#============================================================================== data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 10 _journal_issue 2 _journal_year 2019 _journal_page_first 95 _journal_page_last 101 #=============================================================================== data_global _audit_creation_method 'APEX2 v2014.11-0' _publ_requested_journal ? _publ_contact_author_name ? _publ_contact_author_address ; ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_section_title ; ; _publ_section_abstract ; ; _publ_section_references ; ; _publ_section_comment ; ; data_I _chemical_name_systematic ? _chemical_name_common 'organic compound' _chemical_formula_moiety 'C12 H10 N3, Cl' _chemical_formula_sum 'C12 H10 Cl N3' _chemical_formula_iupac ? _chemical_formula_weight 231.68 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.7908(5) _cell_length_b 10.9756(4) _cell_length_c 15.0251(5) _cell_angle_alpha 90 _cell_angle_beta 105.058(3) _cell_angle_gamma 90 _cell_volume 2196.14(14) _cell_formula_units_Z 8 _cell_measurement_reflns_used 3124 _cell_measurement_theta_min 2.3291 _cell_measurement_theta_max 27.0190 _cell_measurement_temperature 300.(2) _exptl_crystal_description block _exptl_crystal_colour yellow _exptl_crystal_size_max 0.319 _exptl_crystal_size_mid 0.143 _exptl_crystal_size_min 0.079 _exptl_crystal_density_diffrn 1.401 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 960 _exptl_absorpt_coefficient_mu 0.321 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2014/5 (Bruker AXS)' _exptl_absorpt_correction_T_min 0.61 _exptl_absorpt_correction_T_max 0.97 _exptl_special_details ; ; _diffrn_ambient_temperature 300.(2) _diffrn_source 'microfocus sealed tube' _diffrn_source_type ImuS _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'multilayer QUAZAR mirrors' _diffrn_measurement_device_type 'Bruker APEX II QUAZAR three-circle diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 8.3333 _diffrn_reflns_number 17183 _diffrn_reflns_av_R_equivalents 0.1048 _diffrn_reflns_av_unetI/netI 0.0890 _diffrn_reflns_theta_min 2.98 _diffrn_reflns_theta_max 25.68 _diffrn_reflns_theta_full 25.68 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_limit_l_max 18 _refine_special_details ; ; _reflns_number_total 4166 _reflns_number_gt 2066 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.1379 _refine_ls_R_factor_gt 0.0562 _refine_ls_wR_factor_gt 0.1151 _refine_ls_wR_factor_ref 0.1456 _refine_ls_goodness_of_fit_ref 1.024 _refine_ls_restrained_S_all 1.023 _refine_ls_number_reflns 4166 _refine_ls_number_parameters 307 _refine_ls_number_restraints 6 _refine_ls_number_constraints ? _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0513P)^2^+0.0678P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.273 _refine_diff_density_min -0.218 _refine_ls_extinction_method none _refine_ls_extinction_coef ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection 'Bruker Instrument Service v2013.12.0.0 (Bruker AXS)' _computing_cell_refinement 'APEX2 v2014.11-0 (Bruker AXS)' _computing_data_reduction 'SAINT V8.34A (Bruker AXS)' _computing_structure_solution 'SHELXTL V6.14 (Bruker AXS)' _computing_structure_refinement 'SHELXTL V6.14 (Bruker AXS)' _computing_molecular_graphics 'MERCURY (Macrae et al., 2006)' _computing_publication_material 'PLATON V1.16 (Spek, 2009), SHELXTL V6.14 (Bruker AXS)' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.8874(3) 0.2752(3) 0.4313(3) 0.0554(11) Uani d . . . 1 . . H H1 0.8811 0.2288 0.3784 0.066 Uiso calc U . R 1 . . C C2 0.9153(3) 0.2147(4) 0.5167(3) 0.0642(12) Uani d . . . 1 . . H H2 0.9255 0.1308 0.5198 0.077 Uiso calc U . R 1 . . C C3 0.9271(3) 0.2823(4) 0.5945(3) 0.0629(12) Uani d . . . 1 . . H H3 0.9465 0.2447 0.6519 0.075 Uiso calc U . R 1 . . C C4 0.9101(3) 0.4086(4) 0.5889(3) 0.0505(10) Uani d . . . 1 . . C C5 0.9187(3) 0.4860(4) 0.6668(3) 0.0609(11) Uani d . . . 1 . . H H5 0.9392 0.4534 0.7258 0.073 Uiso calc U . R 1 . . C C6 0.8975(3) 0.6047(4) 0.6561(3) 0.0572(11) Uani d . . . 1 . . H H6 0.9015 0.6529 0.7079 0.069 Uiso calc U . R 1 . . C C7 0.8692(3) 0.6588(3) 0.5674(2) 0.0445(9) Uani d . . . 1 . . C C8 0.8473(3) 0.7849(3) 0.5526(3) 0.0521(10) Uani d . . . 1 . . H H8 0.8525 0.8357 0.6032 0.063 Uiso calc U . R 1 . . C C9 0.8195(3) 0.8327(3) 0.4674(3) 0.0503(10) Uani d . . . 1 . . H H9 0.8051 0.9154 0.4592 0.06 Uiso calc U . R 1 . . C C10 0.8122(3) 0.7559(3) 0.3898(3) 0.0427(9) Uani d . . . 1 . . C C11 0.8617(3) 0.5860(3) 0.4913(2) 0.0395(9) Uani d . . . 1 . . C C12 0.8808(2) 0.4585(3) 0.4991(2) 0.0406(9) Uani d . . . 1 . . C C13 0.6765(3) 0.3465(3) 0.6061(2) 0.0383(8) Uani d . . . 1 . . C C14 0.6650(3) 0.2705(3) 0.5282(3) 0.0431(9) Uani d . . . 1 . . H H14 0.68 0.1879 0.536 0.052 Uiso calc U . R 1 . . C C15 0.6328(3) 0.3166(3) 0.4430(3) 0.0456(9) Uani d . . . 1 . . H H15 0.6248 0.2652 0.3924 0.055 Uiso calc U . R 1 . . C C16 0.6106(3) 0.4429(3) 0.4285(2) 0.0406(9) Uani d . . . 1 . . C C17 0.5797(3) 0.4977(4) 0.3397(2) 0.0526(10) Uani d . . . 1 . . H H17 0.5703 0.4491 0.2874 0.063 Uiso calc U . R 1 . . C C18 0.5641(3) 0.6180(4) 0.3301(2) 0.0528(10) Uani d . . . 1 . . H H18 0.5442 0.6513 0.2713 0.063 Uiso calc U . R 1 . . C C19 0.5773(3) 0.6956(3) 0.4079(2) 0.0425(9) Uani d . . . 1 . . C C20 0.5682(3) 0.8234(3) 0.4030(3) 0.0533(10) Uani d . . . 1 . . H H20 0.552 0.8622 0.346 0.064 Uiso calc U . R 1 . . C C21 0.5831(3) 0.8893(3) 0.4814(3) 0.0556(11) Uani d . . . 1 . . H H21 0.5777 0.9738 0.479 0.067 Uiso calc U . R 1 . . C C22 0.6069(3) 0.8287(3) 0.5662(2) 0.0477(10) Uani d . . . 1 . . H H22 0.615 0.8754 0.6193 0.057 Uiso calc U . R 1 . . C C23 0.6050(2) 0.6441(3) 0.4971(2) 0.0347(8) Uani d . . . 