data_pt1matrix_0m_a _audit_creation_date 2015-06-14 _audit_creation_method ; Olex2 1.2-beta (compiled 2014.11.07 svn.r3078 for OlexSys, GUI svn.r4941) ; _shelxl_version_number 2013-4 _publ_contact_author_address ; Mersin University, Faculty of Arts and Science, Department of Chemistry, Mersin, 33343, Turkey ; _publ_contact_author_email 'hakan.arslan@mersin.edu.tr' _publ_contact_author_name 'Hakan Arslan' _publ_contact_author_phone '+905327073122' _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ; Cis-bis[4-fluoro-N-(diethylcarbamothioyl)benzamido-κ2O,S]platinum(II) ; _chemical_name_systematic ; Cis-bis[4-fluoro-N-(diethylcarbamothioyl)benzamido-κ2O,S]platinum(II) ; _chemical_formula_moiety 'C24 H28 F2 N4 O2 Pt S2' _chemical_formula_sum 'C24 H28 F2 N4 O2 Pt S2' _chemical_formula_weight 701.71 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pt' 'Pt' -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'tetragonal' _space_group_IT_number 88 _space_group_name_H-M_alt 'I 41/a' _space_group_name_Hall '-I 4ad' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' _cell_length_a 19.7530(4) _cell_length_b 19.7530(4) _cell_length_c 13.7137(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 5350.8(2) _cell_formula_units_Z 8 _cell_measurement_reflns_used ? _cell_measurement_temperature 296.15 _cell_measurement_theta_max 29.60 _cell_measurement_theta_min 2.74 _shelx_estimated_absorpt_T_max 0.496 _shelx_estimated_absorpt_T_min 0.193 _exptl_absorpt_coefficient_mu 5.443 _exptl_absorpt_correction_T_max 0.7467 _exptl_absorpt_correction_T_min 0.4877 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details '(Blessing, 1995)' _exptl_crystal_colour yellow _exptl_crystal_colour_lustre ? _exptl_crystal_colour_modifier ? _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.742 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 2752 _exptl_crystal_preparation ? _exptl_crystal_size_max 0.45 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.15 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0272 _diffrn_reflns_av_unetI/netI 0.0268 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_k_max 31 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 22890 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.362 _diffrn_reflns_theta_min 1.808 _diffrn_ambient_temperature 296.15 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _diffrn_special_details ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2145 _reflns_number_total 2733 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT (Bruker, 2007)' _computing_data_collection 'APEX2 (Bruker, 2007)' _computing_data_reduction 'SAINT (Bruker, 2007)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'SHELXS97 (Sheldrick, 2008)' _refine_diff_density_max 0.610 _refine_diff_density_min -0.716 _refine_diff_density_rms 0.080 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.058 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 159 _refine_ls_number_reflns 2733 _refine_ls_number_restraints 44 _refine_ls_R_factor_all 0.0405 _refine_ls_R_factor_gt 0.0303 _refine_ls_restrained_S_all 1.051 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0399P)^2^+15.0055P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0787 _refine_ls_wR_factor_ref 0.0847 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Rigid bond restraints All non-hydrogen atoms with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 3.a Secondary CH2 refined with riding coordinates: C9(H9A,H9B), C11(H11A,H11B) 3.b Me refined with riding coordinates: C10(H10A,H10B,H10C), C12(H12A,H12B,H12C) 3.c Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C6(H6), C7(H7) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pt1 Pt 0.5000 0.2500 0.63244(2) 0.05081(11) Uani 1 2 d S TU P . . S1 S 0.52412(10) 0.17706(8) 0.75093(8) 0.0951(5) Uani 1 1 d . U . . . F1 F 0.6091(2) 0.00590(17) 0.1700(2) 0.1045(11) Uani 1 1 d . U . . . O1 O 0.52474(16) 0.18501(15) 0.52311(19) 0.0590(7) Uani 1 1 d . U . . . N1 N 0.5657(2) 0.08933(19) 0.6051(2) 0.0589(9) Uani 1 1 d . U . . . N2 N 0.5828(3) 0.0599(2) 0.7622(3) 0.0947(16) Uani 1 1 d . U . . . C1 C 0.5489(2) 0.1260(2) 0.5291(3) 0.0477(9) Uani 1 1 d . U . . . C2 C 0.56204(19) 0.0924(2) 0.4325(3) 0.0473(9) Uani 1 1 d . U . . . C3 C 0.5615(2) 0.1307(2) 0.3479(3) 0.0603(11) Uani 1 1 d . U . . . H3 H 0.5503 0.1764 0.3509 0.072 Uiso 1 1 calc R . . . . C4 C 0.5774(3) 0.1016(3) 0.2592(3) 0.0717(13) Uani 1 1 d . U . . . H4 H 0.5777 0.1273 0.2024 0.086 Uiso 1 1 calc R . . . . C5 C 0.5925(3) 0.0347(3) 0.2570(3) 0.0719(13) Uani 1 1 d . U . . . C6 C 0.5920(3) -0.0053(3) 0.3379(4) 0.0752(14) Uani 1 1 d . U . . . H6 H 0.6014 -0.0514 0.3337 0.090 Uiso 1 1 calc R . . . . C7 C 0.5769(2) 0.0247(2) 0.4269(3) 0.0631(11) Uani 1 1 d . U . . . H7 H 0.5770 -0.0014 0.4834 0.076 Uiso 1 1 calc R . . . . C8 C 0.5592(3) 0.1063(2) 0.6997(3) 