#============================================================================== data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 10 _journal_issue 3 _journal_year 2019 _journal_page_first 201 _journal_page_last 208 #=============================================================================== data_shelx _publ_section_keywords ; crystal structure, cupper, Schiff base ; #Added by publCIF _publ_section_related_literature ; ; _publ_contact_author_name ; 'Mohamed Gaye' ; _publ_contact_author_address ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar S\'en\'egal ; _publ_contact_author_phone '00221338247804' _publ_contact_author_fax '00221338246318' _publ_contact_author_email 'mlgayeastou@yahoo.fr' _publ_requested_journal 'Acta Cryst. E' _publ_contact_letter ; ; _publ_requested_category EO _publ_section_title ; Title (type here to add) ; loop_ _publ_author_name _publ_author_address _publ_author_footnote _publ_author_email 'Pokpa, Haba' ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar, S\'en\'egal ; . . 'Adama, Sy' ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar, S\'en\'egal ; . . 'Farba Bouyagui, Tamboura' ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar, S\'en\'egal ; . . 'Mamour, Sarr' ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar, S\'en\'egal ; . . 'Ibrahima Elhadji, Thiam' ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar, S\'en\'egal ; . . 'Mohamed, Gaye' ; D\'epartement de Chimie Facult\'e des Sciences et Techniques Universit\'e Cheikh Anta Diop Dakar, S\'en\'egal ; . ; mlgayeastou@yahoo.fr ; 'Aliou Hamady, Barry' ; D\'epartement de Chimie Facult\'e des Sciences Universit\'e de Nouakchott Nouakchott, Mauritanie ; . . 'Pascal, Retailleau' ; Institut de Chimie des Substances Naturelles, CNRS UPR 2301, Universit\'e Paris-Sud, Universit\'e Paris-Saclay., 1, av. de la Terrasse, 91198 Gif-sur-Yvette, France ; . . _publ_section_abstract ; (type here to add) ; _publ_section_references ; Bruker (2016). APEX3, SADABS and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA. Farrugia, J. L. (2012). J. Appl. Cryst. 45, 849-854. Sheldrick, G. M. (2015a). Acta Cryst. A71, 3-8. Sheldrick, G. M. (2015b). Acta Cryst. C71, 3-8. ; _publ_section_figure_captions ; Fig. 1. An ORTEP view of the title compound, showing the atom-numbering scheme and intramolecular H bonds contacts. Displacement ellipsoids are plotted at the 50% probability level. Fig. 2.Molecular representation of the title compound, showing the intermolecular H bonds contacts. ; _publ_section_acknowledgements ; The authors are grateful to the Sonatel Foundation for financial support. ; _audit_update_record ; 2018-02-07 # Formatted by publCIF ; _publcif_datablock.id '{289c58f7-101e-443d-b2ff-5cad87d27cb5}' # publcif _publ_body_element loop start loop_ _publ_body_element _publ_body_title _publ_body_contents section ; Chemical context ; ; ; section ; Structural commentary ; ; Figure 1 shows the structure of the complex. The asymmetric unit contains a ...... ; section ; Supramolecular features ; ; In the crystal,....... ; section ; Database survey ; ; ; section ; Synthesis and crystallization ; ; A mixture of ...... ; section ; Refinement ; ; Crystal data, data collection and structure refinement details are summarized in Table 1. H atoms of =CH, CH~2~ and CH~3~ groups were geometrically optimized and refined as riding model by AFIX instructions with U~iso~(H) = 1.2U~eq~(C)(1.5 for CH~3~, NH and OH~2~ groups). H atoms of NH and OH~2~ groups were generated from difference fourier map and refined using DFIX instructions. ; # publcif _publ_body_element loop end _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C9 H16 Cl2 Cu N4, H2 O' _chemical_formula_sum 'C9 H18 Cl2 Cu N4 O' _chemical_formula_weight 332.71 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 7.4355(3) _cell_length_b 7.2952(3) _cell_length_c 26.2729(11) _cell_angle_alpha 90 _cell_angle_beta 93.461(4) _cell_angle_gamma 90 _cell_volume 1422.52(10) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 5120 _cell_measurement_theta_min 2.4120 _cell_measurement_theta_max 28.6423 _exptl_crystal_description prismatic _exptl_crystal_colour dark _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.554 _exptl_crystal_F_000 684 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.08 _exptl_crystal_size_mid 0.07 _exptl_crystal_size_min 0.06 _exptl_absorpt_coefficient_mu 1.901 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type none _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_measurement_device_type 'KappaCCD' _diffrn_measurement_method 'CCD' _diffrn_detector_area_resol_mean 9 _diffrn_reflns_number 9763 _diffrn_reflns_av_unetI/netI 0.0407 _diffrn_reflns_av_R_equivalents 0.0353 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_theta_min 3.638 _diffrn_reflns_theta_max 28.902 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.884 _diffrn_measured_fraction_theta_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.884 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.884 _diffrn_reflns_point_group_measured_fraction_full 0.990 _reflns_number_total 3299 _reflns_number_gt 2684 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX3 (Bruker, 2016)' _computing_cell_refinement 'SAINT (Bruker, 2016)' _computing_data_reduction 'SAINT (Bruker, 2016)' _computing_structure_solution 'SHELXT (Sheldrick, 2015a)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015b)' _computing_molecular_graphics 'ORTEP3 for Windows (Farrugia, 2012)' _computing_publication_material 'SHELXL-2014/7 (Sheldrick, 2015b)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0353P)^2^+0.3118P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick, 2015b)' _refine_ls_extinction_coef 0.0051(9) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 3299 _refine_ls_number_parameters 167 _refine_ls_number_restraints 5 _refine_ls_R_factor_all 0.0435 _refine_ls_R_factor_gt 0.0328 _refine_ls_wR_factor_ref 0.0815 _refine_ls_wR_factor_gt 0.0773 _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_restrained_S_all 1.063 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.70301(3) 0.21199(3) 0.38618(2) 0.03063(11) Uani 1 1 d . . . . . Cl1 Cl 0.98587(8) 0.12838(9) 0.41049(2) 0.05081(18) Uani 1 1 d D . . . . Cl2 Cl 0.55783(9) -0.10012(7) 0.35567(2) 0.04625(17) Uani 1 1 d . . . . . O1W O 1.1467(4) -0.2456(4) 0.35967(15) 0.1071(10) Uani 1 1 d D . . . . H1WA H 1.085(6) -0.151(5) 0.3629(19) 0.161 Uiso 1 1 d D U . . . H1WB H 1.238(4) -0.181(7) 0.352(2) 0.161 Uiso 1 1 d D U . . . N1 N 0.6135(2) 0.2224(2) 0.45670(7) 0.0313(4) Uani 1 1 d . . . . . N2 N 0.5179(3) 0.2079(3) 0.53336(7) 0.0388(5) Uani 1 1 d D . . . . H2 H 0.514(3) 0.183(3) 0.5641(7) 0.047 Uiso 1 1 d D U . . . N3 N 0.4755(2) 0.3496(2) 0.37180(6) 0.0318(4) Uani 1 1 d . . . . . N4 N 0.7453(3) 0.2927(2) 0.31275(7) 0.0385(5) Uani 1 1 d . . . . . C1 C 0.4412(3) 0.2962(3) 0.45640(8) 0.0304(4) Uani 1 1 d . . . . . C2 C 0.3794(3) 0.2861(3) 0.50441(9) 0.0347(5) Uani 1 1 d . . . . . C3 C 0.6549(3) 0.1714(3) 0.50379(8) 0.0359(5) Uani 1 1 d . . . . . H3 H 0.763427 0.117632 0.515129 0.043 Uiso 1 1 calc R U . . . C4 C 0.3719(3) 0.3681(3) 0.40809(8) 0.0332(5) Uani 1 1 d . . . . . H4 H 0.259578 0.423994 0.403813 0.040 Uiso 1 1 calc R U . . . C5 C 0.4378(3) 0.4133(3) 0.31964(9) 0.0413(5) Uani 1 1 d . . . . . H5A H 0.460524 0.543839 0.317220 0.050 Uiso 1 1 calc R U . . . H5B H 0.313042 0.389929 0.308636 0.050 Uiso 1 1 calc R U . . . C6 C 0.5629(3) 0.3070(3) 0.28702(9) 0.0408(6) Uani 1 1 d . . . . . H6A H 0.514577 0.185104 0.280610 0.049 Uiso 1 1 calc R U . . . H6B H 0.570526 0.368275 0.254450 0.049 Uiso 1 1 calc R U . . . C7 C 0.8351(4) 0.4750(4) 0.31499(11) 0.0584(7) Uani 1 1 d . . . . . H7A H 0.849584 0.518362 0.280981 0.088 Uiso 1 1 calc R U . . . H7B H 0.951191 0.464043 0.332807 0.088 Uiso 1 1 calc R U . . . H7C H 0.762546 0.560092 0.332612 0.088 Uiso 1 1 calc R U . . . C8 C 0.8543(4) 0.1636(4) 0.28414(10) 0.0567(7) Uani 1 1 d . . . . . H8A H 0.856268 0.203173 0.249336 0.085 Uiso 1 1 calc R U . . . H8B H 0.802234 0.043313 0.285251 0.085 Uiso 1 1 calc R U . . . H8C H 0.975033 0.160315 0.299251 0.085 Uiso 1 1 calc R U . . . C9 C 0.2060(3) 0.3362(4) 0.52544(10) 0.0474(6) Uani 1 1 d . . . . . H9A H 0.152063 0.229007 0.539257 0.071 Uiso 1 1 calc R U . . . H9B H 0.126616 0.386333 0.498817 0.071 Uiso 1 1 calc R U . . . H9C H 0.226751 0.425797 0.551910 0.071 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.03292(16) 0.03388(18) 0.02521(17) -0.00073(10) 0.00288(11) -0.00169(11) Cl1 0.0352(3) 0.0656(4) 0.0511(4) -0.0047(3) -0.0022(3) 0.0035(3) Cl2 0.0725(4) 0.0364(3) 0.0301(3) -0.0027(2) 0.0051(3) -0.0137(3) O1W 