1 . . C C24 0.6222(2) 0.5161(3) 0.5053(2) 0.0320(8) Uani d . . . 1 . . Cl Cl1 0.80865(8) 0.56595(7) 0.19214(6) 0.0599(3) Uani d . . . 1 . . Cl Cl2 0.69969(8) 0.53953(7) 0.80849(6) 0.0588(3) Uani d . . . 1 . . N N1 0.7852(3) 0.7986(3) 0.3046(2) 0.0574(9) Uani d . . D 1 . . N N2 0.8337(2) 0.6370(2) 0.40432(19) 0.0385(7) Uani d . . D 1 . . N N3 0.8695(2) 0.3927(3) 0.4209(2) 0.0452(8) Uani d . . . 1 . . N N4 0.7091(2) 0.3058(2) 0.6915(2) 0.0496(8) Uani d . . D 1 . . N N5 0.6532(2) 0.4658(2) 0.59167(18) 0.0346(7) Uani d . . D 1 . . N N6 0.6185(2) 0.7103(2) 0.57571(18) 0.0405(7) Uani d . . . 1 . . H H1N 0.660(2) 0.515(2) 0.6393(16) 0.049 Uiso d U . D 1 . . H H2N 0.825(2) 0.588(2) 0.3557(16) 0.049 Uiso d U . D 1 . . H H3N 0.712(2) 0.362(2) 0.7377(17) 0.049 Uiso d U . D 1 . . H H4N 0.723(2) 0.2258(17) 0.698(2) 0.049 Uiso d U . D 1 . . H H5N 0.784(2) 0.745(2) 0.2591(17) 0.049 Uiso d U . D 1 . . H H6N 0.757(2) 0.8731(19) 0.299(2) 0.049 Uiso d U . D 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.050(3) 0.039(2) 0.080(3) 0.0045(19) 0.021(2) 0.000(2) C2 0.049(3) 0.043(2) 0.102(4) 0.007(2) 0.022(3) 0.021(2) C3 0.041(3) 0.064(3) 0.081(3) -0.001(2) 0.013(2) 0.030(2) C4 0.028(2) 0.059(3) 0.066(3) -0.0014(18) 0.0141(19) 0.011(2) C5 0.047(3) 0.089(3) 0.044(2) -0.006(2) 0.008(2) 0.008(2) C6 0.046(3) 0.077(3) 0.047(3) -0.001(2) 0.009(2) -0.007(2) C7 0.032(2) 0.056(2) 0.045(2) -0.0003(18) 0.0087(18) -0.0078(18) C8 0.038(3) 0.059(3) 0.060(3) -0.0050(19) 0.014(2) -0.026(2) C9 0.051(3) 0.040(2) 0.063(3) -0.0022(18) 0.020(2) -0.0140(19) C10 0.040(2) 0.0313(19) 0.059(2) -0.0001(17) 0.0174(19) -0.0046(18) C11 0.033(2) 0.039(2) 0.049(2) -0.0005(16) 0.0143(18) -0.0006(17) C12 0.031(2) 0.047(2) 0.046(2) -0.0006(17) 0.0146(17) 0.0037(18) C13 0.039(2) 0.0283(18) 0.050(2) 0.0001(16) 0.0153(18) -0.0013(16) C14 0.045(3) 0.0248(18) 0.062(3) -0.0017(16) 0.019(2) -0.0080(17) C15 0.039(2) 0.042(2) 0.059(3) -0.0074(17) 0.018(2) -0.0226(18) C16 0.039(2) 0.041(2) 0.044(2) -0.0082(17) 0.0147(18) -0.0115(17) C17 0.050(3) 0.066(3) 0.041(2) -0.002(2) 0.010(2) -0.012(2) C18 0.049(3) 0.066(3) 0.040(2) 0.002(2) 0.0075(19) 0.008(2) C19 0.032(2) 0.045(2) 0.049(2) 0.0019(17) 0.0098(18) 0.0085(17) C20 0.045(3) 0.049(2) 0.063(3) 0.0017(19) 0.009(2) 0.019(2) C21 0.051(3) 0.033(2) 0.083(3) 0.0045(18) 0.017(2) 0.009(2) C22 0.046(3) 0.034(2) 0.062(3) 0.0017(18) 0.014(2) -0.0049(18) C23 0.029(2) 0.0316(18) 0.044(2) -0.0002(15) 0.0110(16) -0.0010(16) C24 0.028(2) 0.0296(17) 0.039(2) -0.0007(15) 0.0087(16) -0.0006(15) Cl1 0.0997(9) 0.0299(5) 0.0540(6) -0.0013(5) 0.0274(6) -0.0016(4) Cl2 0.0938(9) 0.0293(5) 0.0530(6) -0.0053(5) 0.0185(6) -0.0042(4) N1 0.082(3) 0.0348(18) 0.059(2) 0.0098(17) 0.025(2) 0.0007(16) N2 0.041(2) 0.0316(16) 0.0444(19) 0.0013(13) 0.0136(15) -0.0050(13) N3 0.042(2) 0.0377(17) 0.060(2) 0.0006(14) 0.0211(16) -0.0006(15) N4 0.067(2) 0.0256(16) 0.057(2) 0.0051(16) 0.0172(18) 0.0010(15) N5 0.0375(19) 0.0246(15) 0.0431(18) -0.0014(13) 0.0130(14) -0.0071(12) N6 0.0379(19) 0.0290(15) 0.0552(19) 0.0000(13) 0.0134(15) -0.0030(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 N3 . 1.314(4) ? C1 C2 . 1.407(5) ? C1 H1 . 0.93 ? C2 C3 . 1.358(5) ? C2 H2 . 0.93 ? C3 C4 . 1.404(5) ? C3 H3 . 0.93 ? C4 C12 . 1.414(5) ? C4 C5 . 1.426(5) ? C5 C6 . 1.335(5) ? C5 H5 . 0.93 ? C6 C7 . 1.418(5) ? C6 H6 . 0.93 ? C7 C11 . 1.377(4) ? C7 C8 . 1.422(5) ? C8 C9 . 1.345(5) ? C8 H8 . 0.93 ? C9 C10 . 1.421(4) ? C9 H9 . 0.93 ? C10 N1 . 1.322(4) ? C10 N2 . 1.344(4) ? C11 N2 . 1.381(4) ? C11 C12 . 1.424(4) ? C12 N3 . 1.353(4) ? C13 N4 . 1.323(4) ? C13 N5 . 1.352(4) ? C13 C14 . 1.413(4) ? C14 C15 . 1.340(4) ? C14 H14 . 0.93 ? C15 C16 . 1.424(4) ? C15 H15 . 0.93 ? C16 C24 . 1.381(4) ? C16 C17 . 1.424(4) ? C17 C18 . 1.339(5) ? C17 H17 . 0.93 ? C18 C19 . 1.419(5) ? C18 H18 . 0.93 ? C19 C20 . 1.409(5) ? C19 C23 . 1.412(4) ? C20 C21 . 1.353(5) ? C20 H20 . 0.93 ? C21 C22 . 1.399(5) ? C21 H21 . 0.93 ? C22 N6 . 1.313(4) ? C22 H22 . 0.93 ? C23 N6 . 1.358(4) ? C23 C24 . 1.426(4) ? C24 N5 . 1.372(4) ? N1 H5N . 0.900(17) ? N1 H6N . 0.902(17) ? N2 H2N . 0.889(17) ? N4 H3N . 0.924(17) ? N4 H4N . 0.899(17) ? N5 H1N . 0.880(17) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N3 C1 C2 . . 124.8(4) ? N3 C1 H1 . . 117.6 ? C2 C1 H1 . . 117.6 ? C3 C2 C1 . . 118.0(4) ? C3 C2 H2 . . 121.0 ? C1 C2 H2 . . 121.0 ? C2 C3 C4 . . 120.5(4) ? C2 C3 H3 . . 119.8 ? C4 C3 H3 . . 119.8 ? C3 C4 C12 . . 116.2(4) ? C3 C4 C5 . . 124.2(4) ? C12 C4 C5 . . 119.6(4) ? C6 C5 C4 . . 120.9(4) ? C6 C5 H5 . . 119.5 ? C4 C5 H5 . . 119.5 ? C5 C6 C7 . . 121.3(4) ? C5 C6 H6 . . 119.3 ? C7 C6 H6 . . 119.3 ? C11 C7 C6 . . 118.7(3) ? C11 C7 C8 . . 117.9(3) ? C6 C7 C8 . . 123.3(3) ? C9 C8 C7 . . 121.7(3) ? C9 C8 H8 . . 119.2 ? C7 C8 H8 . . 119.2 ? C8 C9 C10 . . 119.5(3) ? C8 C9 H9 . . 120.3 ? C10 C9 H9 . . 120.3 ? N1 C10 N2 . . 119.7(3) ? N1 C10 C9 . . 121.7(3) ? N2 C10 C9 . . 118.5(3) ? C7 C11 N2 . . 119.5(3) ? C7 C11 C12 . . 122.0(3) ? N2 C11 C12 . . 118.5(3) ? N3 C12 C4 . . 124.2(3) ? N3 C12 C11 . . 118.4(3) ? C4 C12 C11 . . 117.4(3) ? N4 C13 N5 . . 119.3(3) ? N4 C13 C14 . . 122.7(3) ? N5 C13 C14 . . 117.9(3) ? C15 C14 C13 . . 120.4(3) ? C15 C14 H14 . . 119.8 ? C13 C14 H14 . . 119.8 ? C14 C15 C16 . . 121.2(3) ? C14 C15 H15 . . 119.4 ? C16 C15 H15 . . 119.4 ? C24 C16 C15 . . 117.7(3) ? C24 C16 C17 . . 118.6(3) ? C15 C16 C17 . . 123.7(3) ? C18 C17 C16 . . 121.2(3) ? C18 C17 H17 . . 119.4 ? C16 C17 H17 . . 119.4 ? C17 C18 C19 . . 121.4(3) ? C17 C18 H18 . . 119.3 ? C19 C18 H18 . . 119.3 ? C20 C19 C23 . . 116.5(3) ? C20 C19 C18 . . 124.3(3) ? C23 C19 C18 . . 119.1(3) ? C21 C20 C19 . . 119.7(3) ? C21 C20 H20 . . 120.1 ? C19 C20 H20 . . 120.1 ? C20 C21 C22 . . 119.1(3) ? C20 C21 H21 . . 