B(H14J,H14K,H14L), C25B(H25J,H25K,H25L), C28B(H28J,H28K,H28L), C11A(H11G,H11H,H11I), C14A(H14G,H14H,H14I), C25A(H25G, H25H,H25I), C28A(H28G,H28H,H28I), C11C(H11D,H11E,H11F), C14C(H14D,H14E,H14F), C25C(H25D,H25E,H25F), C28C(H28D,H28E,H28F) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pt1 Pt 0.74507(2) 0.36220(2) 0.18402(2) 0.00720(5) Uani 1 1 d . . . . . Br1 Br 0.86282(4) 0.41957(3) -0.15076(2) 0.01650(11) Uani 1 1 d . . . . . Br2 Br 0.50231(4) 0.90387(3) 0.03806(2) 0.02238(12) Uani 1 1 d . . . . . S1 S 0.81806(8) 0.22057(7) 0.21010(4) 0.0115(2) Uani 1 1 d . . . . . S2 S 0.74721(9) 0.37985(7) 0.26896(4) 0.0156(2) Uani 1 1 d . . . . . O1 O 0.7453(2) 0.3518(2) 0.10628(12) 0.0135(7) Uani 1 1 d . . . . . O2 O 0.6790(2) 0.4889(2) 0.15601(12) 0.0120(7) Uani 1 1 d . . . . . N1 N 0.8530(3) 0.2074(3) 0.10195(14) 0.0091(8) Uani 1 1 d . . . . . N2 N 0.8942(3) 0.0859(2) 0.16151(14) 0.0085(8) Uani 1 1 d . . . . . N3 N 0.6458(2) 0.5543(2) 0.23352(14) 0.0103(8) Uani 1 1 d . . . . . N4 N 0.6480(2) 0.5078(2) 0.32264(14) 0.0113(7) Uani 1 1 d . . . . . C1 C 0.8019(3) 0.2891(3) 0.08302(17) 0.0081(9) Uani 1 1 d . . . . . C2 C 0.8117(3) 0.3151(3) 0.02407(17) 0.0089(9) Uani 1 1 d . . . . . C3 C 0.7476(4) 0.3959(3) -0.00024(18) 0.0146(10) Uani 1 1 d . . . . . H3 H 0.6950 0.4307 0.0195 0.018 Uiso 1 1 calc R . . . . C4 C 0.7604(3) 0.4259(3) -0.05332(18) 0.0126(10) Uani 1 1 d . . . . . H4 H 0.7158 0.4799 -0.0704 0.015 Uiso 1 1 calc R . . . . C5 C 0.8401(3) 0.3752(3) -0.08084(17) 0.0104(10) Uani 1 1 d . . . . . C6 C 0.9024(3) 0.2949(3) -0.05734(18) 0.0139(10) Uani 1 1 d . . . . . H6 H 0.9557 0.2606 -0.0768 0.017 Uiso 1 1 calc R . . . . C7 C 0.8875(3) 0.2643(3) -0.00531(17) 0.0120(10) Uani 1 1 d . . . . . H7 H 0.9295 0.2082 0.0104 0.014 Uiso 1 1 calc R . . . . C8 C 0.8550(3) 0.1715(3) 0.15327(17) 0.0089(9) Uani 1 1 d . . . . . C9 C 0.9385(3) 0.0348(3) 0.11820(17) 0.0093(9) Uani 1 1 d . . . . . H9A H 0.9942 -0.0181 0.1326 0.011 Uiso 1 1 calc R . . . . H9B H 0.9616 0.0680 0.0904 0.011 Uiso 1 1 calc R . . . . C10 C 0.8717(3) 0.0100(3) 0.09264(19) 0.0142(10) Uani 1 1 d . . . . . H10A H 0.8404 -0.0149 0.1209 0.017 Uiso 1 1 calc R . . . . H10B H 0.8220 0.0620 0.0726 0.017 Uiso 1 1 calc R . . . . C11 C 0.9243(4) -0.0544(3) 0.0551(2) 0.0197(11) Uani 1 1 d . . . . . H11A H 0.9570 -0.0306 0.0277 0.030 Uiso 1 1 calc GR . . . . H11B H 0.8791 -0.0670 0.0380 0.030 Uiso 1 1 calc GR . . . . H11C H 0.9708 -0.1073 0.0754 0.030 Uiso 1 1 calc GR . . . . C12 C 0.8973(3) 0.0354(3) 0.21466(18) 0.0114(9) Uani 1 1 d . . . . . H12A H 0.8903 -0.0166 0.2103 0.014 Uiso 1 1 calc R . . . . H12B H 0.8429 0.0699 0.2362 0.014 Uiso 1 1 calc R . . . . C13 C 0.9888(4) 0.0083(3) 0.24476(18) 0.0156(10) Uani 1 1 d . . . . . H13A H 0.9959 0.0599 0.2497 0.019 Uiso 1 1 calc R . . . . H13B H 1.0435 -0.0265 0.2236 0.019 Uiso 1 1 calc R . . . . C14 C 0.9876(4) -0.0442(3) 0.29951(18) 0.0170(10) Uani 1 1 d . . . . . H14A H 0.9788 -0.0944 0.2946 0.026 Uiso 1 1 calc GR . . . . H14B H 0.9354 -0.0086 0.3211 0.026 Uiso 1 1 calc GR . . . . H14C H 1.0478 -0.0630 0.3178 0.026 Uiso 1 1 calc GR . . . . C15 C 0.6519(3) 0.5526(3) 0.18170(18) 0.0105(9) Uani 1 1 d . . . . . C16 C 0.6187(3) 0.6376(3) 0.14713(18) 0.0096(9) Uani 1 1 d . . . . . C17 C 0.5801(3) 0.7133(3) 0.16991(18) 0.0173(10) Uani 1 1 d . . . . . H17 H 0.5768 0.7103 0.2077 0.021 Uiso 1 1 calc R . . . . C18 C 0.5467(3) 0.7924(3) 0.1375(2) 0.0209(10) Uani 1 1 d . . . . . H18 H 0.5198 0.8437 0.1529 0.025 Uiso 1 1 calc R . . . . C19 C 0.5528(3) 0.7961(3) 0.08283(19) 0.0158(10) Uani 1 1 d . . . . . C20 C 0.5919(4) 0.7217(3) 0.0596(2) 0.0201(11) Uani 1 1 d . . . . . H20 H 0.5958 0.7250 0.0218 0.024 Uiso 1 1 calc R . . . . C21 C 0.6248(3) 0.6429(3) 0.09190(19) 0.0158(10) Uani 1 1 d . . . . . H21 H 0.6519 0.5919 0.0762 0.019 Uiso 1 1 calc R . . . . C22 C 0.6751(3) 0.4865(3) 0.27342(17) 0.0089(9) Uani 1 1 d . . . . . C23 C 0.6744(3) 0.4442(3) 0.37126(17) 0.0131(9) Uani 1 1 d . . . . . H23A H 0.6920 0.3869 0.3616 0.016 Uiso 1 1 calc R . . . . H23B H 0.6188 0.4577 0.3954 0.016 Uiso 1 1 calc R . . . . C24 C 0.7562(4) 0.4413(4) 0.4008(2) 0.0265(12) Uani 1 1 d . . . . . H24A H 0.7360 0.4961 0.4146 0.032 Uiso 1 1 calc R . . . . H24B H 0.8094 0.4349 0.3756 0.032 Uiso 1 1 calc R . . . . C25 C 0.7904(4) 0.3673(4) 0.4473(2) 0.0230(11) Uani 1 1 d . . . . . H25A H 0.8210 0.3127 0.4334 0.034 Uiso 1 1 calc GR . . . . H25B H 0.7362 0.3688 0.4697 0.034 Uiso 1 1 calc GR . . . . H25C H 0.8360 0.3730 0.4688 0.034 Uiso 1 1 calc GR . . . . C26 C 0.5909(3) 0.5973(3) 0.32984(17) 0.0165(9) Uani 1 1 d . . . . . H26A H 0.5600 0.5989 0.3654 0.020 Uiso 1 1 calc R . . . . H26B H 0.5404 0.6247 0.3025 0.020 Uiso 1 1 calc R . . . . C27 C 0.6482(3) 0.6494(3) 0.32563(18) 0.0149(9) Uani 1 1 d . . . . . H27A H 0.6812 0.6466 0.2907 0.018 Uiso 1 1 calc R . . . . H27B H 0.6966 0.6246 0.3542 0.018 Uiso 1 1 calc R . . . . C28 C 0.5829(4) 0.7429(3) 0.3310(2) 0.0259(12) Uani 1 1 d . . . . . H28A H 0.5349 0.7673 0.3028 0.039 Uiso 1 1 calc GR . . . . H28B H 0.6203 0.7757 0.3277 0.039 Uiso 1 1 calc GR . . . . H28C H 0.5515 0.7455 0.3660 0.039 Uiso 1 1 calc GR . . . . Pt1B Pt 0.27556(2) -0.11779(2) 0.31721(2) 0.00886(5) Uani 1 1 d . . . . . Br1B Br 0.13938(4) -0.17039(3) 0.64948(2) 0.01639(11) Uani 1 1 d . . . . . Br2B Br 0.48337(4) -0.64807(4) 0.47970(3) 0.03836(16) Uani 1 1 d . . . . . S1B S 0.20505(8) 0.02377(7) 0.28994(4) 0.0125(2) Uani 1 1 d . . . . . S2B S 0.28102(10) -0.14024(8) 0.23252(5) 0.0201(3) Uani 1 1 d . . . . . O1B O 0.2722(2) -0.1053(2) 0.39504(12) 0.0142(7) Uani 1 1 d . . . . . O2B O 0.3362(3) -0.2443(2) 0.34767(13) 0.0154(7) Uani 1 1 d . . . . . N1B N 0.1591(3) 0.0375(3) 0.39755(14) 0.0114(8) Uani 1 1 d . . . . . N2B N 0.1196(3) 0.1598(2) 0.33749(14) 0.0097(8) Uani 1 1 d . . . . . N3B N 0.3318(3) -0.3110(3) 0.27584(16) 0.0189(9) Uani 1 1 d . . . . . N4B N 0.3200(3) -0.2748(3) 0.18625(16) 0.0251(10) Uani 1 1 d . . . . . C1B C 0.2116(3) -0.0431(3) 0.41762(18) 0.0101(9) Uani 1 1 d . . . . . C2B C 0.1990(3) -0.0679(3) 0.47538(18) 0.0104(9) Uani 1 1 d . . . . . C3B C 0.2634(3) -0.1471(3) 0.50176(17) 0.0103(9) Uani 1 1 d . . . . . H3B H 0.3186 -0.1812 0.4835 0.012 Uiso 1 1 calc R . . . . C4B C 0.2480(4) -0.1766(3) 0.55382(18) 0.0145(10) Uani 1 1 d . . . . . H4B H 0.2926 -0.2299 0.5717 0.017 Uiso 1 1 calc R . . . . C5B C 0.1654(4) -0.1265(3) 0.57983(17) 0.0118(10) Uani 1 1 d . . . . . C6B C 0.1004(4) -0.0464(3) 0.55509(17) 0.0124(10) Uani 1 1 d . . . . . H6B H 0.0446 -0.0129 0.5732 0.015 Uiso 1 1 calc R . . . . C7B C 0.1193(3) -0.0170(3) 0.50352(17) 0.0103(9) Uani 1 1 d . . . . . H7B H 0.0776 0.0386 0.4868 0.012 Uiso 1 1 calc R . . . . C8B C 0.1606(3) 0.0739(3) 0.34605(17) 0.0098(9) Uani 1 1 d . . . . . C9B C 0.0682(3) 0.2099(3) 0.38049(17) 0.0103(9) Uani 1 1 d . . . . . H9BA H 0.0445 0.1751 0.4067 0.012 Uiso 1 1 calc R . . . . H9BB H 0.0126 0.2618 0.3649 0.012 Uiso 1 1 calc R . . . . C10B C 0.1290(4) 0.2370(4) 0.4093(2) 0.0179(11) Uani 1 1 d . . . . . H10G H 0.1622 0.2628 0.3828 0.021 Uiso 1 1 calc R . . . . H10H H 0.1776 0.1860 0.4309 0.021 Uiso 1 1 calc R . . . . C11B C 0.0684(4) 0.3019(4) 0.4458(2) 0.0208(12) Uani 1 1 d . . . . . H11J H 0.0184 0.3511 0.4247 0.031 Uiso 1 1 calc GR . . . . H11K H 0.1082 0.3213 0.4623 0.031 Uiso 1 1 calc GR . . . . H11L H 0.0396 0.2749 0.4737 0.031 Uiso 1 1 calc GR . . . . C12B C 0.1189(3) 0.2109(3) 0.28534(17) 0.0102(9) Uani 1 1 d . . . . . H12G H 0.1758 0.1777 0.2649 0.012 Uiso 1 1 calc R . . . . H12H H 0.1228 0.2637 0.2910 0.012 Uiso 1 1 calc R . . . . C13B C 0.0304(3) 0.2360(3) 0.25216(17) 0.0117(9) Uani 1 1 d . . . . . H13G H 0.0275 0.1836 0.2449 0.014 Uiso 1 1 calc R . . . . H13H H -0.0270 0.2679 0.2727 0.014 Uiso 1 1 calc R . . . . C14B C 0.0322(4) 0.2917(3) 0.19936(19) 0.0189(11) Uani 1 1 d . . . . . H14J H 0.0858 0.2583 0.1777 0.028 Uiso 1 1 calc GR . . . . H14K H 0.0391 0.3418 0.2065 0.028 Uiso 1 1 calc GR . . . . H14L H -0.0271 0.3107 0.1800 0.028 Uiso 1 1 calc GR . . . . C15B C 0.3429(3) -0.3060(3) 0.32561(19) 0.0114(9) Uani 1 1 d . . . . . C16B C 0.3713(3) -0.3889(3) 0.3629(2) 0.0148(10) Uani 1 1 d . . . . . C17B C 0.3930(3) -0.4652(3) 0.3447(2) 0.0216(11) Uani 1 1 d . . . . . H17B H 0.3865 -0.4651 0.3077 0.026 Uiso 1 1 calc R . . . . C18B C 0.4239(4) -0.5421(3) 0.3795(2) 0.0263(12) Uani 1 1 d . . . . . H18B H 0.4385 -0.5942 0.3667 0.032 Uiso 1 1 calc R . . . . C19B C 0.4332(4) -0.5420(3) 0.4328(2) 0.0237(12) Uani 1 1 d . . . . . C20B C 0.4087(4) -0.4668(3) 0.4527(2) 0.0221(11) Uani 1 1 d . . . . . H20B H 0.4126 -0.4671 0.4899 0.027 Uiso 1 1 calc R . . . . C21B C 0.3781(4) -0.3906(3) 0.4172(2) 0.0177(10) Uani 1 1 d . . . . . H21B H 0.3615 -0.3384 0.4304 0.021 Uiso 1 1 calc R . . . . C22B C 0.3148(3) -0.2485(3) 0.23347(18) 0.0136(10) Uani 1 1 d . . . . . C23B C 0.3131(3) -0.2192(4) 0.13469(18) 0.0235(12) Uani 1 1 d . . . . . H23G H 0.3566 -0.2541 0.1087 0.028 Uiso 1 1 calc R . . . . H23H H 0.3336 -0.1750 0.1395 0.028 Uiso 1 1 calc R . . . . C24B C 0.2137(4) -0.1756(4) 0.11247(19) 0.0231(11) Uani 1 1 d . . . . . H24G H 0.1723 -0.1331 0.1354 0.028 Uiso 1 1 calc R . . . . H24H H 0.1891 -0.2189 0.1135 0.028 Uiso 1 1 calc R . . . . C25B C 0.2092(4) -0.1304(4) 0.0553(2) 0.0271(13) Uani 1 1 d . . . . . H25J H 0.2484 -0.1725 0.0322 0.041 Uiso 1 1 calc GR . . . . H25K H 0.2329 -0.0871 0.0540 0.041 Uiso 1 1 calc GR . . . . H25L H 0.1435 -0.1027 0.0428 0.041 Uiso 1 1 calc GR . . . . C26B C 0.3308(3) -0.3642(4) 0.1835(2) 0.0259(12) Uani 1 1 d . . . . . H26G H 0.2964 -0.3816 0.2138 0.031 Uiso 1 1 calc R . . . . H26H H 0.3023 -0.3637 0.1499 0.031 Uiso 1 1 calc R . . . . C27B C 0.4331(4) -0.4280(4) 0.1856(2) 0.0309(12) Uani 1 1 d . . . . . H27G H 0.4626 -0.4278 0.2186 0.037 Uiso 1 1 calc R . . . . H27H H 0.4675 -0.4125 0.1545 0.037 Uiso 1 1 calc R . . . . C28B C 0.4393(5) -0.5170(4) 0.1846(3) 0.0443(17) Uani 1 1 d . . . . . H28J H 0.4125 -0.5174 0.1511 0.066 Uiso 1 1 calc GR . . . . H28K H 0.4036 -0.5313 0.2149 0.066 Uiso 1 1 calc GR . . . . H28L H 0.5058 -0.5595 0.1873 0.066 Uiso 1 1 calc GR . . . . Pt1A Pt 0.72464(2) -0.13515(2) 0.18117(2) 0.00900(5) Uani 1 1 d . . . . . Br1A Br 0.86343(4) -0.07833(3) -0.14969(2) 0.01508(11) Uani 1 1 d . . . . . Br2A Br 0.51466(4) 0.39255(4) 0.01434(3) 0.03628(15) Uani 1 1 d . . . . . S1A S 0.79745(8) -0.27654(7) 0.20889(4) 0.0126(2) Uani 1 1 d . . . . . S2A S 0.71815(10) -0.11083(8) 0.26544(4) 0.0213(3) Uani 1 1 d . . . . . O1A O 0.7293(2) -0.1491(2) 0.10379(12) 0.0138(7) Uani 1 1 d . . . . . O2A O 0.6618(2) -0.0095(2) 0.15038(12) 0.0144(7) Uani 1 1 d . . . . . N1A N 0.8437(3) -0.2912(3) 0.10140(14) 0.0099(8) Uani 1 1 d . . . . . N2A N 0.8835(3) -0.4126(3) 0.16150(14) 0.0098(8) Uani 1 1 d . . . . . N3A N 0.6679(3) 0.0598(3) 0.22050(16) 0.0192(9) Uani 1 1 d . . . . . N4A N 0.6782(3) 0.0256(3) 0.31027(16) 0.0274(10) Uani 1 1 d . . . . . C1A C 0.7905(3) -0.2103(3) 0.08134(17) 0.0076(9) Uani 1 1 d . . . . . C2A C 0.8040(3) -0.1848(3) 0.02312(17) 0.0078(9) Uani 1 1 d . . . . . C3A C 0.7400(3) -0.1037(3) -0.00220(18) 0.0132(10) Uani 1 1 d . . . . . H3A H 0.6856 -0.0692 0.0165 0.016 Uiso 1 1 calc R . . . . C4A C 0.7562(3) -0.0738(3) -0.05446(17) 0.0108(9) Uani 1 1 d . . . . . H4A H 0.7122 -0.0198 -0.0720 0.013 Uiso 1 1 calc R . . . . C5A C 0.8370(3) -0.1235(3) -0.08063(17) 0.0097(9) Uani 1 1 d . . . . . C6A C 0.8996(3) -0.2040(3) -0.05660(18) 0.0120(10) Uani 1 1 d . . . . . H6A H 0.9544 -0.2378 -0.0753 0.014 Uiso 1 1 calc R . . . . C7A C 0.8820(3) -0.2349(3) -0.00516(17) 0.0113(10) Uani 1 1 d . . . . . H7A H 0.9236 -0.2910 0.0109 0.014 Uiso 1 1 calc R . . . . C8A C 0.8419(3) -0.3265(3) 0.15271(17) 0.0087(9) Uani 1 1 d . . . . . C9A C 0.9354(3) -0.4641(3) 0.11954(18) 0.0112(10) Uani 1 1 d . . . . . H9AA H 0.9913 -0.5150 0.1357 0.013 Uiso 1 1 calc R . . . . H9AB H 0.9588 -0.4296 0.0928 0.013 Uiso 1 1 calc R . . . . C10A C 0.8763(4) -0.4935(4) 0.0914(2) 0.0179(11) Uani 1 1 d . . . . . H10E H 0.8273 -0.4434 0.0695 0.021 Uiso 1 1 calc R . . . . H10F H 0.8436 -0.5192 0.1183 0.021 Uiso 1 1 calc R . . . . C11A C 0.9373(4) -0.5592(4) 0.0556(2) 0.0224(12) Uani 1 1 d . . . . . H11G H 0.9738 -0.5356 0.0309 0.034 Uiso 1 1 calc GR . . . . H11H H 0.8965 -0.5727 0.0353 0.034 Uiso 1 1 calc GR . . . . H11I H 0.9808 -0.6116 0.0778 0.034 Uiso 1 1 calc GR . . . . C12A C 0.8827(3) -0.4632(3) 0.21392(17) 0.0099(9) Uani 1 1 d . . . . . H12E H 0.8787 -0.5160 0.2084 0.012 Uiso 1 1 calc R . . . . H12F H 0.8254 -0.4295 0.2339 0.012 Uiso 1 1 calc R . . . . C13A C 0.9696(3) -0.4877(3) 0.24704(18) 0.0138(10) Uani 1 1 d . . . . . H13E H 0.9721 -0.4351 0.2542 0.017 Uiso 1 1 calc R . . . . H13F H 1.0272 -0.5195 0.2267 0.017 Uiso 1 1 calc R . . . . C14A C 0.9683(4) -0.5432(3) 0.29982(18) 0.0179(11) Uani 1 1 d . . . . . H14G H 0.9654 -0.5952 0.2928 0.027 Uiso 1 1 calc GR . . . . H14H H 0.9127 -0.5110 0.3207 0.027 Uiso 1 1 calc GR . . . . H14I H 1.0260 -0.5592 0.3199 0.027 Uiso 1 1 calc GR . . . . C15A C 0.6553(3) 0.0544(3) 0.17108(19) 0.0137(10) Uani 1 1 d . . . . . C16A C 0.6265(3) 0.1357(3) 0.13270(19) 0.0134(10) Uani 1 1 d . . . . . C17A C 0.6103(3) 0.2128(3) 0.1498(2) 0.0209(11) Uani 1 1 d . . . . . H17A H 0.6209 0.2128 0.1861 0.025 Uiso 1 1 calc R . . . . C18A C 0.5791(4) 0.2885(3) 0.1146(2) 0.0258(12) Uani 1 1 d . . . . . H18A H 0.5675 0.3406 0.1265 0.031 Uiso 1 1 calc R . . . . C19A C 0.5650(3) 0.2875(3) 0.0621(2) 0.0230(11) Uani 1 1 d . . . . . C20A C 0.5828(3) 0.2120(3) 0.0432(2) 0.0189(10) Uani 1 1 d . . . . . H20A H 0.5735 0.2123 0.0066 0.023 Uiso 1 1 calc R . . . . C21A C 0.6146(3) 0.1361(3) 0.07916(19) 0.0152(10) Uani 1 1 d . . . . . H21A H 0.6284 0.0838 0.0668 0.018 Uiso 1 1 calc R . . . . C22A C 0.6850(3) -0.0030(3) 0.26335(19) 0.0173(11) Uani 1 1 d . . . . . C23A C 0.6829(4) -0.0285(4) 0.36245(19) 0.0282(13) Uani 1 1 d . . . . . H23E H 0.6631 -0.0732 0.3579 0.034 Uiso 1 1 calc R . . . . H23F H 0.6383 0.0074 0.3877 0.034 Uiso 1 1 calc R . . . . C24A C 0.7817(4) -0.0708(4) 0.3856(2) 0.0280(12) Uani 1 1 d . . . . . H24E H 0.8059 -0.0272 0.3844 0.034 Uiso 1 1 calc R . . . . H24F H 0.8243 -0.1142 0.3635 0.034 Uiso 1 1 calc R . . . . C25A C 0.7828(4) -0.1141(4) 0.4434(2) 0.0305(14) Uani 1 1 d . . . . . H25G H 0.7456 -0.1470 0.4461 0.046 Uiso 1 1 calc GR . . . . H25H H 0.7554 -0.0702 0.4669 0.046 Uiso 1 1 calc GR . . . . H25I H 0.8483 -0.1527 0.4543 0.046 Uiso 1 1 calc GR . . . . C26A C 0.6688(4) 0.1164(4) 0.3116(2) 0.0287(12) Uani 1 1 d . . . . . H26E H 0.6967 0.1170 0.3451 0.034 Uiso 1 1 calc R . . . . H26F H 0.7041 0.1323 0.2812 0.034 Uiso 1 1 calc R . . . . C27A C 0.5668(4) 0.1802(4) 0.3085(2) 0.0347(13) Uani 1 1 d . . . . . H27E H 0.5318 0.1667 0.3399 0.042 Uiso 1 1 calc R . . . . H27F H 0.5377 0.1782 0.2759 0.042 Uiso 1 1 calc R . . . . C28A C 0.5616(5) 0.2683(4) 0.3071(3) 0.051(2) Uani 1 1 d . . . . . H28G H 0.5910 0.2835 0.2741 0.076 Uiso 1 1 calc GR . . . . H28H H 0.5953 0.2684 0.3380 0.076 Uiso 1 1 calc GR . . . . H28I H 0.4952 0.3102 0.3083 0.076 Uiso 1 1 calc GR . . . . Pt1C Pt 0.25436(2) 0.39054(2) 0.31721(2) 0.00672(5) Uani 1 1 d . . . . . Br1C Br 0.13494(4) 0.33022(3) 0.65107(2) 0.01515(11) Uani 1 1 d . . . . . Br2C Br 0.50095(4) -0.14808(3) 0.46783(2) 0.02194(12) Uani 1 1 d . . . . . S1C S 0.17899(8) 0.53177(7) 0.29096(4) 0.0112(2) Uani 1 1 d . . . . . S2C S 0.25326(9) 0.37168(7) 0.23239(4) 0.0156(2) Uani 1 1 d . . . . . O1C O 