0.0753(17) 0.0758(16) 0.171(3) -0.0401(19) 0.0102(19) 0.0012(14) N1 0.0369(10) 0.0313(9) 0.0255(10) -0.0004(7) 0.0007(7) -0.0036(8) N2 0.0541(12) 0.0391(11) 0.0234(10) 0.0001(8) 0.0050(9) -0.0089(9) N3 0.0390(10) 0.0318(9) 0.0245(9) 0.0026(7) 0.0015(7) -0.0005(8) N4 0.0476(11) 0.0376(10) 0.0315(11) -0.0014(8) 0.0132(9) -0.0049(9) C1 0.0357(11) 0.0258(10) 0.0298(11) -0.0037(8) 0.0038(9) -0.0062(9) C2 0.0451(12) 0.0270(11) 0.0328(12) -0.0041(9) 0.0078(10) -0.0091(9) C3 0.0438(12) 0.0334(11) 0.0300(12) 0.0013(9) -0.0020(10) -0.0050(10) C4 0.0369(11) 0.0279(10) 0.0346(13) 0.0004(9) 0.0002(9) -0.0019(9) C5 0.0484(13) 0.0443(13) 0.0310(12) 0.0090(10) -0.0005(10) 0.0009(11) C6 0.0581(15) 0.0403(13) 0.0238(12) 0.0040(9) 0.0002(10) -0.0018(11) C7 0.0629(17) 0.0542(16) 0.0595(18) 0.0053(13) 0.0148(13) -0.0227(14) C8 0.0662(18) 0.0701(18) 0.0358(15) -0.0055(13) 0.0199(13) 0.0103(15) C9 0.0497(14) 0.0519(14) 0.0422(15) -0.0086(11) 0.0170(11) -0.0052(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 N3 1.9841(18) . y Cu1 N1 2.0072(17) . y Cu1 N4 2.0596(19) . y Cu1 Cl1 2.2452(6) . y Cu1 Cl2 2.6245(6) . y O1W H1WA 0.837(18) . ? O1W H1WB 0.857(18) . ? N1 C3 1.311(3) . ? N1 C1 1.390(3) . ? N2 C3 1.344(3) . ? N2 C2 1.368(3) . ? N2 H2 0.831(16) . ? N3 C4 1.269(3) . ? N3 C5 1.458(3) . ? N4 C8 1.477(3) . ? N4 C6 1.483(3) . ? N4 C7 1.487(3) . ? C1 C2 1.370(3) . ? C1 C4 1.440(3) . ? C2 C9 1.479(3) . ? C3 H3 0.9300 . ? C4 H4 0.9300 . ? C5 C6 1.515(3) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3 Cu1 N1 80.24(7) . . y N3 Cu1 N4 81.58(7) . . y N1 Cu1 N4 158.70(7) . . y N3 Cu1 Cl1 164.82(6) . . y N1 Cu1 Cl1 96.01(5) . . y N4 Cu1 Cl1 98.66(6) . . y N3 Cu1 Cl2 92.90(5) . . y N1 Cu1 Cl2 99.29(5) . . y N4 Cu1 Cl2 92.60(5) . . y Cl1 Cu1 Cl2 102.25(3) . . y H1WA O1W H1WB 91(5) . . ? C3 N1 C1 106.19(18) . . ? C3 N1 Cu1 142.06(16) . . ? C1 N1 Cu1 111.49(13) . . ? C3 N2 C2 109.44(19) . . ? C3 N2 H2 126.3(18) . . ? C2 N2 H2 124.2(18) . . ? C4 N3 C5 125.58(19) . . ? C4 N3 Cu1 117.39(15) . . ? C5 N3 Cu1 116.96(14) . . ? C8 N4 C6 109.11(19) . . ? C8 N4 C7 109.4(2) . . ? C6 N4 C7 110.6(2) . . ? C8 N4 Cu1 114.43(16) . . ? C6 N4 Cu1 105.06(13) . . ? C7 N4 Cu1 108.20(15) . . ? C2 C1 N1 109.54(19) . . ? C2 C1 C4 135.2(2) . . ? N1 C1 C4 115.26(18) . . ? N2 C2 C1 104.54(19) . . ? N2 C2 C9 122.7(2) . . ? C1 C2 C9 132.8(2) . . ? N1 C3 N2 110.3(2) . . ? N1 C3 H3 124.9 . . ? N2 C3 H3 124.9 . . ? N3 C4 C1 115.02(19) . . ? N3 C4 H4 122.5 . . ? C1 C4 H4 122.5 . . ? N3 C5 C6 106.20(18) . . ? N3 C5 H5A 110.5 . . ? C6 C5 H5A 110.5 . . ? N3 C5 H5B 110.5 . . ? C6 C5 H5B 110.5 . . ? H5A C5 H5B 108.7 . . ? N4 C6 C5 110.73(19) . . ? N4 C6 H6A 109.5 . . ? C5 C6 H6A 109.5 . . ? N4 C6 H6B 109.5 . . ? C5 C6 H6B 109.5 . . ? H6A C6 H6B 108.1 . . ? N4 C7 H7A 109.5 . . ? N4 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? N4 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? N4 C8 H8A 109.5 . . ? N4 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? N4 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C2 C9 H9A 109.5 . . ? C2 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C2 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1W H1WA Cl1 0.837(18) 2.52(2) 3.293(3) 154(4) . O1W H1WB Cl2 0.857(18) 2.45(2) 3.244(3) 155(5) 1_655 N2 H2 Cl2 0.831(16) 2.285(17) 3.104(2) 168(2) 3_656 C5 H5A Cl2 0.97 2.86 3.767(2) 155.3 1_565 C6 H6A Cl2 0.97 2.87 3.476(2) 121.3 . C7 H7B O1W 0.96 2.64 3.252(4) 121.9 1_565 C7 H7C Cl2 0.96 2.99 3.908(3) 160.4 1_565 C8 H8B Cl2 0.96 2.87 3.548(3) 128.7 . C8 H8C Cl1 0.96 2.93 3.413(3) 112.5 . _refine_diff_density_max 0.327 _refine_diff_density_min -0.336 _refine_diff_density_rms 0.063 _shelx_res_file ; TITL exp_1_a.res in P2(1)/c shelx.res created by SHELXL-2014/7 at 08:59:43 on 08-Feb-2019 REM Old TITL exp_1 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.160, Rweak 0.005, Alpha 0.041, Orientation as input REM Formula found by SHELXT: C9 N5 Cu Cl2 REM ##### CELL 0.71073 7.435472 7.295155 26.272863 90 93.4607 90 ZERR 4 0.000279 0.000281 0.001102 0 0.0036 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N Cu Cl O UNIT 36 72 16 4 8 4 EQIV $1 1+X,+Y,+Z EQIV $2 1-X,-Y,1-Z EQIV $3 +X,1+Y,+Z DFIX 0.87 N2 H2 HTAB O1W Cl1 HTAB O1W Cl2_$1 HTAB N2 Cl2_$2 HTAB C5 Cl2_$3 HTAB C6 Cl2 HTAB C7 O1W_$3 HTAB C7 Cl2_$3 HTAB C8 Cl2 HTAB C8 Cl1 DANG 2.38 CL1 H1WA