0.0653(12) Uani 1 1 d . U . . . C9 C 0.6129(4) -0.0031(3) 0.7270(4) 0.0966(19) Uani 1 1 d . U . . . H9A H 0.5877 -0.0192 0.6709 0.116 Uiso 1 1 calc R . . . . H9B H 0.6101 -0.0373 0.7776 0.116 Uiso 1 1 calc R . . . . C10 C 0.6850(4) 0.0075(4) 0.6994(6) 0.133(3) Uani 1 1 d . U . . . H10A H 0.7039 -0.0344 0.6765 0.200 Uiso 1 1 calc R . . . . H10B H 0.7100 0.0228 0.7552 0.200 Uiso 1 1 calc R . . . . H10C H 0.6877 0.0408 0.6486 0.200 Uiso 1 1 calc R . . . . C11 C 0.5890(8) 0.0737(5) 0.8694(5) 0.206(7) Uani 1 1 d . U . . . H11A H 0.6341 0.0593 0.8879 0.247 Uiso 1 1 calc R . . . . H11B H 0.5881 0.1225 0.8765 0.247 Uiso 1 1 calc R . . . . C12 C 0.5537(8) 0.0531(7) 0.9267(6) 0.267(9) Uani 1 1 d . U . . . H12A H 0.5676 0.0690 0.9898 0.401 Uiso 1 1 calc R . . . . H12B H 0.5551 0.0045 0.9257 0.401 Uiso 1 1 calc R . . . . H12C H 0.5084 0.0681 0.9136 0.401 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pt1 0.06207(17) 0.05872(17) 0.03166(14) 0.000 0.000 0.01146(10) S1 0.1622(15) 0.0885(10) 0.0346(5) 0.0059(6) 0.0039(7) 0.0501(10) F1 0.150(3) 0.106(2) 0.0571(17) -0.0292(17) 0.0064(19) 0.031(2) O1 0.080(2) 0.0616(18) 0.0350(13) -0.0007(12) -0.0008(13) 0.0191(15) N1 0.082(3) 0.055(2) 0.0395(16) 0.0068(14) 0.0015(16) 0.0065(18) N2 0.160(5) 0.079(3) 0.045(2) 0.014(2) 0.002(3) 0.042(3) C1 0.052(2) 0.048(2) 0.0429(19) 0.0015(16) 0.0024(16) 0.0007(18) C2 0.045(2) 0.055(2) 0.0418(19) -0.0010(16) 0.0031(16) -0.0022(17) C3 0.073(3) 0.063(3) 0.044(2) 0.0019(19) 0.003(2) 0.012(2) C4 0.098(4) 0.074(3) 0.044(2) 0.000(2) 0.005(2) 0.013(3) C5 0.086(3) 0.081(3) 0.048(2) -0.019(2) 0.005(2) 0.006(3) C6 0.101(4) 0.060(3) 0.065(3) -0.012(2) 0.003(3) 0.009(3) C7 0.079(3) 0.060(3) 0.050(2) -0.002(2) 0.000(2) 0.005(2) C8 0.091(3) 0.063(3) 0.043(2) 0.0089(19) 0.001(2) 0.013(2) C9 0.162(6) 0.065(3) 0.063(3) 0.022(2) 0.016(4) 0.029(4) C10 0.168(7) 0.114(6) 0.118(6) 0.049(5) 0.040(5) 0.051(5) C11 0.424(18) 0.147(8) 0.047(3) 0.028(4) 0.024(6) 0.157(10) C12 0.45(2) 0.297(17) 0.057(5) 0.047(8) 0.039(9) 0.157(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pt1 S1 2.2232(13) 6_554 ? Pt1 S1 2.2232(12) . ? Pt1 O1 2.033(3) . ? Pt1 O1 2.033(3) 6_554 ? S1 C8 1.710(5) . ? F1 C5 1.362(5) . ? O1 C1 1.262(5) . ? N1 C1 1.313(5) . ? N1 C8 1.346(5) . ? N2 C8 1.340(6) . ? N2 C9 1.460(7) . ? N2 C11 1.500(8) . ? C1 C2 1.504(5) . ? C2 C3 1.386(6) . ? C2 C7 1.370(6) . ? C3 H3 0.9300 . ? C3 C4 1.381(6) . ? C4 H4 0.9300 . ? C4 C5 1.356(7) . ? C5 C6 1.363(7) . ? C6 H6 0.9300 . ? C6 C7 1.389(7) . ? C7 H7 0.9300 . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C9 C10 1.489(9) . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C11 C12 1.127(16) . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S1 Pt1 S1 86.08(7) 6_554 . ? O1 Pt1 S1 178.19(10) 6_554 . ? O1 Pt1 S1 178.19(10) . 6_554 ? O1 Pt1 S1 94.49(9) . . ? O1 Pt1 S1 94.49(9) 6_554 6_554 ? O1 Pt1 O1 84.98(15) . 6_554 ? C8 S1 Pt1 108.42(15) . . ? C1 O1 Pt1 128.8(2) . . ? C1 N1 C8 127.1(4) . . ? C8 N2 C9 120.9(4) . . ? C8 N2 C11 122.0(5) . . ? C9 N2 C11 116.5(5) . . ? O1 C1 N1 131.1(4) . . ? O1 C1 C2 114.6(3) . . ? N1 C1 C2 114.3(4) . . ? C3 C2 C1 119.6(4) . . ? C7 C2 C1 121.2(4) . . ? C7 C2 C3 119.2(4) . . ? C2 C3 H3 119.8 . . ? C4 C3 C2 120.5(4) . . ? C4 C3 H3 119.8 . . ? C3 C4 H4 120.8 . . ? C5 C4 C3 118.4(5) . . ? C5 C4 H4 120.8 . . ? F1 C5 C6 118.3(5) . . ? C4 C5 F1 118.7(5) . . ? C4 C5 C6 123.0(4) . . ? C5 C6 H6 121.0 . . ? C5 C6 C7 118.0(5) . . ? C7 C6 H6 121.0 . . ? C2 C7 C6 120.7(4) . . ? C2 C7 H7 119.6 . . ? C6 C7 H7 119.6 . . ? N1 C8 S1 129.7(3) . . ? N2 C8 S1 116.0(3) . . ? N2 C8 N1 114.3(4) . . ? N2 C9 H9A 109.5 . . ? N2 C9 H9B 109.5 . . ? N2 C9 C10 110.7(6) . . ? H9A C9 H9B 108.1 . . ? C10 C9 H9A 109.5 . . ? C10 C9 H9B 109.5 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? N2 C11 H11A 106.2 . . ? N2 C11 H11B 106.2 . . ? H11A C11 H11B 106.4 . . ? C12 C11 N2 124.6(15) . . ? C12 C11 H11A 106.2 . . ? C12 C11 H11B 106.2 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Pt1 S1 C8 N1 -7.7(6) . . . . ? Pt1 S1 C8 N2 173.7(4) . . . . ? Pt1 O1 C1 N1 -0.5(7) . . . . ? Pt1 O1 C1 C2 -179.3(3) . . . . ? F1 C5 C6 C7 178.1(5) . . . . ? O1 C1 C2 C3 13.8(6) . . . . ? O1 C1 C2 C7 -168.5(4) . . . . ? N1 C1 C2 C3 -165.1(4) . . . . ? N1 C1 C2 C7 12.5(6) . . . . ? C1 N1 C8 S1 3.8(8) . . . . ? C1 N1 C8 N2 -177.7(5) . . . . ? C1 C2 C3 C4 176.1(4) . . . . ? C1 C2 C7 C6 -177.1(4) . . . . ? C2 C3 C4 C5 0.9(8) . . . . ? C3 C2 C7 C6 0.6(7) . . . . ? C3 C4 C5 F1 -179.1(5) . . . . ? C3 C4 C5 C6 0.8(9) . . . . ? C4 C5 C6 C7 -1.7(9) . . . . ? C5 C6 C7 C2 1.0(8) . . . . ? C7 C2 C3 C4 -1.6(7) . . . . ? C8 N1 C1 O1 1.7(8) . . . . ? C8 N1 C1 C2 -179.5(4) . . . . ? C8 N2 C9 C10 82.3(8) . . . . ? C8 N2 C11 C12 104.8(12) . . . . ? C9 N2 C8 S1 179.0(5) . . . . ? C9 N2 C8 N1 0.2(8) . . . . ? C9 N2 C11 C12 -83.8(14) . . . . ? C11 N2 C8 S1 -10.0(11) . . . . ? C11 N2 C8 N1 