0.2540(2) 0.4015(2) 0.39526(12) 0.0137(7) Uani 1 1 d . . . . . O2C O 0.3228(2) 0.2640(2) 0.34580(12) 0.0132(7) Uani 1 1 d . . . . . N1C N 0.1450(3) 0.5451(3) 0.39935(14) 0.0097(8) Uani 1 1 d . . . . . N2C N 0.1042(3) 0.6673(2) 0.33866(14) 0.0090(8) Uani 1 1 d . . . . . N3C N 0.3523(3) 0.1977(2) 0.26905(14) 0.0104(8) Uani 1 1 d . . . . . N4C N 0.3508(3) 0.2431(2) 0.18003(14) 0.0136(8) Uani 1 1 d . . . . . C1C C 0.1962(3) 0.4637(3) 0.41853(17) 0.0093(9) Uani 1 1 d . . . . . C2C C 0.1864(3) 0.4377(3) 0.47670(17) 0.0090(9) Uani 1 1 d . . . . . C3C C 0.2500(3) 0.3557(3) 0.50091(17) 0.0098(9) Uani 1 1 d . . . . . H3C H 0.3029 0.3213 0.4813 0.012 Uiso 1 1 calc R . . . . C4C C 0.2362(3) 0.3248(3) 0.55330(17) 0.0120(10) Uani 1 1 d . . . . . H4C H 0.2795 0.2698 0.5698 0.014 Uiso 1 1 calc R . . . . C5C C 0.1573(3) 0.3763(3) 0.58132(17) 0.0104(9) Uani 1 1 d . . . . . C6C C 0.0956(3) 0.4580(3) 0.55856(17) 0.0114(10) Uani 1 1 d . . . . . H6C H 0.0429 0.4925 0.5783 0.014 Uiso 1 1 calc R . . . . C7C C 0.1115(3) 0.4890(3) 0.50673(17) 0.0101(9) Uani 1 1 d . . . . . H7C H 0.0709 0.5459 0.4915 0.012 Uiso 1 1 calc R . . . . C8C C 0.1429(3) 0.5813(3) 0.34779(18) 0.0096(9) Uani 1 1 d . . . . . C9C C 0.0590(3) 0.7186(3) 0.38195(17) 0.0092(9) Uani 1 1 d . . . . . H9CA H 0.0371 0.6850 0.4102 0.011 Uiso 1 1 calc R . . . . H9CB H 0.0027 0.7709 0.3676 0.011 Uiso 1 1 calc R . . . . C10C C 0.1258(3) 0.7447(3) 0.40658(19) 0.0151(10) Uani 1 1 d . . . . . H10C H 0.1763 0.6933 0.4266 0.018 Uiso 1 1 calc R . . . . H10D H 0.1561 0.7700 0.3779 0.018 Uiso 1 1 calc R . . . . C11C C 0.0723(4) 0.8097(3) 0.4441(2) 0.0202(11) Uani 1 1 d . . . . . H11D H 0.0190 0.8584 0.4250 0.030 Uiso 1 1 calc GR . . . . H11E H 0.1150 0.8298 0.4567 0.030 Uiso 1 1 calc GR . . . . H11F H 0.0483 0.7826 0.4747 0.030 Uiso 1 1 calc GR . . . . C12C C 0.1006(3) 0.7177(3) 0.28575(17) 0.0100(9) Uani 1 1 d . . . . . H12C H 0.1556 0.6836 0.2644 0.012 Uiso 1 1 calc R . . . . H12D H 0.1067 0.7700 0.2902 0.012 Uiso 1 1 calc R . . . . C13C C 0.0101(3) 0.7442(3) 0.25480(17) 0.0117(9) Uani 1 1 d . . . . . H13C H 0.0036 0.6924 0.2497 0.014 Uiso 1 1 calc R . . . . H13D H -0.0453 0.7791 0.2755 0.014 Uiso 1 1 calc R . . . . C14C C 0.0120(4) 0.7958(3) 0.20072(19) 0.0187(11) Uani 1 1 d . . . . . H14D H 0.0632 0.7595 0.1789 0.028 Uiso 1 1 calc GR . . . . H14E H 0.0226 0.8450 0.2056 0.028 Uiso 1 1 calc GR . . . . H14F H -0.0487 0.8161 0.1827 0.028 Uiso 1 1 calc GR . . . . C15C C 0.3482(3) 0.2010(3) 0.32080(18) 0.0083(9) Uani 1 1 d . . . . . C16C C 0.3821(3) 0.1158(3) 0.35596(17) 0.0093(9) Uani 1 1 d . . . . . C17C C 0.4138(3) 0.0401(3) 0.33479(18) 0.0149(10) Uani 1 1 d . . . . . H17C H 0.4127 0.0421 0.2972 0.018 Uiso 1 1 calc R . . . . C18C C 0.4472(4) -0.0388(3) 0.36779(19) 0.0191(11) Uani 1 1 d . . . . . H18C H 0.4679 -0.0905 0.3531 0.023 Uiso 1 1 calc R . . . . C19C C 0.4498(3) -0.0408(3) 0.42215(19) 0.0135(10) Uani 1 1 d . . . . . C20C C 0.4166(3) 0.0336(3) 0.4449(2) 0.0159(10) Uani 1 1 d . . . . . H20C H 0.4163 0.0311 0.4826 0.019 Uiso 1 1 calc R . . . . C21C C 0.3836(3) 0.1118(3) 0.41129(18) 0.0132(10) Uani 1 1 d . . . . . H21C H 0.3618 0.1633 0.4262 0.016 Uiso 1 1 calc R . . . . C22C C 0.3237(3) 0.2641(3) 0.22904(18) 0.0109(9) Uani 1 1 d . . . . . C23C C 0.3248(3) 0.3055(3) 0.13067(17) 0.0145(9) Uani 1 1 d . . . . . H23C H 0.3816 0.2928 0.1075 0.017 Uiso 1 1 calc R . . . . H23D H 0.3045 0.3636 0.1399 0.017 Uiso 1 1 calc R . . . . C24C C 0.2468(4) 0.3057(4) 0.0997(2) 0.0301(13) Uani 1 1 d . . . . . H24C H 0.1916 0.3133 0.1235 0.036 Uiso 1 1 calc R . . . . H24D H 0.2689 0.2496 0.0871 0.036 Uiso 1 1 calc R . . . . C25C C 0.2164(4) 0.3771(4) 0.0519(2) 0.0247(12) Uani 1 1 d . . . . . H25D H 0.1710 0.3713 0.0303 0.037 Uiso 1 1 calc GR . . . . H25E H 0.2720 0.3730 0.0301 0.037 Uiso 1 1 calc GR . . . . H25F H 0.1865 0.4328 0.0644 0.037 Uiso 1 1 calc GR . . . . C26C C 0.4078(3) 0.1521(3) 0.17397(18) 0.0164(9) Uani 1 1 d . . . . . H26C H 0.4574 0.1251 0.2019 0.020 Uiso 1 1 calc R . . . . H26D H 0.4399 0.1492 0.1388 0.020 Uiso 1 1 calc R . . . . C27C C 0.3506(3) 0.1011(3) 0.17808(18) 0.0150(9) Uani 1 1 d . . . . . H27C H 0.3036 0.1251 0.1488 0.018 Uiso 1 1 calc R . . . . H27D H 0.3158 0.1057 0.2125 0.018 Uiso 1 1 calc R . . . . C28C C 0.4156(4) 0.0065(3) 0.1745(2) 0.0252(12) Uani 1 1 d . . . . . H28D H 0.4463 0.0017 0.1394 0.038 Uiso 1 1 calc GR . . . . H28E H 0.3779 -0.0262 0.1795 0.038 Uiso 1 1 calc GR . . . . H28F H 0.4640 -0.0164 0.2025 0.038 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pt1 0.00963(9) 0.00365(9) 0.00568(9) -0.00062(6) 0.00007(6) -0.00055(7) Br1 0.0252(3) 0.0182(3) 0.0074(2) 0.0035(2) -0.00181(19) -0.0122(2) Br2 0.0185(2) 0.0095(2) 0.0315(3) 0.0090(2) -0.0068(2) -0.00229(19) S1 0.0185(6) 0.0049(5) 0.0072(5) -0.0005(4) -0.0008(4) -0.0018(4) S2 0.0256(6) 0.0063(5) 0.0082(5) -0.0010(4) -0.0043(4) -0.0003(4) O1 0.0159(17) 0.0100(17) 0.0081(15) -0.0017(13) -0.0029(12) 0.0008(13) O2 0.0179(17) 0.0030(15) 0.0089(15) 0.0004(12) -0.0001(12) 0.0005(13) N1 0.0110(19) 0.008(2) 0.0057(17) 0.0007(15) 0.0019(14) -0.0032(15) N2 0.0095(18) 0.0054(19) 0.0096(18) -0.0019(15) 0.0031(14) -0.0027(15) N3 0.0065(17) 0.0098(18) 0.0134(18) -0.0045(15) -0.0011(14) -0.0011(14) N4 0.0109(18) 0.0098(18) 0.0115(18) -0.0028(14) -0.0025(14) -0.0022(14) C1 0.008(2) 0.008(2) 0.009(2) -0.0037(17) -0.0004(16) -0.0030(17) C2 0.011(2) 0.008(2) 0.008(2) -0.0003(18) -0.0017(17) -0.0046(18) C3 0.016(2) 0.013(3) 0.013(2) -0.0013(19) -0.0009(18) -0.004(2) C4 0.013(2) 0.009(2) 0.011(2) 0.0031(19) -0.0073(18) -0.0022(19) C5 0.020(3) 0.011(2) 0.006(2) 0.0003(18) -0.0011(18) -0.012(2) C6 0.015(3) 0.014(3) 0.011(2) -0.005(2) -0.0003(18) -0.004(2) C7 0.013(2) 0.014(3) 0.008(2) -0.0031(19) -0.0004(17) -0.006(2) C8 0.006(2) 0.009(2) 0.012(2) -0.0016(18) 0.0002(16) -0.0041(17) C9 0.010(2) 0.004(2) 0.009(2) -0.0003(18) 0.0007(17) 0.0016(17) C10 0.010(2) 0.015(3) 0.018(2) -0.007(2) 0.0012(18) -0.005(2) C11 0.021(3) 0.018(3) 0.023(3) -0.008(2) 0.003(2) -0.010(2) C12 0.012(2) 0.006(2) 0.014(2) -0.0011(18) 0.0031(17) -0.0021(17) C13 0.024(3) 0.011(2) 0.010(2) 0.0002(18) -0.0010(18) -0.007(2) C14 0.025(3) 0.011(2) 0.011(2) 0.0039(18) 0.0003(18) -0.006(2) C15 0.002(2) 0.015(2) 0.013(2) -0.0045(18) 0.0033(16) -0.0016(17) C16 0.0028(19) 0.007(2) 0.017(2) -0.0026(17) -0.0016(16) 0.0004(16) C17 0.022(3) 0.010(2) 0.017(2) -0.0009(18) -0.0089(18) -0.0030(19) C18 0.022(3) 0.008(2) 0.027(3) -0.0018(19) -0.009(2) -0.0008(19) C19 0.011(2) 0.010(2) 0.021(2) 0.0086(19) -0.0080(18) -0.0018(18) C20 0.016(2) 0.013(2) 0.018(2) 0.0065(19) 0.0049(19) 0.0013(19) C21 0.011(2) 0.012(2) 0.017(2) -0.0023(19) 0.0032(17) 0.0018(18) C22 0.007(2) 0.006(2) 0.012(2) 0.0003(16) -0.0033(15) -0.0018(16) C23 0.014(2) 0.021(2) 0.008(2) -0.0030(18) 0.0005(16) -0.0104(19) C24 0.028(3) 0.025(3) 0.029(3) 0.006(2) -0.014(2) -0.015(2) C25 0.022(3) 0.020(3) 0.023(3) 0.002(2) -0.006(2) -0.007(2) C26 0.017(2) 0.020(2) 0.013(2) -0.0046(18) 0.0034(17) -0.0079(19) C27 0.014(2) 0.014(2) 0.018(2) -0.0031(18) -0.0012(17) -0.0066(18) C28 0.033(3) 0.015(3) 0.030(3) -0.012(2) 0.005(2) -0.009(2) Pt1B 0.01303(10) 0.00579(9) 0.00655(9) -0.00127(7) 0.00055(6) -0.00297(7) Br1B 0.0248(3) 0.0164(3) 0.0078(2) 0.0030(2) -0.00061(19) -0.0104(2) Br2B 0.0251(3) 0.0148(3) 0.0686(4) 0.0194(3) -0.0190(3) -0.0086(2) S1B 0.0213(6) 0.0071(5) 0.0066(5) -0.0004(4) -0.0012(4) -0.0041(4) S2B 0.0392(8) 0.0119(6) 0.0095(5) -0.0029(4) 0.0000(5) -0.0111(5) O1B 0.0188(17) 0.0073(16) 0.0091(15) -0.0013(12) -0.0025(12) 0.0015(13) O2B 0.0216(18) 0.0111(17) 0.0117(16) -0.0024(13) 0.0016(13) -0.0056(14) N1B 0.015(2) 0.008(2) 0.0078(18) 0.0022(15) -0.0031(14) -0.0037(16) N2B 0.0112(19) 0.0069(19) 0.0092(18) -0.0019(15) 0.0021(14) -0.0023(15) N3B 0.019(2) 0.012(2) 0.019(2) -0.0051(16) -0.0061(16) 0.0016(16) N4B 0.026(2) 0.022(2) 0.018(2) -0.0095(18) -0.0043(17) 0.0009(18) C1B 0.008(2) 0.010(2) 0.013(2) -0.0038(18) -0.0024(16) -0.0032(18) C2B 0.013(2) 0.008(2) 0.011(2) -0.0024(18) -0.0055(17) -0.0049(18) C3B 0.006(2) 0.007(2) 0.011(2) 0.0024(17) -0.0010(16) 0.0019(17) C4B 0.016(2) 0.011(2) 0.014(2) 0.0028(19) -0.0043(18) -0.0048(19) C5B 0.020(3) 0.014(3) 0.005(2) 0.0010(18) -0.0031(18) -0.011(2) C6B 0.019(3) 0.010(2) 0.009(2) -0.0019(19) -0.0018(18) -0.006(2) C7B 0.013(2) 0.004(2) 0.007(2) 0.0009(17) -0.0038(17) 0.0012(18) C8B 0.006(2) 0.010(2) 0.011(2) -0.0032(18) -0.0013(16) -0.0007(17) C9B 0.010(2) 0.011(2) 0.008(2) -0.0046(18) 0.0035(17) -0.0026(18) C10B 0.018(3) 0.023(3) 0.019(2) -0.011(2) 0.003(2) -0.012(2) C11B 0.023(3) 0.019(3) 0.023(3) -0.011(2) 0.004(2) -0.009(2) C12B 0.014(2) 0.008(2) 0.008(2) 0.0003(17) 0.0023(16) -0.0053(17) C13B 0.015(2) 0.008(2) 0.011(2) 0.0024(17) 0.0011(17) -0.0056(18) C14B 0.025(3) 0.016(3) 0.013(2) 0.002(2) -0.0030(19) -0.008(2) C15B 0.005(2) 0.007(2) 0.018(2) -0.0031(18) -0.0003(17) 0.0016(17) C16B 0.008(2) 0.009(2) 0.023(2) -0.0010(19) -0.0010(18) -0.0009(18) C17B 0.015(2) 0.012(2) 0.035(3) -0.002(2) -0.014(2) -0.0018(19) C18B 0.018(3) 0.010(2) 0.052(4) -0.003(2) -0.012(2) -0.005(2) C19B 0.013(2) 0.008(2) 0.044(3) 0.013(2) -0.010(2) -0.0038(19) C20B 0.014(2) 0.015(3) 0.026(3) 0.003(2) 0.001(2) 0.002(2) C21B 0.013(2) 0.006(2) 0.025(3) 0.0019(19) 0.0032(19) 0.0021(18) C22B 0.010(2) 0.014(2) 0.014(2) -0.0058(18) 0.0003(17) -0.0010(18) C23B 0.017(2) 0.037(3) 0.013(2) -0.014(2) 0.0037(18) -0.007(2) C24B 0.025(3) 0.028(3) 0.020(2) -0.001(2) -0.004(2) -0.016(2) C25B 0.029(3) 0.030(3) 0.026(3) 0.003(2) -0.009(2) -0.017(3) C26B 0.015(2) 0.041(3) 0.025(3) -0.005(2) 0.002(2) -0.016(2) C27B 0.022(3) 0.033(3) 0.039(3) -0.018(3) 0.004(2) -0.009(2) C28B 0.040(4) 0.029(4) 0.068(5) -0.026(3) 0.013(3) -0.014(3) Pt1A 0.01354(10) 0.00753(9) 0.00564(9) -0.00120(7) 0.00045(6) -0.00434(7) Br1A 0.0192(3) 0.0198(3) 0.0076(2) 0.0027(2) -0.00006(19) -0.0114(2) Br2A 0.0302(3) 0.0130(3) 0.0609(4) 0.0147(3) -0.0192(3) -0.0093(2) S1A 0.0202(6) 0.0083(5) 0.0065(5) 0.0003(4) -0.0007(4) -0.0043(4) S2A 0.0433(8) 0.0160(6) 0.0068(5) -0.0024(4) 0.0003(5) -0.0147(6) O1A 0.0176(17) 0.0124(17) 0.0077(15) -0.0006(13) 0.0003(12) -0.0033(14) O2A 0.0219(18) 0.0088(17) 0.0114(15) -0.0026(13) 0.0006(13) -0.0055(14) N1A 0.0129(19) 0.012(2) 0.0047(17) 0.0000(15) -0.0003(14) -0.0061(16) N2A 0.0106(19) 0.008(2) 0.0092(18) -0.0008(15) 0.0007(14) -0.0026(15) N3A 0.022(2) 0.012(2) 0.017(2) -0.0056(16) -0.0081(16) 0.0009(17) N4A 0.032(3) 0.021(2) 0.017(2) -0.0096(18) -0.0080(18) 0.0036(19) C1A 0.009(2) 0.007(2) 0.008(2) -0.0027(17) -0.0006(16) -0.0038(17) C2A 0.009(2) 0.009(2) 0.006(2) 0.0014(17) -0.0023(16) -0.0053(18) C3A 0.012(2) 0.017(3) 0.010(2) -0.005(2) 0.0009(17) -0.0047(19) C4A 0.011(2) 0.009(2) 0.009(2) 0.0024(18) -0.0043(17) -0.0016(18) C5A 0.017(2) 0.012(2) 0.006(2) -0.0007(18) -0.0010(17) -0.013(2) C6A 0.011(2) 0.013(3) 0.010(2) -0.0024(19) 0.0005(18) -0.0030(19) C7A 0.014(2) 0.013(3) 0.009(2) -0.0042(19) 0.0021(17) -0.007(2) C8A 0.006(2) 0.011(2) 0.009(2) 0.0001(17) -0.0015(15) -0.0035(17) C9A 0.012(2) 0.008(2) 0.011(2) -0.0013(18) 0.0003(18) -0.0016(18) C10A 0.015(3) 0.022(3) 0.018(2) -0.007(2) 0.001(2) -0.009(2) C11A 0.030(3) 0.020(3) 0.022(3) -0.009(2) 0.007(2) -0.014(2) C12A 0.009(2) 0.008(2) 0.009(2) 0.0016(17) 0.0020(16) -0.0024(17) C13A 0.015(2) 0.015(2) 0.009(2) 0.0010(18) -0.0009(17) -0.0057(19) C14A 0.029(3) 0.014(3) 0.009(2) 0.0038(19) -0.0011(19) -0.010(2) C15A 0.002(2) 0.016(3) 0.019(2) -0.007(2) 0.0025(17) 0.0004(18) C16A 0.002(2) 0.010(2) 0.024(2) -0.0028(19) -0.0001(17) 0.0007(17) C17A 0.013(2) 0.015(2) 0.033(3) -0.002(2) -0.009(2) -0.0034(19) C18A 0.018(3) 0.013(2) 0.044(3) -0.003(2) -0.011(2) -0.004(2) C19A 0.011(2) 0.008(2) 0.043(3) 0.008(2) -0.005(2) -0.0011(18) C20A 0.013(2) 0.016(3) 0.023(3) 0.002(2) 0.0016(19) -0.0045(19) C21A 0.013(2) 0.009(2) 0.020(2) -0.0035(19) 0.0061(18) -0.0021(18) C22A 0.009(2) 0.022(3) 0.016(2) -0.008(2) -0.0037(18) -0.0009(19) C23A 0.022(3) 0.039(3) 0.012(2) -0.011(2) -0.0041(19) 0.000(2) C24A 0.029(3) 0.030(3) 0.025(3) -0.001(2) -0.007(2) -0.013(2) C25A 0.034(3) 0.041(4) 0.025(3) -0.004(3) -0.004(2) -0.024(3) C26A 0.021(3) 0.050(4) 0.019(3) -0.003(2) 0.000(2) -0.019(3) C27A 0.020(3) 0.042(3) 0.044(3) -0.019(3) 0.005(2) -0.012(2) C28A 0.048(4) 0.037(4) 0.075(5) -0.039(4) 0.022(4) -0.018(3) Pt1C 0.00903(9) 0.00357(9) 0.00500(8) -0.00074(6) 0.00036(6) -0.00043(7) Br1C 0.0195(3) 0.0196(3) 0.0072(2) 0.0026(2) 0.00032(19) -0.0111(2) Br2C 0.0242(3) 0.0094(2) 0.0273(3) 0.0079(2) -0.0097(2) -0.0051(2) S1C 0.0183(6) 0.0051(5) 0.0064(5) -0.0005(4) -0.0005(4) -0.0017(4) S2C 0.0260(6) 0.0068(5) 0.0069(5) -0.0011(4) -0.0039(4) 0.0001(4) O1C 0.0184(17) 0.0096(17) 0.0055(14) -0.0010(12) -0.0006(12) 0.0006(13) O2C 0.0185(17) 0.0080(17) 0.0093(15) -0.0030(13) 0.0009(12) -0.0017(13) N1C 0.0119(19) 0.009(2) 0.0070(17) -0.0008(15) 0.0003(14) -0.0039(15) N2C 0.0120(19) 0.0028(18) 0.0084(17) 0.0000(15) 0.0025(14) -0.0005(14) N3C 0.0114(18) 0.0068(18) 0.0129(18) -0.0008(14) -0.0010(14) -0.0038(14) N4C 0.0163(19) 0.0136(19) 0.0117(18) -0.0029(15) 0.0022(14) -0.0072(16) C1C 0.009(2) 0.010(2) 0.009(2) -0.0020(18) -0.0015(16) -0.0038(17) C2C 0.012(2) 0.008(2) 0.009(2) -0.0040(18) -0.0016(17) -0.0049(18) C3C 0.008(2) 0.006(2) 0.011(2) -0.0007(18) 0.0003(16) 0.0006(17) C4C 0.015(2) 0.011(2) 0.009(2) 0.0019(18) -0.0009(18) -0.0059(19) C5C 0.015(2) 0.013(2) 0.005(2) -0.0008(18) -0.0009(17) -0.008(2) C6C 0.014(2) 0.012(3) 0.007(2) -0.0024(19) 0.0020(17) -0.0047(19) C7C 0.011(2) 0.004(2) 0.010(2) 0.0029(17) -0.0054(17) 0.0016(18) C8C 0.006(2) 0.008(2) 0.012(2) -0.0038(18) -0.0002(16) -0.0001(16) C9C 0.010(2) 0.009(2) 0.007(2) -0.0026(18) 0.0010(17) -0.0030(18) C10C 0.014(2) 0.016(3) 0.018(2) -0.010(2) 0.0045(19) -0.008(2) C11C 0.027(3) 0.016(3) 0.023(3) -0.011(2) 0.000(2) -0.011(2) C12C 0.015(2) 0.007(2) 0.0055(19) 0.0000(17) 0.0024(16) -0.0032(17) C13C 0.015(2) 0.007(2) 0.010(2) 0.0033(17) -0.0011(16) -0.0040(17) C14C 0.025(3) 0.013(2) 0.014(2) 0.0012(19) 0.0009(19) -0.005(2) C15C 0.004(2) 0.003(2) 0.017(2) -0.0018(17) -0.0014(16) -0.0002(16) C16C 0.008(2) 0.009(2) 0.012(2) -0.0027(17) 0.0005(16) -0.0039(17) C17C 0.019(2) 0.011(2) 0.013(2) 0.0003(17) -0.0082(18) -0.0045(19) C18C 0.027(3) 0.003(2) 0.024(3) -0.0018(18) -0.011(2) -0.0024(19) C19C 0.012(2) 0.008(2) 0.020(2) 0.0069(18) -0.0071(18) -0.0052(18) C20C 0.012(2) 0.011(2) 0.018(2) -0.0016(19) 0.0018(18) 0.0005(19) C21C 0.014(2) 0.006(2) 0.013(2) -0.0007(18) 0.0003(17) 0.0014(18) C22C 0.009(2) 0.010(2) 0.013(2) -0.0061(17) -0.0001(16) -0.0022(17) C23C 0.020(2) 0.015(2) 0.010(2) -0.0018(18) 0.0042(17) -0.0094(19) C24C 0.035(3) 0.031(3) 0.031(3) 0.012(2) -0.018(2) -0.024(3) C25C 0.035(3) 0.021(3) 0.023(3) 0.003(2) -0.011(2) -0.017(2) C26C 0.011(2) 0.018(2) 0.018(2) -0.0085(18) 0.0018(17) -0.0031(18) C27C 0.012(2) 0.014(2) 0.017(2) -0.0014(18) -0.0015(17) -0.0037(18) C28C 0.026(3) 0.014(3) 0.034(3) -0.006(2) 0.004(2) -0.007(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pt1 S1 2.2344(12) . ? Pt1 S2 2.2355(10) . ? Pt1 O1 2.013(3) . ? Pt1 O2 2.021(3) . ? Br1 C5 1.889(5) . ? Br2 C19 1.896(5) . ? S1 C8 1.736(4) . ? S2 C22 1.730(4) . ? O1 C1 1.277(5) . ? O2 C15 1.282(5) . ? N1 C1 1.322(6) . ? N1 C8 1.345(6) . ? N2 C8 1.336(6) . ? N2 C9 1.472(5) . ? N2 C12 1.476(6) . ? N3 C15 1.317(6) . ? N3 C22 1.356(6) . ? N4 C22 1.349(5) . ? N4 C23 1.466(6) . ? N4 C26 1.464(5) . ? C1 C2 1.506(6) . ? C2 C3 1.398(7) . ? C2 C7 1.388(6) . ? C3 H3 0.9500 . ? C3 C4 1.395(7) . ? C4 H4 0.9500 . ? C4 C5 1.394(7) . ? C5 C6 1.376(7) . ? C6 H6 0.9500 . ? C6 C7 1.383(7) . ? C7 H7 0.9500 . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.522(6) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C10 C11 1.514(6) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C12 C13 1.525(6) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.537(7) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C16 1.488(7) . ? C16 C17 1.402(6) . ? C16 C21 1.389(6) . ? C17 H17 0.9500 . ? C17 C18 1.386(7) . ? C18 H18 0.9500 . ? C18 C19 1.377(7) . ? C19 C20 1.391(7) . ? C20 H20 0.9500 . ? C20 C21 1.381(7) . ? C21 H21 0.9500 . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C24 1.515(6) . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? C24 C25 1.529(7) . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C26 C27 1.527(6) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C27 C28 1.530(6) . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? Pt1B S1B 2.2366(12) . ? Pt1B S2B 2.2401(11) . ? Pt1B O1B 2.019(3) . ? Pt1B O2B 2.029(4) . ? Br1B C5B 1.896(5) . ? Br2B C19B 1.900(5) . ? S1B C8B 1.739(4) . ? S2B C22B 1.731(5) . ? O1B C1B 1.282(5) . ? O2B C15B 1.264(5) . ? N1B C1B 1.318(6) . ? N1B C8B 1.358(6) . ? N2B C8B 1.339(6) . ? N2B C9B 1.479(5) . ? N2B C12B 1.467(6) . ? N3B C15B 1.312(6) . ? N3B C22B 1.350(6) . ? N4B C22B 1.341(6) . ? N4B C23B 1.475(7) . ? N4B C26B 1.518(7) . ? C1B C2B 1.482(6) . ? C2B C3B 1.400(6) . ? C2B C7B 1.404(6) . ? C3B H3B 0.9500 . ? C3B C4B 1.380(7) . ? C4B H4B 0.9500 . ? C4B C5B 1.398(7) . ? C5B C6B 1.398(7) . ? C6B H6B 0.9500 . ? C6B C7B 1.385(7) . ? C7B H7B 0.9500 . ? C9B H9BA 0.9900 . ? C9B H9BB 0.9900 . ? C9B C10B 1.518(6) . ? C10B H10G 0.9900 . ? C10B H10H 0.9900 . ? C10B C11B 1.526(6) . ? C11B H11J 0.9800 . ? C11B H11K 0.9800 . ? C11B H11L 0.9800 . ? C12B H12G 0.9900 . ? C12B H12H 0.9900 . ? C12B C13B 1.534(6) . ? C13B H13G 0.9900 . ? C13B H13H 0.9900 . ? C13B C14B 1.527(7) . ? C14B H14J 0.9800 . ? C14B H14K 0.9800 . ? C14B H14L 0.9800 . ? C15B C16B 1.497(7) . ? C16B C17B 1.384(7) . ? C16B C21B 1.385(7) . ? C17B H17B 0.9500 . ? C17B C18B 1.389(7) . ? C18B H18B 0.9500 . ? C18B C19B 1.373(8) . ? C19B C20B 1.376(8) . ? C20B H20B 0.9500 . ? C20B C21B 1.389(7) . ? C21B H21B 0.9500 . ? C23B H23G 0.9900 . ? C23B H23H 0.9900 . ? C23B C24B 1.510(7) . ? C24B H24G 0.9900 . ? C24B H24H 0.9900 . ? C24B C25B 1.523(7) . ? C25B H25J 0.9800 . ? C25B H25K 0.9800 . ? C25B H25L 0.9800 . ? C26B H26G 0.9900 . ? C26B H26H 0.9900 . ? C26B C27B 1.500(7) . ? C27B H27G 0.9900 . ? C27B H27H 0.9900 . ? C27B C28B 1.528(8) . ? C28B H28J 0.9800 . ? C28B H28K 0.9800 . ? C28B H28L 0.9800 . ? Pt1A S1A 2.2373(12) . ? Pt1A S2A 2.2385(11) . ? Pt1A O1A 2.013(3) . ? Pt1A O2A 2.018(3) . ? Br1A C5A 1.894(5) . ? Br2A C19A 1.899(5) . ? S1A C8A 1.739(4) . ? S2A C22A 1.722(5) . ? O1A C1A 1.273(5) . ? O2A C15A 1.281(6) . ? N1A C1A 1.325(6) . ? N1A C8A 1.349(6) . ? N2A C8A 1.343(6) . ? N2A C9A 1.470(5) . ? N2A C12A 1.472(6) . ? N3A C15A 1.310(6) . ? N3A C22A 1.360(7) . ? N4A C22A 1.349(6) . ? N4A C23A 1.480(7) . ? N4A C26A 1.542(7) . ? C1A C2A 1.498(6) . ? C2A C3A 1.409(7) . ? C2A C7A 1.386(6) . ? C3A H3A 0.9500 . ? C3A C4A 1.390(7) . ? C4A H4A 0.9500 . ? C4A C5A 1.382(6) . ? C5A C6A 1.384(7) . ? C6A H6A 0.9500 . ? C6A C7A 1.384(7) . ? C7A H7A 0.9500 . ? C9A H9AA 0.9900 . ? C9A H9AB 0.9900 . ? C9A C10A 1.513(6) . ? C10A H10E 0.9900 . ? C10A H10F 0.9900 . ? C10A C11A 1.525(6) . ? C11A H11G 0.9800 . ? C11A H11H 0.9800 . ? C11A H11I 0.9800 . ? C12A H12E 0.9900 . ? C12A H12F 0.9900 . ? C12A C13A 1.515(6) . ? C13A H13E 0.9900 . ? C13A H13F 0.9900 . ? C13A C14A 1.523(7) . ? C14A H14G 0.9800 . ? C14A H14H 0.9800 . ? C14A H14I 0.9800 . ? C15A C16A 1.491(7) . ? C16A C17A 1.402(6) . ? C16A C21A 1.385(6) . ? C17A H17A 0.9500 . ? C17A C18A 1.378(7) . ? C18A H18A 0.9500 . ? C18A C19A 1.373(7) . ? C19A C20A 1.392(7) . ? C20A H20A 0.9500 . ? C20A C21A 1.391(7) . ? C21A H21A 0.9500 . ? C23A H23E 0.9900 . ? C23A H23F 0.9900 . ? C23A C24A 1.511(7) . ? C24A H24E 0.9900 . ? C24A H24F 0.9900 . ? C24A C25A 1.534(8) . ? C25A H25G 0.9800 . ? C25A H25H 0.9800 . ? C25A H25I 0.9800 . ? C26A H26E 0.9900 . ? C26A H26F 0.9900 . ? C26A C27A 1.497(7) . ? C27A H27E 0.9900 . ? C27A H27F 0.9900 . ? C27A C28A 1.508(8) . ? C28A H28G 0.9800 . ? C28A H28H 0.9800 . ? C28A H28I 0.9800 . ? Pt1C S1C 2.2313(11) . ? Pt1C S2C 2.2368(10) . ? Pt1C O1C 2.023(3) . ? Pt1C O2C 2.023(3) . ? Br1C C5C 1.894(5) . ? Br2C C19C 1.901(5) . ? S1C C8C 1.740(4) . ? S2C C22C 1.734(5) . ? O1C C1C 1.277(5) . ? O2C C15C 1.265(5) . ? N1C C1C 1.319(6) . ? N1C C8C 1.352(6) . ? N2C C8C 1.342(6) . ? N2C C9C 1.477(5) . ? N2C C12C 1.469(6) . ? N3C C15C 1.321(6) . ? N3C C22C 1.342(6) . ? N4C C22C 1.343(5) . ? N4C C23C 1.470(6) . ? N4C C26C 1.478(5) . ? C1C C2C 1.488(6) . ? C2C C3C 1.406(6) . ? C2C C7C 1.393(6) . ? C3C H3C 0.9500 . ? C3C C4C 1.388(6) . ? C4C H4C 0.9500 . ? C4C C5C 1.399(6) . ? C5C C6C 1.383(7) . ? C6C H6C 0.9500 . ? C6C C7C 1.385(6) . ? C7C H7C 0.9500 . ? C9C H9CA 0.9900 . ? C9C H9CB 0.9900 . ? C9C C10C 1.525(6) . ? C10C H10C 0.9900 . ? C10C H10D 0.9900 . ? C10C C11C 1.522(6) . ? C11C H11D 0.9800 . ? C11C H11E 0.9800 . ? C11C H11F 0.9800 . ? C12C H12C 0.9900 . ? C12C H12D 0.9900 . ? C12C C13C 1.524(6) . ? C13C H13C 0.9900 . ? C13C H13D 0.9900 . ? C13C C14C 1.518(7) . ? C14C H14D 0.9800 . ? C14C H14E 0.9800 . ? C14C H14F 0.9800 . ? C15C C16C 1.496(7) . ? C16C C17C 1.387(6) . ? C16C C21C 1.397(6) . ? C17C H17C 0.9500 . ? C17C C18C 1.390(7) . ? C18C H18C 0.9500 . ? C18C C19C 1.379(7) . ? C19C C20C 1.386(7) . ? C20C H20C 0.9500 . ? C20C C21C 1.390(7) . ? C21C H21C 0.9500 . ? C23C H23C 0.9900 . ? C23C H23D 0.9900 . ? C23C C24C 1.505(6) . ? C24C H24C 0.9900 . ? C24C H24D 0.9900 . ? C24C C25C 1.525(7) . ? C25C H25D 0.9800 . ? C25C H25E 0.9800 . ? C25C H25F 0.9800 . ? C26C H26C 0.9900 . ? C26C H26D 0.9900 . ? C26C C27C 1.510(6) . ? C27C H27C 0.9900 . ? C27C H27D 0.9900 . ? C27C C28C 1.535(6) . ? C28C H28D 0.9800 . ? C28C H28E 0.9800 . ? C28C H28F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S1 Pt1 S2 88.48(4) . . ? O1 Pt1 S1 93.92(10) . . ? O1 Pt1 S2 176.74(11) . . ? O1 Pt1 O2 82.70(13) . . ? O2 Pt1 S1 176.61(8) . . ? O2 Pt1 S2 94.91(9) . . ? C8 S1 Pt1 107.99(17) . . ? C22 S2 Pt1 107.51(15) . . ? C1 O1 Pt1 127.1(3) . . ? C15 O2 Pt1 128.8(3) . . ? C1 N1 C8 125.3(4) . . ? C8 N2 C9 122.4(4) . . ? C8 N2 C12 122.7(4) . . ? C9 N2 C12 115.0(4) . . ? C15 N3 C22 127.6(4) . . ? C22 N4 C23 122.7(4) . . ? C22 N4 C26 120.7(4) . . ? C26 N4 C23 116.6(3) . . ? O1 C1 N1 131.1(4) . . ? O1 C1 C2 112.9(4) . . ? N1 C1 C2 116.0(4) . . ? C3 C2 C1 118.7(4) . . ? C7 C2 C1 121.6(4) . . ? C7 C2 C3 119.4(4) . . ? C2 C3 H3 119.8 . . ? C4 C3 C2 120.4(4) . . ? C4 C3 H3 119.8 . . ? C3 C4 H4 120.6 . . ? C5 C4 C3 118.8(5) . . ? C5 C4 H4 120.6 . . ? C4 C5 Br1 118.8(4) . . ? C6 C5 Br1 120.2(4) . . ? C6 C5 C4 121.0(4) . . ? C5 C6 H6 120.0 . . ? C5 C6 C7 119.9(4) . . ? C7 C6 H6 120.0 . . ? C2 C7 H7 119.8 . . ? C6 C7 C2 120.5(5) . . ? C6 C7 H7 119.8 . . ? N1 C8 S1 129.1(4) . . ? N2 C8 S1 115.9(3) . . ? N2 C8 N1 114.9(4) . . ? N2 C9 H9A 108.9 . . ? N2 C9 H9B 108.9 . . ? N2 C9 C10 113.3(4) . . ? H9A C9 H9B 107.7 . . ? C10 C9 H9A 108.9 . . ? C10 C9 H9B 108.9 . . ? C9 C10 H10A 109.4 . . ? C9 C10 H10B 109.4 . . ? H10A C10 H10B 108.0 . . ? C11 C10 C9 111.3(4) . . ? C11 C10 H10A 109.4 . . ? C11 C10 H10B 109.4 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N2 C12 H12A 109.0 . . ? N2 C12 H12B 109.0 . . ? N2 C12 C13 113.0(4) . . ? H12A C12 H12B 107.8 . . ? C13 C12 H12A 109.0 . . ? C13 C12 H12B 109.0 . . ? C12 C13 H13A 109.6 . . ? C12 C13 H13B 109.6 . . ? C12 C13 C14 110.4(4) . . ? H13A C13 H13B 108.1 . . ? C14 C13 H13A 109.6 . . ? C14 C13 H13B 109.6 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? O2 C15 N3 130.0(5) . . ? O2 C15 C16 114.3(4) . . ? N3 C15 C16 115.6(4) . . ? C17 C16 C15 120.4(4) . . ? C21 C16 C15 120.3(4) . . ? C21 C16 C17 119.3(4) . . ? C16 C17 H17 119.9 . . ? C18 C17 C16 120.2(4) . . ? C18 C17 H17 119.9 . . ? C17 C18 H18 120.2 . . ? C19 C18 C17 119.5(4) . . ? C19 C18 H18 120.2 . . ? C18 C19 Br2 119.9(4) . . ? C18 C19 C20 121.0(5) . . ? C20 C19 Br2 119.0(4) . . ? C19 C20 H20 120.3 . . ? C21 C20 C19 119.4(5) . . ? C21 C20 H20 120.3 . . ? C16 C21 H21 119.7 . . ? C20 C21 C16 120.6(4) . . ? C20 C21 H21 119.7 . . ? N3 C22 S2 128.2(3) . . ? N4 C22 S2 117.5(3) . . ? N4 C22 N3 114.1(4) . . ? N4 C23 H23A 109.0 . . ? N4 C23 H23B 109.0 . . ? N4 C23 C24 113.0(4) . . ? H23A C23 H23B 107.8 . . ? C24 C23 H23A 109.0 . . ? C24 C23 H23B 109.0 . . ? C23 C24 H24A 109.2 . . ? C23 C24 H24B 109.2 . . ? C23 C24 C25 112.0(4) . . ? H24A C24 H24B 107.9 . . ? C25 C24 H24A 109.2 . . ? C25 C24 H24B 109.2 . . ? C24 C25 H25A 109.5 . . ? C24 C25 H25B 109.5 . . ? C24 C25 H25C 109.5 . . ? H25A C25 H25B 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? N4 C26 H26A 108.9 . . ? N4 C26 H26B 108.9 . . ? N4 C26 C27 113.5(4) . . ? H26A C26 H26B 107.7 . . ? C27 C26 H26A 108.9 . . ? C27 C26 H26B 108.9 . . ? C26 C27 H27A 109.6 . . ? C26 C27 H27B 109.6 . . ? C26 C27 C28 110.3(4) . . ? H27A C27 H27B 108.1 . . ? C28 C27 H27A 109.6 . . ? C28 C27 H27B 109.6 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28B 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? S1B Pt1B S2B 89.79(4) . . ? O1B Pt1B S1B 93.66(10) . . ? O1B Pt1B S2B 176.40(10) . . ? O1B Pt1B O2B 82.12(13) . . ? O2B Pt1B S1B 175.63(9) . . ? O2B Pt1B S2B 94.40(9) . . ? C8B S1B Pt1B 107.90(17) . . ? C22B S2B Pt1B 107.77(16) . . ? C1B O1B Pt1B 126.7(3) . . ? C15B O2B Pt1B 127.3(3) . . ? C1B N1B C8B 125.8(4) . . ? C8B N2B C9B 121.4(4) . . ? C8B N2B C12B 123.4(4) . . ? C12B N2B C9B 115.1(4) . . ? C15B N3B C22B 126.7(4) . . ? C22B N4B C23B 122.9(4) . . ? C22B N4B C26B 120.8(4) . . ? C23B N4B C26B 116.3(4) . . ? O1B C1B N1B 130.4(4) . . ? O1B C1B C2B 113.4(4) . . ? N1B C1B C2B 116.2(4) . . ? C3B C2B C1B 119.6(4) . . ? C3B C2B C7B 118.7(4) . . ? C7B C2B C1B 121.5(4) . . ? C2B C3B H3B 119.4 . . ? C4B C3B C2B 121.2(4) . . ? C4B C3B H3B 119.4 . . ? C3B C4B H4B 120.6 . . ? C3B C4B C5B 118.8(5) . . ? C5B C4B H4B 120.6 . . ? C4B C5B Br1B 118.9(4) . . ? C6B C5B Br1B 119.4(4) . . ? C6B C5B C4B 121.6(4) . . ? C5B C6B H6B 120.8 . . ? C7B C6B C5B 118.3(4) . . ? C7B C6B H6B 120.8 . . ? C2B C7B H7B 119.4 . . ? C6B C7B C2B 121.3(4) . . ? C6B C7B H7B 119.4 . . ? N1B C8B S1B 128.6(4) . . ? N2B C8B S1B 116.2(3) . . ? N2B C8B N1B 115.2(4) . . ? N2B C9B H9BA 109.0 . . ? N2B C9B H9BB 109.0 . . ? N2B C9B C10B 113.1(4) . . ? H9BA C9B H9BB 107.8 . . ? C10B C9B H9BA 109.0 . . ? C10B C9B H9BB 109.0 . . ? C9B C10B H10G 109.5 . . ? C9B C10B H10H 109.5 . . ? C9B C10B C11B 110.7(4) . . ? H10G C10B H10H 108.1 . . ? C11B C10B H10G 109.5 . . ? C11B C10B H10H 109.5 . . ? C10B C11B H11J 109.5 . . ? C10B C11B H11K 109.5 . . ? C10B C11B H11L 109.5 . . ? H11J C11B H11K 109.5 . . ? H11J C11B H11L 109.5 . . ? H11K C11B H11L 109.5 . . ? N2B C12B H12G 108.9 . . ? N2B C12B H12H 108.9 . . ? N2B C12B C13B 113.3(4) . . ? H12G C12B H12H 107.7 . . ? C13B C12B H12G 108.9 . . ? C13B C12B H12H 108.9 . . ? C12B C13B H13G 109.5 . . ? C12B C13B H13H 109.5 . . ? H13G C13B H13H 108.1 . . ? C14B C13B C12B 110.7(4) . . ? C14B C13B H13G 109.5 . . ? C14B C13B H13H 109.5 . . ? C13B C14B H14J 109.5 . . ? C13B C14B H14K 109.5 . . ? C13B C14B H14L 109.5 . . ? H14J C14B H14K 109.5 . . ? H14J C14B H14L 109.5 . . ? H14K C14B H14L 109.5 . . ? O2B C15B N3B 131.6(5) . . ? O2B C15B C16B 113.9(4) . . ? N3B C15B C16B 114.4(4) . . ? C17B C16B C15B 121.8(4) . . ? C17B C16B C21B 118.3(5) . . ? C21B C16B C15B 119.9(4) . . ? C16B C17B H17B 119.5 . . ? C16B C17B C18B 120.9(5) . . ? C18B C17B H17B 119.5 . . ? C17B C18B H18B 120.4 . . ? C19B C18B C17B 119.3(5) . . ? C19B C18B H18B 120.4 . . ? C18B C19B Br2B 119.2(4) . . ? C18B C19B C20B 121.3(5) . . ? C20B C19B Br2B 119.5(4) . . ? C19B C20B H20B 120.7 . . ? C19B C20B C21B 118.6(5) . . ? C21B C20B H20B 120.7 . . ? C16B C21B C20B 121.5(5) . . ? C16B C21B H21B 119.3 . . ? C20B C21B H21B 119.3 . . ? N3B C22B S2B 129.0(3) . . ? N4B C22B S2B 117.0(4) . . ? N4B C22B N3B 113.9(4) . . ? N4B C23B H23G 109.1 . . ? N4B C23B H23H 109.1 . . ? N4B C23B C24B 112.3(4) . . ? H23G C23B H23H 107.9 . . ? C24B C23B H23G 109.1 . . ? C24B C23B H23H 109.1 . . ? C23B C24B H24G 109.1 . . ? C23B C24B H24H 109.1 . . ? C23B C24B C25B 112.5(4) . . ? H24G C24B H24H 107.8 . . ? C25B C24B H24G 109.1 . . ? C25B C24B H24H 109.1 . . ? C24B C25B H25J 109.5 . . ? C24B C25B H25K 109.5 . . ? C24B C25B H25L 109.5 . . ? H25J C25B H25K 109.5 . . ? H25J C25B H25L 109.5 . . ? H25K C25B H25L 109.5 . . ? N4B C26B H26G 109.4 . . ? N4B C26B H26H 109.4 . . ? H26G C26B H26H 108.0 . . ? C27B C26B N4B 111.3(4) . . ? C27B C26B H26G 109.4 . . ? C27B C26B H26H 109.4 . . ? C26B C27B H27G 109.9 . . ? C26B C27B H27H 109.9 . . ? C26B C27B C28B 108.9(5) . . ? H27G C27B H27H 108.3 . . ? C28B C27B H27G 109.9 . . ? C28B C27B H27H 109.9 . . ? C27B C28B H28J 109.5 . . ? C27B C28B H28K 109.5 . . ? C27B C28B H28L 109.5 . . ? H28J C28B H28K 109.5 . . ? H28J C28B H28L 109.5 . . ? H28K C28B H28L 109.5 . . ? S1A Pt1A S2A 90.14(4) . . ? O1A Pt1A S1A 93.38(10) . . ? O1A Pt1A S2A 176.26(10) . . ? O1A Pt1A O2A 82.30(13) . . ? O2A Pt1A S1A 175.59(9) . . ? O2A Pt1A S2A 94.16(9) . . ? C8A S1A Pt1A 107.63(17) . . ? C22A S2A Pt1A 107.57(16) . . ? C1A O1A Pt1A 127.2(3) . . ? C15A O2A Pt1A 128.1(3) . . ? C1A N1A C8A 125.0(4) . . ? C8A N2A C9A 122.4(4) . . ? C8A N2A C12A 123.0(4) . . ? C9A N2A C12A 114.6(4) . . ? C15A N3A C22A 126.4(4) . . ? C22A N4A C23A 122.4(5) . . ? C22A N4A C26A 120.7(4) . . ? C23A N4A C26A 116.8(4) . . ? O1A C1A N1A 130.3(4) . . ? O1A C1A C2A 113.6(4) . . ? N1A C1A C2A 116.1(4) . . ? C3A C2A C1A 118.5(4) . . ? C7A C2A C1A 122.1(4) . . ? C7A C2A C3A 119.1(4) . . ? C2A C3A H3A 119.9 . . ? C4A C3A C2A 120.2(4) . . ? C4A C3A H3A 119.9 . . ? C3A C4A H4A 120.4 . . ? C5A C4A C3A 119.2(5) . . ? C5A C4A H4A 120.4 . . ? C4A C5A Br1A 118.8(4) . . ? C4A C5A C6A 121.2(4) . . ? C6A C5A Br1A 120.0(3) . . ? C5A C6A H6A 120.2 . . ? C5A C6A C7A 119.6(4) . . ? C7A C6A H6A 120.2 . . ? C2A C7A H7A 119.7 . . ? C6A C7A C2A 120.6(5) . . ? C6A C7A H7A 119.7 . . ? N1A C8A S1A 129.3(4) . . ? N2A C8A S1A 115.9(3) . . ? N2A C8A N1A 114.7(4) . . ? N2A C9A H9AA 108.9 . . ? N2A C9A H9AB 108.9 . . ? N2A C9A C10A 113.5(4) . . ? H9AA C9A H9AB 107.7 . . ? C10A C9A H9AA 108.9 . . ? C10A C9A H9AB 108.9 . . ? C9A C10A H10E 109.4 . . ? C9A C10A H10F 109.4 . . ? C9A C10A C11A 111.4(4) . . ? H10E C10A H10F 108.0 . . ? C11A C10A H10E 109.4 . . ? C11A C10A H10F 109.4 . . ? C10A C11A H11G 109.5 . . ? C10A C11A H11H 109.5 . . ? C10A C11A H11I 109.5 . . ? H11G C11A H11H 109.5 . . ? H11G C11A H11I 109.5 . . ? H11H C11A H11I 109.5 . . ? N2A C12A H12E 109.0 . . ? N2A C12A H12F 109.0 . . ? N2A C12A C13A 112.9(4) . . ? H12E C12A H12F 107.8 . . ? C13A C12A H12E 109.0 . . ? C13A C12A H12F 109.0 . . ? C12A C13A H13E 109.4 . . ? C12A C13A H13F 109.4 . . ? C12A C13A C14A 111.3(4) . . ? H13E C13A H13F 108.0 . . ? C14A C13A H13E 109.4 . . ? C14A C13A H13F 109.4 . . ? C13A C14A H14G 109.5 . . ? C13A C14A H14H 109.5 . . ? C13A C14A H14I 109.5 . . ? H14G C14A H14H 109.5 . . ? H14G C14A H14I 109.5 . . ? H14H C14A H14I 109.5 . . ? O2A C15A N3A 