120.5 ? C22 C21 H21 . . 120.5 ? N6 C22 C21 . . 124.3(3) ? N6 C22 H22 . . 117.9 ? C21 C22 H22 . . 117.9 ? N6 C23 C19 . . 123.6(3) ? N6 C23 C24 . . 118.0(3) ? C19 C23 C24 . . 118.3(3) ? N5 C24 C16 . . 119.8(3) ? N5 C24 C23 . . 118.9(3) ? C16 C24 C23 . . 121.3(3) ? C10 N1 H5N . . 117.(2) ? C10 N1 H6N . . 114.(2) ? H5N N1 H6N . . 127.(3) ? C10 N2 C11 . . 122.9(3) ? C10 N2 H2N . . 118.(2) ? C11 N2 H2N . . 119.(2) ? C1 N3 C12 . . 116.4(3) ? C13 N4 H3N . . 116.0(19) ? C13 N4 H4N . . 117.(2) ? H3N N4 H4N . . 127.(3) ? C13 N5 C24 . . 122.9(3) ? C13 N5 H1N . . 119.(2) ? C24 N5 H1N . . 118.(2) ? C22 N6 C23 . . 116.7(3) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N3 C1 C2 C3 . . . . -1.6(6) ? C1 C2 C3 C4 . . . . 1.0(6) ? C2 C3 C4 C12 . . . . 0.0(5) ? C2 C3 C4 C5 . . . . 178.6(4) ? C3 C4 C5 C6 . . . . -177.3(4) ? C12 C4 C5 C6 . . . . 1.2(6) ? C4 C5 C6 C7 . . . . -2.1(6) ? C5 C6 C7 C11 . . . . 1.3(5) ? C5 C6 C7 C8 . . . . -179.1(4) ? C11 C7 C8 C9 . . . . 0.4(5) ? C6 C7 C8 C9 . . . . -179.2(4) ? C7 C8 C9 C10 . . . . -0.5(5) ? C8 C9 C10 N1 . . . . -180.0(4) ? C8 C9 C10 N2 . . . . 0.0(5) ? C6 C7 C11 N2 . . . . 179.7(3) ? C8 C7 C11 N2 . . . . 0.1(5) ? C6 C7 C11 C12 . . . . 0.4(5) ? C8 C7 C11 C12 . . . . -179.2(3) ? C3 C4 C12 N3 . . . . -0.6(5) ? C5 C4 C12 N3 . . . . -179.3(3) ? C3 C4 C12 C11 . . . . 179.1(3) ? C5 C4 C12 C11 . . . . 0.5(5) ? C7 C11 C12 N3 . . . . 178.5(3) ? N2 C11 C12 N3 . . . . -0.8(5) ? C7 C11 C12 C4 . . . . -1.3(5) ? N2 C11 C12 C4 . . . . 179.5(3) ? N4 C13 C14 C15 . . . . -179.3(3) ? N5 C13 C14 C15 . . . . 0.5(5) ? C13 C14 C15 C16 . . . . 0.9(5) ? C14 C15 C16 C24 . . . . -0.8(5) ? C14 C15 C16 C17 . . . . 177.5(3) ? C24 C16 C17 C18 . . . . 1.3(5) ? C15 C16 C17 C18 . . . . -177.0(4) ? C16 C17 C18 C19 . . . . -0.2(6) ? C17 C18 C19 C20 . . . . 176.0(4) ? C17 C18 C19 C23 . . . . -1.7(5) ? C23 C19 C20 C21 . . . . -1.7(5) ? C18 C19 C20 C21 . . . . -179.4(3) ? C19 C20 C21 C22 . . . . -0.4(5) ? C20 C21 C22 N6 . . . . 1.8(6) ? C20 C19 C23 N6 . . . . 2.8(5) ? C18 C19 C23 N6 . . . . -179.4(3) ? C20 C19 C23 C24 . . . . -175.5(3) ? C18 C19 C23 C24 . . . . 2.3(5) ? C15 C16 C24 N5 . . . . -0.7(5) ? C17 C16 C24 N5 . . . . -179.1(3) ? C15 C16 C24 C23 . . . . 177.8(3) ? C17 C16 C24 C23 . . . . -0.6(5) ? N6 C23 C24 N5 . . . . -1.1(4) ? C19 C23 C24 N5 . . . . 177.3(3) ? N6 C23 C24 C16 . . . . -179.6(3) ? C19 C23 C24 C16 . . . . -1.2(5) ? N1 C10 N2 C11 . . . . -179.5(3) ? C9 C10 N2 C11 . . . . 0.6(5) ? C7 C11 N2 C10 . . . . -0.6(5) ? C12 C11 N2 C10 . . . . 178.7(3) ? C2 C1 N3 C12 . . . . 1.0(5) ? C4 C12 N3 C1 . . . . 0.1(5) ? C11 C12 N3 C1 . . . . -179.6(3) ? N4 C13 N5 C24 . . . . 177.7(3) ? C14 C13 N5 C24 . . . . -2.1(5) ? C16 C24 N5 C13 . . . . 2.2(5) ? C23 C24 N5 C13 . . . . -176.4(3) ? C21 C22 N6 C23 . . . . -0.9(5) ? C19 C23 N6 C22 . . . . -1.5(5) ? C24 C23 N6 C22 . . . . 176.8(3) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C9 H9 Cl1 2_655 0.93 2.92 3.636(4) 135.1 ? C14 H14 Cl2 2_646 0.93 2.97 3.681(4) 133.9 ? N5 H1N Cl2 . 0.880(17) 2.47(2) 3.255(3) 148.(3) ? N2 H2N Cl1 . 0.889(17) 2.42(2) 3.212(3) 148.(3) ? N4 H3N Cl2 . 0.924(17) 2.24(2) 3.132(3) 161.(3) ? N4 H4N Cl2 2_646 0.899(17) 2.32(2) 3.181(3) 161.(3) ? N1 H5N Cl1 . 0.900(17) 2.27(2) 3.125(3) 158.(3) ? N1 H6N Cl1 2_655 0.902(17) 2.317(18) 3.212(3) 172.(3) ? _shelx_res_file ; test_APO1_0m_a.res created by SHELXL-2014/7 TITL test_APO1_0m_a.res in P2(1)/n CELL 0.71073 13.7908 10.9756 15.0251 90.000 105.058 90.000 ZERR 8.000 0.0005 0.0004 0.0005 0.000 0.003 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N Cl UNIT 96 80 24 8 SHEL 7 0.82 OMIT 12 0 0 OMIT 12 3 0 HTAB ACTA CONF EQIV $1 -x+3/2, y+1/2, -z+1/2 HTAB C9 Cl1_$1 EQIV $2 -x+3/2, y-1/2, -z+3/2 HTAB C14 Cl2_$2 HTAB N5 Cl2 HTAB N2 Cl1 HTAB N4 Cl2 HTAB N4 Cl2_$2 HTAB N1 Cl1 HTAB N1 Cl1_$1 L.S. 10 BOND $H FMAP 2 PLAN 20 SIZE 0.079 0.143 0.319 DFIX 0.89 0.02 N5 H1N N2 H2N DFIX 0.89 0.02 N4 H3n N4 H4n N1 H5n N1 H6n TEMP 26.730 WGHT 0.051300 0.067800 FVAR 0.27252 C1 1 0.887381 0.275240 0.431339 11.00000 0.04977 0.03911 = 0.07975 -0.00046 0.02127 0.00447 AFIX 43 H1 2 0.881086 0.228761 0.378386 11.00000 -1.20000 AFIX 0 C2 1 0.915335 0.214679 0.516699 11.00000 0.04892 0.04319 = 0.10172 0.02100 0.02180 0.00711 AFIX 43 H2 2 0.925459 0.130846 0.519783 11.00000 -1.20000 AFIX 0 C3 1 0.927101 0.282313 0.594490 11.00000 0.04142 0.06417 = 0.08148 0.02978 0.01312 -0.00104 AFIX 43 H3 2 0.946523 0.244736 0.651860 11.00000 -1.20000 AFIX 0 C4 1 0.910147 0.408558 0.588899 11.00000 0.02824 0.05862 = 0.06578 0.01057 0.01412 -0.00137 C5 1 0.918657 0.486011 0.666791 11.00000 0.04728 0.08896 = 0.04433 0.00828 0.00781 -0.00636 AFIX 43 H5 2 0.939189 0.453399 0.725839 11.00000 -1.20000 AFIX 0 C6 1 0.897549 0.604707 0.656091 11.00000 0.04558 0.07725 = 0.04699 -0.00729 0.00882 -0.00089 AFIX 43 H6 2 0.901524 0.652853 0.707851 11.00000 -1.20000 AFIX 0 C7 1 0.869199 0.658794 0.567400 11.00000 0.03170 0.05573 = 0.04539 -0.00778 0.00870 -0.00030 C8 1 0.847349 0.784934 0.552643 11.00000 0.03807 0.05902 = 0.06012 -0.02629 0.01414 -0.00505 AFIX 43 H8 2 0.852459 0.835658 0.603235 11.00000 -1.20000 AFIX 0 C9 1 0.819480 0.832736 0.467363 11.00000 0.05087 0.03984 = 0.06321 -0.01402 0.02047 -0.00222 AFIX 43 H9 2 0.805072 0.915398 0.459241 11.00000 -1.20000 AFIX 0 C10 1 0.812226 0.755943 0.389786 11.00000 0.04048 0.03134 = 0.05874 -0.00463 0.01742 -0.00006 C11 1 0.861666 0.586009 0.491269 11.00000 0.03260 0.03862 = 0.04926 -0.00061 0.01426 -0.00048 C12 1 0.880783 0.458455 0.499110 11.00000 0.03106 0.04740 = 0.04592 0.00374 0.01463 -0.00057 C13 1 0.676488 0.346542 0.606093 11.00000 0.03869 0.02828 = 0.05015 -0.00132 0.01529 0.00013 C14 1 0.665040 0.270471 0.528156 11.00000 0.04513 0.02477 = 0.06244 -0.00799 