171.3(8) . . . . ? C11 N2 C9 C10 -89.2(9) . . . . ? _shelx_res_checksum 63626 _shelx_hkl_file ; 1 1 0 0.00 0.10 2 0 0 3864.01 83.39 -2 2 0 2092.19 43.80 2 2 0 2136.09 43.80 -3 1 0 0.00 0.40 3 -1 0 0.00 0.10 3 -3 0 0.00 0.30 3 3 0 0.00 0.20 4 2 0 9999.00 206.88 4 0 0 2030.50 42.10 4 -2 0 243.08 5.20 4 -4 0 502.85 11.10 4 4 0 513.35 10.70 5 3 0 0.00 0.40 5 1 0 0.00 0.30 5 -1 0 0.00 0.30 5 -3 0 0.00 0.20 5 -5 0 0.00 0.50 5 5 0 0.00 0.50 6 4 0 1785.92 39.00 6 2 0 5646.83 118.59 0 -6 0 173.28 3.50 6 0 0 167.58 3.80 -2 -6 0 1955.30 38.90 6 -2 0 1887.01 39.90 6 -4 0 1177.38 24.70 6 -6 0 516.65 12.40 6 6 0 540.35 13.20 7 5 0 0.00 0.50 7 3 0 0.10 0.60 7 3 0 0.00 0.70 7 1 0 0.00 0.30 1 -7 0 0.00 0.20 7 -1 0 0.00 0.50 -1 -7 0 0.00 0.20 -7 3 0 0.00 0.40 7 -3 0 0.00 0.30 -3 -7 0 0.00 0.20 7 -5 0 0.00 0.50 7 -7 0 0.00 0.70 7 7 0 0.00 0.40 7 7 0 0.00 0.50 8 6 0 374.26 8.40 8 6 0 375.06 10.20 8 4 0 1394.56 29.20 8 2 0 1452.35 32.30 8 0 0 849.61 17.90 0 -8 0 845.02 17.00 -2 -8 0 1377.26 28.20 8 -4 0 696.13 15.00 4 8 0 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41.80 2.60 20 10 -4 53.09 2.60 -10 20 -4 56.49 5.10 20 10 -4 57.79 2.70 -10 20 4 55.49 4.50 20 8 -4 61.19 4.50 20 8 -4 66.79 2.70 -8 20 -4 65.99 2.70 -8 20 4 65.79 2.90 -6 20 -4 83.69 3.00 20 6 -4 71.99 2.90 20 6 -4 73.59 2.90 -6 20 4 80.99 3.20 20 6 4 92.19 4.50 20 4 -4 86.19 4.00 20 4 -4 78.19 4.80 -4 20 -4 88.29 3.00 -4 20 4 85.99 3.20 20 2 -4 95.19 3.20 20 2 -4 98.69 5.30 -2 20 -4 102.29 3.30 -2 20 4 96.19 3.30 20 0 -4 99.09 4.20 0 20 -4 92.49 3.20 20 0 -4 86.09 3.00 0 -20 -4 89.79 2.70 0 20 4 96.99 3.30 2 20 -4 100.39 3.40 20 -2 -4 91.59 4.00 20 -2 -4 98.69 5.80 -2 -20 -4 87.39 2.60 2 20 4 96.09 3.30 20 -4 -4 97.29 8.70 20 -4 -4 100.39 3.20 -4 -20 -4 96.29 3.60 4 20 -4 93.39 3.30 20 -4 -4 101.79 3.20 4 20 4 101.39 3.50 20 -6 -4 67.09 6.20 20 -6 -4 66.99 2.60 6 20 -4 65.19 2.90 -6 -20 -4 66.29 3.50 6 20 4 67.89 2.90 -8 -20 -4 34.50 7.60 20 -8 -4 35.10 2.10 8 20 -4 34.80 2.20 20 -8 -4 34.70 4.80 8 20 4 39.50 2.40 -10 -20 -4 27.50 2.80 20 -10 -4 21.20 3.90 10 20 -4 26.80 2.20 20 -10 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2.80 1.40 21 1 -4 0.00 1.10 -1 21 -4 3.20 1.20 21 1 -4 0.30 1.10 -1 21 4 0.40 1.20 21 -1 -4 1.50 1.10 21 -1 -4 1.60 1.20 1 21 -4 2.40 1.20 1 21 4 1.90 1.30 3 21 -4 0.90 1.10 21 -3 -4 0.10 2.30 21 -3 -4 0.10 1.00 3 21 4 3.30 1.40 21 -5 -4 0.80 1.10 21 -5 -4 0.00 2.30 5 21 -4 1.30 1.30 21 -5 -4 1.40 2.40 5 21 4 