130.2(5) . . ? O2A C15A C16A 114.2(4) . . ? N3A C15A C16A 115.6(4) . . ? C17A C16A C15A 121.1(4) . . ? C21A C16A C15A 120.0(4) . . ? C21A C16A C17A 118.8(5) . . ? C16A C17A H17A 119.6 . . ? C18A C17A C16A 120.8(5) . . ? C18A C17A H17A 119.6 . . ? C17A C18A H18A 120.5 . . ? C19A C18A C17A 119.1(5) . . ? C19A C18A H18A 120.5 . . ? C18A C19A Br2A 119.3(4) . . ? C18A C19A C20A 121.9(5) . . ? C20A C19A Br2A 118.8(4) . . ? C19A C20A H20A 120.9 . . ? C21A C20A C19A 118.3(5) . . ? C21A C20A H20A 120.9 . . ? C16A C21A C20A 121.0(4) . . ? C16A C21A H21A 119.5 . . ? C20A C21A H21A 119.5 . . ? N3A C22A S2A 129.7(3) . . ? N4A C22A S2A 117.4(4) . . ? N4A C22A N3A 112.8(4) . . ? N4A C23A H23E 109.3 . . ? N4A C23A H23F 109.3 . . ? N4A C23A C24A 111.7(5) . . ? H23E C23A H23F 107.9 . . ? C24A C23A H23E 109.3 . . ? C24A C23A H23F 109.3 . . ? C23A C24A H24E 109.3 . . ? C23A C24A H24F 109.3 . . ? C23A C24A C25A 111.4(5) . . ? H24E C24A H24F 108.0 . . ? C25A C24A H24E 109.3 . . ? C25A C24A H24F 109.3 . . ? C24A C25A H25G 109.5 . . ? C24A C25A H25H 109.5 . . ? C24A C25A H25I 109.5 . . ? H25G C25A H25H 109.5 . . ? H25G C25A H25I 109.5 . . ? H25H C25A H25I 109.5 . . ? N4A C26A H26E 109.6 . . ? N4A C26A H26F 109.6 . . ? H26E C26A H26F 108.1 . . ? C27A C26A N4A 110.5(4) . . ? C27A C26A H26E 109.6 . . ? C27A C26A H26F 109.6 . . ? C26A C27A H27E 110.0 . . ? C26A C27A H27F 110.0 . . ? C26A C27A C28A 108.4(5) . . ? H27E C27A H27F 108.4 . . ? C28A C27A H27E 110.0 . . ? C28A C27A H27F 110.0 . . ? C27A C28A H28G 109.5 . . ? C27A C28A H28H 109.5 . . ? C27A C28A H28I 109.5 . . ? H28G C28A H28H 109.5 . . ? H28G C28A H28I 109.5 . . ? H28H C28A H28I 109.5 . . ? S1C Pt1C S2C 88.66(4) . . ? O1C Pt1C S1C 93.98(10) . . ? O1C Pt1C S2C 176.67(11) . . ? O1C Pt1C O2C 82.36(13) . . ? O2C Pt1C S1C 176.34(8) . . ? O2C Pt1C S2C 95.01(9) . . ? C8C S1C Pt1C 108.02(17) . . ? C22C S2C Pt1C 107.33(15) . . ? C1C O1C Pt1C 127.0(3) . . ? C15C O2C Pt1C 128.4(3) . . ? C1C N1C C8C 125.7(4) . . ? C8C N2C C9C 121.5(4) . . ? C8C N2C C12C 123.8(4) . . ? C12C N2C C9C 114.8(4) . . ? C15C N3C C22C 127.4(4) . . ? C22C N4C C23C 123.8(4) . . ? C22C N4C C26C 119.4(4) . . ? C23C N4C C26C 116.8(3) . . ? O1C C1C N1C 130.7(4) . . ? O1C C1C C2C 112.9(4) . . ? N1C C1C C2C 116.4(4) . . ? C3C C2C C1C 118.8(4) . . ? C7C C2C C1C 121.9(4) . . ? C7C C2C C3C 119.1(4) . . ? C2C C3C H3C 119.7 . . ? C4C C3C C2C 120.5(4) . . ? C4C C3C H3C 119.7 . . ? C3C C4C H4C 120.6 . . ? C3C C4C C5C 118.8(5) . . ? C5C C4C H4C 120.6 . . ? C4C C5C Br1C 118.2(4) . . ? C6C C5C Br1C 120.5(3) . . ? C6C C5C C4C 121.3(4) . . ? C5C C6C H6C 120.3 . . ? C5C C6C C7C 119.4(4) . . ? C7C C6C H6C 120.3 . . ? C2C C7C H7C 119.6 . . ? C6C C7C C2C 120.8(4) . . ? C6C C7C H7C 119.6 . . ? N1C C8C S1C 128.8(4) . . ? N2C C8C S1C 115.2(3) . . ? N2C C8C N1C 115.9(4) . . ? N2C C9C H9CA 109.1 . . ? N2C C9C H9CB 109.1 . . ? N2C C9C C10C 112.6(4) . . ? H9CA C9C H9CB 107.8 . . ? C10C C9C H9CA 109.1 . . ? C10C C9C H9CB 109.1 . . ? C9C C10C H10C 109.5 . . ? C9C C10C H10D 109.5 . . ? H10C C10C H10D 108.1 . . ? C11C C10C C9C 110.8(4) . . ? C11C C10C H10C 109.5 . . ? C11C C10C H10D 109.5 . . ? C10C C11C H11D 109.5 . . ? C10C C11C H11E 109.5 . . ? C10C C11C H11F 109.5 . . ? H11D C11C H11E 109.5 . . ? H11D C11C H11F 109.5 . . ? H11E C11C H11F 109.5 . . ? N2C C12C H12C 108.8 . . ? N2C C12C H12D 108.8 . . ? N2C C12C C13C 113.9(4) . . ? H12C C12C H12D 107.7 . . ? C13C C12C H12C 108.8 . . ? C13C C12C H12D 108.8 . . ? C12C C13C H13C 109.5 . . ? C12C C13C H13D 109.5 . . ? H13C C13C H13D 108.1 . . ? C14C C13C C12C 110.7(4) . . ? C14C C13C H13C 109.5 . . ? C14C C13C H13D 109.5 . . ? C13C C14C H14D 109.5 . . ? C13C C14C H14E 109.5 . . ? C13C C14C H14F 109.5 . . ? H14D C14C H14E 109.5 . . ? H14D C14C H14F 109.5 . . ? H14E C14C H14F 109.5 . . ? O2C C15C N3C 130.8(4) . . ? O2C C15C C16C 114.2(4) . . ? N3C C15C C16C 115.0(4) . . ? C17C C16C C15C 121.5(4) . . ? C17C C16C C21C 118.9(4) . . ? C21C C16C C15C 119.6(4) . . ? C16C C17C H17C 119.5 . . ? C16C C17C C18C 120.9(4) . . ? C18C C17C H17C 119.5 . . ? C17C C18C H18C 120.6 . . ? C19C C18C C17C 118.8(4) . . ? C19C C18C H18C 120.6 . . ? C18C C19C Br2C 119.6(3) . . ? C18C C19C C20C 122.0(5) . . ? C20C C19C Br2C 118.4(4) . . ? C19C C20C H20C 120.8 . . ? C19C C20C C21C 118.3(4) . . ? C21C C20C H20C 120.8 . . ? C16C C21C H21C 119.5 . . ? C20C C21C C16C 121.0(4) . . ? C20C C21C H21C 119.5 . . ? N3C C22C S2C 128.5(3) . . ? N3C C22C N4C 115.0(4) . . ? N4C C22C S2C 116.4(4) . . ? N4C C23C H23C 108.8 . . ? N4C C23C H23D 108.8 . . ? N4C C23C C24C 113.7(4) . . ? H23C C23C H23D 107.7 . . ? C24C C23C H23C 108.8 . . ? C24C C23C H23D 108.8 . . ? C23C C24C H24C 109.3 . . ? C23C C24C H24D 109.3 . . ? C23C C24C C25C 111.5(4) . . ? H24C C24C H24D 108.0 . . ? C25C C24C H24C 109.3 . . ? C25C C24C H24D 109.3 . . ? C24C C25C H25D 109.5 . . ? C24C C25C H25E 109.5 . . ? C24C C25C H25F 109.5 . . ? H25D C25C H25E 109.5 . . ? H25D C25C H25F 109.5 . . ? H25E C25C H25F 109.5 . . ? N4C C26C H26C 108.8 . . ? N4C C26C H26D 108.8 . . ? N4C C26C C27C 113.8(4) . . ? H26C C26C H26D 107.7 . . ? C27C C26C H26C 108.8 . . ? C27C C26C H26D 108.8 . . ? C26C C27C H27C 109.5 . . ? C26C C27C H27D 109.5 . . ? C26C C27C C28C 110.6(4) . . ? H27C C27C H27D 108.1 . . ? C28C C27C H27C 109.5 . . ? C28C C27C H27D 109.5 . . ? C27C C28C H28D 109.5 . . ? C27C C28C H28E 109.5 . . ? C27C C28C H28F 109.5 . . ? H28D C28C H28E 109.5 . . ? H28D C28C H28F 109.5 . . ? H28E C28C H28F 109.5 . . ? _shelx_res_file ; TITL cu_18_046_4BrPrPt3_0m_a.res in P-1 REM Old TITL cu_18_046_4BrPrPt3_0m in P-1 REM SHELXT solution in P-1 REM R1 0.135, Rweak 0.001, Alpha 0.073, Orientation as input REM Formula found by SHELXT: C115 Br8 N21 Pt4 S8 CELL 1.54178 15.7174 17.5696 25.3974 80.253 85.604 63.888 ZERR 8 0.0006 0.0006 0.0009 0.002 0.002 0.001 LATT 1 SFAC C H Br N O Pt S UNIT 224 288 16 32 16 8 16 L.S. 10 PLAN 5 SIZE 0.12 0.17 0.18 TEMP -173.16 BOND $H LIST 6 fmap 2 acta REM REM REM WGHT 0.036400 16.921499 FVAR 0.08333 PT1 6 0.745073 0.362202 0.184025 11.00000 0.00963 0.00365 = 0.00568 -0.00062 0.00007 -0.00055 BR1 3 0.862821 0.419569 -0.150759 11.00000 0.02518 0.01818 = 0.00743 0.00351 -0.00181 -0.01221 BR2 3 0.502309 0.903874 0.038064 11.00000 0.01849 0.00946 = 0.03148 0.00902 -0.00678 -0.00229 S1 7 0.818064 0.220567 0.210096 11.00000 0.01853 0.00489 = 0.00725 -0.00045 -0.00080 -0.00175 S2 7 0.747213 0.379848 0.268960 11.00000 0.02557 0.00635 = 0.00824 -0.00103 -0.00430 -0.00027 O1 5 0.745274 0.351811 0.106283 11.00000 0.01591 0.01002 = 0.00814 -0.00168 -0.00288 0.00084 O2 5 0.678989 0.488914 0.156009 11.00000 0.01791 0.00305 = 0.00894 0.00040 -0.00012 0.00054 N1 4 0.853035 0.207414 0.101948 11.00000 0.01096 0.00844 = 0.00569 0.00070 0.00187 -0.00322 N2 4 0.894208 0.085854 0.161512 11.00000 0.00950 0.00539 = 0.00960 -0.00190 0.00311 -0.00267 N3 4 0.645792 0.554340 0.233523 11.00000 0.00646 0.00976 = 0.01340 -0.00455 -0.00111 -0.00113 N4 4 0.648045 0.507783 0.322640 11.00000 0.01093 0.00980 = 0.01148 -0.00275 -0.00247 -0.00215 C1 1 0.801864 0.289105 0.083017 11.00000 0.00770 0.00786 = 0.00923 -0.00367 -0.00036 -0.00304 C2 1 0.811687 0.315071 0.024075 11.00000 0.01129 0.00775 = 0.00806 -0.00025 -0.00171 -0.00460 C3 1 0.747618 0.395946 -0.000236 11.00000 0.01597 0.01270 = 0.01260 -0.00126 -0.00088 -0.00404 AFIX 43 H3 2 0.695049 0.430701 0.019488 11.00000 -1.20000 AFIX 0 C4 1 0.760436 0.425933 -0.053325 11.00000 0.01325 0.00943 = 0.01145 0.00311 -0.00730 -0.00216 AFIX 43 H4 2 0.715751 0.479939 -0.070404 11.00000 -1.20000 AFIX 0 C5 1 0.840052 0.375153 -0.080837 11.00000 0.02048 0.01075 = 0.00577 0.00031 -0.00105 -0.01240 C6 1 0.902429 0.294916 -0.057344 11.00000 0.01474 0.01439 = 0.01145 -0.00458 -0.00032 -0.00447 AFIX 43 H6 2 0.955677 0.260572 -0.076828 11.00000 -1.20000 AFIX 0 C7 1 0.887497 0.264329 -0.005313 11.00000 0.01331 0.01433 = 0.00838 -0.00307 -0.00042 -0.00563 AFIX 43 H7 2 0.929456 0.208161 0.010422 11.00000 -1.20000 AFIX 0 C8 1 0.855002 0.171504 0.153272 11.00000 0.00583 0.00941 = 0.01225 -0.00156 0.00017 -0.00409 C9 1 0.938547 0.034766 0.118202 11.00000 0.00972 0.00356 = 0.00923 -0.00031 0.00067 0.00160 AFIX 23 H9A 2 0.994162 -0.018081 0.132640 11.00000 -1.20000 H9B 2 0.961577 0.068039 0.090351 11.00000 -1.20000 AFIX 0 C10 1 0.871725 0.009989 0.092639 11.00000 0.01037 0.01468 = 0.01823 -0.00664 0.00118 -0.00474 AFIX 23 H10A 2 0.840356 -0.014894 0.120947 11.00000 -1.20000 H10B 2 0.821971 0.061960 0.072568 11.00000 -1.20000 AFIX 0 C11 1 0.924289 -0.054388 0.055134 11.00000 0.02143 0.01788 = 0.02326 -0.00841 0.00334 -0.01038 AFIX 137 H11A 2 0.957020 -0.030551 0.027735 11.00000 -1.50000 H11B 2 0.879123 -0.066982 0.038004 11.00000 -1.50000 H11C 2 0.970758 -0.107315 0.075381 11.00000 -1.50000 AFIX 0 C12 1 0.897253 0.035354 0.214657 11.00000 0.01165 0.00595 = 0.01386 -0.00106 0.00306 -0.00207 AFIX 23 H12A 2 0.890288 -0.016569 0.210321 11.00000 -1.20000 H12B 2 0.842943 0.069852 0.236182 11.00000 -1.20000 AFIX 0 C13 1 0.988791 0.008329 0.244755 11.00000 0.02428 0.01127 = 0.00976 0.00025 -0.00097 -0.00697 AFIX 23 H13A 2 0.995939 0.059902 0.249724 11.00000 -1.20000 H13B 2 1.043530 -0.026520 0.223617 11.00000 -1.20000 AFIX 0 C14 1 0.987616 -0.044171 0.299514 11.00000 0.02482 0.01141 = 0.01113 0.00386 0.00032 -0.00647 AFIX 137 H14A 2 0.978832 -0.094379 0.294566 11.00000 -1.50000 H14B 2 0.935423 -0.008564 0.321104 11.00000 -1.50000 H14C 2 1.047842 -0.063046 0.317791 11.00000 -1.50000 AFIX 0 C15 1 0.651881 0.552612 0.181703 11.00000 0.00227 0.01453 = 0.01297 -0.00454 0.00326 -0.00165 C16 1 0.618718 0.637616 0.147133 11.00000 0.00280 0.00657 = 0.01747 -0.00262 -0.00155 0.00038 C17 1 0.580118 0.713250 0.169908 11.00000 0.02173 0.01003 = 0.01680 -0.00088 -0.00885 -0.00297 AFIX 43 H17 2 0.576826 0.710268 0.207660 11.00000 -1.20000 AFIX 0 C18 1 0.546733 0.792386 0.137512 11.00000 0.02242 0.00767 = 0.02749 -0.00180 -0.00929 -0.00076 AFIX 43 H18 2 0.519836 0.843666 0.152927 11.00000 -1.20000 AFIX 0 C19 1 0.552839 0.796130 0.082825 11.00000 0.01119 0.00952 = 0.02097 0.00864 -0.00801 -0.00180 C20 1 0.591879 0.721674 0.059568 11.00000 0.01644 0.01318 = 0.01772 0.00654 0.00488 0.00132 AFIX 43 H20 2 0.595826 0.724996 0.021799 11.00000 -1.20000 AFIX 0 C21 1 0.624834 0.642904 0.091895 11.00000 0.01050 0.01235 = 0.01660 -0.00230 0.00324 0.00185 AFIX 43 H21 2 0.651928 0.591881 0.076212 11.00000 -1.20000 AFIX 0 C22 1 0.675108 0.486518 0.273416 11.00000 0.00739 0.00612 = 0.01182 0.00029 -0.00329 -0.00177 C23 1 0.674438 0.444211 0.371262 11.00000 0.01394 0.02096 = 0.00781 -0.00301 0.00050 -0.01036 AFIX 23 H23A 2 0.692022 0.386852 0.361614 11.00000 -1.20000 H23B 2 0.618807 0.457726 0.395367 11.00000 -1.20000 AFIX 0 C24 1 0.756227 0.441305 0.400814 11.00000 0.02784 0.02463 = 0.02892 0.00646 -0.01361 -0.01478 AFIX 23 H24A 2 0.736004 0.496137 0.414632 11.00000 -1.20000 H24B 2 0.809386 0.434919 0.375615 11.00000 -1.20000 AFIX 0 C25 1 0.790436 0.367299 0.447331 11.00000 0.02243 0.02046 = 0.02310 0.00175 -0.00586 -0.00749 AFIX 137 H25A 2 0.821020 0.312705 0.433355 11.00000 -1.50000 H25B 2 0.736232 0.368754 0.469685 11.00000 -1.50000 H25C 2 0.835984 0.373000 0.468771 11.00000 -1.50000 AFIX 0 C26 1 0.590927 0.597347 0.329839 11.00000 0.01717 0.01951 = 0.01281 -0.00458 0.00338 -0.00787 AFIX 23 H26A 2 0.559993 0.598882 0.365352 11.00000 -1.20000 H26B 2 0.540368 0.624687 0.302496 11.00000 -1.20000 AFIX 0 C27 1 0.648164 0.649353 0.325635 11.00000 0.01403 0.01406 = 0.01765 -0.00311 -0.00123 -0.00660 AFIX 23 H27A 2 0.681219 0.646644 0.290727 11.00000 -1.20000 H27B 2 0.696604 0.624562 0.354162 11.00000 -1.20000 AFIX 0 C28 1 0.582865 0.742868 0.331025 11.00000 0.03286 0.01512 = 0.03025 -0.01220 0.00514 -0.00851 AFIX 137 H28A 2 0.534928 0.767269 0.302782 11.00000 -1.50000 H28B 2 0.620302 0.775681 0.327743 11.00000 -1.50000 H28C 2 0.551547 0.745538 0.366003 11.00000 -1.50000 AFIX 0 PT1B 6 0.275563 -0.117793 0.317208 11.00000 0.01303 0.00579 = 0.00655 -0.00127 0.00055 -0.00297 BR1B 3 0.139379 -0.170393 0.649479 11.00000 0.02478 0.01638 = 0.00782 0.00301 -0.00061 -0.01038 BR2B 3 0.483372 -0.648067 0.479703 11.00000 0.02506 0.01478 = 0.06855 0.01939 -0.01898 -0.00864 S1B 7 0.205052 0.023773 0.289944 11.00000 0.02131 0.00713 = 0.00665 -0.00040 -0.00123 -0.00415 S2B 7 0.281020 -0.140244 0.232521 11.00000 0.03922 0.01192 = 0.00951 -0.00291 0.00001 -0.01110 O1B 5 0.272156 -0.105319 0.395036 11.00000 0.01878 0.00733 = 0.00913 -0.00132 -0.00253 0.00145 O2B 5 0.336241 -0.244329 0.347669 11.00000 0.02161 0.01110 = 0.01169 -0.00235 0.00159 -0.00556 N1B 4 0.159144 0.037526 0.397553 11.00000 0.01549 0.00837 = 0.00780 0.00222 -0.00308 -0.00369 N2B 4 0.119618 0.159751 0.337493 11.00000 0.01122 0.00686 = 0.00924 -0.00189 0.00208 -0.00232 N3B 4 0.331832 -0.311011 0.275842 11.00000 0.01890 0.01182 = 0.01895 -0.00509 -0.00613 0.00158 N4B 4 0.320008 -0.274755 0.186248 11.00000 0.02642 0.02159 = 0.01814 -0.00953 -0.00426 0.00086 C1B 1 0.211575 -0.043095 0.417618 11.00000 0.00814 0.00956 = 0.01295 -0.00381 -0.00244 -0.00315 C2B 1 0.198994 -0.067853 0.475382 11.00000 0.01322 0.00838 = 0.01100 -0.00237 -0.00555 -0.00486 C3B 1 0.263361 -0.147121 0.501759 11.00000 0.00623 0.00722 = 0.01086 0.00238 -0.00096 0.00186 AFIX 43 H3B 2 0.318613 -0.181226 0.483501 11.00000 -1.20000 AFIX 0 C4B 1 0.247953 -0.176587 0.553821 11.00000 0.01636 0.01081 = 0.01406 0.00279 -0.00432 -0.00483 AFIX 43 H4B 2 0.292631 -0.229931 0.571662 11.00000 -1.20000 AFIX 0 C5B 1 0.165392 -0.126502 0.579833 11.00000 0.01988 0.01428 = 0.00502 0.00097 -0.00311 -0.01131 C6B 1 0.100367 -0.046379 0.555094 11.00000 0.01879 0.00954 = 0.00921 -0.00185 -0.00178 -0.00616 AFIX 43 H6B 2 0.044566 -0.012905 0.573210 11.00000 -1.20000 AFIX 0 C7B 1 0.119323 -0.017014 0.503516 11.00000 0.01343 0.00444 = 0.00724 0.00095 -0.00383 0.00121 AFIX 43 H7B 2 0.077610 0.038606 0.486849 11.00000 -1.20000 AFIX 0 C8B 1 0.160640 0.073868 0.346051 11.00000 0.00608 0.01004 = 0.01101 -0.00320 -0.00129 -0.00068 C9B 1 0.068194 0.209939 0.380492 11.00000 0.01041 0.01081 = 0.00817 -0.00457 0.00348 -0.00260 AFIX 23 H9BA 2 0.044534 0.175130 0.406711 11.00000 -1.20000 H9BB 2 0.012596 0.261796 0.364932 11.00000 -1.20000 AFIX 0 C10B 1 0.129047 0.237015 0.409346 11.00000 0.01752 0.02301 = 0.01878 -0.01128 0.00341 -0.01163 AFIX 23 H10G 2 0.162170 0.262802 0.382841 11.00000 -1.20000 H10H 2 0.177554 0.186003 0.430881 11.00000 -1.20000 AFIX 0 C11B 1 0.068394 0.301888 0.445779 11.00000 0.02291 0.01933 = 0.02260 -0.01107 0.00403 -0.00917 AFIX 137 H11J 2 0.018442 0.351119 0.424728 11.00000 -1.50000 H11K 2 0.108223 0.321317 0.462265 11.00000 -1.50000 H11L 2 0.039571 0.274881 0.473738 11.00000 -1.50000 AFIX 0 C12B 1 0.118890 0.210889 0.285345 11.00000 0.01425 0.00784 = 0.00811 0.00033 0.00234 -0.00527 AFIX 23 H12G 2 0.175779 0.177729 0.264942 11.00000 -1.20000 H12H 2 0.122760 0.263680 0.290959 11.00000 -1.20000 AFIX 0 C13B 1 0.030362 0.236023 0.252161 11.00000 0.01528 0.00802 = 0.01059 0.00239 0.00107 -0.00555 AFIX 23 H13G 2 0.027468 0.183586 0.244927 11.00000 -1.20000 H13H 2 -0.027016 0.267907 0.272656 11.00000 -1.20000 AFIX 0 C14B 1 0.032198 0.291695 0.199362 11.00000 0.02521 0.01582 = 0.01347 0.00187 -0.00303 -0.00777 AFIX 137 H14J 2 0.085753 0.258296 0.177655 11.00000 -1.50000 H14K 2 0.039086 0.341803 0.206489 11.00000 -1.50000 H14L 2 -0.027064 0.310724 