0.01943 -0.00167 AFIX 43 H14 2 0.679970 0.187907 0.536019 11.00000 -1.20000 AFIX 0 C15 1 0.632799 0.316600 0.442990 11.00000 0.03923 0.04187 = 0.05874 -0.02260 0.01815 -0.00736 AFIX 43 H15 2 0.624795 0.265167 0.392406 11.00000 -1.20000 AFIX 0 C16 1 0.610567 0.442852 0.428479 11.00000 0.03858 0.04116 = 0.04429 -0.01153 0.01475 -0.00816 C17 1 0.579728 0.497722 0.339682 11.00000 0.04996 0.06628 = 0.04082 -0.01241 0.01042 -0.00188 AFIX 43 H17 2 0.570252 0.449147 0.287407 11.00000 -1.20000 AFIX 0 C18 1 0.564135 0.617954 0.330112 11.00000 0.04942 0.06627 = 0.04030 0.00759 0.00750 0.00205 AFIX 43 H18 2 0.544235 0.651310 0.271271 11.00000 -1.20000 AFIX 0 C19 1 0.577343 0.695552 0.407887 11.00000 0.03248 0.04549 = 0.04908 0.00849 0.00985 0.00191 C20 1 0.568204 0.823367 0.402951 11.00000 0.04502 0.04912 = 0.06311 0.01923 0.00937 0.00174 AFIX 43 H20 2 0.551965 0.862231 0.345993 11.00000 -1.20000 AFIX 0 C21 1 0.583144 0.889335 0.481395 11.00000 0.05095 0.03304 = 0.08276 0.00858 0.01723 0.00446 AFIX 43 H21 2 0.577713 0.973798 0.478980 11.00000 -1.20000 AFIX 0 C22 1 0.606876 0.828719 0.566194 11.00000 0.04644 0.03427 = 0.06242 -0.00495 0.01397 0.00174 AFIX 43 H22 2 0.614958 0.875351 0.619302 11.00000 -1.20000 AFIX 0 C23 1 0.604962 0.644122 0.497052 11.00000 0.02933 0.03158 = 0.04393 -0.00105 0.01103 -0.00024 C24 1 0.622215 0.516058 0.505312 11.00000 0.02778 0.02957 = 0.03870 -0.00055 0.00873 -0.00070 CL1 4 0.808653 0.565945 0.192140 11.00000 0.09973 0.02992 = 0.05405 -0.00155 0.02738 -0.00131 CL2 4 0.699692 0.539529 0.808491 11.00000 0.09377 0.02930 = 0.05303 -0.00418 0.01850 -0.00526 N1 3 0.785191 0.798607 0.304613 11.00000 0.08188 0.03483 = 0.05899 0.00067 0.02469 0.00982 N2 3 0.833717 0.637033 0.404318 11.00000 0.04097 0.03159 = 0.04442 -0.00499 0.01358 0.00133 N3 3 0.869506 0.392702 0.420938 11.00000 0.04191 0.03770 = 0.06026 -0.00061 0.02108 0.00063 N4 3 0.709057 0.305751 0.691527 11.00000 0.06664 0.02557 = 0.05728 0.00102 0.01717 0.00507 N5 3 0.653178 0.465783 0.591674 11.00000 0.03752 0.02463 = 0.04308 -0.00711 0.01302 -0.00142 N6 3 0.618485 0.710317 0.575710 11.00000 0.03788 0.02900 = 0.05522 -0.00298 0.01339 -0.00004 H1N 2 0.660405 0.514812 0.639330 11.00000 -1.20000 H2N 2 0.825170 0.588171 0.355683 11.00000 -1.20000 H3N 2 0.711980 0.362318 0.737738 11.00000 -1.20000 H4N 2 0.723088 0.225759 0.698414 11.00000 -1.20000 H5N 2 0.783632 0.744745 0.259098 11.00000 -1.20000 H6N 2 0.756659 0.873090 0.299417 11.00000 -1.20000 HKLF 4 REM test_APO1_0m_a.res in P2(1)/n REM R1 = 0.0562 for 2066 Fo > 4sig(Fo) and 0.1379 for all 4166 data REM 307 parameters refined using 6 restraints END WGHT 0.0513 0.0679 REM Instructions for potential hydrogen bonds HTAB C9 Cl1_$1 HTAB C14 Cl2_$2 HTAB N5 Cl2 HTAB N2 Cl1 HTAB N4 Cl2 HTAB N4 Cl2_$2 HTAB N1 Cl1 HTAB N1 Cl1_$1 REM Highest difference peak 0.273, deepest hole -0.218, 1-sigma level 0.052 Q1 1 0.6814 0.3267 0.8130 11.00000 0.05 0.27 Q2 1 0.6827 0.8569 0.2979 11.00000 0.05 0.24 Q3 1 0.5756 0.6347 0.3915 11.00000 0.05 0.23 Q4 1 0.6475 0.9430 0.3429 11.00000 0.05 0.22 Q5 1 0.7817 0.5695 0.2877 11.00000 0.05 0.21 Q6 1 0.7872 0.4725 0.8475 11.00000 0.05 0.20 Q7 1 0.5829 0.6727 0.4587 11.00000 0.05 0.19 Q8 1 0.8705 0.4345 0.5509 11.00000 0.05 0.19 Q9 1 0.9717 0.2797 0.6884 11.00000 0.05 0.19 Q10 1 0.6391 0.4861 0.5344 11.00000 0.05 0.19 Q11 1 0.6383 0.3086 0.3406 11.00000 0.05 0.19 Q12 1 0.8438 0.6222 0.2900 11.00000 0.05 0.18 Q13 1 0.6215 0.6761 0.5321 11.00000 0.05 0.18 Q14 1 0.6033 0.4415 0.4711 11.00000 0.05 0.18 Q15 1 0.8624 0.7067 0.5754 11.00000 0.05 0.18 Q16 1 0.7200 0.5477 0.9100 11.00000 0.05 0.17 Q17 1 0.9256 0.4579 0.6151 11.00000 0.05 0.17 Q18 1 0.7014 0.3728 0.7807 11.00000 0.05 0.17 Q19 1 0.8759 0.4180 0.4713 11.00000 0.05 0.17 Q20 1 0.7004 0.3349 0.6392 11.00000 0.05 0.17 ; _shelx_res_checksum 16256 _shelx_hkl_file ; -2 0 0 771.72 45.60 2 0 0 753.82 46.10 3 0 0 2.10 1.80 -3 0 0 0.30 1.30 4 0 0 5617.84 335.17 -4 0 0 5651.83 334.27 -5 0 0 -0.60 1.80 5 0 0 1.60 2.30 6 0 0 46.20 6.20 -6 0 0 57.29 5.40 7 0 0 6.80 3.50 -7 0 0 4.70 2.70 8 0 0 87.09 9.00 -8 0 0 84.19 7.80 -9 0 0 7.00 3.20 9 0 0 7.60 4.30 -10 0 0 119.19 10.60 10 0 0 130.19 12.30 -11 0 0 9.70 4.00 11 0 0 14.30 5.10 12 0 0 20.30 6.00 -12 0 0 28.90 5.70 -13 0 0 20.40 5.90 -14 0 0 16.00 5.40 14 0 0 16.20 7.20 -15 0 0 14.50 5.90 15 0 0 6.20 6.00 16 0 0 11.70 6.50 -16 0 0 22.10 8.80 -16 0 0 11.90 6.00 0 -1 0 0.20 0.20 -2 -1 0 -0.80 0.60 2 -1 0 0.20 1.80 -2 -1 0 0.10 0.30 2 1 0 1.50 1.40 -2 1 0 1.50 1.30 -3 -1 0 17.60 1.40 3 -1 0 16.80 2.90 -3 -1 0 18.80 1.80 3 1 0 20.60 2.80 -3 1 0 19.40 2.60 4 -1 0 4420.66 256.67 -4 -1 0 4307.47 255.27 -4 -1 0 4436.06 254.97 4 1 0 4232.78 256.27 -4 1 0 4122.19 255.77 5 -1 0 161.18 12.70 -5 -1 0 184.08 10.60 -5 -1 0 169.68 11.40 5 1 0 175.68 12.70 -5 1 0 160.78 11.90 6 -1 0 98.49 9.40 -6 -1 0 101.79 7.80 -6 -1 0 120.49 6.80 -6 1 0 91.79 8.60 6 1 0 90.19 9.40 -7 -1 0 7.60 2.50 -7 -1 0 11.00 1.40 7 -1 0 7.00 3.50 7 1 0 8.20 4.10 -7 1 0 4.10 3.10 -8 -1 0 249.58 17.00 8 -1 0 259.17 18.80 -8 -1 0 260.57 15.40 -8 1 0 234.58 17.30 8 1 0 239.58 18.30 -9 -1 0 0.60 2.40 -9 -1 0 0.90 0.90 9 -1 0 2.20 4.00 -9 1 0 3.40 3.30 9 1 0 3.80 3.30 10 -1 0 0.20 3.50 -10 -1 0 2.70 3.00 -10 1 0 -3.50 3.20 10 1 0 -0.10 4.30 -11 -1 0 1.70 3.20 11 -1 0 -2.90 3.70 -11 1 0 5.40 4.00 11 1 0 4.80 3.90 -12 -1 0 -3.80 3.60 12 -1 0 3.60 4.60 12 1 0 -0.70 5.00 -12 1 0 4.40 4.40 -13 -1 0 -0.60 3.50 13 -1 0 -10.10 4.80 13 1 0 0.50 4.30 -13 1 0 4.50 4.70 14 -1 0 2.50 4.70 -14 -1 0 -5.60 3.90 14 1 0 4.30 5.30 -14 1 0 7.90 5.30 -15 -1 0 2.70 4.40 15 -1 0 -1.40 4.90 -15 1 0 4.60 5.40 15 1 0 0.20 4.60 16 -1 0 3.70 5.10 -16 -1 0 3.00 5.80 -16 -1 0 -2.60 4.80 16 1 0 -4.70 5.90 -16 1 0 -5.50 