1.20 1.20 21 -7 -4 0.00 3.00 21 -7 -4 0.00 1.10 7 21 -4 0.00 2.10 7 21 4 1.40 1.20 21 -9 -4 0.70 1.20 9 21 -4 0.00 2.10 21 -9 -4 1.30 2.40 -9 -21 -4 0.00 3.80 9 21 -4 0.60 1.40 9 21 4 0.70 1.40 -21 9 4 0.00 1.20 11 21 -4 1.50 1.60 21 -11 -4 0.40 2.60 -11 -21 -4 2.20 2.20 11 21 -4 3.90 3.10 -21 11 4 2.80 1.40 11 21 4 1.90 1.40 13 21 -4 0.00 9.60 13 21 -4 0.60 1.60 -21 13 4 2.00 1.50 13 21 4 0.50 1.30 15 21 -4 1.30 1.60 -21 15 4 0.50 1.50 15 21 4 2.30 1.60 17 21 -4 0.40 2.90 17 21 4 1.30 1.70 19 21 -4 0.00 1.70 19 21 4 0.30 1.80 21 21 -4 1.70 2.10 22 20 -4 4.30 3.40 22 18 -4 5.00 2.00 -22 -18 -4 9.70 1.80 -18 22 4 1.30 3.90 -22 -16 -4 6.30 1.60 22 16 -4 7.20 1.90 -16 22 4 4.80 3.10 22 14 -4 8.00 2.70 22 14 -4 12.60 1.90 -14 22 4 8.90 1.80 22 12 -4 13.00 3.30 22 12 -4 11.80 1.80 -12 22 4 11.10 1.90 -10 22 -4 16.50 3.70 22 10 -4 17.60 9.30 22 10 -4 17.30 1.70 -10 22 4 15.60 1.90 22 8 -4 26.60 2.10 22 8 -4 25.40 1.90 -8 22 -4 38.00 2.50 -8 22 4 26.30 2.10 22 6 -4 33.50 2.30 22 6 -4 34.80 5.30 -6 22 -4 48.10 2.60 22 6 4 49.20 4.90 -6 22 4 41.00 2.70 -4 22 -4 63.39 2.70 22 4 -4 47.80 4.10 22 4 -4 50.59 2.50 -4 22 4 48.20 2.60 22 2 -4 56.39 2.60 22 2 -4 56.09 5.50 -2 22 -4 66.79 2.80 -2 22 4 50.89 2.60 22 0 -4 46.30 5.20 22 0 -4 40.40 2.50 0 22 -4 46.60 2.40 0 22 4 44.40 2.40 22 -2 -4 44.00 2.30 2 22 -4 47.40 2.60 22 -2 -4 44.80 2.40 2 22 4 48.10 2.70 22 -4 -4 46.90 9.30 22 -4 -4 45.00 5.20 4 22 -4 46.20 2.50 22 -4 -4 46.70 2.50 4 22 4 46.30 2.50 6 22 -4 42.30 2.70 22 -6 -4 39.00 3.20 22 -6 -4 30.40 3.60 22 -6 -4 35.10 2.20 6 22 4 38.40 2.60 22 -8 -4 29.10 4.80 22 -8 -4 28.80 2.30 8 22 -4 29.30 2.30 8 22 4 33.60 2.50 -22 8 4 27.00 2.10 22 -10 -4 22.60 4.70 -10 -22 -4 24.50 6.80 10 22 -4 28.90 3.00 10 22 -4 22.10 2.10 22 -10 -4 27.10 2.20 -22 10 4 28.10 2.20 10 22 4 24.70 2.10 12 22 -4 20.20 4.80 12 22 -4 19.70 2.10 -12 -22 -4 16.00 2.80 -22 12 4 21.70 1.90 12 22 4 19.90 2.00 14 22 -4 12.00 1.90 14 22 4 12.80 2.00 16 22 -4 6.80 1.80 16 22 4 7.80 3.10 18 22 -4 5.40 2.10 18 22 4 1.30 1.80 20 22 -4 0.00 1.80 20 22 4 2.30 2.10 23 19 -4 0.00 2.00 23 17 -4 0.00 1.70 -23 -17 -4 0.70 1.80 -17 23 4 0.00 1.80 -23 -15 -4 1.80 4.40 23 15 -4 0.90 1.70 -15 23 4 0.00 1.70 23 13 -4 2.90 1.60 -13 23 4 0.00 1.60 23 11 -4 1.10 12.60 -11 23 -4 2.10 3.00 23 11 -4 1.20 1.50 -11 23 4 1.90 1.70 23 9 -4 0.00 1.30 23 9 -4 2.80 1.40 -9 23 -4 0.00 2.80 -9 23 4 1.00 1.50 -7 23 -4 2.40 1.30 23 7 -4 0.40 1.20 23 7 -4 