0.180048 11.00000 -1.50000 AFIX 0 C15B 1 0.342900 -0.306042 0.325614 11.00000 0.00503 0.00667 = 0.01844 -0.00307 -0.00026 0.00159 C16B 1 0.371300 -0.388899 0.362918 11.00000 0.00833 0.00922 = 0.02312 -0.00104 -0.00098 -0.00086 C17B 1 0.392958 -0.465244 0.344657 11.00000 0.01458 0.01238 = 0.03530 -0.00229 -0.01407 -0.00176 AFIX 43 H17B 2 0.386550 -0.465062 0.307738 11.00000 -1.20000 AFIX 0 C18B 1 0.423926 -0.542118 0.379535 11.00000 0.01780 0.00993 = 0.05176 -0.00317 -0.01180 -0.00530 AFIX 43 H18B 2 0.438499 -0.594221 0.366669 11.00000 -1.20000 AFIX 0 C19B 1 0.433248 -0.541981 0.432829 11.00000 0.01256 0.00847 = 0.04450 0.01250 -0.01024 -0.00380 C20B 1 0.408705 -0.466843 0.452676 11.00000 0.01423 0.01483 = 0.02598 0.00339 0.00102 0.00156 AFIX 43 H20B 2 0.412591 -0.467121 0.489858 11.00000 -1.20000 AFIX 0 C21B 1 0.378118 -0.390556 0.417190 11.00000 0.01331 0.00571 = 0.02487 0.00192 0.00317 0.00213 AFIX 43 H21B 2 0.361509 -0.338368 0.430442 11.00000 -1.20000 AFIX 0 C22B 1 0.314841 -0.248477 0.233465 11.00000 0.00976 0.01355 = 0.01422 -0.00576 0.00030 -0.00097 C23B 1 0.313122 -0.219169 0.134686 11.00000 0.01744 0.03738 = 0.01337 -0.01409 0.00370 -0.00681 AFIX 23 H23G 2 0.356630 -0.254115 0.108659 11.00000 -1.20000 H23H 2 0.333604 -0.174973 0.139524 11.00000 -1.20000 AFIX 0 C24B 1 0.213716 -0.175602 0.112472 11.00000 0.02523 0.02830 = 0.01975 -0.00076 -0.00442 -0.01555 AFIX 23 H24G 2 0.172348 -0.133125 0.135380 11.00000 -1.20000 H24H 2 0.189112 -0.218921 0.113532 11.00000 -1.20000 AFIX 0 C25B 1 0.209218 -0.130448 0.055291 11.00000 0.02857 0.03021 = 0.02584 0.00337 -0.00861 -0.01724 AFIX 137 H25J 2 0.248393 -0.172519 0.032194 11.00000 -1.50000 H25K 2 0.232911 -0.087070 0.054049 11.00000 -1.50000 H25L 2 0.143456 -0.102702 0.042837 11.00000 -1.50000 AFIX 0 C26B 1 0.330836 -0.364230 0.183487 11.00000 0.01507 0.04095 = 0.02518 -0.00515 0.00196 -0.01571 AFIX 23 H26G 2 0.296386 -0.381645 0.213753 11.00000 -1.20000 H26H 2 0.302337 -0.363739 0.149921 11.00000 -1.20000 AFIX 0 C27B 1 0.433097 -0.427991 0.185557 11.00000 0.02171 0.03287 = 0.03943 -0.01753 0.00354 -0.00929 AFIX 23 H27G 2 0.462592 -0.427820 0.218582 11.00000 -1.20000 H27H 2 0.467513 -0.412455 0.154524 11.00000 -1.20000 AFIX 0 C28B 1 0.439332 -0.517044 0.184616 11.00000 0.03975 0.02870 = 0.06817 -0.02614 0.01347 -0.01378 AFIX 137 H28J 2 0.412540 -0.517434 0.151123 11.00000 -1.50000 H28K 2 0.403634 -0.531329 0.214859 11.00000 -1.50000 H28L 2 0.505821 -0.559475 0.187262 11.00000 -1.50000 AFIX 0 PT1A 6 0.724637 -0.135146 0.181171 11.00000 0.01354 0.00753 = 0.00564 -0.00120 0.00045 -0.00434 BR1A 3 0.863432 -0.078326 -0.149686 11.00000 0.01918 0.01983 = 0.00761 0.00269 -0.00006 -0.01139 BR2A 3 0.514664 0.392546 0.014336 11.00000 0.03025 0.01300 = 0.06092 0.01466 -0.01924 -0.00927 S1A 7 0.797451 -0.276544 0.208886 11.00000 0.02023 0.00835 = 0.00652 0.00030 -0.00070 -0.00426 S2A 7 0.718149 -0.110825 0.265437 11.00000 0.04328 0.01602 = 0.00684 -0.00242 0.00026 -0.01469 O1A 5 0.729286 -0.149091 0.103791 11.00000 0.01759 0.01236 = 0.00767 -0.00061 0.00026 -0.00331 O2A 5 0.661813 -0.009541 0.150378 11.00000 0.02195 0.00885 = 0.01141 -0.00256 0.00062 -0.00551 N1A 4 0.843733 -0.291243 0.101398 11.00000 0.01291 0.01242 = 0.00466 0.00003 -0.00027 -0.00608 N2A 4 0.883467 -0.412638 0.161501 11.00000 0.01060 0.00782 = 0.00925 -0.00077 0.00069 -0.00262 N3A 4 0.667870 0.059754 0.220502 11.00000 0.02181 0.01211 = 0.01711 -0.00558 -0.00812 0.00092 N4A 4 0.678185 0.025641 0.310268 11.00000 0.03151 0.02149 = 0.01661 -0.00962 -0.00799 0.00359 C1A 1 0.790513 -0.210275 0.081341 11.00000 0.00883 0.00738 = 0.00756 -0.00271 -0.00056 -0.00381 C2A 1 0.804003 -0.184812 0.023116 11.00000 0.00928 0.00891 = 0.00602 0.00143 -0.00233 -0.00525 C3A 1 0.740015 -0.103665 -0.002199 11.00000 0.01203 0.01663 = 0.01034 -0.00531 0.00095 -0.00466 AFIX 43 H3A 2 0.685617 -0.069244 0.016514 11.00000 -1.20000 AFIX 0 C4A 1 0.756181 -0.073779 -0.054456 11.00000 0.01117 0.00879 = 0.00872 0.00239 -0.00434 -0.00160 AFIX 43 H4A 2 0.712202 -0.019792 -0.071971 11.00000 -1.20000 AFIX 0 C5A 1 0.837006 -0.123542 -0.080634 11.00000 0.01713 0.01243 = 0.00629 -0.00067 -0.00096 -0.01272 C6A 1 0.899639 -0.204014 -0.056600 11.00000 0.01055 0.01296 = 0.01025 -0.00242 0.00049 -0.00304 AFIX 43 H6A 2 0.954430 -0.237835 -0.075292 11.00000 -1.20000 AFIX 0 C7A 1 0.881956 -0.234913 -0.005164 11.00000 0.01351 0.01290 = 0.00924 -0.00420 0.00207 -0.00674 AFIX 43 H7A 2 0.923618 -0.290966 0.010907 11.00000 -1.20000 AFIX 0 C8A 1 0.841864 -0.326523 0.152711 11.00000 0.00606 0.01057 = 0.00912 0.00006 -0.00150 -0.00347 C9A 1 0.935409 -0.464072 0.119544 11.00000 0.01220 0.00760 = 0.01082 -0.00129 0.00033 -0.00161 AFIX 23 H9AA 2 0.991278 -0.515047 0.135700 11.00000 -1.20000 H9AB 2 0.958766 -0.429649 0.092797 11.00000 -1.20000 AFIX 0 C10A 1 0.876306 -0.493498 0.091403 11.00000 0.01477 0.02242 = 0.01839 -0.00737 0.00130 -0.00858 AFIX 23 H10E 2 0.827346 -0.443397 0.069497 11.00000 -1.20000 H10F 2 0.843647 -0.519167 0.118330 11.00000 -1.20000 AFIX 0 C11A 1 0.937297 -0.559221 0.055640 11.00000 0.02969 0.01983 = 0.02222 -0.00892 0.00710 -0.01405 AFIX 137 H11G 2 0.973771 -0.535643 0.030913 11.00000 -1.50000 H11H 2 0.896484 -0.572653 0.035268 11.00000 -1.50000 H11I 2 0.980840 -0.611611 0.077753 11.00000 -1.50000 AFIX 0 C12A 1 0.882666 -0.463169 0.213916 11.00000 0.00910 0.00808 = 0.00948 0.00160 0.00202 -0.00237 AFIX 23 H12E 2 0.878719 -0.515989 0.208441 11.00000 -1.20000 H12F 2 0.825439 -0.429480 0.233901 11.00000 -1.20000 AFIX 0 C13A 1 0.969617 -0.487727 0.247043 11.00000 0.01501 0.01533 = 0.00905 0.00102 -0.00090 -0.00572 AFIX 23 H13E 2 0.972133 -0.435106 0.254232 11.00000 -1.20000 H13F 2 1.027213 -0.519461 0.226654 11.00000 -1.20000 AFIX 0 C14A 1 0.968285 -0.543237 0.299818 11.00000 0.02858 0.01433 = 0.00928 0.00383 -0.00110 -0.00978 AFIX 137 H14G 2 0.965356 -0.595177 0.292777 11.00000 -1.50000 H14H 2 0.912676 -0.511041 0.320696 11.00000 -1.50000 H14I 2 1.025968 -0.559213 0.319941 11.00000 -1.50000 AFIX 0 C15A 1 0.655305 0.054440 0.171084 11.00000 0.00219 0.01650 = 0.01885 -0.00740 0.00246 0.00039 C16A 1 0.626485 0.135724 0.132705 11.00000 0.00249 0.01015 = 0.02372 -0.00280 -0.00013 0.00073 C17A 1 0.610263 0.212769 0.149816 11.00000 0.01309 0.01494 = 0.03264 -0.00201 -0.00901 -0.00335 AFIX 43 H17A 2 0.620915 0.212792 0.186130 11.00000 -1.20000 AFIX 0 C18A 1 0.579052 0.288503 0.114622 11.00000 0.01792 0.01340 = 0.04392 -0.00302 -0.01068 -0.00359 AFIX 43 H18A 2 0.567456 0.340646 0.126535 11.00000 -1.20000 AFIX 0 C19A 1 0.564961 0.287501 0.062094 11.00000 0.01079 0.00840 = 0.04285 0.00776 -0.00476 -0.00113 C20A 1 0.582814 0.212011 0.043162 11.00000 0.01323 0.01630 = 0.02294 0.00203 0.00161 -0.00447 AFIX 43 H20A 2 0.573530 0.212308 0.006591 11.00000 -1.20000 AFIX 0 C21A 1 0.614592 0.136133 0.079157 11.00000 0.01300 0.00900 = 0.02012 -0.00350 0.00612 -0.00208 AFIX 43 H21A 2 0.628354 0.083784 0.066840 11.00000 -1.20000 AFIX 0 C22A 1 0.684951 -0.002951 0.263350 11.00000 0.00942 0.02240 = 0.01611 -0.00793 -0.00373 -0.00086 C23A 1 0.682944 -0.028477 0.362446 11.00000 0.02225 0.03947 = 0.01200 -0.01084 -0.00415 -0.00037 AFIX 23 H23E 2 0.663101 -0.073185 0.357858 11.00000 -1.20000 H23F 2 0.638325 0.007386 0.387727 11.00000 -1.20000 AFIX 0 C24A 1 0.781713 -0.070823 0.385551 11.00000 0.02930 0.03020 = 0.02457 -0.00111 -0.00745 -0.01283 AFIX 23 H24E 2 0.805911 -0.027204 0.384400 11.00000 -1.20000 H24F 2 0.824266 -0.114243 0.363530 11.00000 -1.20000 AFIX 0 C25A 1 0.782834 -0.114102 0.443420 11.00000 0.03382 0.04143 = 0.02479 -0.00351 -0.00421 -0.02384 AFIX 137 H25G 2 0.745574 -0.147001 0.446063 11.00000 -1.50000 H25H 2 0.755353 -0.070220 0.466921 11.00000 -1.50000 H25I 2 0.848293 -0.152740 0.454252 11.00000 -1.50000 AFIX 0 C26A 1 0.668779 0.116406 0.311634 11.00000 0.02063 0.05027 = 0.01863 -0.00268 -0.00041 -0.01924 AFIX 23 H26E 2 0.696715 0.117044 0.345100 11.00000 -1.20000 H26F 2 0.704056 0.132305 0.281210 11.00000 -1.20000 AFIX 0 C27A 1 0.566799 0.180242 0.308491 11.00000 0.01997 0.04208 = 0.04385 -0.01895 0.00530 -0.01152 AFIX 23 H27E 2 0.531830 0.166684 0.339934 11.00000 -1.20000 H27F 2 0.537655 0.178181 0.275879 11.00000 -1.20000 AFIX 0 C28A 1 0.561622 0.268310 0.307106 11.00000 0.04800 0.03654 = 0.07537 -0.03928 0.02244 -0.01800 AFIX 137 H28G 2 0.591005 0.283495 0.274104 11.00000 -1.50000 H28H 2 0.595338 0.268435 0.337966 11.00000 -1.50000 H28I 2 0.495157 0.310241 0.308349 11.00000 -1.50000 AFIX 0 PT1C 6 0.254363 0.390537 0.317207 11.00000 0.00903 0.00357 = 0.00500 -0.00074 0.00036 -0.00043 BR1C 3 0.134944 0.330220 0.651068 11.00000 0.01955 0.01964 = 0.00725 0.00260 0.00032 -0.01108 BR2C 3 0.500946 -0.148084 0.467828 11.00000 0.02417 0.00945 = 0.02729 0.00786 -0.00967 -0.00508 S1C 7 0.178987 0.531769 0.290958 11.00000 0.01829 0.00511 = 0.00638 -0.00053 -0.00051 -0.00172 S2C 7 0.253260 0.371675 0.232386 11.00000 0.02597 0.00675 = 0.00690 -0.00115 -0.00393 0.00013 O1C 5 0.254023 0.401467 0.395264 11.00000 0.01845 0.00965 = 0.00554 -0.00096 -0.00062 0.00059 O2C 5 0.322766 0.264017 0.345805 11.00000 0.01851 0.00796 = 0.00928 -0.00304 0.00087 -0.00171 N1C 4 0.144965 0.545073 0.399353 11.00000 0.01189 0.00928 = 0.00698 -0.00076 0.00025 -0.00394 N2C 4 0.104183 0.667259 0.338660 11.00000 0.01200 0.00277 = 0.00837 0.00002 0.00254 -0.00051 N3C 4 0.352256 0.197739 0.269049 11.00000 0.01139 0.00677 = 0.01290 -0.00077 -0.00101 -0.00384 N4C 4 0.350762 0.243055 0.180026 11.00000 0.01632 0.01355 = 0.01165 -0.00286 0.00224 -0.00718 C1C 1 0.196237 0.463706 0.418526 11.00000 0.00866 0.00997 = 0.00947 -0.00203 -0.00151 -0.00382 C2C 1 0.186385 0.437685 0.476699 11.00000 0.01182 0.00812 = 0.00896 -0.00402 -0.00162 -0.00489 C3C 1 0.250014 0.355750 0.500911 11.00000 0.00819 0.00600 = 0.01102 -0.00068 0.00033 0.00057 AFIX 43 H3C 2 0.302889 0.321271 0.481254 11.00000 -1.20000 AFIX 0 C4C 1 0.236193 0.324838 0.553301 11.00000 0.01546 0.01054 = 0.00894 0.00193 -0.00092 -0.00586 AFIX 43 H4C 2 0.279523 0.269763 0.569826 11.00000 -1.20000 AFIX 0 C5C 1 0.157264 0.376303 0.581316 11.00000 0.01521 0.01304 = 0.00471 -0.00082 -0.00090 -0.00790 C6C 1 0.095606 0.457999 0.558555 11.00000 0.01371 0.01222 = 0.00729 -0.00241 0.00204 -0.00471 AFIX 43 H6C 2 0.042866 0.492507 0.578281 11.00000 -1.20000 AFIX 0 C7C 1 0.111524 0.488979 0.506734 11.00000 0.01050 0.00436 = 0.00951 0.00288 -0.00538 0.00160 AFIX 43 H7C 2 0.070897 0.545899 0.491486 11.00000 -1.20000 AFIX 0 C8C 1 0.142881 0.581253 0.347785 11.00000 0.00582 0.00826 = 0.01228 -0.00383 -0.00016 -0.00008 C9C 1 0.058968 0.718636 0.381952 11.00000 0.01040 0.00904 = 0.00715 -0.00263 0.00101 -0.00302 AFIX 23 H9CA 2 0.037067 0.684951 0.410164 11.00000 -1.20000 H9CB 2 0.002676 0.770895 0.367575 11.00000 -1.20000 AFIX 0 C10C 1 0.125770 0.744739 0.406583 11.00000 0.01403 0.01643 = 0.01832 -0.01015 0.00450 -0.00783 AFIX 23 H10C 2 0.176272 0.693338 0.426629 11.00000 -1.20000 H10D 2 0.156133 0.769971 0.377851 11.00000 -1.20000 AFIX 0 C11C 1 0.072254 0.809678 0.444074 11.00000 0.02659 0.01610 = 0.02295 -0.01076 -0.00029 -0.01113 AFIX 137 H11D 2 0.018962 0.858433 0.424987 11.00000 -1.50000 H11E 2 0.115018 0.829831 0.456676 11.00000 -1.50000 H11F 2 0.048323 0.782588 0.474699 11.00000 -1.50000 AFIX 0 C12C 1 0.100626 0.717717 0.285754 11.00000 0.01469 0.00736 = 0.00551 0.00001 0.00238 -0.00317 AFIX 23 H12C 2 0.155561 0.683628 0.264442 11.00000 -1.20000 H12D 2 0.106736 0.769978 0.290246 11.00000 -1.20000 AFIX 0 C13C 1 0.010130 0.744210 0.254798 11.00000 0.01514 0.00747 = 0.00969 0.00333 -0.00108 -0.00397 AFIX 23 H13C 2 0.003577 0.692390 0.249748 11.00000 -1.20000 H13D 2 -0.045296 0.779068 0.275517 11.00000 -1.20000 AFIX 0 C14C 1 0.011975 0.795764 0.200717 11.00000 0.02547 0.01252 = 0.01360 0.00119 0.00087 -0.00547 AFIX 137 H14D 2 0.063239 0.759471 0.178945 11.00000 -1.50000 H14E 2 0.022619 0.845040 0.205633 11.00000 -1.50000 H14F 2 -0.048740 0.816068 0.182654 11.00000 -1.50000 AFIX 0 C15C 1 0.348166 0.200951 0.320803 11.00000 0.00408 0.00253 = 0.01716 -0.00180 -0.00139 -0.00019 C16C 1 0.382110 0.115771 0.355956 11.00000 0.00764 0.00870 = 0.01225 -0.00274 0.00049 -0.00388 C17C 1 0.413841 0.040051 0.334790 11.00000 0.01942 0.01082 = 0.01265 0.00029 -0.00817 -0.00450 AFIX 43 H17C 2 0.412733 0.042139 0.297215 11.00000 -1.20000 AFIX 0 C18C 1 0.447240 -0.038843 0.367785 11.00000 0.02692 0.00344 = 0.02427 -0.00183 -0.01107 -0.00243 AFIX 43 H18C 2 0.467902 -0.090456 0.353144 11.00000 -1.20000 AFIX 0 C19C 1 0.449815 -0.040775 0.422152 11.00000 0.01207 0.00758 = 0.01961 0.00692 -0.00713 -0.00522 C20C 1 0.416563 0.033552 0.444930 11.00000 0.01225 0.01120 = 0.01764 -0.00156 0.00178 0.00049 AFIX 43 H20C 2 0.416316 0.031065 0.482597 11.00000 -1.20000 AFIX 0 C21C 1 0.383606 0.111782 0.411293 11.00000 0.01359 0.00642 = 0.01281 -0.00068 0.00027 0.00137 AFIX 43 H21C 2 0.361766 0.163320 0.426155 11.00000 -1.20000 AFIX 0 C22C 1 0.323712 0.264056 0.229042 11.00000 0.00884 0.01042 = 0.01287 -0.00611 -0.00008 -0.00223 C23C 1 0.324789 0.305544 0.130669 11.00000 0.02007 0.01479 = 0.01003 -0.00178 0.00424 -0.00944 AFIX 23 H23C 2 0.381562 0.292834 0.107530 11.00000 -1.20000 H23D 2 0.304530 0.363594 0.139893 11.00000 -1.20000 AFIX 0 C24C 1 0.246761 0.305672 0.099726 11.00000 0.03521 0.03079 = 0.03146 0.01176 -0.01812 -0.02368 AFIX 23 H24C 2 0.191585 0.313330 0.123529 11.00000 -1.20000 H24D 2 0.268943 0.249646 0.087138 11.00000 -1.20000 AFIX 0 C25C 1 0.216350 0.377064 0.051864 11.00000 0.03530 0.02100 = 0.02290 0.00267 -0.01147 -0.01716 AFIX 137 H25D 2 0.171003 0.371293 0.030302 11.00000 -1.50000 H25E 2 0.272015 0.372961 0.030085 11.00000 -1.50000 H25F 2 0.186485 0.432828 0.064439 11.00000 -1.50000 AFIX 0 C26C 1 0.407766 0.152061 0.173975 11.00000 0.01131 0.01796 = 0.01833 -0.00845 0.00180 -0.00312 AFIX 23 H26C 2 0.457390 0.125126 0.201858 11.00000 -1.20000 H26D 2 0.439943 0.149187 0.138796 11.00000 -1.20000 AFIX 0 C27C 1 0.350619 0.101138 0.178083 11.00000 0.01155 0.01410 = 0.01706 -0.00141 -0.00154 -0.00365 AFIX 23 H27C 2 0.303583 0.125101 0.148829 11.00000 -1.20000 H27D 2 0.315820 0.105669 0.212467 11.00000 -1.20000 AFIX 0 C28C 1 0.415571 0.006511 0.174544 11.00000 0.02607 0.01386 = 0.03406 -0.00576 0.00389 -0.00710 AFIX 137 H28D 2 0.446329 0.001713 0.139413 11.00000 -1.50000 H28E 2 0.377874 -0.026178 0.179488 11.00000 -1.50000 H28F 2 0.463973 -0.016408 0.202474 11.00000 -1.50000 AFIX 0 HKLF 4 REM cu_18_046_4BrPrPt3_0m_a.res in P-1 REM R1 = 0.0322 for 18197 Fo > 4sig(Fo) and 0.0483 for all 24579 data REM 1421 parameters refined using 0 restraints END WGHT 0.0364 16.9397 REM Highest difference peak 1.558, deepest hole -2.362, 1-sigma level 0.182 Q1 1 0.5958 0.1017 0.3244 11.00000 0.05 1.56 Q2 1 0.4043 -0.3537 0.1752 11.00000 0.05 1.50 Q3 1 0.3517 -0.4203 0.1770 11.00000 0.05 1.05 Q4 1 0.6488 0.1705 0.3197 11.00000 0.05 1.00 Q5 1 0.3634 -0.2584 0.1786 11.00000 0.05 0.96 ; _shelx_res_checksum 60497 _shelx_hkl_file ; -1 0 0 56.19 2.50 -1 0 0 51.29 2.60 -1 0 0 47.90 2.50 -1 0 0 57.09 2.50 1 0 0 55.39 2.50 1 0 0 51.29 2.50 1 0 0 51.59 2.50 -2 0 0 2521.25 106.29 -2 0 0 2500.45 106.49 -2 0 0 2414.86 106.39 -2 0 0 2413.56 106.29 2 0 0 2592.84 106.39 2 0 0 2652.23 106.39 2 0 0 2560.94 106.19 2 0 0 2543.45 106.49 -3 0 0 364.56 16.20 -3 0 0 387.16 16.50 -3 0 0 401.06 16.40 -3 0 0 340.97 16.50 3 0 0 367.06 16.10 