5.70 0 -2 0 41.50 2.60 0 -2 0 36.50 2.50 1 -2 0 5.70 1.50 -1 -2 0 3.90 0.70 1 -2 0 3.80 0.80 -1 -2 0 3.60 1.10 -2 -2 0 10.00 1.20 2 -2 0 11.60 2.30 -2 -2 0 9.70 1.20 2 -2 0 9.50 1.10 -2 2 0 6.60 2.00 -3 -2 0 38.50 2.60 3 -2 0 35.70 4.30 -3 -2 0 39.70 2.90 3 -2 0 38.50 2.80 3 2 0 43.70 3.90 -3 2 0 43.20 4.20 4 -2 0 5.60 2.50 -4 -2 0 7.00 1.40 4 -2 0 6.90 1.00 -4 -2 0 7.40 0.90 4 2 0 7.10 2.30 -4 2 0 5.60 2.60 5 -2 0 0.40 2.40 -5 -2 0 1.50 0.70 -5 -2 0 2.30 1.50 -5 2 0 2.80 2.40 5 2 0 -0.80 2.50 -6 -2 0 3.80 0.90 -6 -2 0 2.20 1.90 6 -2 0 5.30 3.30 6 2 0 1.40 2.50 -6 2 0 0.60 2.50 -7 -2 0 22.90 3.30 -7 -2 0 25.20 2.10 7 -2 0 20.70 4.60 7 2 0 24.60 4.80 -7 2 0 13.20 3.70 -8 -2 0 0.40 0.70 8 -2 0 1.00 3.00 -8 -2 0 -2.30 2.00 8 2 0 0.10 3.40 -8 2 0 3.60 3.40 -9 -2 0 0.20 2.50 -9 -2 0 3.30 1.10 9 -2 0 0.60 3.20 -9 2 0 7.20 3.70 9 2 0 3.40 3.30 10 -2 0 9.80 4.50 -10 -2 0 9.30 3.00 -10 2 0 7.00 4.10 10 2 0 9.80 4.80 -11 -2 0 4.10 3.20 11 -2 0 3.20 4.30 11 2 0 -0.60 4.60 -11 2 0 5.10 3.80 12 -2 0 1.90 5.10 -12 -2 0 2.20 3.30 12 2 0 8.80 4.80 -12 2 0 10.60 5.20 -13 -2 0 -2.20 3.20 13 -2 0 2.30 5.50 -13 2 0 -4.00 4.80 13 2 0 3.60 4.60 -14 -2 0 -4.50 3.50 14 -2 0 -1.50 4.30 -14 2 0 1.50 4.30 14 2 0 6.70 5.90 -15 -2 0 6.30 6.40 15 -2 0 -7.20 3.80 -15 -2 0 -0.80 4.60 15 2 0 -1.30 4.60 -15 2 0 -0.90 6.20 -16 -2 0 -5.10 4.10 16 -2 0 -4.80 4.10 -16 -2 0 2.70 6.80 -16 2 0 -11.70 5.30 16 2 0 -0.10 5.70 0 -3 0 -0.20 0.60 0 -3 0 0.60 0.50 1 -3 0 8.20 1.00 -1 -3 0 8.50 1.10 -1 -3 0 6.90 1.30 1 -3 0 10.60 1.90 -2 -3 0 5.30 1.00 2 -3 0 3.90 2.00 -2 -3 0 8.10 1.90 -2 -3 0 7.70 1.60 2 -3 0 8.10 1.00 -2 3 0 7.80 2.20 3 -3 0 1.30 2.00 3 -3 0 5.20 0.90 -3 -3 0 3.10 1.00 -3 -3 0 4.70 0.90 -3 -3 0 3.00 1.20 -3 3 0 5.20 2.60 4 -3 0 29.00 4.20 -4 -3 0 23.00 2.00 4 -3 0 23.10 2.20 -4 -3 0 20.40 2.30 -4 3 0 26.00 4.20 4 3 0 22.80 3.10 -5 -3 0 65.09 5.10 5 -3 0 80.39 7.40 5 -3 0 63.19 4.70 -5 -3 0 68.89 4.50 -5 3 0 64.39 6.70 5 3 0 68.09 6.40 -6 -3 0 44.40 4.10 -6 -3 0 46.30 3.30 6 -3 0 46.60 3.60 6 -3 0 41.50 6.00 6 3 0 37.50 5.40 -6 3 0 38.10 5.60 7 -3 0 11.30 4.00 7 -3 0 17.30 2.30 -7 -3 0 15.70 2.50 -7 -3 0 12.30 1.60 -7 3 0 20.20 4.40 7 3 0 14.00 3.90 8 -3 0 4.20 3.40 -8 -3 0 3.00 1.00 -8 -3 0 6.40 2.50 -8 3 0 0.90 2.90 8 3 0 4.40 3.00 -9 -3 0 1.30 1.00 -9 -3 0 0.70 2.40 9 -3 0 -1.70 3.20 9 3 0 -4.40 3.10 -9 3 0 3.80 3.90 -10 -3 0 1.80 2.70 10 -3 0 -0.90 3.70 -10 3 0 -2.90 3.90 10 3 0 1.80 3.20 -11 -3 0 4.30 3.30 11 -3 0 0.00 3.90 11 3 0 9.40 5.00 -11 3 0 2.90 4.80 -12 -3 0 15.70 3.80 12 -3 0 21.60 6.20 -12 3 0 7.80 5.70 12 3 0 18.70 5.60 -13 -3 0 4.10 4.00 13 -3 0 -0.20 5.00 -13 3 0 -10.10 4.70 13 3 0 -2.60 3.90 -14 -3 0 -1.50 3.80 14 -3 0 -0.30 5.40 -14 -3 0 -10.00 4.60 -14 3 0 -1.50 4.30 14 3 0 -2.50 5.20 -15 -3 0 16.70 4.80 -15 -3 0 -6.20 6.60 15 -3 0 -4.40 5.10 -15 3 0 -4.90 6.30 0 -4 0 53.59 4.00 0 -4 0 49.40 3.40 0 -4 0 43.40 3.20 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6.00 5.40 -14 -6 0 7.60 6.10 -14 -6 0 2.70 3.40 14 -6 0 -2.50 6.00 -14 6 0 -6.70 5.60 0 -7 0 1.20 1.00 0 -7 0 0.60 1.40 1 -7 0 0.00 0.90 1 -7 0 -0.60 1.80 -1 -7 0 1.00 1.10 -1 -7 0 -0.70 0.80 -2 -7 0 -0.40 1.00 2 -7 0 2.30 2.10 2 -7 0 1.70 1.30 -2 -7 0 1.90 1.20 -3 -7 0 -0.50 2.60 -3 -7 0 0.00 1.10 3 -7 0 3.40 1.40 -3 -7 0 0.10 1.70 3 -7 0 0.50 2.60 -3 -7 0 -0.30 1.60 -3 7 0 -1.10 3.20 4 -7 0 -2.60 2.60 -4 -7 0 2.40 1.10 -4 -7 0 2.30 1.40 -4 -7 0 1.80 1.60 -4 -7 0 1.10 2.30 4 -7 0 1.80 1.20 -4 7 0 4.50 3.50 5 -7 0 5.30 3.30 -5 -7 0 1.90 1.60 5 -7 0 1.80 1.60 -5 -7 0 0.00 1.30 -5 -7 0 2.50 2.50 -5 7 0 -1.40 2.80 -6 -7 0 14.30 4.20 6 -7 0 13.10 2.30 6 -7 0 4.60 4.10 -6 -7 0 10.60 2.00 -6 7 0 11.40 4.80 7 -7 0 4.60 1.80 -7 -7 0 3.50 2.10 -7 -7 0 6.90 3.40 7 -7 0 11.90 5.10 -7 7 0 13.60 5.20 8 -7 0 6.50 4.30 -8 -7 0 9.20 5.00 -8 -7 0 7.30 2.20 -8 7 0 2.40 5.30 9 -7 0 -5.00 3.40 -9 -7 0 -1.50 4.70 -9 -7 0 3.10 2.40 -9 7 0 6.20 5.10 10 -7 0 0.30 5.10 -10 -7 0 -0.10 2.20 -10 -7 0 -6.50 4.70 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3 85.59 7.00 -3 4 -3 89.99 6.90 -3 4 -3 86.69 8.30 4 -4 3 26.90 2.60 4 -4 3 23.10 4.40 -4 -4 -3 19.00 3.20 -4 -4 -3 30.50 4.90 -4 4 -3 18.10 3.40 4 4 3 27.70 3.80 -4 4 -3 13.40 4.20 5 -4 3 216.88 13.80 -5 -4 -3 242.98 16.50 5 -4 3 201.78 16.00 -5 -4 -3 217.28 14.70 -5 4 -3 218.98 15.40 5 4 3 217.08 15.20 -5 4 -3 214.58 16.20 -6 -4 -3 6.30 3.80 -6 -4 -3 10.00 2.90 6 -4 3 13.40 1.90 6 -4 3 12.40 4.50 6 4 3 10.70 3.40 -6 4 -3 13.50 3.90 -6 4 -3 11.80 3.70 7 -4 3 5.50 1.50 -7 -4 -3 2.80 2.70 7 -4 3 3.30 4.10 -7 -4 -3 2.60 3.60 -7 4 -3 9.70 3.90 7 4 3 1.70 3.00 -7 4 -3 6.30 3.50 -8 -4 -3 19.80 6.40 -8 -4 -3 18.90 4.10 8 -4 3 16.00 5.10 -8 4 -3 27.00 5.60 8 4 3 14.20 4.70 -8 4 -3 18.40 5.70 9 -4 3 31.30 6.80 -9 -4 -3 47.60 8.40 -9 -4 -3 37.40 5.50 -9 4 -3 46.10 7.50 -9 4 -3 40.30 7.10 9 4 3 47.10 7.20 -10 -4 -3 11.30 4.40 10 -4 3 15.40 5.50 -10 -4 -3 9.00 6.40 -10 4 -3 9.00 5.00 10 4 3 6.60 4.60 -10 4 -3 12.40 5.10 -11 -4 -3 8.80 6.90 -11 -4 -3 7.80 4.40 11 -4 3 2.80 4.70 -11 4 -3 5.50 5.80 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121.09 10.10 5 -5 -3 129.99 10.30 -5 -5 3 127.59 8.00 -5 5 3 126.99 10.50 -4 -5 3 2.00 0.70 -4 -5 3 -0.20 1.30 4 -5 -3 4.30 1.40 -4 -5 3 0.50 1.50 4 -5 -3 -1.10 2.10 -4 5 3 -0.70 3.00 -3 -5 3 290.97 16.90 3 -5 -3 222.28 16.30 3 -5 -3 277.77 17.50 -3 -5 3 271.67 16.90 -3 -5 3 266.47 16.00 -3 5 3 264.07 18.20 2 -5 -3 1.40 1.10 -2 -5 3 4.00 2.20 -2 -5 3 2.70 0.90 -2 -5 3 1.70 1.60 2 -5 -3 2.00 1.80 -2 5 3 5.70 3.20 1 -5 -3 107.89 7.90 1 -5 -3 108.49 7.40 -1 -5 3 119.79 8.20 -1 -5 3 107.29 7.00 -1 5 3 104.49 9.00 0 -5 3 -0.40 2.10 0 -5 -3 0.80 1.10 0 -5 -3 0.50 1.80 0 -5 3 -1.00 1.00 -1 -5 -3 79.99 5.60 1 -5 3 72.69 6.50 1 -5 3 76.29 5.20 -1 -5 -3 64.59 