0.00 2.80 -7 23 4 0.00 1.40 23 5 -4 0.40 1.20 23 5 -4 1.20 2.20 -5 23 -4 3.00 1.30 -5 23 4 0.00 1.30 23 5 4 1.10 2.30 23 3 -4 2.00 1.30 -3 23 -4 3.20 1.40 23 3 -4 1.90 1.30 -3 23 4 1.90 1.50 23 1 -4 0.40 1.20 -1 23 -4 3.30 1.40 23 1 -4 1.80 2.50 -1 23 4 3.70 1.50 23 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2.40 0.60 6 5 -5 8.20 0.70 -6 -5 -5 7.30 0.60 5 -6 -5 8.50 0.70 6 5 -5 7.50 0.50 -5 6 -5 7.10 0.60 6 5 5 8.80 0.60 6 3 -5 3.70 2.00 -3 6 -5 4.00 0.50 -6 -3 -5 4.70 1.40 -3 6 -5 4.80 0.70 6 3 -5 4.30 0.50 3 -6 -5 3.30 1.20 3 -6 -5 3.90 1.10 -3 6 5 4.60 1.30 6 3 5 3.60 0.70 6 1 -5 2.30 0.40 -1 6 -5 2.30 0.20 1 -6 -5 2.30 0.40 -6 -1 -5 1.70 0.30 6 1 -5 2.90 0.30 6 1 5 2.30 0.90 -1 6 5 2.10 0.40 -6 1 -5 5.40 0.40 -1 -6 -5 4.20 0.50 6 -1 -5 4.90 0.80 6 -1 -5 4.20 0.50 6 -1 5 4.70 0.40 6 -3 -5 223.98 5.10 -6 3 -5 217.18 5.70 3 6 -5 217.38 6.20 -3 -6 -5 217.48 4.80 6 -3 -5 222.68 5.40 3 6 5 222.38 5.30 6 -3 5 224.98 5.20 6 -5 -5 28.30 1.10 -5 -6 -5 31.00 1.30 6 -5 -5 28.70 1.10 5 6 -5 29.60 1.10 5 6 5 30.20 2.30 6 -5 5 28.80 2.00 7 6 -5 127.89 3.30 6 -7 -5 131.19 3.30 -7 -6 -5 130.29 3.10 7 6 -5 128.49 3.90 7 6 5 130.19 3.20 -6 7 5 127.29 3.20 4 -7 -5 74.99 2.00 -4 7 -5 79.79 2.10 7 4 -5 77.29 2.00 7 4 5 79.49 2.40 -4 7 5 77.69 2.10 7 2 -5 85.89 3.10 -2 7 -5 94.69 3.70 -2 7 -5 91.99 1.90 7 2 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10 5 -5 2.90 1.10 10 5 -5 2.90 0.60 10 5 5 3.80 1.00 -5 10 5 3.40 0.60 10 3 -5 0.10 0.50 -3 10 -5 0.10 0.40 10 3 -5 0.90 0.70 3 -10 -5 0.00 0.50 -3 10 5 0.80 0.50 10 3 5 0.50 3.10 -1 10 -5 0.00 1.00 10 1 -5 1.10 0.90 1 -10 -5 0.00 0.70 10 1 -5 0.40 0.50 -1 10 -5 0.00 0.40 -1 10 5 0.20 0.50 10 1 5 0.70 0.40 1 10 -5 89.79 3.90 10 -1 -5 88.39 2.40 1 10 -5 96.79 2.70 -1 -10 -5 88.19 2.30 10 -1 -5 90.39 2.50 -10 1 -5 93.59 2.80 1 10 5 87.49 2.50 10 -1 5 92.79 3.70 3 10 -5 51.69 1.60 -3 -10 -5 45.80 1.50 3 10 -5 51.09 2.80 10 -3 -5 50.39 1.60 10 -3 -5 50.29 2.70 -10 3 -5 52.79 1.60 3 10 5 47.90 1.70 10 -5 -5 63.39 3.10 -5 -10 -5 74.49 7.60 5 10 -5 64.19 3.10 5 10 -5 66.79 2.10 -5 -10 -5 62.59 1.80 10 -5 -5 64.99 2.90 5 10 5 62.99 2.00 5 10 5 67.79 2.10 10 -5 5 66.19 3.30 -7 -10 -5 26.20 1.20 7 10 -5 26.70 1.90 10 -7 -5 23.80 2.10 7 10 -5 28.00 1.40 10 -7 -5 27.30 1.20 10 -7 5 28.70 1.80 7 10 5 27.30 1.60 7 10 5 25.20 1.30 10 -9 -5 22.80 1.20 -9 -10 -5 23.70 1.20 9 10 -5 24.30 1.70 9 10 -5 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