3 0 0 354.66 16.50 3 0 0 396.66 16.40 3 0 0 354.36 16.30 -4 0 0 596.54 25.30 -4 0 0 603.44 25.70 -4 0 0 569.54 25.30 -4 0 0 611.14 25.60 -4 0 0 563.84 25.30 4 0 0 553.34 25.50 4 0 0 574.24 25.30 4 0 0 606.44 25.60 4 0 0 576.34 25.20 -5 0 0 1143.09 48.80 -5 0 0 1152.48 48.80 -5 0 0 1128.89 49.30 -5 0 0 1140.69 49.10 -5 0 0 1126.49 48.80 5 0 0 1144.19 48.70 5 0 0 1096.29 49.20 5 0 0 1147.09 48.70 5 0 0 1181.78 49.20 -6 0 0 102.19 5.70 -6 0 0 97.09 6.10 -6 0 0 99.49 5.90 -6 0 0 105.69 5.90 -6 0 0 90.29 6.50 -6 0 0 103.09 5.90 -6 0 0 110.99 6.10 6 0 0 98.29 5.60 6 0 0 110.49 5.70 6 0 0 114.69 5.80 6 0 0 100.79 6.20 6 0 0 120.89 6.20 6 0 0 98.69 7.10 -7 0 0 585.94 26.20 -7 0 0 596.94 26.80 -7 0 0 561.04 26.10 -7 0 0 612.84 26.70 -7 0 0 535.35 26.10 -7 0 0 560.74 26.00 7 0 0 589.84 26.10 7 0 0 615.04 26.70 7 0 0 610.54 26.00 7 0 0 603.64 26.00 7 0 0 591.74 26.00 -8 0 0 1925.71 78.19 -8 0 0 1672.83 78.29 -8 0 0 1830.62 78.19 -8 0 0 1876.51 79.09 -8 0 0 1701.23 78.79 -8 0 0 1873.41 78.39 -8 0 0 1868.81 78.19 -8 0 0 1679.63 79.09 -8 0 0 1835.62 78.09 8 0 0 1862.91 77.89 8 0 0 1858.61 77.99 8 0 0 1764.22 78.19 8 0 0 1891.61 78.39 8 0 0 1899.21 78.09 8 0 0 1941.01 78.99 8 0 0 1720.13 78.89 8 0 0 1834.62 78.89 -9 0 0 475.15 22.90 -9 0 0 461.25 23.50 -9 0 0 468.35 23.20 -9 0 0 490.65 22.80 -9 0 0 485.95 22.50 -9 0 0 478.05 22.50 -9 0 0 481.75 23.50 -9 0 0 497.05 22.80 -9 0 0 468.35 22.80 -9 0 0 499.45 22.50 -9 0 0 488.75 24.00 -9 0 0 451.35 23.80 9 0 0 502.95 22.70 9 0 0 494.35 22.60 9 0 0 519.35 22.30 9 0 0 499.55 22.20 9 0 0 470.95 23.90 9 0 0 468.95 24.00 9 0 0 498.35 22.90 9 0 0 511.85 23.60 9 0 0 522.25 22.80 9 0 0 529.95 23.50 9 0 0 475.55 22.40 9 0 0 495.05 23.20 -10 0 0 249.88 13.40 -10 0 0 252.87 14.10 -10 0 0 258.97 13.40 -10 0 0 253.87 14.50 -10 0 0 288.87 15.10 -10 0 0 235.08 13.70 -10 0 0 274.97 14.70 -10 0 0 250.77 15.00 -10 0 0 238.68 14.30 -10 0 0 256.67 13.60 10 0 0 243.88 13.90 10 0 0 255.37 14.90 10 0 0 267.97 13.50 10 0 0 285.97 15.00 10 0 0 258.87 13.60 10 0 0 268.47 14.30 10 0 0 260.17 13.10 10 0 0 286.87 14.20 10 0 0 259.57 12.90 10 0 0 266.67 13.90 -11 0 0 14.00 4.60 -11 0 0 13.80 4.10 -11 0 0 2.00 4.10 -11 0 0 6.10 3.50 -11 0 0 5.00 3.90 -11 0 0 8.40 4.20 -11 0 0 8.60 3.90 -11 0 0 5.20 3.40 11 0 0 5.20 4.40 11 0 0 6.40 3.20 11 0 0 3.40 4.10 11 0 0 17.60 4.10 11 0 0 9.40 3.30 11 0 0 5.80 3.20 11 0 0 3.10 3.80 11 0 0 5.70 4.50 11 0 0 5.50 3.70 11 0 0 18.20 7.90 -12 0 0 176.98 10.50 -12 0 0 192.48 12.70 -12 0 0 187.48 11.50 -12 0 0 193.98 11.80 -12 0 0 180.08 11.60 -12 0 0 163.88 11.80 12 0 0 192.08 11.30 12 0 0 165.98 10.80 12 0 0 178.48 12.00 12 0 0 178.48 11.40 12 0 0 168.18 12.00 12 0 0 188.68 10.20 -13 0 0 629.74 32.00 -13 0 0 722.73 31.60 -13 0 0 679.83 31.80 -13 0 0 665.43 31.80 13 0 0 654.73 31.80 13 0 0 688.73 31.70 13 0 0 637.64 32.20 13 0 0 675.63 30.10 13 0 0 690.23 31.80 13 0 0 716.83 31.50 -14 0 0 21.70 4.50 -14 0 0 11.70 4.20 -14 0 0 17.00 4.30 -14 0 0 16.30 4.60 14 0 0 10.80 3.70 14 0 0 19.70 5.00 14 0 0 13.10 4.10 14 0 0 22.00 5.10 -15 0 0 302.17 15.60 -15 0 0 295.87 15.30 -15 0 0 293.67 15.90 -15 0 0 292.57 15.70 15 0 0 303.57 15.70 15 0 0 325.87 15.20 15 0 0 299.37 15.40 15 0 0 287.67 15.70 -16 0 0 79.69 6.70 -16 0 0 84.49 6.60 -16 0 0 73.79 7.00 16 0 0 83.99 6.20 16 0 0 84.19 6.30 16 0 0 80.39 8.20 16 0 0 74.69 7.20 -17 0 0 163.58 11.80 -17 0 0 194.08 10.30 17 0 0 202.58 10.70 17 0 0 204.08 10.20 17 0 0 213.48 10.40 17 -1 0 1.50 2.20 -17 1 0 8.30 3.10 -17 1 0 2.70 2.50 16 -1 0 185.88 10.10 16 -1 0 197.18 11.40 16 -1 0 189.48 10.60 16 -1 0 182.98 13.50 -16 1 0 213.48 10.80 -16 1 0 206.18 10.70 15 -1 0 18.40 3.30 15 -1 0 11.90 3.30 15 -1 0 21.60 4.60 15 -1 0 17.80 4.00 -15 1 0 12.20 3.60 -15 1 0 11.60 3.30 -15 1 0 14.40 3.40 -15 1 0 11.90 3.70 14 -1 0 261.57 17.50 14 -1 0 262.87 15.20 14 -1 0 271.47 14.90 14 -1 0 261.37 15.20 -14 1 0 291.27 16.10 -14 1 0 294.27 15.50 -14 1 0 285.17 14.80 -14 1 0 277.97 15.10 13 -1 0 48.10 7.00 13 -1 0 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136.69 10.30 -11 3 0 133.19 10.20 -11 3 0 145.89 10.00 10 -3 0 108.19 12.50 10 -3 0 100.59 8.50 10 -3 0 116.09 7.70 10 -3 0 105.79 8.60 10 -3 0 121.09 7.20 10 -3 0 94.49 12.20 10 -3 0 91.79 10.20 10 -3 0 116.79 8.70 10 -3 0 113.49 7.90 -10 3 0 106.49 9.50 -10 3 0 105.49 8.70 -10 3 0 111.59 9.60 -10 3 0 110.89 9.50 -10 3 0 94.19 9.50 -10 3 0 115.59 8.60 9 -3 0 209.18 11.20 9 -3 0 213.58 11.90 9 -3 0 216.08 13.10 9 -3 0 204.68 15.70 9 -3 0 213.78 11.20 9 -3 0 211.18 12.80 9 -3 0 219.78 11.90 9 -3 0 227.88 15.80 -9 3 0 223.28 13.00 -9 3 0 224.78 12.10 -9 3 0 218.88 13.10 -9 3 0 221.98 13.10 -9 3 0 216.88 13.30 8 -3 0 73.99 8.40 8 -3 0 77.39 7.80 8 -3 0 85.39 10.20 8 -3 0 79.49 5.60 8 -3 0 79.09 6.60 8 -3 0 70.39 7.50 8 -3 0 74.29 7.00 8 -3 0 86.59 7.10 8 -3 0 83.29 5.60 -8 3 0 72.79 9.20 -8 3 0 85.99 6.30 -8 3 0 72.09 8.30 -8 3 0 75.09 8.70 -8 3 0 82.69 7.50 -8 3 0 84.39 9.20 -8 3 0 77.29 7.80 7 -3 0 229.88 13.90 7 -3 0 254.37 13.10 7 -3 0 240.98 13.90 7 -3 0 246.48 12.20 7 -3 0 238.38 12.00 7 -3 0 241.78 12.20 7 -3 0 246.08 13.30 7 -3 0 249.28 13.80 -7 3 0 259.97 14.80 -7 3 0 259.87 12.60 -7 3 0 250.17 13.20 -7 3 0 250.17 13.80 -7 3 0 248.68 14.90 -7 3 0 239.78 14.50 -7 3 0 262.97 12.70 -7 3 0 247.68 14.00 -7 3 0 258.27 14.40 6 -3 0 28.80 3.60 6 -3 0 27.90 3.50 6 -3 0 23.50 2.90 6 -3 0 24.90 2.80 -6 3 0 26.30 3.50 -6 3 0 23.90 2.60 -6 3 0 23.80 3.70 -6 3 0 28.10 3.70 -6 3 0 23.60 3.60 5 -3 0 94.99 5.50 5 -3 0 87.19 7.40 5 -3 0 81.89 5.50 5 -3 0 88.89 4.90 5 -3 0 88.39 4.90 -5 3 0 87.49 4.40 -5 3 0 88.89 5.20 -5 3 0 66.99 5.00 -5 3 0 85.99 5.50 -5 3 0 76.19 4.60 -5 3 0 74.29 7.00 -5 3 0 73.19 5.00 4 -3 0 6.50 1.40 4 -3 0 7.10 1.60 4 -3 0 5.00 1.30 4 -3 0 4.30 2.00 -4 3 0 7.20 1.10 -4 3 0 6.30 1.40 -4 3 0 4.60 1.60 -4 3 0 6.40 1.60 -4 3 0 5.90 1.30 -4 3 0 6.00 2.70 -4 3 0 3.80 1.20 3 -3 0 46.50 3.10 3 -3 0 42.20 3.40 3 -3 0 49.40 2.90 3 -3 0 41.60 3.10 -3 3 0 46.70 3.20 -3 3 0 46.60 3.20 -3 3 0 45.20 2.80 -3 3 0 51.09 2.80 -3 3 0 43.90 2.50 -3 3 0 45.40 2.60 2 -3 0 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18.90 1.50 -4 -3 0 73.79 4.60 -4 -3 0 81.09 4.20 -4 -3 0 81.79 4.30 -4 -3 0 82.49 4.20 -4 -3 0 86.79 4.70 4 3 0 78.19 4.20 4 3 0 77.29 4.50 4 3 0 85.29 4.30 4 3 0 80.49 3.60 4 3 0 82.59 3.60 -5 -3 0 73.89 4.20 -5 -3 0 70.09 4.00 -5 -3 0 71.49 3.70 -5 -3 0 70.09 4.00 -5 -3 0 71.29 4.40 5 3 0 61.99 4.10 5 3 0 68.19 3.30 5 3 0 68.49 4.00 5 3 0 69.39 3.30 5 3 0 62.09 4.30 -6 -3 0 88.29 4.60 -6 -3 0 82.89 4.70 -6 -3 0 85.29 5.10 -6 -3 0 79.99 4.80 -6 -3 0 87.89 5.30 6 3 0 73.79 5.30 6 3 0 81.79 5.00 6 3 0 80.79 4.10 6 3 0 84.89 4.90 6 3 0 77.49 4.00 -7 -3 0 74.99 4.90 -7 -3 0 82.29 5.10 -7 -3 0 82.09 5.50 -7 -3 0 70.49 4.50 -7 -3 0 74.89 4.30 -7 -3 0 74.69 4.50 -7 -3 0 68.19 5.30 7 3 0 61.79 4.00 7 3 0 71.69 5.20 7 3 0 70.79 4.70 -8 -3 0 37.10 4.00 -8 -3 0 43.80 3.20 -8 -3 0 33.00 4.50 -8 -3 0 36.90 3.90 -8 -3 0 38.70 3.30 -8 -3 0 38.20 4.00 -8 -3 0 35.60 3.30 8 3 0 41.00 5.00 8 3 0 35.80 3.10 8 3 0 29.20 3.10 -9 -3 0 276.07 15.30 -9 -3 0 280.97 13.00 -9 -3 0 269.17 14.30 -9 -3 0 285.37 13.90 -9 -3 0 246.18 14.70 -9 -3 0 282.37 14.20 -9 -3 0 291.67 13.40 -9 -3 0 282.37 13.20 -9 -3 0 299.97 14.30 -9 -3 0 278.87 14.40 9 3 0 301.47 14.00 9 3 0 296.17 15.40 9 3 0 256.77 14.90 9 3 0 258.17 14.70 9 3 0 230.28 15.10 9 3 0 262.27 15.10 9 3 0 270.27 12.90 9 3 0 265.67 12.80 -10 -3 0 154.38 14.40 -10 -3 0 153.88 10.60 -10 -3 0 181.68 9.80 -10 -3 0 175.58 10.40 -10 -3 0 196.48 10.80 -10 -3 0 177.38 11.50 -10 -3 0 147.19 14.00 -10 -3 0 173.28 10.30 -10 -3 0 186.28 9.50 -10 -3 0 184.98 9.60 -10 -3 0 183.18 11.60 10 3 0 196.98 10.20 10 3 0 179.58 11.50 10 3 0 175.48 10.90 10 3 0 188.18 11.20 10 3 0 192.48 13.10 10 3 0 164.98 11.20 -11 -3 0 10.50 6.70 -11 -3 0 21.80 3.80 -11 -3 0 24.00 6.70 -11 -3 0 18.60 3.80 -11 -3 0 26.50 4.60 -11 -3 0 16.00 4.60 -11 -3 0 26.90 6.10 -11 -3 0 32.20 4.40 -11 -3 0 21.50 3.30 -11 -3 0 24.50 3.80 -11 -3 0 26.20 4.50 -11 -3 0 27.90 5.00 11 3 0 32.90 6.20 11 3 0 22.50 4.60 11 3 0 19.60 3.60 11 3 0 20.90 6.10 11 3 0 26.90 4.70 11 3 0 22.10 4.70 11 3 0 25.30 4.90 -12 -3 0 164.28 9.60 -12 -3 0 167.38 10.80 -12 -3 0 159.48 9.50 -12 -3 0 142.49 12.80 -12 -3 0 166.68 12.20 -12 -3 0 162.18 12.60 -12 -3 0 149.99 10.20 -12 -3 0 137.89 9.90 -12 -3 0 164.88 9.20 12 3 0 153.78 10.30 12 3 0 151.98 10.10 12 3 0 130.59 10.30 12 3 0 154.08 11.80 12 3 0 168.28 10.50 12 3 0 147.69 10.50 -13 -3 0 21.30 3.90 -13 -3 0 18.80 4.40 -13 -3 0 16.20 4.20 -13 -3 0 18.70 4.30 -13 -3 0 12.10 3.40 -13 -3 0 21.60 6.00 -13 -3 0 18.50 6.10 13 3 0 10.90 4.10 13 3 0 20.60 7.00 13 3 0 22.40 4.30 13 3 0 18.20 4.50 13 3 0 22.50 4.50 13 3 0 15.20 4.40 -14 -3 0 306.97 16.50 -14 -3 0 322.17 16.60 -14 -3 0 313.67 15.50 -14 -3 0 315.37 16.50 -14 -3 0 293.47 17.50 -14 -3 0 307.87 15.30 14 3 0 291.17 16.10 14 3 0 321.97 16.60 14 3 0 313.57 16.70 14 3 0 290.57 18.20 -15 -3 0 10.60 5.50 -15 -3 0 12.10 3.80 -15 -3 0 9.50 3.90 -15 -3 0 11.90 4.40 15 3 0 7.50 4.10 15 3 0 17.20 4.20 15 3 0 18.20 6.20 -16 -3 0 187.78 11.00 -16 -3 0 201.38 10.90 -16 -3 0 171.48 10.40 -16 -3 0 183.88 11.90 16 3 0 177.78 10.90 16 3 0 164.58 10.50 16 3 0 186.68 10.90 -17 -3 0 14.50 3.30 -17 -3 0 15.70 3.10 -17 -3 0 15.00 4.00 -17 -3 0 12.60 3.00 17 3 0 7.70 2.90 17 3 0 10.10 3.20 -18 -3 0 205.38 10.80 -18 -3 0 206.18 12.20 18 3 0 237.78 11.40 15 -4 0 5.10 2.30 15 -4 0 3.90 3.30 -15 4 0 4.90 2.40 14 -4 0 1.80 2.60 14 -4 0 -1.40 2.90 14 -4 0 2.60 3.00 -14 4 0 -0.70 3.20 -14 4 0 -0.40 2.50 13 -4 0 60.59 5.40 13 -4 0 58.79 7.80 13 -4 0 44.10 6.60 13 -4 0 68.69 6.20 13 -4 0 60.09 6.70 13 -4 0 62.09 6.30 -13 4 0 59.29 6.60 -13 4 0 51.89 8.70 -13 4 0 40.50 6.00 12 -4 0 756.72 33.40 12 -4 0 768.12 34.50 12 -4 0 661.93 36.50 12 -4 0 803.02 34.60 12 -4 0 719.63 34.30 12 -4 0 756.32 33.30 -12 4 0 739.43 34.60 -12 4 0 771.22 34.90 11 -4 0 58.69 7.10 11 -4 0 68.79 10.10 11 -4 0 70.29 6.10 11 -4 0 72.89 6.00 11 -4 0 46.30 7.00 11 -4 0 41.70 6.70 11 -4 0 59.39 8.90 11 -4 0 48.60 7.10 -11 4 0 57.49 9.00 -11 4 0 53.09 7.20 -11 4 0 64.59 10.00 -11 4 0 52.59 6.80 -11 4 0 48.50 6.60 -11 4 0 51.99 7.80 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7.50 -7 4 0 40.80 5.90 -7 4 0 43.50 6.80 -7 4 0 49.00 6.90 -7 4 0 49.80 4.80 -7 4 0 42.60 6.50 -7 4 0 44.40 9.50 -7 4 0 54.59 7.60 6 -4 0 378.16 16.30 6 -4 0 349.96 18.30 6 -4 0 320.87 18.10 6 -4 0 389.56 16.50 6 -4 0 349.96 17.10 -6 4 0 328.77 17.90 -6 4 0 323.47 18.40 -6 4 0 354.86 18.20 -6 4 0 371.76 18.30 -6 4 0 395.96 17.10 -6 4 0 287.17 19.00 -6 4 0 335.07 16.20 5 -4 0 153.98 7.60 5 -4 0 144.39 7.60 5 -4 0 141.69 8.00 5 -4 0 141.89 8.20 -5 4 0 155.88 8.30 -5 4 0 142.79 7.50 -5 4 0 154.48 8.50 4 -4 0 4060.29 165.78 4 -4 0 4158.58 165.68 4 -4 0 3977.10 164.98 4 -4 0 3975.50 164.98 4 -4 0 3902.91 165.08 -4 4 0 4004.10 164.68 -4 4 0 3831.42 165.58 -4 4 0 3952.50 164.18 -4 4 0 3844.42 165.48 -4 4 0 3402.46 164.18 3 -4 0 402.76 17.30 3 -4 0 393.26 17.90 3 -4 0 404.16 17.40 3 -4 0 422.96 17.80 -3 4 0 373.56 17.70 -3 4 0 369.86 16.70 -3 4 0 411.46 17.00 -3 4 0 395.06 17.80 -3 4 0 353.66 17.20 2 -4 0 2949.21 120.69 2 -4 0 2825.72 120.39 2 -4 0 2915.81 120.39 2 -4 0 2798.62 120.89 2 -4 0 3145.59 120.79 -2 4 0 2720.93 119.99 -2 4 0 2820.32 119.99 -2 4 0 2867.61 119.99 -2 4 0 2827.52 120.79 -2 4 0 2676.33 119.99 1 -4 0 754.42 32.80 1 -4 0 741.93 32.90 1 -4 0 823.62 32.90 1 -4 0 833.62 32.40 1 -4 0 699.63 32.70 -1 4 0 743.73 32.50 -1 4 0 752.02 32.50 -1 4 0 797.32 33.00 -1 4 0 741.63 32.50 0 -4 0 2099.49 93.49 0 -4 0 2099.99 93.39 0 -4 0 2557.94 93.89 0 -4 0 2073.69 93.59 0 4 0 2154.28 93.59 0 4 0 2328.37 93.39 0 4 0 2174.28 93.59 0 4 0 2278.37 93.79 -1 -4 0 201.18 9.30 -1 -4 0 205.48 9.40 1 4 0 185.88 9.40 1 4 0 220.28 9.40 1 4 0 201.48 9.50 1 4 0 221.18 9.20 1 4 0 233.18 9.30 -2 -4 0 871.41 37.80 -2 -4 0 861.41 37.30 -2 -4 0 903.11 37.80 -2 -4 0 844.12 37.50 -2 -4 0 862.61 37.30 2 4 0 863.91 37.60 2 4 0 929.91 37.50 2 4 0 936.41 37.70 -3 -4 0 7.80 0.90 -3 -4 0 10.10 1.50 -3 -4 0 10.10 0.80 -3 -4 0 12.40 1.60 -3 -4 0 8.60 0.90 3 4 0 11.10 1.00 3 4 0 7.50 0.90 3 4 0 8.60 1.20 -4 -4 0 1811.82 76.59 -4 -4 0 1954.80 76.29 -4 -4 0 1741.33 75.99 -4 -4 0 1866.91 76.59 -4 -4 0 1811.72 75.39 -4 -4 0 1732.03 75.79 -4 -4 0 1839.92 75.89 4 4 0 1706.53 75.99 4 4 0 1793.52 75.99 4 4 0 1683.03 75.79 -5 -4 0 2919.61 120.39 -5 -4 0 2928.31 119.49 -5 -4 0 2789.32 119.79 -5 -4 0 2937.31 119.39 -5 -4 0 2896.41 119.79 5 4 0 2696.33 119.99 5 4 0 2760.92 119.79 5 4 0 2735.43 119.69 -6 -4 0 1030.70 42.20 -6 -4 0 1030.90 43.10 -6 -4 0 1004.30 42.10 -6 -4 0 1012.10 42.50 -6 -4 0 885.01 43.20 6 4 0 1019.40 42.60 6 4 0 939.31 42.60 6 4 0 943.51 41.40 -7 -4 0 608.64 26.60 -7 -4 0 562.14 26.10 -7 -4 0 637.44 27.00 -7 -4 0 620.84 26.40 -7 -4 0 577.44 25.80 -7 -4 0 607.24 25.90 7 4 0 566.44 25.00 7 4 0 602.04 26.30 7 4 0 594.04 25.00 7 4 0 519.05 26.60 -8 -4 0 4080.59 163.28 -8 -4 0 3687.43 162.18 -8 -4 0 3979.80 162.68 -8 -4 0 3920.01 162.58 -8 -4 0 4128.29 163.78 -8 -4 0 3874.41 162.68 -8 -4 0 3971.00 163.38 8 4 0 3502.05 161.58 8 4 0 3486.45 161.58 -9 -4 0 954.50 46.40 -9 -4 0 991.20 46.50 -9 -4 0 1155.18 47.10 -9 -4 0 1077.49 45.70 -9 -4 0 1047.70 45.30 -9 -4 0 1057.69 45.60 -9 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34.10 5.60 -16 -4 0 53.79 7.80 -16 -4 0 42.00 5.00 16 4 0 30.20 4.60 16 4 0 33.90 5.20 16 4 0 49.30 11.80 16 4 0 38.20 5.70 -17 -4 0 30.50 5.70 -17 -4 0 40.10 4.60 -17 -4 0 30.60 5.00 -17 -4 0 30.90 4.90 17 4 0 31.50 4.90 17 4 0 24.00 3.80 -18 -4 0 1.20 2.30 -18 -4 0 3.40 2.70 -18 -4 0 3.00 2.40 -18 -4 0 1.10 4.80 18 4 0 0.30 2.40 18 4 0 4.00 2.70 14 -5 0 131.09 7.90 14 -5 0 116.79 7.90 14 -5 0 138.19 8.30 -14 5 0 143.49 8.10 13 -5 0 46.20 4.60 13 -5 0 41.10 6.00 13 -5 0 37.90 5.30 13 -5 0 41.80 5.30 -13 5 0 37.30 5.30 -13 5 0 55.09 6.60 -13 5 0 40.10 6.00 12 -5 0 127.89 8.60 12 -5 0 149.59 9.60 12 -5 0 140.89 8.30 12 -5 0 129.39 8.90 12 -5 0 122.89 11.80 12 -5 0 124.29 9.40 -12 5 0 144.29 10.50 -12 5 0 139.39 9.40 -12 5 0 124.79 9.80 11 -5 0 99.69 6.90 11 -5 0 98.69 12.50 11 -5 0 80.69 8.10 11 -5 0 81.69 7.80 11 -5 0 82.59 11.90 11 -5 0 72.29 8.10 11 -5 0 87.29 6.90 -11 5 0 98.89 9.20 -11 5 0 94.89 9.80 -11 5 0 102.79 8.30 10 -5 0 108.19 7.90 10 -5 0 95.49 9.00 10 -5 0 99.49 9.30 10 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0 142.49 13.40 -7 5 0 156.48 9.20 -7 5 0 156.78 12.90 6 -5 0 6.60 5.20 6 -5 0 8.20 3.50 6 -5 0 6.30 2.40 6 -5 0 8.10 2.50 6 -5 0 8.90 4.80 6 -5 0 6.60 2.10 6 -5 0 9.80 5.00 -6 5 0 12.50 4.10 -6 5 0 6.30 4.50 -6 5 0 1.20 5.60 -6 5 0 3.90 4.30 -6 5 0 8.90 2.40 -6 5 0 1.90 5.80 -6 5 0 9.40 3.90 5 -5 0 167.48 8.50 5 -5 0 169.28 8.80 5 -5 0 164.88 8.60 5 -5 0 167.88 9.40 -5 5 0 173.98 11.40 -5 5 0 173.58 9.30 -5 5 0 155.78 10.50 -5 5 0 152.88 11.20 -5 5 0 174.78 11.90 4 -5 0 5.40 2.40 4 -5 0 4.90 1.60 4 -5 0 7.80 1.60 4 -5 0 3.30 1.60 4 -5 0 5.20 3.60 -4 5 0 5.80 1.30 -4 5 0 6.10 2.10 3 -5 0 158.78 9.40 3 -5 0 189.88 8.80 3 -5 0 200.28 9.30 3 -5 0 182.88 8.80 -3 5 0 184.08 9.30 -3 5 0 175.98 8.10 2 -5 0 3.10 1.40 2 -5 0 2.30 1.40 2 -5 0 -0.40 1.00 2 -5 0 1.80 1.00 -2 5 0 1.10 1.10 -2 5 0 1.00 0.60 -2 5 0 0.30 0.80 1 -5 0 35.70 2.30 1 -5 0 31.60 2.70 1 -5 0 38.40 1.90 1 -5 0 36.40 2.80 1 -5 0 33.50 3.20 -1 5 0 32.40 2.60 -1 5 0 36.50 2.10 -1 5 0 36.20 2.70 -1 5 0 35.30 2.30 0 -5 0 1.10 0.50 