DANG 2.2 H1WB Cl2_$1 L.S. 10 PLAN 20 HTAB BOND $H list 4 REM CONF fmap 2 acta OMIT -1 1 1 OMIT -1 1 2 OMIT 2 1 0 OMIT 1 1 0 OMIT 1 1 2 OMIT 1 1 1 OMIT 0 1 6 DFIX 0.82 O1W H1WA O1W H1WB REM REM REM WGHT 0.035300 0.311800 EXTI 0.005093 FVAR 0.91336 CU1 4 0.703014 0.211992 0.386184 11.00000 0.03292 0.03388 = 0.02521 -0.00073 0.00288 -0.00169 CL1 5 0.985866 0.128375 0.410487 11.00000 0.03521 0.06558 = 0.05107 -0.00467 -0.00222 0.00351 CL2 5 0.557828 -0.100122 0.355669 11.00000 0.07248 0.03640 = 0.03012 -0.00267 0.00514 -0.01368 O1W 6 1.146660 -0.245583 0.359674 11.00000 0.07526 0.07582 = 0.17054 -0.04012 0.01016 0.00123 H1WA 2 1.084755 -0.150929 0.362936 11.00000 -1.50000 H1WB 2 1.237893 -0.180973 0.352457 11.00000 -1.50000 N1 3 0.613538 0.222367 0.456696 11.00000 0.03692 0.03126 = 0.02545 -0.00038 0.00071 -0.00365 N2 3 0.517941 0.207945 0.533361 11.00000 0.05409 0.03913 = 0.02336 0.00009 0.00499 -0.00887 H2 2 0.513850 0.182832 0.564131 11.00000 -1.20000 N3 3 0.475460 0.349620 0.371797 11.00000 0.03899 0.03177 = 0.02448 0.00258 0.00150 -0.00047 N4 3 0.745349 0.292744 0.312749 11.00000 0.04764 0.03758 = 0.03148 -0.00144 0.01321 -0.00488 C1 1 0.441154 0.296200 0.456402 11.00000 0.03574 0.02576 = 0.02978 -0.00371 0.00375 -0.00620 C2 1 0.379360 0.286090 0.504410 11.00000 0.04508 0.02699 = 0.03283 -0.00409 0.00775 -0.00915 C3 1 0.654882 0.171394 0.503792 11.00000 0.04382 0.03335 = 0.02997 0.00131 -0.00203 -0.00499 AFIX 43 H3 2 0.763427 0.117632 0.515129 11.00000 -1.20000 AFIX 0 C4 1 0.371896 0.368121 0.408093 11.00000 0.03690 0.02793 = 0.03463 0.00038 0.00024 -0.00192 AFIX 43 H4 2 0.259578 0.423994 0.403813 11.00000 -1.20000 AFIX 0 C5 1 0.437812 0.413287 0.319639 11.00000 0.04841 0.04426 = 0.03101 0.00896 -0.00050 0.00094 AFIX 23 H5A 2 0.460524 0.543839 0.317220 11.00000 -1.20000 H5B 2 0.313042 0.389929 0.308636 11.00000 -1.20000 AFIX 0 C6 1 0.562875 0.307011 0.287016 11.00000 0.05808 0.04031 = 0.02384 0.00398 0.00020 -0.00183 AFIX 23 H6A 2 0.514577 0.185104 0.280610 11.00000 -1.20000 H6B 2 0.570526 0.368275 0.254450 11.00000 -1.20000 AFIX 0 C7 1 0.835122 0.474954 0.314985 11.00000 0.06293 0.05416 = 0.05949 0.00532 0.01483 -0.02268 AFIX 137 H7A 2 0.849584 0.518362 0.280981 11.00000 -1.50000 H7B 2 0.951191 0.464043 0.332807 11.00000 -1.50000 H7C 2 0.762546 0.560092 0.332612 11.00000 -1.50000 AFIX 0 C8 1 0.854252 0.163582 0.284143 11.00000 0.06623 0.07006 = 0.03583 -0.00547 0.01992 0.01029 AFIX 137 H8A 2 0.856268 0.203173 0.249336 11.00000 -1.50000 H8B 2 0.802234 0.043313 0.285251 11.00000 -1.50000 H8C 2 0.975033 0.160315 0.299251 11.00000 -1.50000 AFIX 0 C9 1 0.205993 0.336202 0.525443 11.00000 0.04969 0.05191 = 0.04218 -0.00857 0.01697 -0.00520 AFIX 137 H9A 2 0.152063 0.229007 0.539257 11.00000 -1.50000 H9B 2 0.126616 0.386333 0.498817 11.00000 -1.50000 H9C 2 0.226751 0.425797 0.551910 11.00000 -1.50000 AFIX 0 HKLF 4 REM exp_1_a.res in P2(1)/c REM R1 = 0.0328 for 2684 Fo > 4sig(Fo) and 0.0435 for all 3299 data REM 167 parameters refined using 5 restraints END WGHT 0.0353 0.3118 REM Instructions for potential hydrogen bonds HTAB O1W Cl1 HTAB O1W Cl2_$1 HTAB N2 Cl2_$2 HTAB C5 Cl2_$3 HTAB C6 Cl2 HTAB C7 O1W_$3 HTAB C7 Cl2_$3 HTAB C8 Cl2 HTAB C8 Cl1 REM Highest difference peak 0.327, deepest hole -0.336, 1-sigma level 0.063 Q1 1 1.1300 -0.1567 0.3372 11.00000 0.05 0.31 Q2 1 0.4060 0.3225 0.4334 11.00000 0.05 0.30 Q3 1 1.0218 0.1205 0.4173 11.00000 0.05 0.28 Q4 1 0.5683 0.3122 0.3818 11.00000 0.05 0.27 Q5 1 0.1772 0.4652 0.5266 11.00000 0.05 0.27 Q6 1 0.9779 0.2311 0.4025 11.00000 0.05 0.26 Q7 1 0.4566 0.3615 0.3520 11.00000 0.05 0.25 Q8 1 0.4677 0.4129 0.3869 11.00000 0.05 0.25 Q9 1 0.4471 0.2747 0.5231 11.00000 0.05 0.24 Q10 1 1.0848 -0.1705 0.3818 11.00000 0.05 0.24 Q11 1 0.4686 0.3226 0.3596 11.00000 0.05 0.24 Q12 1 0.5804 0.1786 0.5181 11.00000 0.05 0.23 Q13 1 0.9908 0.2083 0.3909 11.00000 0.05 0.22 Q14 1 0.4183 0.3330 0.4823 11.00000 0.05 0.22 Q15 1 0.6266 -0.0958 0.3308 11.00000 0.05 0.22 Q16 1 0.2871 0.4960 0.4125 11.00000 0.05 0.21 Q17 1 0.3151 0.3292 0.5131 11.00000 0.05 0.21 Q18 1 0.7295 0.2780 0.3429 11.00000 0.05 0.21 Q19 1 0.9894 0.0417 0.4500 11.00000 0.05 0.20 Q20 1 1.2749 -0.1988 0.3610 11.00000 0.05 0.20 ; 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-2 5 80.6229 6.80877 5 -1 -2 5 82.3510 7.00310 4 -1 2 5 83.3281 6.08887 5 1 2 -5 96.3476 8.44485 4 1 2 -5 87.7821 7.29841 5 -1 -2 4 48.7654 4.71042 5 1 2 -4 47.5292 6.30339 4 1 2 -4 45.7756 4.94507 5 -1 2 4 48.1346 3.94160 2 -1 -2 4 36.2293 4.63308 1 -1 2 4 47.0105 3.89427 5 -1 -2 3 1918.02 81.5007 5 -1 -2 3 1857.35 82.8832 4 -1 2 3 1923.15 79.0655 5 -1 2 3 1674.07 79.3953 6 1 2 -3 1907.78 83.5866 4 -1 -2 3 1889.55 82.4819 1 1 2 -3 1992.81 81.3748 5 -1 2 3 2023.82 79.0605 2 1 -2 -2 208.145 9.95977 5 1 2 -2 218.912 12.9465 1 1 2 -2 216.331 11.8973 5 -1 2 2 212.542 9.70577 5 1 2 -2 198.477 13.7827 4 -1 -2 2 198.583 13.1597 4 -1 -2 2 195.510 12.6186 1 -1 -2 2 199.479 11.8326 5 1 2 -1 382.904 21.7483 4 -1 -2 1 365.638 19.5336 5 1 2 -1 406.533 20.6120 1 1 2 -1 408.864 19.4640 5 1 2 0 4063.59 168.635 3 1 2 0 4187.31 169.065 5 -1 -2 0 3980.43 169.797 5 1 2 0 3995.98 170.145 1 -1 -2 -1 25215.4 1061.16 5 1 2 1 26384.8 1060.25 3 1 2 1 26156.2 1060.30 5 -1 -2 -2 11042.0 490.300 4 1 2 2 12161.5 488.287 3 1 -2 2 12002.4 485.247 2 1 2 2 12235.4 488.057 5 -1 -2 -2 11354.6 489.983 6 1 2 3 7302.97 286.707 5 1 -2 3 6796.15 284.043 2 -1 -2 -3 6591.38 288.382 6 1 2 3 6945.28 286.848 3 -1 -2 -3 7143.49 289.374 4 -1 -2 -4 3672.85 150.095 4 -1 -2 -4 3336.69 147.548 3 -1 -2 -4 3402.79 149.454 6 1 -2 4 3365.13 145.276 2 1 2 4 3706.98 148.182 3 1 2 4 3679.40 148.782 6 1 -2 5 879.922 39.9355 2 1 2 5 915.602 42.3978 3 1 2 5 889.969 42.6563 6 -1 -2 -5 843.632 43.2664 6 -1 -2 -5 852.910 41.7259 3 -1 -2 -5 958.996 43.8518 4 1 2 6 1279.73 58.7365 3 1 -2 6 1254.87 56.3935 2 -1 -2 -6 1353.16 59.9484 4 1 2 6 1318.20 59.5188 6 -1 -2 -6 1277.73 60.3764 6 -1 -2 -6 1209.28 58.1047 3 1 2 7 47.9281 7.60434 3 1 -2 7 54.4939 4.62815 3 1 2 7 72.1422 8.37681 6 -1 -2 -7 42.3739 7.03641 4 -1 -2 -7 43.2054 5.88025 3 1 -2 7 41.4452 5.00688 2 -1 -2 -7 56.3718 7.42932 6 1 -2 8 1431.76 61.9752 3 -1 -2 -8 1303.82 64.9793 3 1 2 8 1459.41 67.0105 6 1 2 8 1481.35 66.3443 3 1 -2 8 1380.15 63.5714 2 -1 -2 -8 1487.97 66.1143 4 -1 -2 -9 3047.45 129.057 4 1 -2 9 3044.23 125.315 3 1 -2 9 2950.49 124.193 4 -1 -2 -9 2648.91 128.177 3 1 2 9 3042.01 130.433 6 1 2 9 3063.14 129.738 3 1 -2 9 2899.98 126.912 2 1 -2 10 3719.54 152.663 4 -1 -2 -10 3222.88 157.606 3 1 2 10 3752.15 159.645 3 1 2 10 3797.74 160.532 6 1 -2 10 3631.18 154.906 3 1 -2 10 3691.68 156.935 2 -1 -2 -10 3890.71 158.563 4 -1 -2 -11 82.2176 9.48209 4 1 -2 11 67.0390 7.74743 2 1 -2 11 70.0903 7.01049 3 1 2 11 75.3412 10.8205 3 1 -2 11 62.6318 4.53797 4 1 2 11 61.9669 9.86364 6 1 -2 12 541.823 29.7264 2 1 2 12 472.309 31.0102 3 1 -2 12 527.236 23.0022 4 1 2 12 542.967 33.0481 6 1 -2 12 531.772 28.0098 3 -1 -2 -12 598.998 30.6887 4 -1 -2 -13 621.583 33.7960 4 1 2 13 643.333 37.3899 6 1 -2 13 569.993 33.2558 2 1 -2 13 635.615 32.3705 3 1 -2 14 3216.12 137.124 3 -1 -2 -14 3163.02 137.801 4 1 -2 14 2955.00 138.158 2 1 2 14 3327.59 143.406 6 1 2 15 762.792 46.1470 6 -1 -2 -15 879.296 42.6077 4 1 -2 15 777.305 42.5715 2 1 -2 15 774.927 40.8507 3 1 -2 16 1563.15 77.2328 2 -1 -2 -16 1691.26 76.0102 4 1 -2 16 1594.57 75.4216 3 1 2 16 1622.90 81.9568 6 -1 -2 -17 966.183 47.7229 4 1 -2 17 951.956 48.0852 3 1 2 17 908.225 53.6110 6 -1 -2 -17 864.445 50.4910 3 1 -2 17 945.019 49.8378 2 -1 -2 -18 930.107 50.0143 4 1 2 18 983.941 57.5900 6 1 -2 18 1055.59 51.9419 3 -1 -2 -18 1021.33 55.1766 3 1 -2 18 1042.19 53.7670 2 -1 -2 -19 561.708 37.0032 3 -1 -2 -19 567.184 32.3531 4 1 -2 19 538.904 35.3232 5 1 2 19 543.888 38.7670 6 1 -2 19 577.856 35.1840 2 1 2 20 1171.78 67.7424 6 -1 -2 -20 1175.84 64.2842 3 -1 -2 -20 1246.16 59.2406 4 -1 -2 -21 1431.93 67.7708 4 1 2 21 1445.94 78.1709 6 -1 -2 -21 1378.70 73.8050 3 -1 -2 -22 49.8089 14.3469 3 1 2 22 62.8635 16.2271 6 -1 -2 -22 55.6456 10.7380 4 -1 -2 -23 351.703 29.1967 3 -1 -2 -23 325.722 23.2049 4 1 2 23 369.304 33.1875 6 -1 -2 -24 111.197 18.5077 3 1 2 24 91.1851 19.4876 6 -1 -2 -24 105.853 13.2777 4 1 2 25 643.711 47.2931 6 -1 -2 -25 584.657 42.0284 3 1 2 26 18.0871 15.7034 6 -1 -2 -26 39.8524 15.4056 3 -1 -2 -27 4.58588 13.5667 3 1 2 27 3.13979 16.7450 6 1 2 28 787.990 54.3377 6 -1 -2 -28 576.209 44.7553 3 1 2 29 3.39862 18.3554 6 -1 -2 -29-2.45157 15.6664 3 1 2 30 91.8384 23.5649 6 -1 -2 -30 63.2542 20.2701 3 -1 -2 -31 117.530 23.2704 3 1 2 31 95.3700 26.0112 6 -1 -2 -32 145.128 25.6200 3 -1 3 32 371.035 40.9749 6 1 -3 -31 18.5335 20.0999 3 -1 3 31 14.8155 20.0154 6 -1 3 30 46.4465 