6.00 -1 5 -3 73.89 4.90 -2 -5 -3 0.60 1.40 2 -5 3 -1.40 2.00 -2 -5 -3 1.40 2.10 2 -5 3 -0.70 1.10 -2 5 -3 -0.80 1.20 -2 5 -3 -0.40 2.30 -3 -5 -3 7.80 1.90 -3 -5 -3 3.50 2.60 3 -5 3 3.30 2.50 3 -5 3 6.40 1.50 -3 5 -3 9.30 3.40 3 5 3 6.50 1.90 -3 5 -3 6.10 1.80 -4 -5 -3 -1.20 2.70 -4 -5 -3 0.90 1.70 4 -5 3 -0.60 3.00 4 -5 3 -0.50 1.00 4 5 3 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4.50 -12 7 3 -0.50 6.50 11 -7 -3 1.90 5.60 -11 -7 3 10.60 2.20 -11 7 3 -0.20 6.00 10 -7 -3 33.90 7.20 -10 -7 3 26.20 3.00 -10 -7 3 31.10 2.90 -10 7 3 21.40 7.60 -9 -7 3 89.79 6.50 -9 -7 3 90.29 6.30 9 -7 -3 122.89 11.40 -9 7 3 92.19 11.00 -8 -7 3 25.20 3.20 8 -7 -3 30.50 6.30 -8 -7 3 26.90 2.50 -8 7 3 22.10 6.30 -7 -7 3 0.30 1.00 -7 -7 3 -5.10 1.70 7 -7 -3 0.40 3.70 -7 7 3 -3.40 4.20 -6 -7 3 2.30 2.00 -6 -7 3 0.40 1.80 6 -7 -3 1.00 2.80 6 -7 -3 -0.50 1.20 -6 -7 3 2.00 1.10 -6 7 3 4.30 3.60 5 -7 -3 36.90 3.60 -5 -7 3 35.90 2.90 -5 -7 3 29.60 4.00 -5 -7 3 36.90 4.10 -5 7 3 37.80 6.30 -4 -7 3 8.10 2.90 -4 -7 3 13.90 2.40 4 -7 -3 15.20 2.30 -4 -7 3 10.80 1.60 4 -7 -3 10.90 3.10 -4 7 3 14.80 3.90 3 -7 -3 42.50 5.00 -3 -7 3 43.80 4.40 -3 -7 3 50.39 4.30 -3 -7 3 41.50 5.30 3 -7 -3 48.90 4.00 -3 -7 3 49.80 3.60 -3 7 3 36.40 5.90 -2 -7 3 92.29 7.30 -2 -7 3 89.49 6.20 -2 -7 3 102.09 8.30 2 -7 -3 89.59 7.20 2 -7 -3 88.69 6.60 -2 7 3 89.09 8.50 -1 -7 3 153.18 10.90 -1 -7 3 196.48 12.50 1 -7 -3 183.88 11.30 1 -7 -3 162.78 11.60 0 -7 -3 126.29 9.00 0 -7 3 118.69 8.20 0 -7 3 123.09 9.80 0 -7 -3 125.69 8.50 1 -7 3 93.19 6.40 -1 -7 -3 88.89 7.10 1 -7 3 92.09 8.20 -1 -7 -3 87.89 6.70 2 -7 3 14.50 2.00 -2 -7 -3 15.60 3.10 2 -7 3 8.90 3.40 -2 -7 -3 11.40 2.30 -3 -7 -3 1.20 2.40 3 -7 3 2.70 3.30 3 -7 3 3.00 1.60 -3 -7 -3 3.40 1.80 -4 -7 -3 2.80 2.00 4 -7 3 3.60 1.50 -4 -7 -3 4.10 3.10 4 -7 3 7.20 3.80 -5 -7 -3 46.40 6.50 -5 -7 -3 36.40 4.50 5 -7 3 42.50 4.00 5 -7 3 51.99 7.60 -6 -7 -3 88.89 7.30 -6 -7 -3 85.99 9.60 6 -7 3 77.09 9.90 6 -7 3 84.39 6.50 -7 -7 -3 83.69 9.90 7 -7 3 63.99 6.50 7 -7 3 66.99 9.70 -7 -7 -3 73.39 7.10 -8 -7 -3 21.40 4.20 8 -7 3 28.30 7.10 -8 -7 -3 32.10 7.20 -9 -7 -3 -3.00 2.70 -9 -7 -3 -0.70 4.70 9 -7 3 0.10 4.50 10 -7 3 9.60 5.70 -10 -7 -3 15.30 3.90 -10 -7 -3 8.90 5.80 -11 -7 -3 -4.10 6.20 -11 -7 -3 2.50 3.40 11 -7 3 -0.90 5.80 -12 -7 -3 3.20 4.00 12 -7 3 -1.30 5.00 -12 -7 -3 0.10 6.80 -13 -8 3 -2.20 5.70 -13 -8 3 -0.30 2.30 13 -8 -3 -0.30 5.00 -12 -8 3 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4 6.50 4.80 -8 -3 -4 2.30 3.30 -8 -3 -4 0.60 4.30 -8 3 -4 8.10 4.80 8 3 4 -0.10 3.70 -8 3 -4 6.50 4.00 -9 -3 -4 3.40 3.60 -9 -3 -4 -2.00 4.60 9 -3 4 0.50 4.00 9 3 4 -4.60 3.80 -9 3 -4 1.00 4.80 -9 3 -4 1.00 4.80 -10 -3 -4 9.90 4.40 -10 -3 -4 6.10 6.70 10 -3 4 3.60 4.40 10 3 4 -2.20 3.70 -10 3 -4 -6.60 3.80 -10 3 -4 -0.30 5.30 11 -3 4 2.40 4.60 -11 -3 -4 -2.20 3.90 -11 -3 -4 17.50 7.20 -11 3 -4 3.30 5.90 -11 3 -4 -0.80 5.80 11 3 4 5.70 4.90 -12 -3 -4 3.40 5.20 -12 -3 -4 4.90 6.70 12 -3 4 -8.20 3.50 -12 3 -4 2.60 6.30 12 3 4 10.60 5.50 -12 3 -4 2.80 5.10 -13 -3 -4 -1.70 4.70 -13 -3 -4 -3.50 6.10 13 -3 4 2.60 4.70 13 3 4 -3.40 5.30 -13 3 -4 -0.20 6.20 -13 3 -4 2.60 6.40 -14 -3 -4 2.20 4.90 14 -3 4 -0.40 5.80 -14 -3 -4 8.70 8.00 -14 3 -4 3.90 6.80 14 3 4 5.00 4.90 -14 3 -4 -3.30 5.40 -16 -4 4 16.80 4.00 -16 4 4 12.70 7.30 -15 -4 4 1.40 3.40 -15 4 4 9.20 6.80 -14 -4 4 5.00 2.80 -14 4 4 3.60 5.60 -13 -4 4 5.40 2.80 -13 4 4 7.40 4.90 -12 -4 4 2.20 2.10 -12 4 4 13.10 5.20 -11 -4 4 83.09 5.20 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142.19 9.70 -1 4 -4 146.79 9.70 -2 -4 -4 22.50 2.80 -2 -4 -4 21.80 3.60 2 -4 4 22.70 4.40 2 -4 4 22.40 2.30 -2 4 -4 22.30 2.90 2 4 4 25.90 3.20 -2 4 -4 24.90 4.10 -3 -4 -4 151.08 10.70 3 -4 4 136.49 9.00 3 -4 4 133.99 11.20 -3 -4 -4 145.29 9.70 -3 4 -4 137.39 9.70 3 4 4 125.09 9.80 -3 4 -4 129.19 10.50 4 -4 4 3.30 1.40 4 -4 4 0.90 2.80 -4 -4 -4 3.90 3.20 -4 -4 -4 6.70 2.10 -4 4 -4 4.40 2.90 -4 4 -4 0.30 2.10 4 4 4 2.50 2.30 5 -4 4 4.70 1.30 -5 -4 -4 4.90 2.60 -5 -4 -4 6.50 3.40 5 -4 4 3.60 3.00 -5 4 -4 8.00 4.00 5 4 4 5.60 3.30 -5 4 -4 6.40 3.00 6 -4 4 6.90 3.50 -6 -4 -4 11.70 4.00 -6 -4 -4 11.60 3.30 6 -4 4 8.80 1.70 -6 4 -4 9.10 3.60 -6 4 -4 11.70 4.60 6 4 4 10.70 3.40 -7 -4 -4 14.10 4.80 -7 -4 -4 8.80 3.50 7 -4 4 9.20 2.10 7 -4 4 11.60 4.60 7 4 4 10.90 4.10 -7 4 -4 16.80 4.20 -7 4 -4 12.70 4.80 -8 -4 -4 14.20 4.20 -8 -4 -4 11.70 5.40 8 -4 4 14.30 5.40 8 4 4 14.60 4.60 -8 4 -4 16.60 5.20 -8 4 -4 25.40 5.80 9 -4 4 5.90 4.30 -9 -4 -4 7.90 4.00 -9 -4 -4 5.70 5.00 9 4 4 9.20 4.70 -9 4 -4 17.40 6.30 -9 4 -4 6.60 5.10 -10 -4 -4 -1.10 5.80 10 -4 4 2.20 4.70 -10 -4 -4 2.60 3.80 -10 4 -4 -1.60 3.80 10 4 4 8.20 5.20 -10 4 -4 7.40 4.90 -11 -4 -4 21.10 5.10 11 -4 4 13.70 5.70 -11 -4 -4 16.90 8.30 11 4 4 25.90 7.00 -11 4 -4 38.90 8.50 -11 4 -4 22.40 6.30 12 -4 4 -1.90 4.40 -12 -4 -4 5.00 7.40 -12 -4 -4 -0.60 4.30 -12 4 -4 6.20 6.90 -12 4 -4 9.50 6.20 12 4 4 -2.50 4.80 -13 -4 -4 10.00 5.00 -13 -4 -4 16.90 9.00 13 -4 4 15.80 7.20 -13 4 -4 8.20 7.50 13 4 4 9.90 6.10 -13 4 -4 17.40 6.50 14 -4 4 5.40 5.00 -14 -4 -4 -2.00 4.70 -14 -4 -4 0.70 5.90 -14 4 -4 -3.10 4.90 -14 4 -4 0.90 5.80 14 4 4 3.80 4.70 -15 -5 4 2.80 3.00 -15 5 4 4.10 7.10 -14 -5 4 3.60 2.50 -14 5 4 2.20 6.00 -13 -5 4 2.40 2.20 -13 5 4 7.40 6.10 -12 -5 4 3.30 2.00 -12 5 4 -4.20 5.20 -11 -5 4 -1.10 0.60 -11 -5 4 -0.90 1.50 -11 5 4 5.10 5.20 -10 5 4 5.10 5.00 -9 5 4 5.00 3.70 -8 5 4 1.40 3.30 7 -5 -4 6.50 1.60 -7 5 4 -1.40 2.90 6 -5 -4 6.60 3.00 6 -5 -4 3.80 1.40 -6 5 4 10.00 4.00 -5 -5 4 55.19 3.80 5 -5 -4 54.49 6.20 -5 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12 -5 4 -5.70 4.50 -12 -5 -4 -7.40 4.00 -12 -5 -4 -6.60 6.10 -12 5 -4 -3.00 5.20 12 5 4 -0.20 5.00 -12 5 -4 7.30 6.50 -13 -5 -4 1.20 4.40 -13 -5 -4 9.00 7.40 13 -5 4 -6.50 3.60 -13 5 -4 -2.40 5.80 13 5 4 -5.00 4.50 -13 5 -4 -8.90 5.10 -15 -6 4 1.10 2.80 -15 6 4 -6.70 6.60 -14 -6 4 2.10 2.60 -14 6 4 -0.40 6.30 -13 -6 4 17.10 3.00 -13 6 4 22.40 6.70 -12 -6 4 2.60 1.90 -12 6 4 0.50 5.90 -11 -6 4 0.60 0.70 -11 -6 4 1.00 1.40 -11 6 4 -1.90 3.80 -10 6 4 4.60 5.20 -9 6 4 59.29 8.20 -8 6 4 -2.30 4.10 -7 6 4 25.20 5.20 6 -6 -4 6.10 3.30 6 -6 -4 7.70 2.00 -6 -6 4 10.60 1.80 -6 -6 4 10.70 1.10 -6 6 4 15.50 4.70 -5 -6 4 95.59 7.10 -5 -6 4 93.89 6.10 5 -6 -4 101.19 6.90 -5 -6 4 105.69 7.70 5 -6 -4 90.09 8.50 -5 6 4 93.39 9.70 -4 -6 4 64.89 4.20 -4 -6 4 53.99 5.50 4 -6 -4 62.99 6.20 4 -6 -4 56.69 4.70 -4 -6 4 60.49 5.40 -4 6 4 72.29 7.70 -3 -6 4 262.87 16.60 3 -6 -4 277.07 17.10 -3 -6 4 257.47 17.90 3 -6 -4 280.77 18.30 -3 -6 4 295.67 17.90 -3 6 4 261.87 19.00 2 -6 -4 17.60 3.20 -2 -6 4 18.10 3.70 2 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-6 4 0.10 4.50 -7 -6 -4 -2.70 3.30 -7 -6 -4 3.00 2.90 -7 6 -4 5.30 3.40 -7 6 -4 -0.40 4.10 8 -6 4 6.60 4.50 -8 -6 -4 15.10 3.90 -8 -6 -4 16.50 5.70 -8 6 -4 20.60 5.00 -8 6 -4 17.40 6.60 -9 -6 -4 13.00 6.10 -9 -6 -4 -1.70 3.30 9 -6 4 10.40 5.30 -9 6 -4 5.10 4.50 -10 -6 -4 25.10 7.50 -10 -6 -4 21.70 4.90 10 -6 4 9.50 5.70 -10 6 -4 24.40 6.40 11 -6 4 6.30 5.30 -11 -6 -4 9.90 6.00 -11 -6 -4 7.40 4.60 -11 6 -4 7.90 4.80 12 -6 4 -0.60 5.70 -12 -6 -4 2.60 4.10 -12 -6 -4 0.60 6.30 -12 6 -4 0.40 6.20 13 -6 4 7.50 6.10 -13 -6 -4 9.10 5.40 -13 -6 -4 11.20 7.00 -13 6 -4 4.90 6.40 -14 -7 4 -0.30 2.50 -14 7 4 9.80 7.70 -13 -7 4 15.20 2.70 -13 7 4 17.10 6.60 -12 -7 4 1.90 1.80 -12 7 4 5.00 6.50 -11 -7 4 0.80 1.00 -11 -7 4 2.50 1.60 -11 7 4 -4.10 4.40 -10 -7 4 0.00 1.30 -10 -7 4 2.40 1.00 -10 7 4 2.40 4.60 -9 -7 4 -2.00 1.00 -9 -7 4 -0.90 1.40 -9 7 4 5.00 5.70 -8 -7 4 6.90 1.30 -8 -7 4 14.50 2.10 -8 7 4 8.30 5.40 -7 -7 4 36.50 4.70 -7 -7 4 36.10 3.60 -7 -7 4 32.20 2.70 -7 7 4 48.30 7.50 6 -7 -4 12.60 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6.90 -14 -5 5 3.60 2.50 -14 5 5 3.90 5.30 -13 -5 5 7.40 2.20 -13 5 5 8.10 5.20 -12 -5 5 2.10 1.70 -12 -5 5 0.80 0.60 -12 5 5 2.80 4.40 -11 5 5 10.30 4.80 -10 5 5 4.00 4.70 -9 5 5 38.30 6.80 -8 5 5 -3.60 3.40 7 -5 -5 98.49 9.70 -7 5 5 104.29 10.00 6 -5 -5 4.20 1.50 6 -5 -5 1.60 2.90 -6 5 5 8.00 3.80 5 -5 -5 51.59 6.20 -5 -5 5 49.80 3.10 5 -5 -5 50.49 4.00 -5 -5 5 40.00 3.60 -5 -5 5 47.80 5.10 -5 5 5 59.59 6.60 4 -5 -5 -0.40 2.40 4 -5 -5 -0.30 1.20 -4 -5 5 -0.60 1.70 -4 -5 5 0.30 0.60 -4 -5 5 0.60 1.50 -4 5 5 -1.90 2.30 -4 5 5 0.00 2.60 -3 -5 5 9.20 2.40 -3 -5 5 7.60 1.10 -3 -5 5 5.20 2.00 3 -5 -5 6.70 1.50 3 -5 -5 15.90 3.20 -3 5 5 5.30 3.00 -3 5 5 6.30 2.30 3 5 -5 9.50 2.40 2 -5 -5 -0.20 1.10 2 -5 -5 2.60 2.20 -2 -5 5 -0.90 0.80 -2 -5 5 0.00 1.70 -2 -5 5 0.50 2.10 -2 5 5 -1.00 1.10 -2 5 5 -3.20 2.00 2 5 -5 1.10 1.60 1 -5 -5 119.49 8.90 1 -5 -5 119.99 8.10 -1 -5 5 117.49 7.60 -1 -5 5 112.79 9.00 -1 5 5 122.79 7.80 1 5 -5 113.59 8.20 -1 5 5 111.19 8.80 0 -5 -5 -1.10 1.10 0 -5 5 2.40 2.30 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10.70 3.90 1 1 10 7.60 1.80 -1 1 -10 6.70 2.80 -1 1 -10 6.80 3.60 -2 -1 -10 20.20 3.80 2 -1 10 20.40 4.80 -2 -1 -10 25.50 5.20 2 -1 10 21.20 2.80 -2 1 -10 15.70 4.40 2 1 10 15.10 4.40 2 1 10 9.40 2.50 -2 1 -10 10.70 3.70 3 -1 10 2.10 4.40 3 -1 10 3.80 1.80 -3 -1 -10 6.70 3.20 -3 -1 -10 5.40 4.30 -3 1 -10 2.60 3.40 3 1 10 1.00 1.60 -3 1 -10 6.30 3.70 3 1 10 1.30 3.40 -4 -1 -10 182.48 13.60 4 -1 10 166.68 11.00 -4 -1 -10 169.08 13.70 4 -1 10 142.09 13.80 4 1 10 116.99 13.00 -4 1 -10 157.18 13.30 -4 1 -10 169.18 13.40 -5 -1 -10 -1.70 4.30 5 -1 10 -1.00 3.60 -5 -1 -10 -4.60 3.50 5 1 10 1.50 4.50 -5 1 -10 0.30 4.30 -5 1 -10 0.80 3.60 -6 -1 -10 27.60 6.30 6 -1 10 22.60 6.40 -6 -1 -10 24.40 5.60 -6 1 -10 22.90 6.20 6 1 10 15.60 6.60 -6 1 -10 22.50 6.00 -7 -1 -10 0.20 4.40 -7 -1 -10 10.90 4.90 7 -1 10 1.30 5.10 -7 1 -10 2.70 4.40 -7 1 -10 -7.60 4.00 7 1 10 2.50 4.00 8 -1 10 9.30 6.50 -8 -1 -10 7.80 6.60 -8 -1 -10 15.90 6.40 -8 1 -10 15.10 5.80 8 1 10 19.00 6.80 -8 1 -10 22.00 7.10 -9 -1 -10 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10 67.99 6.50 6 2 -10 98.59 10.00 -5 -2 10 27.60 2.80 5 -2 -10 21.10 4.90 -5 -2 10 32.70 4.80 -5 2 10 24.50 3.40 5 2 -10 28.40 5.20 -5 2 10 30.30 4.50 4 -2 -10 12.90 3.90 -4 -2 10 6.00 2.90 -4 -2 10 12.70 1.90 -4 2 10 10.00 2.50 -4 2 10 11.40 3.10 4 2 -10 7.80 3.90 -3 -2 10 0.70 1.20 -3 -2 10 -1.50 2.30 3 -2 -10 -3.20 2.30 -3 2 10 0.80 1.60 -3 2 10 -0.60 1.90 3 2 -10 3.80 3.30 2 -2 -10 2.10 1.40 2 -2 -10 2.70 3.40 -2 -2 10 1.10 1.40 -2 -2 10 -1.30 2.10 -2 2 10 1.90 1.90 -2 2 10 0.40 1.90 2 2 -10 -1.70 2.30 1 -2 -10 2.10 2.00 -1 -2 10 2.10 2.60 1 -2 -10 2.30 3.40 -1 -2 10 0.80 1.40 -1 2 10 6.10 2.10 1 2 -10 5.70 2.90 -1 2 10 2.20 2.80 0 -2 -10 40.90 5.80 0 -2 10 33.20 5.90 0 -2 -10 46.70 4.80 0 -2 10 37.10 3.80 0 2 10 41.70 4.30 0 2 -10 48.90 6.00 0 2 10 47.90 5.80 -1 -2 -10 69.89 6.10 -1 -2 -10 64.69 7.60 1 -2 10 49.80 4.70 1 -2 10 58.49 7.70 -1 2 -10 61.99 6.70 1 2 10 56.39 6.80 1 2 10 46.20 5.00 -2 -2 -10 103.59 9.00 2 -2 10 96.39 11.00 2 -2 10 98.09 7.50 -2 -2 -10 125.89 10.40 2 2 10 107.59 8.20 -2 2 -10 117.29 10.00 2 2 10 103.29 9.90 -3 -2 -10 15.20 4.70 3 -2 10 15.20 2.60 -3 -2 -10 18.80 3.90 3 -2 10 10.40 4.70 3 2 10 12.80 4.70 -3 2 -10 12.30 3.90 4 -2 10 18.90 2.90 4 -2 10 15.70 5.40 -4 -2 -10 26.30 6.30 -4 -2 -10 20.70 5.10 4 2 10 23.70 6.00 -4 2 -10 17.40 4.70 -5 -2 -10 12.30 5.70 5 -2 10 3.50 4.10 -5 -2 -10 1.80 4.40 -5 2 -10 7.80 4.70 5 2 10 10.50 4.60 -6 -2 -10 33.10 7.20 -6 -2 -10 32.50 6.40 6 -2 10 33.40 7.40 6 2 10 29.20 6.40 -6 2 -10 26.60 6.20 -7 -2 -10 -5.80 4.20 -7 -2 -10 -7.20 4.60 7 -2 10 11.20 4.90 -7 2 -10 1.20 5.10 7 2 10 -0.40 3.90 -8 -2 -10 27.50 6.70 8 -2 10 31.10 7.60 -8 -2 -10 47.10 8.70 8 2 10 36.30 7.60 -8 2 -10 40.10 8.10 -9 -2 -10 -3.30 5.50 -9 -2 -10 3.00 5.40 9 -2 10 -1.80 4.50 -9 2 -10 -8.20 5.30 9 2 10 3.50 5.60 10 -2 10 2.90 5.10 -10 -2 -10 -1.20 5.30 -10 -2 -10 2.20 5.10 10 2 10 0.30 4.30 -10 2 -10 -3.00 4.80 11 -2 10 1.80 6.00 -11 -2 -10 -6.60 4.80 -11 -2 -10 8.70 7.10 11 2 10 -2.40 5.60 -11 2 -10 -1.70 6.70 -15 -3 10 -1.80 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6.30 7 -4 -10 54.29 8.00 -7 -4 10 56.49 4.10 7 4 -10 57.29 8.30 -7 4 10 55.39 6.30 -6 -4 10 4.70 3.50 6 -4 -10 -3.20 3.70 -6 -4 10 0.90 1.10 -6 4 10 -0.70 2.30 6 4 -10 -1.10 3.00 -6 4 10 1.70 2.70 -5 -4 10 8.50 3.30 -5 -4 10 8.60 1.50 5 -4 -10 9.80 4.40 -5 4 10 5.50 2.50 5 4 -10 9.30 3.70 -5 4 10 3.30 2.80 -4 -4 10 5.00 3.10 -4 -4 10 0.80 1.30 4 -4 -10 4.20 3.90 4 4 -10 -6.10 2.90 -4 4 10 -0.80 2.00 -4 4 10 0.70 2.60 -3 -4 10 7.30 3.30 3 -4 -10 10.90 4.50 3 -4 -10 9.00 2.50 -3 -4 10 12.50 1.90 -3 4 10 13.70 3.30 3 4 -10 12.80 4.20 -3 4 10 12.50 3.20 2 -4 -10 0.30 3.60 -2 -4 10 0.40 1.00 2 -4 -10 1.60 1.90 -2 -4 10 -0.80 3.30 -2 4 10 2.70 2.50 -2 4 10 2.20 2.00 2 4 -10 5.00 3.20 1 -4 -10 21.70 4.70 -1 -4 10 21.90 2.70 -1 -4 10 18.80 4.60 1 -4 -10 30.30 3.70 -1 4 10 28.80 4.10 -1 4 10 23.30 4.10 1 4 -10 26.00 4.30 0 -4 10 0.60 3.00 0 -4 10 0.40 1.50 0 -4 -10 2.40 3.50 0 -4 -10 4.90 2.10 0 4 10 -3.10 1.70 0 4 -10 2.80 2.90 0 4 10 3.20 2.80 1 -4 10 75.89 9.60 1 -4 10 79.59 6.50 -1 -4 -10 97.89 9.60 -1 -4 -10 100.29 7.70 -1 4 -10 78.09 8.10 1 4 10 87.49 8.50 -2 -4 -10 10.90 3.60 2 -4 10 8.60 2.20 -2 -4 -10 3.30 3.60 2 -4 10 4.10 3.70 2 4 10 9.00 4.00 -2 4 -10 6.40 3.30 -3 -4 -10 148.09 11.20 -3 -4 -10 134.69 11.70 3 -4 10 121.69 8.70 3 -4 10 103.69 12.40 3 4 10 99.69 11.00 -3 4 -10 126.49 10.90 -4 -4 -10 -0.20 4.60 -4 -4 -10 10.00 3.70 4 -4 10 -4.10 4.80 4 -4 10 4.70 1.90 4 4 10 4.90 4.40 -4 4 -10 12.50 4.10 -5 -4 -10 31.70 5.50 -5 -4 -10 20.80 6.60 5 -4 10 21.50 6.30 -5 4 -10 21.70 5.60 5 4 10 26.50 6.10 6 -4 10 -0.60 5.30 -6 -4 -10 9.80 4.90 -6 -4 -10 2.20 4.90 -6 4 -10 -2.80 4.10 6 4 10 2.90 3.60 -7 -4 -10 12.10 5.20 -7 -4 -10 18.90 6.10 7 -4 10 11.60 5.80 -7 4 -10 17.20 5.20 7 4 10 14.60 5.70 -8 -4 -10 8.20 5.90 8 -4 10 1.20 5.70 -8 -4 -10 2.20 6.50 8 4 10 -1.80 4.10 -8 4 -10 4.90 4.60 -9 -4 -10 19.30 6.90 9 -4 10 10.70 6.20 -9 -4 -10 3.40 6.00 -9 4 -10 16.80 6.80 9 4 10 11.90 5.90 -10 -4 -10 2.20 6.20 10 -4 10 3.80 5.50 -10 -4 -10 0.90 6.30 10 4 10 1.60 4.80 -10 4 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7.70 -3 5 10 52.09 6.20 -3 5 10 57.29 5.60 3 5 -10 70.59 7.70 2 -5 -10 0.50 2.00 -2 -5 10 2.70 1.50 -2 -5 10 -1.40 2.90 2 -5 -10 -5.90 3.40 -2 5 10 1.80 2.70 2 5 -10 -1.40 2.80 -2 5 10 1.50 2.30 -1 -5 10 15.40 5.00 1 -5 -10 17.80 3.00 -1 -5 10 14.50 2.40 1 -5 -10 16.90 4.70 -1 5 10 21.20 3.80 1 5 -10 18.20 4.10 0 -5 -10 -0.60 2.90 0 -5 10 -1.10 1.20 0 -5 -10 -2.70 1.60 0 -5 10 1.90 3.30 0 5 -10 1.30 2.80 0 5 10 0.20 2.50 1 -5 10 1.40 4.10 1 -5 10 4.30 1.90 -1 -5 -10 1.50 3.30 -1 -5 -10 3.90 2.80 -1 5 -10 0.50 2.70 1 5 10 6.80 3.30 2 -5 10 -1.50 4.70 -2 -5 -10 -2.70 3.90 -2 -5 -10 -0.80 2.40 2 -5 10 -0.40 1.80 -2 5 -10 -6.00 2.40 2 5 10 2.70 3.30 3 -5 10 3.50 4.40 3 -5 10 9.70 2.30 -3 -5 -10 20.40 5.70 -3 -5 -10 5.90 3.30 3 5 10 9.10 4.20 -3 5 -10 14.30 4.10 -4 -5 -10 1.50 3.70 -4 -5 -10 -5.90 3.30 4 -5 10 -0.50 2.00 4 -5 10 3.30 4.20 4 5 10 0.40 3.60 -4 5 -10 -0.50 2.50 5 -5 10 9.10 2.90 -5 -5 -10 15.00 5.40 5 -5 10 13.80 5.70 -5 -5 -10 14.30 4.80 -5 5 -10 20.90 4.40 5 5 10 15.40 5.10 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2.20 5.90 6 -5 11 1.00 4.60 -6 5 -11 0.00 3.20 7 -5 11 3.20 4.70 -7 -5 -11 10.90 6.80 -7 -5 -11 9.00 5.50 -7 5 -11 9.80 5.30 -8 -5 -11 4.80 5.50 8 -5 11 -7.20 5.50 -8 -5 -11 -7.00 4.70 -8 5 -11 6.60 5.20 -13 -6 11 0.50 1.40 -13 -6 11 -1.70 4.30 -13 6 11 9.20 7.10 12 -6 -11 12.20 6.00 -12 -6 11 1.90 1.30 -12 -6 11 1.50 4.30 -12 6 11 0.00 6.00 11 -6 -11 -4.10 4.10 -11 -6 11 -0.20 1.20 -11 -6 11 5.50 3.70 -11 6 11 7.30 6.30 -10 -6 11 -0.80 1.10 -10 -6 11 7.00 4.50 10 -6 -11 -0.20 5.00 -10 6 11 -12.30 5.00 -10 6 11 3.80 4.50 -9 -6 11 3.60 1.30 -9 -6 11 -2.00 3.10 9 -6 -11 2.40 4.80 -9 6 11 6.50 5.70 -9 6 11 3.00 4.40 -8 -6 11 -0.20 1.40 8 -6 -11 0.00 3.70 -8 -6 11 2.00 3.50 -8 6 11 4.90 3.50 -7 -6 11 13.40 4.40 -7 -6 11 15.80 2.20 7 -6 -11 21.50 6.20 -7 6 11 18.10 4.10 -7 6 11 19.00 4.80 7 6 -11 21.90 5.80 6 -6 -11 4.80 4.40 -6 -6 11 10.10 4.00 -6 -6 11 1.90 1.40 -6 6 11 6.30 3.40 -6 6 11 5.80 2.90 6 6 -11 1.00 4.40 -5 -6 11 22.50 5.50 -5 -6 11 19.40 2.60 5 -6 -11 24.00 5.50 -5 6 11 19.20 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11 2.90 2.60 -2 -10 -11 3.70 3.00 2 -10 11 5.00 6.50 -15 0 12 -5.00 2.50 -14 0 12 0.80 2.60 -13 0 12 2.10 2.40 -12 0 12 3.30 2.80 12 0 -12 18.10 8.20 -11 0 12 0.50 2.20 11 0 -12 -2.40 5.60 -10 0 12 2.90 2.50 10 0 -12 2.60 4.70 -9 0 12 0.90 2.00 9 0 -12 0.30 5.50 -9 0 12 0.50 2.80 -8 0 12 214.88 15.50 -8 0 12 185.08 13.40 8 0 -12 206.38 17.80 7 0 -12 -8.00 4.30 -7 0 12 2.70 2.00 -7 0 12 1.00 3.50 -6 0 12 254.07 17.20 6 0 -12 259.07 20.50 -6 0 12 286.27 19.10 -5 0 12 -1.00 3.10 5 0 -12 2.10 4.80 -5 0 12 0.90 2.10 4 0 -12 227.38 17.00 -4 0 12 196.28 14.00 -4 0 12 216.08 15.90 3 0 -12 4.20 4.20 -3 0 12 8.20 2.30 -3 0 12 3.70 3.30 -2 0 12 77.99 6.40 2 0 -12 76.19 8.80 -2 0 12 70.19 8.20 -1 0 12 0.50 2.20 -1 0 12 0.30 3.10 1 0 -12 1.30 3.30 0 0 -12 94.59 9.30 0 0 12 82.99 7.10 0 0 12 79.59 9.20 -1 0 -12 -2.00 4.10 1 0 12 4.30 4.50 1 0 12 -2.50 1.60 2 0 12 63.39 5.30 -2 0 -12 50.39 7.70 2 0 12 35.80 7.10 3 0 12 -6.30 3.40 -3 0 -12 -1.00 3.60 -4 0 -12 52.79 8.20 4 0 12 46.10 8.20 -5 0 -12 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