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14 5 0 216.28 13.20 14 5 0 187.08 14.30 14 5 0 229.38 13.00 14 5 0 213.68 13.60 14 5 0 220.18 13.10 -15 -5 0 0.60 5.00 -15 -5 0 5.40 3.30 -15 -5 0 14.70 4.30 -15 -5 0 8.80 6.60 -15 -5 0 8.40 3.10 -15 -5 0 6.20 3.50 -15 -5 0 5.40 3.80 15 5 0 8.40 4.00 15 5 0 10.30 5.60 15 5 0 5.40 3.30 15 5 0 9.90 5.20 15 5 0 9.90 6.70 -16 -5 0 116.99 8.30 -16 -5 0 91.09 10.60 -16 -5 0 91.99 8.50 -16 -5 0 124.39 8.10 -16 -5 0 86.99 6.80 -16 -5 0 87.79 8.10 16 5 0 115.49 8.40 16 5 0 106.89 10.30 16 5 0 102.99 7.80 -17 -5 0 6.10 2.80 -17 -5 0 2.90 2.70 -17 -5 0 3.00 2.90 -17 -5 0 18.70 5.80 -17 -5 0 -1.90 2.90 17 5 0 2.80 3.10 17 5 0 2.10 2.60 -18 -5 0 158.98 9.30 -18 -5 0 172.68 19.20 -18 -5 0 167.48 9.20 -18 -5 0 165.68 9.00 18 5 0 162.28 8.90 18 5 0 160.68 9.20 14 -6 0 -0.30 2.10 14 -6 0 0.70 2.80 -14 6 0 3.10 2.10 -14 6 0 -0.60 2.30 13 -6 0 -1.20 2.40 13 -6 0 -2.60 3.40 13 -6 0 2.60 2.50 13 -6 0 -3.00 2.40 -13 6 0 -0.30 2.50 12 -6 0 1.80 2.60 12 -6 0 0.30 2.90 12 -6 0 1.60 3.20 12 -6 0 -3.40 3.60 12 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15.80 10 7 0 244.28 16.10 -11 -7 0 4.20 4.40 -11 -7 0 11.70 3.20 -11 -7 0 16.30 2.90 -11 -7 0 14.60 2.80 -11 -7 0 8.90 3.70 -11 -7 0 13.60 4.80 -11 -7 0 14.20 6.30 -11 -7 0 8.70 4.00 11 7 0 12.70 4.60 11 7 0 13.30 3.70 11 7 0 14.30 6.60 11 7 0 16.20 3.70 11 7 0 16.50 4.30 11 7 0 13.60 6.00 11 7 0 11.70 6.20 11 7 0 9.00 4.90 -12 -7 0 152.08 9.00 -12 -7 0 149.09 9.10 -12 -7 0 144.59 9.50 -12 -7 0 147.39 9.90 -12 -7 0 150.68 12.30 -12 -7 0 144.79 10.70 -12 -7 0 143.49 11.30 -12 -7 0 136.59 10.40 12 7 0 158.78 12.70 12 7 0 159.08 10.80 12 7 0 151.28 10.00 12 7 0 147.99 10.00 12 7 0 154.48 11.70 12 7 0 168.58 11.30 12 7 0 161.48 11.10 -13 -7 0 1.20 2.60 -13 -7 0 -1.80 5.90 -13 -7 0 6.10 4.00 -13 -7 0 2.40 3.50 -13 -7 0 -2.40 2.40 -13 -7 0 2.40 3.30 -13 -7 0 8.10 4.00 -13 -7 0 -7.20 6.40 13 7 0 -7.10 3.10 13 7 0 5.20 6.90 13 7 0 1.20 3.40 13 7 0 1.40 4.40 13 7 0 5.00 4.50 13 7 0 10.10 8.50 13 7 0 3.60 5.00 13 7 0 -3.10 3.90 -14 -7 0 383.86 18.40 -14 -7 0 381.56 19.40 -14 -7 0 400.76 19.70 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4.00 9 10 0 1.80 4.70 9 10 0 -0.50 3.90 9 10 0 0.10 2.50 9 10 0 0.60 3.30 9 10 0 4.80 4.80 9 10 0 5.10 5.20 9 10 0 2.10 4.10 -10 -10 0 1.40 2.00 -10 -10 0 0.90 2.10 -10 -10 0 -2.00 2.90 -10 -10 0 0.20 4.20 -10 -10 0 2.10 7.40 -10 -10 0 11.30 7.40 10 10 0 6.10 5.20 10 10 0 2.10 4.10 10 10 0 1.00 4.70 10 10 0 3.10 4.30 10 10 0 0.80 5.10 10 10 0 -1.90 3.70 10 10 0 4.20 3.10 10 10 0 5.50 3.70 -11 -10 0 -1.50 2.90 -11 -10 0 0.50 6.10 -11 -10 0 1.10 2.20 -11 -10 0 -0.50 4.70 -11 -10 0 1.00 5.80 -11 -10 0 -0.40 2.30 11 10 0 -3.00 3.30 11 10 0 -5.00 4.20 11 10 0 7.20 3.50 11 10 0 -9.10 4.70 11 10 0 6.30 3.70 11 10 0 -0.30 4.80 11 10 0 -0.80 4.70 -12 -10 0 -1.40 2.40 -12 -10 0 3.50 2.90 -12 -10 0 0.80 2.90 -12 -10 0 6.20 4.80 -12 -10 0 15.80 5.60 -12 -10 0 4.80 6.00 12 10 0 4.30 4.10 12 10 0 -1.30 5.00 12 10 0 4.80 5.00 12 10 0 -9.20 7.30 12 10 0 4.80 3.60 12 10 0 4.20 4.50 12 10 0 2.70 4.20 -13 -10 0 -0.30 2.50 -13 -10 0 0.90 3.00 -13 -10 0 3.50 4.10 -13 -10 0 -3.30 2.90 -13 -10 0 4.80 4.90 13 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13.30 4.50 6 -11 0 18.80 4.80 6 -11 0 20.30 4.10 6 -11 0 20.20 3.80 -6 11 0 17.70 5.60 -6 11 0 17.20 4.60 -6 11 0 14.40 4.40 -6 11 0 22.10 5.30 -6 11 0 19.20 4.80 -6 11 0 20.50 6.90 -6 11 0 24.60 4.90 -6 11 0 17.90 8.30 -6 11 0 32.60 7.10 5 -11 0 112.09 9.20 5 -11 0 114.79 7.80 5 -11 0 102.59 8.50 5 -11 0 107.79 7.60 5 -11 0 79.29 10.90 -5 11 0 113.99 9.40 -5 11 0 107.59 11.00 -5 11 0 105.79 10.20 -5 11 0 111.99 9.20 -5 11 0 82.19 8.70 -5 11 0 117.49 12.40 -5 11 0 92.69 10.00 -5 11 0 102.09 8.90 -5 11 0 105.09 9.30 4 -11 0 5.70 6.50 4 -11 0 0.50 2.70 4 -11 0 -0.90 3.30 4 -11 0 -1.50 5.40 4 -11 0 -1.80 3.00 -4 11 0 0.40 5.50 -4 11 0 -3.90 4.00 -4 11 0 0.90 4.10 -4 11 0 -1.50 3.70 -4 11 0 4.10 4.80 -4 11 0 -2.10 4.20 -4 11 0 1.90 4.00 -4 11 0 -8.50 4.40 -4 11 0 7.00 5.40 3 -11 0 90.59 11.70 3 -11 0 111.79 12.50 3 -11 0 100.09 7.40 3 -11 0 90.89 13.20 3 -11 0 94.89 7.00 3 -11 0 106.09 7.60 -3 11 0 96.29 9.00 -3 11 0 114.59 8.90 -3 11 0 102.59 9.50 -3 11 0 92.49 10.00 -3 11 0 97.49 9.70 -3 11 0 98.99 9.00 -3 11 0 98.69 9.30 -3 11 0 114.59 8.70 -3 11 0 85.19 10.00 2 -11 0 24.60 4.20 2 -11 0 32.60 4.60 2 -11 0 23.90 5.20 -2 11 0 31.00 5.60 -2 11 0 27.10 5.10 -2 11 0 42.40 6.90 -2 11 0 47.50 6.90 -2 11 0 25.70 5.40 -2 11 0 33.50 5.60 -2 11 0 36.90 5.90 -2 11 0 33.50 5.20 1 -11 0 3.40 3.30 1 -11 0 5.20 2.40 1 -11 0 4.30 2.30 1 -11 0 -1.60 3.60 -1 11 0 -1.20 3.20 -1 11 0 7.10 4.70 -1 11 0 13.00 6.90 -1 11 0 -1.60 4.20 -1 11 0 5.90 4.10 -1 11 0 4.10 4.20 -1 11 0 -1.20 3.90 -1 11 0 -2.30 4.10 0 -11 0 -3.20 4.20 0 -11 0 -0.80 2.70 0 -11 0 -1.60 1.80 0 -11 0 0.90 2.20 0 11 0 4.70 4.50 0 11 0 1.60 9.20 0 11 0 5.20 4.00 0 11 0 2.40 8.00 0 11 0 -1.10 8.30 0 11 0 -1.50 2.80 0 11 0 3.70 4.00 0 11 0 -1.00 3.50 0 11 0 -3.90 4.20 0 11 0 -4.40 4.20 0 11 0 1.40 4.80 0 11 0 1.70 3.70 0 11 0 3.00 5.40 -1 -11 0 11.30 3.00 -1 -11 0 12.60 2.30 -1 -11 0 10.90 2.50 1 11 0 8.30 2.90 1 11 0 10.20 4.00 1 11 0 12.10 4.00 1 11 0 -0.30 5.20 1 11 0 8.40 4.40 1 11 0 17.80 5.40 1 11 0 4.20 7.20 1 11 0 20.60 4.90 1 11 0 6.30 4.10 1 11 0 9.20 8.20 1 11 0 17.20 4.10 -2 -11 0 -1.90 3.00 -2 -11 0 -0.90 2.40 -2 -11 0 2.20 2.20 -2 -11 0 3.10 2.10 -2 -11 0 3.40 1.60 2 11 0 0.90 2.30 2 11 0 1.60 4.20 2 11 0 6.00 5.90 2 11 0 -0.30 4.80 2 11 0 -1.20 3.30 2 11 0 3.90 5.60 2 11 0 2.90 3.60 2 11 0 2.10 4.80 2 11 0 -0.20 6.50 2 11 0 -0.90 3.30 2 11 0 9.50 3.70 2 11 0 8.30 7.20 2 11 0 3.70 6.40 -3 -11 0 3.00 3.10 -3 -11 0 3.00 1.50 -3 -11 0 1.60 1.90 -3 -11 0 -2.60 2.00 -3 -11 0 4.20 2.50 3 11 0 1.50 1.80 3 11 0 0.50 5.20 3 11 0 -1.30 3.20 3 11 0 -0.90 4.30 3 11 0 -1.20 5.60 3 11 0 -1.20 3.30 3 11 0 2.00 2.20 3 11 0 -3.80 6.00 3 11 0 3.70 6.70 3 11 0 6.00 4.70 3 11 0 -2.80 3.10 3 11 0 3.90 3.50 -4 -11 0 -1.00 1.70 -4 -11 0 -0.40 1.30 -4 -11 0 3.90 3.30 -4 -11 0 2.20 2.50 4 11 0 -1.60 3.10 4 11 0 1.30 5.00 4 11 0 -3.10 7.90 4 11 0 -3.20 5.90 4 11 0 1.30 3.20 4 11 0 3.60 6.40 4 11 0 2.20 4.30 4 11 0 -5.40 3.30 4 11 0 2.80 1.90 4 11 0 4.60 2.10 4 11 0 7.10 4.00 4 11 0 -2.10 5.50 4 11 0 -2.70 3.00 4 11 0 0.90 4.30 -5 -11 0 8.40 2.90 -5 -11 0 7.50 3.70 -5 -11 0 7.80 1.60 -5 -11 0 10.00 2.00 5 11 0 13.00 3.80 5 11 0 14.30 3.50 5 11 0 12.30 2.50 5 11 0 25.80 7.40 5 11 0 7.10 3.40 5 11 0 8.00 2.30 5 11 0 2.50 5.00 5 11 0 9.40 4.20 5 11 0 8.30 4.20 5 11 0 17.10 4.30 5 11 0 11.10 5.10 -6 -11 0 54.89 4.00 -6 -11 0 59.89 5.90 -6 -11 0 55.49 3.70 6 11 0 49.00 5.70 6 11 0 49.99 6.60 6 11 0 58.09 5.90 6 11 0 44.80 8.00 6 11 0 48.30 6.90 6 11 0 59.99 7.10 6 11 0 54.99 5.00 6 11 0 44.60 8.00 6 11 0 38.40 6.80 6 11 0 54.69 6.00 6 11 0 51.99 7.30 -7 -11 0 6.00 4.70 -7 -11 0 9.50 2.10 -7 -11 0 10.60 3.60 7 11 0 15.80 3.60 7 11 0 0.60 4.80 7 11 0 2.30 3.10 7 11 0 9.00 4.20 7 11 0 8.40 5.90 7 11 0 5.60 5.90 7 11 0 14.00 4.30 7 11 0 13.10 4.90 7 11 0 8.90 2.60 7 11 0 10.20 6.20 7 11 0 3.00 3.50 -8 -11 0 44.90 3.60 -8 -11 0 37.50 3.70 -8 -11 0 42.70 5.30 -8 -11 0 51.59 7.00 -8 -11 0 34.00 6.60 8 11 0 34.60 5.40 8 11 0 42.90 5.90 8 11 0 41.10 7.10 8 11 0 41.10 5.70 8 11 0 35.20 5.60 8 11 0 50.19 8.00 8 11 0 43.90 7.40 8 11 0 41.90 5.70 8 11 0 34.10 5.10 -9 -11 0 29.20 3.70 -9 -11 0 25.40 4.20 -9 -11 0 35.60 3.50 9 11 0 21.60 4.00 9 11 0 29.80 4.80 9 11 0 30.00 5.30 9 11 0 33.60 5.50 9 11 0 31.90 5.20 9 11 0 35.50 6.90 9 11 0 32.90 5.90 9 11 0 28.40 6.40 9 11 0 35.70 5.60 -10 -11 0 214.28 11.30 -10 -11 0 209.98 10.70 -10 -11 0 198.48 10.70 -10 -11 0 213.68 14.30 10 11 0 210.88 13.50 10 11 0 221.68 12.80 10 11 0 207.88 11.90 10 11 0 175.38 12.40 10 11 0 213.68 12.00 10 11 0 193.18 12.70 10 11 0 196.68 13.90 -11 -11 0 6.90 3.20 -11 -11 0 2.50 2.60 -11 -11 0 -2.00 11.30 -11 -11 0 -5.70 11.50 -11 -11 0 8.50 2.60 -11 -11 0 4.40 5.60 11 11 0 2.30 4.20 11 11 0 6.40 4.40 11 11 0 10.50 4.50 11 11 0 9.90 3.90 11 11 0 3.60 5.00 11 11 0 7.20 3.80 11 11 0 6.80 4.80 11 11 0 8.00 6.20 -12 -11 0 93.79 9.80 -12 -11 0 84.59 6.20 -12 -11 0 78.99 10.60 -12 -11 0 82.99 6.70 -12 -11 0 93.69 7.00 -12 -11 0 80.09 10.00 12 11 0 66.39 8.90 12 11 0 78.69 8.10 12 11 0 84.39 9.40 12 11 0 100.49 7.40 12 11 0 72.69 7.40 12 11 0 88.49 10.30 12 11 0 70.29 10.80 12 11 0 68.19 8.20 -13 -11 0 1.70 4.50 -13 -11 0 2.00 3.20 -13 -11 0 -3.10 5.00 -13 -11 0 1.90 3.10 -13 -11 0 3.20 2.90 13 11 0 3.50 5.50 13 11 0 0.40 3.70 13 11 0 4.90 4.70 13 11 0 6.40 4.50 13 11 0 2.90 3.30 13 11 0 7.90 4.80 13 11 0 -4.40 6.90 -14 -11 0 150.18 10.10 -14 -11 0 143.19 10.80 -14 -11 0 158.38 9.40 -14 -11 0 155.58 11.00 -14 -11 0 150.48 9.20 -14 -11 0 162.08 10.40 14 11 0 149.19 9.30 14 11 0 138.69 11.50 14 11 0 155.68 12.00 14 11 0 145.19 11.20 14 11 0 120.29 13.70 14 11 0 156.98 10.20 14 11 0 141.09 11.00 -15 -11 0 34.30 5.00 -15 -11 0 48.20 7.10 -15 -11 0 46.50 5.40 -15 -11 0 26.50 4.60 -15 -11 0 38.90 6.00 -15 -11 0 44.80 7.50 15 11 0 31.20 5.70 15 11 0 36.40 6.20 15 11 0 40.10 5.50 15 11 0 37.30 5.50 -16 -11 0 41.30 5.90 -16 -11 0 41.30 5.00 -16 -11 0 47.70 6.50 -16 -11 0 30.70 4.50 -16 -11 0 25.10 4.00 -16 -11 0 34.70 6.30 16 11 0 42.00 6.10 16 11 0 34.40 5.90 16 11 0 32.90 5.60 16 11 0 53.79 6.80 16 11 0 30.80 5.00 -17 -11 0 20.60 4.60 -17 -11 0 34.90 5.40 -17 -11 0 26.10 4.20 -17 -11 0 26.90 4.10 -17 -11 0 30.20 4.50 17 11 0 27.60 4.50 17 11 0 21.00 4.30 17 11 0 23.10 6.20 17 11 0 26.10 4.50 17 11 0 22.00 5.00 -18 -11 0 70.69 6.90 -18 -11 0 74.39 5.90 -18 -11 0 72.09 5.20 -18 -11 0 72.29 6.00 -18 -11 0 63.49 5.60 18 11 0 66.09 8.40 18 11 0 75.39 6.60 18 11 0 67.49 6.50 18 11 0 71.49 5.20 -19 -11 0 173.38 8.80 -19 -11 0 161.18 8.10 19 11 0 180.68 9.30 19 11 0 149.09 9.00 9 -12 0 5.00 2.30 9 -12 0 1.80 3.00 9 -12 0 -0.40 2.90 9 -12 0 2.60 3.10 -9 12 0 3.80 3.70 -9 12 0 0.70 2.60 8 -12 0 117.79 8.50 8 -12 0 118.59 7.20 8 -12 0 108.99 7.90 8 -12 0 127.69 7.30 8 -12 0 99.89 8.70 -8 12 0 107.79 8.40 -8 12 0 120.59 8.40 -8 12 0 119.79 8.70 -8 12 0 117.69 8.20 7 -12 0 265.57 13.40 7 -12 0 252.77 13.90 7 -12 0 268.97 13.30 7 -12 0 251.77 18.70 7 -12 0 271.27 14.40 7 -12 0 246.78 13.70 -7 12 0 256.77 14.10 -7 12 0 259.87 13.90 -7 12 0 231.68 13.10 -7 12 0 275.37 15.00 -7 12 0 258.37 13.70 -7 12 0 261.27 14.00 6 -12 0 999.70 43.20 6 -12 0 920.91 43.70 6 -12 0 1004.30 43.00 6 -12 0 975.70 44.00 6 -12 0 1023.20 43.30 -6 12 0 1010.80 44.30 -6 12 0 957.10 43.80 -6 12 0 963.90 43.50 -6 12 0 996.40 45.10 -6 12 0 977.60 44.60 -6 12 0 886.01 42.80 -6 12 0 953.30 44.00 5 -12 0 358.66 18.30 5 -12 0 380.36 19.60 5 -12 0 361.96 18.30 5 -12 0 367.86 17.70 5 -12 0 359.86 17.50 -5 12 0 348.87 18.70 -5 12 0 305.67 23.20 -5 12 0 308.77 17.90 -5 12 0 353.36 19.40 -5 12 0 361.36 18.60 -5 12 0 381.16 20.40 -5 12 0 346.97 18.60 -5 12 0 347.87 19.50 4 -12 0 999.40 43.00 4 -12 0 1004.00 43.10 4 -12 0 943.51 44.40 4 -12 0 999.30 43.50 4 -12 0 945.61 43.50 -4 12 0 990.00 45.20 -4 12 0 955.50 44.70 -4 12 0 1005.40 44.20 -4 12 0 991.40 44.20 -4 12 0 1000.70 44.00 -4 12 0 933.91 45.90 -4 12 0 910.91 44.00 -4 12 0 866.31 42.90 -4 12 0 932.81 44.80 -4 12 0 1009.90 44.40 3 -12 0 13.40 3.80 3 -12 0 9.20 6.20 3 -12 0 9.50 3.70 3 -12 0 12.60 7.60 -3 12 0 10.60 5.10 -3 12 0 1.90 4.40 -3 12 0 2.70 5.10 -3 12 0 14.40 4.70 -3 12 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2.90 -8 13 0 20.50 4.20 -8 13 0 17.20 3.70 -8 13 0 23.10 4.60 7 -13 0 121.69 9.20 7 -13 0 119.59 9.10 7 -13 0 133.69 9.00 7 -13 0 137.89 8.00 7 -13 0 140.99 8.00 -7 13 0 138.19 8.90 -7 13 0 138.39 12.40 -7 13 0 133.49 8.70 -7 13 0 133.59 8.90 -7 13 0 138.29 9.10 6 -13 0 22.40 4.10 6 -13 0 20.90 3.60 6 -13 0 16.40 5.10 6 -13 0 20.80 4.40 6 -13 0 32.50 5.30 -6 13 0 26.20 4.90 -6 13 0 20.40 4.30 -6 13 0 15.20 4.20 -6 13 0 19.60 3.90 -6 13 0 19.20 3.80 -6 13 0 14.80 3.90 5 -13 0 59.79 6.20 5 -13 0 87.09 8.10 5 -13 0 67.79 8.70 5 -13 0 59.29 9.70 5 -13 0 63.29 6.50 5 -13 0 55.19 7.10 -5 13 0 80.99 7.20 -5 13 0 60.39 8.00 -5 13 0 62.29 7.00 -5 13 0 43.40 7.40 -5 13 0 75.59 6.90 4 -13 0 4.80 4.40 4 -13 0 1.40 3.10 4 -13 0 4.10 3.30 4 -13 0 11.60 7.00 -4 13 0 2.30 3.70 -4 13 0 3.40 4.80 -4 13 0 -2.30 3.70 -4 13 0 1.50 4.40 -4 13 0 5.90 6.60 -4 13 0 -5.00 3.70 3 -13 0 160.38 12.80 3 -13 0 161.28 10.20 3 -13 0 174.38 11.10 3 -13 0 160.38 10.20 -3 13 0 169.78 12.50 -3 13 0 165.58 12.10 -3 13 0 171.28 11.30 -3 13 0 180.18 17.60 -3 13 0 186.18 13.70 -3 13 0 154.08 12.40 -3 13 0 169.28 11.70 -3 13 0 181.68 11.60 2 -13 0 2.20 3.00 2 -13 0 11.30 7.00 2 -13 0 6.20 3.60 -2 13 0 -1.90 5.80 -2 13 0 5.80 4.10 -2 13 0 4.10 4.30 -2 13 0 5.80 5.00 -2 13 0 4.70 4.70 -2 13 0 3.20 4.10 -2 13 0 -5.30 6.90 -2 13 0 -3.30 5.90 -2 13 0 4.00 4.50 1 -13 0 36.60 5.10 1 -13 0 43.30 5.60 1 -13 0 40.40 5.10 -1 13 0 43.80 7.00 -1 13 0 32.90 5.80 -1 13 0 45.10 7.20 -1 13 0 38.40 7.10 -1 13 0 38.90 6.00 -1 13 0 43.20 7.70 -1 13 0 35.00 6.00 -1 13 0 24.40 8.00 -1 13 0 36.00 5.80 0 -13 0 -1.00 4.20 0 -13 0 4.30 5.80 0 -13 0 -0.80 2.60 0 -13 0 -4.00 2.50 0 13 0 -4.70 5.00 0 13 0 -6.90 5.20 0 13 0 2.50 4.00 0 13 0 5.60 4.50 0 13 0 1.20 4.30 0 13 0 -0.50 3.80 0 13 0 -4.50 4.10 0 13 0 -0.40 4.00 -1 -13 0 33.70 4.50 -1 -13 0 29.30 6.00 -1 -13 0 33.80 5.50 1 13 0 48.90 8.80 1 13 0 37.00 6.10 1 13 0 42.40 6.50 1 13 0 37.40 6.20 1 13 0 39.40 7.00 1 13 0 27.10 5.10 1 13 0 31.60 5.80 1 13 0 31.70 7.60 1 13 0 34.20 6.10 1 13 0 32.90 5.10 -2 -13 0 6.20 2.20 -2 -13 0 0.90 4.20 -2 -13 0 0.90 2.60 2 13 0 0.80 3.60 2 13 0 2.00 4.90 2 13 0 9.40 3.60 2 13 0 0.10 4.20 2 13 0 17.60 7.40 2 13 0 2.40 6.10 2 13 0 5.10 5.60 2 13 0 9.40 4.20 2 13 0 2.60 3.60 2 13 0 5.40 3.60 2 13 0 0.80 4.50 -3 -13 0 0.80 3.70 -3 -13 0 4.80 2.40 -3 -13 0 0.40 1.80 3 13 0 0.70 3.30 3 13 0 0.50 4.80 3 13 0 -3.20 5.80 3 13 0 -4.10 4.30 3 13 0 -5.40 6.60 3 13 0 2.70 3.40 3 13 0 -2.80 5.20 3 13 0 -0.10 3.70 3 13 0 -1.10 3.50 3 13 0 4.40 6.10 3 13 0 5.30 3.50 3 13 0 8.10 4.60 3 13 0 -0.60 4.00 -4 -13 0 12.60 2.20 -4 -13 0 10.60 3.90 -4 -13 0 13.30 2.60 4 13 0 17.20 3.70 4 13 0 15.70 6.30 4 13 0 15.90 4.00 4 13 0 9.90 6.40 4 13 0 17.20 5.00 4 13 0 16.10 4.20 4 13 0 16.40 5.20 4 13 0 9.20 7.70 4 13 0 18.20 5.50 4 13 0 15.80 3.70 4 13 0 12.90 4.30 4 13 0 2.00 5.40 4 13 0 20.20 6.10 -5 -13 0 14.10 2.60 -5 -13 0 18.80 4.20 -5 -13 0 17.30 5.10 -5 -13 0 18.30 2.90 5 13 0 9.80 6.20 5 13 0 22.10 5.00 5 13 0 11.00 3.80 5 13 0 12.40 5.40 5 13 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13.00 6.70 9 13 0 20.30 4.70 9 13 0 19.80 4.40 9 13 0 18.80 5.10 9 13 0 24.40 6.60 9 13 0 33.40 5.30 9 13 0 23.50 4.70 9 13 0 26.80 4.50 9 13 0 24.80 5.60 9 13 0 21.80 6.60 9 13 0 31.30 7.00 -10 -13 0 77.59 7.30 -10 -13 0 75.69 5.80 -10 -13 0 77.09 6.00 -10 -13 0 67.19 9.90 10 13 0 80.79 7.40 10 13 0 73.59 8.40 10 13 0 77.39 8.20 10 13 0 76.39 9.10 10 13 0 81.29 7.20 10 13 0 52.09 9.60 10 13 0 84.19 9.60 10 13 0 82.29 10.00 10 13 0 78.39 7.90 -11 -13 0 12.70 3.00 -11 -13 0 11.50 9.10 -11 -13 0 12.10 3.20 -11 -13 0 14.00 3.90 11 13 0 15.40 4.90 11 13 0 11.50 4.10 11 13 0 5.30 5.80 11 13 0 6.80 5.50 11 13 0 6.90 4.60 11 13 0 10.40 5.00 11 13 0 5.60 5.40 11 13 0 11.60 3.90 11 13 0 6.90 5.10 11 13 0 12.20 4.60 11 13 0 0.50 7.20 -12 -13 0 87.49 7.10 -12 -13 0 99.49 7.70 -12 -13 0 78.59 11.20 -12 -13 0 85.59 6.60 12 13 0 78.89 10.10 12 13 0 86.69 7.90 12 13 0 81.19 7.70 12 13 0 100.29 8.10 12 13 0 92.49 9.40 12 