22.3010 6 1 -3 -30 51.1780 20.1774 3 1 -3 -29 49.7554 19.9408 3 -1 3 28 483.855 44.4242 6 1 -3 -28 488.239 42.0064 3 1 -3 -27 105.112 23.5999 3 -1 3 27 90.5401 22.6562 6 -1 3 26 151.861 25.1822 6 1 -3 -26 203.911 25.4052 3 1 3 -25 157.517 17.7903 3 1 -3 -25 199.601 26.2624 3 1 -3 -24 65.2220 19.5302 3 1 3 -24 81.7010 13.1561 3 1 3 -23 133.531 15.1083 3 1 3 -22 38.6536 13.1701 2 1 3 -22 44.7119 10.2936 3 1 3 -21 167.181 19.4710 2 1 3 -21 209.127 17.0861 3 1 3 -20 71.4356 10.4746 3 1 3 -20 77.2216 9.54465 4 1 3 -20 83.5005 13.5858 2 -1 3 19 147.115 15.3916 5 1 3 -19 91.3681 14.2156 2 1 3 -19 107.007 10.8470 4 1 3 -19 96.6589 11.7122 3 -1 3 19 111.381 14.6881 2 -1 3 18 63.3352 11.9653 5 -1 -3 18 39.5545 8.22467 5 1 3 -18 41.1971 8.37789 3 1 3 -18 55.3789 11.5137 2 -1 3 18 53.8900 10.6189 2 1 -3 -18 46.8871 10.6117 3 1 3 -18 40.3652 7.72798 4 1 3 -17 1288.09 58.5895 3 -1 3 17 1308.75 62.2155 2 1 -3 -17 1173.80 66.0743 3 -1 -3 17 1254.94 63.1248 5 -1 3 17 1276.67 62.1261 5 -1 -3 17 1208.06 62.5579 2 1 3 -17 1220.20 58.2717 4 1 3 -17 1200.72 62.8051 2 -1 3 16 486.845 29.4305 5 1 3 -16 502.294 27.4161 4 -1 3 16 520.047 30.3036 2 -1 -3 16 443.063 29.5134 5 1 3 -16 538.238 31.4650 2 1 -3 -16 423.991 31.8338 3 1 3 -16 496.715 26.6721 3 1 3 -15 943.696 44.4792 3 1 -3 -15 878.814 51.4763 3 1 3 -15 961.979 45.8090 4 -1 -3 15 912.064 48.5287 5 1 3 -15 912.320 48.8184 2 -1 3 15 941.163 47.6479 5 -1 3 15 941.879 47.6771 2 -1 3 14 923.242 48.4622 5 1 3 -14 1049.95 50.7595 2 -1 3 14 969.296 48.2233 2 1 3 -14 955.058 47.1917 4 1 -3 -14 950.975 53.2501 3 -1 -3 14 989.895 50.0027 5 1 3 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124.803 10.4659 5 1 3 -9 109.807 10.8567 4 -1 -3 8 1404.64 66.1876 4 -1 3 8 1574.74 64.8535 2 1 3 -8 1450.89 66.6086 2 -1 -3 8 1467.99 66.1402 5 -1 3 8 1469.98 66.3583 6 1 3 -8 1452.02 67.4551 4 1 3 -8 1467.25 66.2247 5 1 -3 -8 1372.97 68.8965 3 -1 3 8 1412.71 64.0018 5 -1 3 7 7266.29 328.350 6 1 3 -7 8190.70 329.249 2 1 3 -7 7882.36 330.483 4 1 -3 -7 7730.13 331.834 3 -1 3 7 8031.94 326.207 5 1 3 -7 7910.82 328.436 5 -1 -3 7 8114.03 328.575 5 -1 -3 7 8104.62 329.607 1 -1 3 6 1833.01 76.6768 5 -1 3 6 1815.45 78.4343 6 -1 -3 6 1699.74 78.8047 5 1 3 -6 1780.32 79.0700 5 1 3 -6 1700.22 81.1637 4 -1 -3 6 1893.15 80.5433 1 -1 -3 6 1775.22 80.9950 4 1 -3 -6 1791.33 81.9908 3 1 3 -6 1846.70 79.8358 2 1 3 -5 831.143 44.7334 4 -1 3 5 927.851 41.5142 6 1 3 -5 907.296 42.4381 5 -1 -3 5 885.030 44.8387 4 -1 -3 5 887.799 42.3246 5 -1 -3 5 990.153 44.2980 1 -1 3 5 928.613 40.0036 5 -1 3 4 4834.41 200.883 6 -1 -3 4 4676.46 205.931 4 -1 3 4 4749.39 199.421 5 1 3 -4 4994.20 199.577 3 1 3 -4 5037.45 202.520 5 -1 -3 4 4707.94 202.713 5 -1 -3 4 4872.38 204.429 1 -1 -3 3 468.733 23.1188 5 -1 3 3 450.476 19.5079 5 -1 -3 3 475.801 24.8005 1 1 3 -3 449.650 20.7605 3 1 3 -3 429.558 22.5900 5 -1 -3 3 430.715 25.8673 4 1 3 -2 4199.16 174.713 1 -1 -3 2 4080.25 178.247 4 1 3 -2 4219.60 173.222 5 1 3 -2 4080.98 171.893 3 -1 -3 2 4185.29 174.052 5 1 3 -1 3138.89 132.296 5 -1 -3 1 3225.03 133.486 5 -1 -3 1 3074.02 137.750 4 1 3 -1 3269.31 134.201 1 1 3 -1 3070.67 131.752 3 1 3 0 9278.84 381.771 1 1 3 0 9527.24 379.972 5 1 3 0 8954.66 379.824 3 -1 -3 0 9191.22 381.200 5 1 3 1 769.006 35.9298 3 1 3 1 765.599 35.3222 5 1 3 1 769.090 37.0205 1 1 -3 2 5495.72 220.584 1 -1 3 -2 5345.64 220.087 2 1 3 2 5254.53 222.737 5 -1 -3 -2 5320.32 226.666 6 1 3 2 5284.62 223.674 3 1 3 3 4649.06 194.038 3 -1 -3 -3 4284.35 197.997 4 1 -3 3 4563.71 190.588 1 1 -3 3 4694.43 190.350 5 -1 3 -3 4754.67 190.349 2 -1 -3 -3 4616.04 196.732 6 -1 -3 -3 4732.59 194.328 3 1 3 3 4350.08 192.740 5 -1 -3 -4 6514.90 283.062 3 1 3 4 6710.11 281.763 5 -1 -3 -4 6959.24 285.883 6 1 -3 4 6940.27 279.778 5 -1 -3 -4 7445.20 288.700 4 1 3 4 6594.84 283.216 3 -1 3 -4 6717.70 279.322 2 1 3 5 97.6774 9.54498 3 1 -3 5 88.9707 6.65745 5 -1 -3 -5 76.1904 9.03612 6 -1 3 -5 77.1775 6.26724 2 -1 -3 -5 80.6296 8.14902 3 -1 -3 -5 99.4573 11.6139 4 -1 -3 -6 582.739 31.7789 3 1 -3 6 575.949 29.0170 2 -1 -3 -6 620.671 33.9621 6 -1 3 -6 611.370 28.7366 2 1 3 6 598.590 32.1715 3 1 3 6 637.519 32.6912 6 1 -3 6 628.430 29.5693 5 -1 -3 -6 612.380 35.0558 4 -1 -3 -7 292.408 19.1760 3 1 -3 7 324.576 17.2570 2 1 -3 7 294.560 14.6950 3 -1 -3 -7 323.385 22.4341 4 1 3 7 310.708 20.0036 6 1 3 7 296.633 19.6808 3 -1 -3 -7 329.456 