13 0 94.09 12.20 12 13 0 71.29 9.90 12 13 0 82.79 11.00 12 13 0 73.99 9.90 12 13 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66.59 7.20 16 13 0 64.39 9.10 16 13 0 55.89 5.90 16 13 0 58.29 7.90 16 13 0 60.39 7.50 16 13 0 70.49 7.40 -17 -13 0 50.29 6.50 -17 -13 0 60.39 5.30 -17 -13 0 51.09 6.70 -17 -13 0 44.70 6.40 -17 -13 0 55.49 5.10 17 13 0 52.39 6.40 17 13 0 52.59 7.50 17 13 0 44.60 6.40 17 13 0 36.20 6.40 17 13 0 57.69 7.00 -18 -13 0 27.10 4.40 -18 -13 0 30.40 4.60 -18 -13 0 21.80 3.50 18 13 0 28.60 6.10 18 13 0 17.40 3.60 18 13 0 23.70 4.50 -19 -13 0 37.20 3.30 7 -14 0 0.50 2.40 7 -14 0 1.90 5.70 7 -14 0 2.40 3.90 7 -14 0 2.90 2.80 -7 14 0 0.20 3.10 -7 14 0 0.40 2.40 -7 14 0 -0.30 3.80 -7 14 0 4.20 3.10 6 -14 0 2.30 4.10 6 -14 0 4.10 2.90 6 -14 0 7.70 5.60 6 -14 0 -2.40 3.60 -6 14 0 0.30 3.40 -6 14 0 -0.60 2.90 -6 14 0 1.20 3.30 -6 14 0 -2.00 3.10 -6 14 0 -4.10 3.30 5 -14 0 5.50 5.90 5 -14 0 -0.10 2.90 5 -14 0 -1.10 3.30 5 -14 0 -0.50 4.30 5 -14 0 0.30 3.40 -5 14 0 -0.20 3.50 -5 14 0 -2.40 3.30 -5 14 0 3.00 7.70 -5 14 0 3.90 3.10 -5 14 0 -2.70 2.80 -5 14 0 -1.60 3.10 -5 14 0 -2.70 3.50 4 -14 0 1.30 3.30 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5.90 11 15 0 23.10 4.40 11 15 0 18.20 5.90 11 15 0 12.60 5.00 11 15 0 20.70 7.40 11 15 0 23.00 6.30 11 15 0 26.30 4.60 11 15 0 17.30 4.90 11 15 0 8.60 4.50 -12 -15 0 26.60 4.60 -12 -15 0 35.20 5.20 -12 -15 0 36.90 5.00 12 15 0 27.80 5.50 12 15 0 30.60 5.50 12 15 0 31.50 6.50 12 15 0 29.20 6.70 12 15 0 26.40 4.70 12 15 0 41.00 6.80 12 15 0 22.70 8.60 12 15 0 27.10 6.10 -13 -15 0 16.40 3.70 -13 -15 0 14.00 4.50 -13 -15 0 17.80 4.00 -13 -15 0 17.20 5.90 13 15 0 14.00 6.60 13 15 0 10.20 4.80 13 15 0 11.00 5.00 13 15 0 0.40 5.00 13 15 0 11.50 3.80 13 15 0 9.40 5.70 13 15 0 19.30 5.10 -14 -15 0 142.69 8.80 -14 -15 0 132.29 8.70 -14 -15 0 135.39 9.80 -14 -15 0 138.49 9.80 14 15 0 133.99 8.80 14 15 0 111.89 9.20 14 15 0 132.19 10.80 14 15 0 112.19 10.50 14 15 0 118.89 10.80 14 15 0 135.79 10.10 14 15 0 116.59 9.80 -15 -15 0 70.79 9.90 -15 -15 0 65.69 8.80 -15 -15 0 84.49 6.70 -15 -15 0 67.49 7.40 -15 -15 0 75.89 7.20 -15 -15 0 72.49 6.10 15 15 0 58.89 7.50 15 15 0 52.39 8.00 15 15 0 71.59 6.40 15 15 0 62.59 8.60 15 15 0 62.89 7.10 15 15 0 67.49 7.10 15 15 0 70.69 7.60 -16 -15 0 25.00 6.40 -16 -15 0 23.30 4.50 -16 -15 0 20.20 4.10 -16 -15 0 24.50 3.60 -16 -15 0 31.10 4.90 16 15 0 28.50 5.10 16 15 0 18.50 3.30 16 15 0 40.40 6.30 16 15 0 29.80 4.40 16 15 0 31.40 5.00 16 15 0 27.80 4.40 -17 -15 0 82.59 5.90 -17 -15 0 68.19 8.10 -17 -15 0 85.59 5.80 -17 -15 0 59.19 8.30 17 15 0 68.69 7.30 17 15 0 75.09 6.90 17 15 0 64.79 7.00 17 15 0 72.39 6.30 17 15 0 67.49 6.80 -18 -15 0 37.40 4.80 -18 -15 0 42.20 5.10 18 15 0 39.70 5.20 18 15 0 33.90 4.50 5 -16 0 49.10 4.60 5 -16 0 43.60 5.40 -5 16 0 40.50 6.60 -5 16 0 51.39 5.50 -5 16 0 53.89 5.10 -5 16 0 49.70 5.30 -5 16 0 47.50 7.60 4 -16 0 57.69 5.70 4 -16 0 53.49 5.60 -4 16 0 59.39 5.90 -4 16 0 58.69 5.70 -4 16 0 53.89 5.70 -4 16 0 62.19 6.20 -4 16 0 57.19 5.70 3 -16 0 7.00 4.30 3 -16 0 16.20 4.30 -3 16 0 14.50 4.20 -3 16 0 15.30 3.40 -3 16 0 25.80 4.30 -3 16 0 21.60 3.70 -3 16 0 16.50 3.50 -3 16 0 17.00 4.00 2 -16 0 147.49 9.90 2 -16 0 151.48 9.80 2 -16 0 149.69 11.10 -2 16 0 154.68 11.40 -2 16 0 161.38 11.30 -2 16 0 148.49 10.50 -2 16 0 167.88 10.30 -2 16 0 162.38 10.00 -2 16 0 148.29 10.40 -2 16 0 149.99 9.80 -2 16 0 156.58 10.50 1 -16 0 731.33 37.00 1 -16 0 773.32 37.10 1 -16 0 834.12 36.70 1 -16 0 761.42 37.40 -1 16 0 855.71 38.40 -1 16 0 815.82 38.10 -1 16 0 832.02 38.00 -1 16 0 863.91 37.40 -1 16 0 845.92 37.20 -1 16 0 856.71 37.60 -1 16 0 846.12 37.70 -1 16 0 791.72 37.60 0 -16 0 11.20 3.70 0 -16 0 4.70 4.10 0 -16 0 3.30 4.50 0 16 0 6.40 5.70 0 16 0 -5.10 4.30 0 16 0 -2.20 3.60 0 16 0 2.00 3.90 0 16 0 5.30 4.60 0 16 0 6.70 4.30 0 16 0 7.80 4.60 -1 -16 0 648.54 29.80 -1 -16 0 603.74 29.50 -1 -16 0 630.04 29.40 1 16 0 629.84 30.60 1 16 0 655.93 30.90 1 16 0 655.13 30.80 1 16 0 662.83 31.10 1 16 0 650.93 31.70 1 16 0 673.63 31.90 -2 -16 0 492.75 24.60 -2 -16 0 516.35 24.00 -2 -16 0 482.75 24.00 2 16 0 547.85 26.80 2 16 0 522.05 25.40 2 16 0 546.35 26.00 2 16 0 520.65 25.60 2 16 0 502.25 25.30 2 16 0 516.45 25.40 2 16 0 540.75 26.10 2 16 0 553.04 26.30 2 16 0 486.95 26.00 -3 -16 0 1257.37 55.19 -3 -16 0 1313.17 55.69 3 16 0 1269.97 56.59 3 16 0 1287.57 56.79 3 16 0 1178.48 57.09 3 16 0 1272.77 57.09 3 16 0 1292.77 57.39 3 16 0 1263.07 57.79 3 16 0 1312.87 58.09 3 16 0 1256.27 56.89 3 16 0 1259.27 56.69 3 16 0 1306.07 56.69 -4 -16 0 8.20 3.10 -4 -16 0 4.40 3.10 4 16 0 7.40 3.70 4 16 0 14.00 6.00 4 16 0 3.60 3.80 4 16 0 0.20 3.60 4 16 0 7.30 4.70 4 16 0 13.40 5.10 4 16 0 -7.10 5.80 4 16 0 22.50 6.40 4 16 0 2.20 4.40 4 16 0 5.20 3.90 -5 -16 0 135.09 8.30 -5 -16 0 143.99 8.30 5 16 0 142.49 9.50 5 16 0 137.19 9.40 5 16 0 143.09 11.10 5 16 0 134.19 9.40 5 16 0 132.49 11.90 5 16 0 138.39 9.60 5 16 0 126.49 10.90 5 16 0 137.59 12.00 5 16 0 138.09 10.50 5 16 0 140.69 10.30 -6 -16 0 28.90 4.80 -6 -16 0 26.00 3.80 6 16 0 29.40 7.00 6 16 0 27.70 5.60 6 16 0 21.30 4.90 6 16 0 33.20 6.70 6 16 0 36.50 5.70 6 16 0 19.90 5.40 6 16 0 23.80 6.70 6 16 0 34.20 5.00 6 16 0 31.00 4.80 6 16 0 47.50 7.60 6 16 0 18.80 4.20 -7 -16 0 746.23 33.60 -7 -16 0 730.73 33.50 7 16 0 768.42 37.30 7 16 0 753.52 35.90 7 16 0 769.32 34.80 7 16 0 754.22 35.40 7 16 0 722.43 36.30 7 16 0 766.42 34.90 7 16 0 790.22 34.80 7 16 0 756.72 36.80 7 16 0 778.72 35.50 -8 -16 0 146.29 8.60 -8 -16 0 142.29 8.60 8 16 0 136.29 10.90 8 16 0 134.59 10.60 8 16 0 140.59 9.70 8 16 0 174.58 12.50 8 16 0 143.49 12.80 8 16 0 135.89 12.40 8 16 0 145.79 9.60 8 16 0 140.59 9.60 8 16 0 135.69 10.20 -9 -16 0 262.27 14.40 -9 -16 0 262.77 13.30 -9 -16 0 271.47 13.70 9 16 0 266.67 16.00 9 16 0 253.17 14.20 9 16 0 251.07 14.20 9 16 0 233.98 16.60 9 16 0 249.78 15.10 9 16 0 253.87 14.80 9 16 0 271.77 16.50 9 16 0 265.17 17.50 9 16 0 258.47 17.70 9 16 0 272.87 14.40 9 16 0 264.27 15.50 -10 -16 0 132.89 9.30 -10 -16 0 136.29 8.60 -10 -16 0 151.68 9.90 10 16 0 147.09 9.60 10 16 0 124.09 10.10 10 16 0 146.39 12.10 10 16 0 116.39 11.70 10 16 0 141.09 11.10 10 16 0 136.89 9.20 10 16 0 129.59 12.10 10 16 0 116.69 10.80 10 16 0 126.39 14.70 10 16 0 139.09 10.20 10 16 0 132.49 10.60 -11 -16 0 916.41 40.00 -11 -16 0 911.61 40.30 -11 -16 0 864.11 40.00 11 16 0 905.11 40.80 11 16 0 812.92 43.80 11 16 0 891.51 40.90 11 16 0 903.71 42.40 11 16 0 926.91 42.20 11 16 0 936.01 41.80 11 16 0 894.51 40.70 11 16 0 845.62 41.80 11 16 0 917.41 42.80 11 16 0 976.80 43.40 -12 -16 0 116.59 11.80 -12 -16 0 86.29 7.10 -12 -16 0 80.99 7.90 -12 -16 0 77.99 7.80 12 16 0 87.59 9.00 12 16 0 88.89 8.60 12 16 0 84.99 10.40 12 16 0 93.59 10.00 12 16 0 88.59 7.50 12 16 0 78.49 10.90 -13 -16 0 19.40 4.20 -13 -16 0 16.90 4.90 -13 -16 0 23.70 4.10 -13 -16 0 12.30 5.80 13 16 0 21.30 4.70 13 16 0 10.10 5.10 13 16 0 25.60 4.20 13 16 0 8.80 5.60 13 16 0 15.00 4.20 13 16 0 28.40 6.00 13 16 0 22.00 5.50 13 16 0 20.10 4.80 -14 -16 0 128.29 10.30 -14 -16 0 142.99 8.90 -14 -16 0 129.19 9.10 -14 -16 0 131.89 10.20 14 16 0 127.79 9.90 14 16 0 113.99 10.90 14 16 0 146.89 9.90 14 16 0 145.09 10.50 14 16 0 153.98 10.90 14 16 0 151.48 10.60 14 16 0 137.09 9.00 -15 -16 0 71.79 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19 0 0.80 2.70 4 19 0 2.40 2.90 4 19 0 -2.80 2.90 4 19 0 4.20 6.50 4 19 0 2.20 4.80 4 19 0 3.00 3.90 -5 -19 0 13.30 5.40 5 19 0 6.40 3.50 5 19 0 8.00 6.20 5 19 0 19.40 5.10 5 19 0 12.60 3.50 5 19 0 3.40 4.40 5 19 0 10.80 3.10 5 19 0 6.50 2.90 5 19 0 8.50 5.10 -6 -19 0 12.30 5.20 6 19 0 7.80 5.10 6 19 0 5.60 5.00 6 19 0 7.00 3.10 6 19 0 11.90 4.00 6 19 0 10.40 3.30 6 19 0 7.40 3.20 6 19 0 8.10 5.40 6 19 0 4.50 4.20 -7 -19 0 11.80 5.10 7 19 0 8.20 4.70 7 19 0 7.40 4.60 7 19 0 4.00 3.60 7 19 0 10.90 3.30 7 19 0 5.40 3.20 7 19 0 11.60 5.20 7 19 0 10.70 3.10 7 19 0 2.50 6.00 -8 -19 0 12.40 5.10 8 19 0 -0.60 3.70 8 19 0 5.10 4.30 8 19 0 7.50 6.80 8 19 0 -2.20 3.10 8 19 0 -2.80 4.80 8 19 0 1.90 3.50 8 19 0 3.20 2.70 8 19 0 2.60 4.60 8 19 0 2.30 3.10 -9 -19 0 -4.40 4.90 9 19 0 -0.50 4.10 9 19 0 1.20 2.90 9 19 0 6.00 2.80 9 19 0 0.80 4.70 9 19 0 -0.70 3.50 9 19 0 12.60 4.20 9 19 0 7.50 5.80 9 19 0 0.10 4.30 9 19 0 1.90 3.30 -10 -19 0 64.69 9.40 -10 -19 0 45.70 6.00 10 19 0 39.40 7.30 10 19 0 51.59 6.10 10 19 0 37.50 6.50 10 19 0 48.00 7.60 10 19 0 37.40 5.60 10 19 0 53.19 6.60 10 19 0 41.30 6.00 10 19 0 44.40 5.60 10 19 0 39.80 5.50 -11 -19 0 0.40 5.60 -11 -19 0 4.30 5.00 11 19 0 1.00 3.90 11 19 0 -1.20 2.90 11 19 0 4.00 4.40 11 19 0 6.40 3.70 11 19 0 -4.30 2.70 11 19 0 1.70 4.60 11 19 0 5.20 3.60 -12 -19 0 36.00 5.50 12 19 0 27.20 5.10 12 19 0 17.40 4.70 12 19 0 20.10 3.60 12 19 0 26.10 3.80 12 19 0 23.10 4.90 12 19 0 32.20 5.20 12 19 0 38.20 5.60 -13 -19 0 3.40 4.30 13 19 0 0.20 3.80 13 19 0 -4.60 3.10 13 19 0 3.50 3.90 13 19 0 3.90 3.00 13 19 0 -1.50 2.40 13 19 0 2.50 3.20 13 19 0 3.00 4.10 -14 -19 0 47.60 8.20 -14 -19 0 50.99 6.40 14 19 0 50.89 6.40 14 19 0 52.59 6.40 14 19 0 61.59 5.00 14 19 0 51.09 5.60 14 19 0 38.30 6.50 -15 -19 0 68.19 6.80 15 19 0 57.49 6.90 15 19 0 45.10 7.10 15 19 0 71.19 5.50 15 19 0 47.00 7.10 15 19 0 65.99 5.50 2 20 0 269.47 13.50 2 20 0 272.07 13.30 2 20 0 280.27 13.50 2 20 0 259.97 13.80 2 20 0 262.07 13.30 3 20 0 218.68 12.50 3 20 0 196.88 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20 2 17.20 3.30 13 20 2 19.40 4.20 13 20 2 17.70 3.10 13 20 2 11.80 6.90 14 20 2 250.37 13.70 14 20 2 261.27 13.80 14 20 2 269.77 13.70 14 20 2 263.87 12.90 14 20 2 280.57 13.80 5 21 2 4.20 3.00 5 21 2 7.90 2.90 5 21 2 5.90 3.30 5 21 2 -1.30 5.10 5 21 2 6.10 3.10 6 21 2 0.20 5.40 6 21 2 0.50 3.40 6 21 2 0.50 3.40 6 21 2 0.90 4.60 7 21 2 15.40 3.20 7 21 2 20.00 3.80 7 21 2 23.30 5.50 7 21 2 10.20 3.90 7 21 2 14.30 3.90 7 21 2 17.10 5.20 8 21 2 31.60 5.60 8 21 2 22.50 5.00 8 21 2 20.60 3.30 8 21 2 30.50 5.10 8 21 2 23.00 5.30 8 21 2 14.20 6.30 8 21 2 14.60 7.10 9 21 2 -0.80 2.90 9 21 2 0.70 3.50 9 21 2 2.70 4.70 9 21 2 1.70 4.30 9 21 2 -1.20 3.30 9 21 2 -0.80 4.60 10 21 2 2.50 3.80 10 21 2 8.50 4.50 10 21 2 -0.20 3.60 10 21 2 3.20 3.70 10 21 2 -0.50 5.10 10 21 2 9.90 3.30 11 21 2 33.40 4.40 11 21 2 32.90 5.00 11 21 2 35.30 6.10 12 21 2 34.70 5.50 12 21 2 27.40 3.80 12 21 2 39.90 4.70 12 21 2 29.40 4.60 12 21 2 27.80 4.80 13 20 -3 2.60 3.00 13 20 -3 -2.10 2.40 13 20 -3 3.40 4.40 13 20 -3 6.40 4.10 13 20 -3 0.80 3.40 12 20 -3 0.80 2.50 12 20 -3 2.60 5.00 12 20 -3 5.90 4.90 12 20 -3 1.20 3.20 12 20 -3 2.90 4.10 12 20 -3 6.90 4.60 11 20 -3 5.00 6.00 11 20 -3 3.30 3.40 11 20 -3 1.30 5.40 11 20 -3 -0.40 3.60 11 20 -3 1.90 3.20 11 20 -3 -0.10 2.50 11 20 -3 7.00 2.50 10 20 -3 1.10 4.30 10 20 -3 -3.40 3.60 10 20 -3 -2.30 2.70 10 20 -3 1.70 3.00 10 20 -3 0.10 2.50 9 20 -3 0.30 4.10 9 20 -3 -1.50 2.50 9 20 -3 -1.10 3.50 9 20 -3 -2.00 2.40 9 20 -3 2.10 3.70 9 20 -3 -3.10 4.00 8 20 -3 -1.70 4.40 8 20 -3 3.30 2.70 8 20 -3 1.70 4.20 8 20 -3 0.80 2.50 8 20 -3 -0.20 3.20 8 20 -3 2.20 3.50 8 20 -3 -1.80 5.40 7 20 -3 1.90 6.30 7 20 -3 -0.80 3.20 7 20 -3 5.20 2.60 7 20 -3 -2.20 2.80 7 20 -3 2.10 2.50 7 20 -3 -1.00 3.40 6 20 -3 -3.70 2.70 6 20 -3 2.10 2.70 6 20 -3 -2.40 2.70 6 20 -3 -8.30 5.60 6 20 -3 5.10 3.70 6 20 -3 0.00 3.40 6 20 -3 -1.60 5.30 5 20 -3 0.90 2.50 5 20 -3 2.70 3.80 5 20 -3 -1.20 2.50 5 20 -3 -0.20 3.10 5 20 -3 1.30 2.80 4 20 -3 0.00 2.70 4 20 -3 -1.10 4.80 4 20 -3 3.70 4.60 4 20 -3 0.40 3.50 4 20 -3 -1.10 2.70 3 20 -3 -1.20 3.20 3 20 -3 -3.70 4.00 3 20 -3 0.40 2.60 3 20 -3 0.50 2.80 3 20 -3 -0.10 2.70 14 19 -3 105.29 11.50 14 19 -3 106.89 6.80 14 19 -3 105.49 7.70 14 19 -3 82.49 7.80 14 19 -3 95.19 7.60 -14 -19 3 83.99 9.80 -14 -19 3 92.19 8.50 -14 -19 3 110.09 7.40 13 19 -3 3.50 3.90 13 19 -3 12.50 3.40 13 19 -3 10.60 2.50 13 19 -3 6.50 4.00 13 19 -3 8.20 3.40 13 19 -3 9.40 4.10 -13 -19 3 9.90 4.40 -13 -19 3 6.90 3.70 12 19 -3 44.80 5.10 12 19 -3 40.10 5.60 12 19 -3 38.70 5.80 12 19 -3 30.30 5.40 12 19 -3 45.60 4.90 12 19 -3 40.20 5.50 12 19 -3 34.20 5.50 -12 -19 3 40.10 6.50 -12 -19 3 39.30 5.80 11 19 -3 -1.70 2.50 11 19 -3 4.60 3.40 11 19 -3 5.50 4.50 11 19 -3 -2.60 3.50 11 19 -3 -5.80 4.00 11 19 -3 1.70 2.60 11 19 -3 1.50 4.90 -11 -19 3 -4.30 4.10 -11 -19 3 0.00 6.60 -11 -19 3 11.20 5.80 10 19 -3 40.80 6.60 10 19 -3 58.39 7.10 10 19 -3 54.39 6.30 10 19 -3 45.90 5.30 10 19 -3 52.89 5.20 10 19 -3 57.39 6.70 10 19 -3 39.20 6.50 10 19 -3 37.40 6.00 -10 -19 3 50.79 7.40 -10 -19 3 48.00 7.40 9 19 -3 5.80 4.10 9 19 -3 5.00 5.60 9 19 -3 8.40 5.00 9 19 -3 13.60 3.70 9 19 -3 7.70 3.10 9 19 -3 10.70 3.20 9 19 -3 10.60 3.80 9 19 -3 18.80 3.90 9 19 -3 17.20 6.30 -9 -19 3 22.00 4.50 -9 -19 3 10.80 4.40 8 19 -3 -1.50 3.40 8 19 -3 -2.00 3.40 8 19 -3 7.10 5.10 8 19 -3 -0.50 2.90 8 19 -3 -3.10 2.70 8 19 -3 -0.50 2.70 8 19 -3 2.00 4.50 -8 -19 3 3.80 4.40 -8 -19 3 -1.00 4.20 7 19 -3 7.60 3.90 7 19 -3 7.20 3.00 7 19 -3 10.30 3.80 7 19 -3 9.60 3.30 7 19 -3 6.50 5.00 7 19 -3 7.30 3.10 7 19 -3 11.10 4.70 -7 -19 3 9.60 4.40 -7 -19 3 1.20 4.30 6 19 -3 11.30 4.30 6 19 -3 7.90 3.30 6 19 -3 9.30 3.60 6 19 -3 9.10 3.20 6 19 -3 16.50 5.40 6 19 -3 7.00 3.20 6 19 -3 6.50 5.10 -6 -19 3 1.40 4.60 -6 -19 3 5.30 4.50 5 19 -3 3.40 3.20 5 19 -3 2.50 5.20 5 19 -3 4.80 2.90 5 19 -3 -2.50 2.90 5 19 -3 3.30 3.10 5 19 -3 -1.10 4.00 5 19 -3 13.00 5.60 -5 -19 3 4.00 4.30 -5 -19 3 1.20 4.40 4 19 -3 -4.00 3.00 4 19 -3 2.70 3.90 4 19 -3 8.20 3.50 4 19 -3 -3.70 6.50 4 19 -3 2.30 2.80 4 19 -3 -1.60 4.00 4 19 -3 3.80 2.90 -4 -19 3 7.30 4.20 3 19 -3 31.50 4.80 3 19 -3 31.80 4.40 3 19 -3 35.00 5.40 3 19 -3 36.50 5.20 3 19 -3 41.60 5.20 3 19 -3 29.40 4.50 -3 -19 3 26.90 4.90 -3 -19 3 34.90 6.00 2 19 -3 38.10 5.20 2 19 -3 37.60 4.60 2 19 -3 33.10 5.80 2 19 -3 21.70 4.50 2 19 -3 36.00 4.40 2 19 -3 38.70 5.90 -2 -19 3 34.90 4.90 -2 -19 3 30.60 5.40 1 19 -3 20.60 4.80 1 19 -3 18.60 3.70 1 19 -3 10.20 3.40 1 19 -3 22.40 4.80 1 19 -3 18.40 4.20 1 19 -3 27.40 5.70 -1 -19 3 8.70 4.40 15 18 -3 414.36 18.60 15 18 -3 351.16 17.70 15 18 -3 384.06 17.60 15 18 -3 391.16 19.30 15 18 -3 415.46 18.70 15 18 -3 401.56 18.50 -15 -18 3 357.96 17.90 -15 -18 3 351.36 17.60 -15 -18 3 369.46 17.50 14 18 -3 3.70 4.00 14 18 -3 -1.20 3.40 14 18 -3 -3.10 2.20 14 18 -3 10.50 6.50 14 18 -3 -0.40 3.00 14 18 -3 -1.10 3.90 14 18 -3 1.20 3.20 -14 -18 3 -2.40 3.00 13 18 -3 359.06 17.30 13 18 -3 361.36 17.90 13 18 -3 368.36 18.80 13 18 -3 348.57 17.20 13 18 -3 338.77 18.60 13 18 -3 372.46 17.90 13 18 -3 391.16 18.90 -13 -18 3 336.87 17.60 -13 -18 3 356.46 17.90 -13 -18 3 351.96 17.30 12 18 -3 87.29 8.50 12 18 -3 74.09 7.60 12 18 -3 76.39 6.50 12 18 -3 87.69 8.70 12 18 -3 84.89 7.50 12 18 -3 84.89 8.50 12 18 -3 79.79 6.60 -12 -18 3 83.79 7.10 -12 -18 3 73.19 9.40 11 18 -3 76.49 7.00 11 18 -3 97.69 9.80 11 18 -3 114.09 9.90 11 18 -3 110.89 8.40 11 18 -3 94.89 7.90 11 18 -3 92.69 6.90 11 18 -3 99.09 9.30 -11 -18 3 101.19 7.90 -11 -18 3 94.19 7.60 -11 -18 3 99.09 10.80 10 18 -3 457.45 20.90 10 18 -3 415.06 22.60 10 18 -3 424.06 20.70 10 18 -3 447.26 21.70 10 18 -3 417.86 20.70 10 18 -3 426.76 21.80 10 18 -3 453.45 22.20 10 18 -3 450.45 23.30 10 18 -3 399.26 20.40 -10 -18 3 428.16 20.50 -10 -18 3 433.66 20.40 -10 -18 3 427.56 22.30 9 18 -3 377.36 18.80 9 18 -3 388.76 19.50 9 18 -3 374.56 21.00 9 18 -3 431.66 20.70 9 18 -3 393.06 18.80 9 18 -3 377.26 20.70 9 18 -3 370.66 18.40 9 18 -3 384.96 18.70 9 18 -3 321.