21.6649 6 1 -3 7 285.708 17.2180 5 1 -3 8 1343.48 59.4109 2 1 3 8 1341.28 62.6103 3 -1 -3 -8 1308.69 64.6967 6 1 3 8 1286.05 62.5242 6 -1 -3 -8 1345.96 64.9075 4 1 -3 8 1314.32 56.3981 3 -1 -3 -8 1259.26 61.9565 3 1 -3 8 1281.16 59.7249 5 -1 -3 -9 173.430 14.0610 3 1 -3 9 169.284 12.4935 5 1 -3 9 154.830 11.5988 2 -1 -3 -9 184.949 16.6445 4 1 3 9 152.454 14.4846 3 1 -3 9 146.305 9.38955 3 1 3 9 164.776 14.5272 6 1 -3 10 1.84099 2.60727 5 -1 -3 -10 4.02285 7.05895 4 1 3 10-4.94964 6.25151 6 1 -3 10-0.76472 2.35479 4 1 -3 10 2.34810 1.83808 3 1 3 10 8.27685 6.54377 3 1 -3 10 1.65048 2.90580 2 -1 -3 -10-1.19615 3.23029 3 1 -3 11 75.4833 8.62662 5 1 -3 11 95.9269 8.19157 4 -1 -3 -11 71.3857 9.10413 3 1 3 11 60.4699 10.7653 3 1 -3 11 65.0061 6.21875 3 1 -3 11 76.1138 8.21545 2 1 3 11 103.600 12.7477 6 1 -3 12 146.114 10.2766 4 1 3 12 153.061 15.7108 6 1 3 12 163.647 16.2950 3 1 -3 12 158.785 10.6478 3 -1 -3 -12 124.529 13.2237 3 1 -3 12 154.840 12.5664 2 1 -3 12 131.587 12.5966 5 1 -3 13 349.011 19.8512 3 -1 -3 -13 312.957 23.7307 3 1 -3 13 370.257 23.5292 5 1 -3 13 362.976 18.7890 4 1 3 13 357.034 25.9234 3 1 3 13 365.522 25.9935 6 1 -3 13 363.135 22.6350 2 -1 -3 -14 836.754 47.7449 3 1 -3 14 847.714 45.3250 2 1 3 14 944.028 49.6670 3 1 -3 14 953.038 43.0099 3 1 -3 14 889.445 46.5460 5 1 -3 14 861.289 39.4748 4 1 3 14 876.524 49.2336 6 1 -3 15 1064.17 51.4920 3 1 3 15 1131.58 58.5588 3 -1 -3 -15 1013.70 56.5631 3 1 -3 15 1115.52 55.0514 2 1 3 15 1063.87 58.3755 6 1 -3 15 1125.58 55.9290 5 -1 -3 -15 1113.52 57.0060 4 1 -3 16 10.0821 5.07287 5 1 3 16 1.79778 9.58827 6 -1 -3 -16-1.65871 4.69965 3 -1 -3 -16-1.45958 9.32811 4 1 3 16 11.7090 10.7850 3 1 -3 16 2.64583 4.07528 2 1 -3 17 67.6950 10.0066 2 1 -3 17 48.8938 9.09491 5 -1 -3 -17 55.3942 9.91811 3 1 3 17 43.6297 11.5318 6 -1 -3 -17 38.3497 11.0366 4 1 3 18 1929.97 93.7445 6 1 -3 18 1728.94 88.7619 5 1 -3 18 1830.22 88.6052 2 -1 -3 -18 1933.53 89.0019 4 -1 -3 -19 305.141 24.0749 4 1 3 19 306.047 27.6631 6 1 3 20 33.3110 12.6213 6 -1 -3 -20 72.6121 12.5771 4 1 3 21 9.33850 11.7958 6 -1 -3 -21 1.51567 9.94324 4 -1 -3 -22 714.339 42.6954 4 1 3 22 774.549 49.7524 6 1 3 23 1072.44 65.1344 6 -1 -3 -23 1085.15 57.5663 4 1 3 24 61.9577 17.7703 6 -1 -3 -24 108.048 20.9161 3 -1 -3 -24 65.7194 13.2588 4 -1 -3 -25 104.699 20.4262 3 1 3 25 107.067 21.5474 6 1 3 26 397.501 37.5259 6 -1 -3 -26 455.051 36.8020 3 -1 -3 -27 440.165 37.2572 3 1 3 27 444.920 40.5221 6 -1 -3 -28 25.6666 16.9905 3 1 3 28 6.39371 17.4927 6 -1 -3 -29 410.252 37.7717 3 1 3 29 458.914 42.1381 6 1 3 30 740.211 55.9247 6 -1 -3 -30 692.216 51.0091 3 1 3 31 78.8963 26.8898 6 -1 4 31 160.165 28.6432 6 -1 4 30 23.3243 20.1423 6 -1 4 29 89.1751 22.2248 6 -1 4 28 484.580 42.5568 6 -1 4 27 427.667 38.6521 6 -1 4 26 2.77545 15.1763 6 1 -4 -25 19.9136 10.0353 3 -1 4 25 5.28043 14.4496 6 -1 4 24 881.863 55.0591 6 1 -4 -24 818.484 54.4711 3 1 -4 -23 13.3184 8.53519 3 1 4 -23 11.5662 11.8880 2 -1 4 23 28.6140 14.1221 6 1 -4 -22 5.15134 7.94349 3 -1 4 22 22.5932 12.8059 6 1 4 -22 14.8256 11.5300 2 1 -4 -21 2.47591 7.01541 3 -1 4 21 4.27597 11.1074 6 1 4 -21 15.8795 10.8669 2 1 -4 -20 324.874 29.0827 3 -1 4 20 422.107 31.2118 6 1 4 -20 378.966 21.3575 3 1 4 -20 332.583 27.1468 2 1 -4 -19 478.188 36.4791 3 -1 4 19 556.171 33.0006 5 1 4 -19 540.924 27.2642 3 -1 4 19 513.856 36.2429 6 1 4 -19 494.908 33.7781 2 1 -4 -18 2.23181 5.71775 3 1 4 -18 1.70323 4.87265 3 1 4 -18 10.7195 9.52029 2 -1 4 18 5.16572 9.73990 2 -1 4 18-2.52322 8.55132 5 -1 4 18-5.37253 9.67217 6 -1 -4 17 665.467 39.6925 5 1 -4 -17 693.896 44.6591 3 -1 4 17 725.410 38.8819 5 -1 4 17 706.097 39.2059 2 -1 4 17 668.271 41.7862 6 1 4 -17 731.773 41.0254 2 1 4 -17 688.667 33.0202 3 1 -4 -16 227.097 22.3129 3 -1 -4 16 286.294 20.9628 5 1 4 -16 256.381 21.1701 2 -1 4 16 240.162 21.6758 6 -1 4 16 274.558 20.7369 2 -1 4 16 294.413 20.4156 5 1 4 -16 260.567 14.7315 3 1 4 -15 155.603 9.83683 3 -1 4 15 146.360 14.2446 2 -1 4 15 155.445 14.5948 5 1 -4 -15 173.674 17.7373 3 -1 4 15 165.953 16.7332 6 -1 -4 15 182.316 15.2852 5 1 4 -15 143.522 15.2847 2 1 -4 -14 62.8614 10.8968 3 -1 4 14 56.1662 9.17940 5 -1 4 14 54.7859 9.19510 2 -1 4 14 63.4579 10.4423 6 1 4 -14 57.1948 10.0951 2 1 4 -14 55.2200 5.07355 3 -1 -4 14 43.4707 7.45517 5 -1 4 13 714.463 38.5324 6 1 4 -13 672.184 29.3466 3 -1 4 13 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-3 5998.88 240.638 4 2 -3 4 249.471 12.9471 2 2 3 4 219.998 16.2568 5 2 3 4 269.607 17.4924 3 -2 -3 -4 243.965 18.9246 6 2 -3 4 267.498 13.8259 6 -2 -3 -4 261.486 19.3200 4 2 -3 5 41.4619 4.82615 6 2 3 5 36.2073 7.52456 3 -2 -3 -5 39.0028 7.43822 6 2 3 5 39.1906 6.71966 5 2 -3 5 37.7335 4.03790 2 -2 -3 -5 46.7095 9.27865 4 2 3 6 796.044 42.3975 3 2 -3 6 873.257 38.7302 2 -2 -3 -6 765.357 44.7282 6 2 3 6 819.252 41.8782 5 2 -3 6 831.726 40.1346 6 -2 -3 -6 887.603 44.6251 4 -2 -3 -7 1990.95 88.8357 4 -2 -3 -7 1837.10 90.3067 6 2 3 7 1882.14 87.2030 3 2 3 7 1916.34 86.6926 5 2 -3 7 1907.35 83.0473 2 2 3 8 1375.54 65.6456 3 2 -3 8 1389.77 61.6765 2 -2 -3 -8 1356.91 66.1698 4 -2 -3 -8 1281.43 68.0213 6 2 3 9 309.346 22.5605 6 2 3 9 304.743 21.9444 3 -2 -3 -9 308.119 22.0724 4 -2 -3 -9 304.084 23.4671 6 2 -3 9 282.056 17.9065 2 -2 -3 -10 168.871 17.3820 6 2 3 10 180.168 17.2257 3 2 3 10 192.504 17.4513 6 2 -3 10 189.673 12.6697 3 2 -3 10 218.968 14.6159 2 2 3 11 899.316 52.5692 6 2 -3 11 966.011 47.1952 3 2 3 11 1039.99 53.2132 3 -2 -3 -11 970.951 55.5618 6 -2 -3 -11 1129.31 53.3726 4 2 -3 11 1062.59 49.7343 2 2 3 12 1629.27 78.6513 3 -2 -3 -12 1708.74 77.4768 4 2 -3 12 1587.36 72.2825 3 2 -3 12 1612.42 74.6799 2 2 3 12 1481.11 78.1574 6 2 3 13 921.005 52.1155 6 2 -3 13 928.511 45.7554 3 2 3 13 964.938 51.8928 3 2 -3 13 987.634 44.0546 4 -2 -3 -13 945.278 49.9073 4 -2 -3 -13 827.180 49.1351 3 2 -3 13 964.654 48.1096 2 -2 -3 -14 629.497 37.5616 3 2 -3 14 625.740 33.3882 3 2 3 14 645.319 39.3589 3 -2 -3 -14 577.890 36.3693 4 2 -3 14 621.556 30.1033 4 2 -3 14 690.651 36.4184 2 -2 -3 -15 917.398 51.6953 3 2 -3 15 979.714 47.8742 3 -2 -3 -15 883.923 50.4149 4 2 3 15 978.975 54.7246 6 2 -3 15 974.209 42.2425 4 2 -3 15 980.549 50.3838 2 -2 -3 -16 1160.66 65.7774 3 -2 -3 -16 1333.51 64.9328 4 2 -3 16 1368.81 62.9185 3 2 3 16 1296.53 69.3672 6 2 -3 16 1313.23 65.1892 2 2 -3 17 2506.83 111.466 3 -2 -3 -17 2217.03 115.007 3 2 3 17 2611.69 119.921 6 2 -3 17 2606.65 115.123 2 -2 -3 -18 532.172 32.5835 4 2 -3 18 513.231 30.6557 3 2 -3 18 507.160 33.2184 2 2 3 18 500.706 36.7516 6 2 -3 19 522.363 31.6492 3 -2 -3 -19 521.846 32.8383 4 2 3 19 537.407 38.8773 6 -2 -3 -20 348.445 24.9255 4 2 -3 20 302.719 22.8308 3 2 3 20 326.888 29.9202 6 2 3 21 688.958 46.8758 6 -2 -3 -21 670.000 39.3550 4 2 3 22 259.095 27.2044 6 -2 -3 -22 233.376 20.6990 4 2 3 23 8.02623 13.3224 6 -2 -3 -23 1.35860 8.68290 4 -2 -3 -24 514.913 39.3507 3 2 3 24 532.733 41.9243 6 -2 -3 -25 453.217 38.0515 3 2 3 25 534.539 42.3975 6 2 3 26 187.371 26.5358 6 2 3 27 28.2785 18.6249 6 2 3 28 342.771 36.6692 6 2 -3 29 21.9277 14.3412 6 2 3 29 33.8819 19.2218 6 2 -3 30 303.485 35.0706 6 2 3 30 365.321 39.4614 6 2 -3 31 98.3658 19.9964 6 -2 4 31 28.3871 20.3595 6 -2 4 30 187.617 31.4910 6 -2 4 29 39.2893 21.8952 6 -2 4 28 43.8969 19.3904 6 -2 4 27 51.0322 20.4996 6 2 4 -27 70.3128 19.0275 2 2 4 -26 258.924 27.8135 2 2 -4 -25 532.079 41.1716 3 2 4 -25 461.711 37.0357 2 -2 4 25 473.673 40.4498 6 2 4 -24 66.6297 17.1838 2 2 -4 -24 66.4790 15.5559 3 -2 4 24 92.3080 18.9453 6 2 -4 -23 537.933 42.2207 3 -2 4 23 555.634 42.1723 6 2 4 -23 558.902 38.8537 2 2 -4 -22 48.3473 13.0412 3 -2 4 22 32.0784 14.5488 6 2 4 -21 11.5170 11.8226 2 2 -4 -21 5.48502 8.11653 3 -2 4 21 2.15956 11.6660 6 2 4 -20 262.113 18.9171 3 2 4 -20 263.790 24.2352 2 2 -4 -20 269.480 26.6743 3 -2 4 20 239.698 23.9645 6 -2 4 19 107.489 13.9770 5 -2 4 19 110.001 14.3894 2 2 4 -19 95.8121 16.1175 2 2 4 -19 120.896 12.2051 3 2 -4 -19 127.431 17.6056 3 -2 4 18 2.40888 7.83311 5 2 4 -18 5.06941 9.57186 2 2 4 -18 5.32198 8.94629 4 2 4 -18 3.47235 6.83453 3 -2 4 18-3.49277 8.94798 2 2 -4 -18-2.45970 7.57338 3 -2 4 17 1094.36 55.3303 2 2 4 -17 1269.72 54.0120 3 -2 4 17 993.112 54.9134 5 2 4 -17 1161.01 57.9762 4 -2 4 17 1117.21 59.9825 6 2 -4 -17 1177.51 65.5551 3 2 4 -17 1051.05 59.1245 2 2 -4 -16 77.3346 13.6254 3 2 4 -16 62.7687 12.6274 5 -2 4 16 66.3824 10.5815 5 -2 -4 16 45.2696 9.27841 5 -2 4 16 87.8531 10.9636 2 2 4 -16 91.6961 13.3862 2 2 4 -16 72.4119 9.07178 3 -2 4 16 78.9813 12.9417 6 2 4 -16 77.9978 12.0820 4 2 4 -15 947.406 49.5238 2 2 -4 -15 883.370 53.1852 3 2 4 -15 932.942 43.0763 3 -2 -4 15 919.084 48.2672 5 2 4 -15 893.570 48.4693 4 -2 4 15 867.414 44.8283 2 -2 4 15 881.702 48.6417 6 -2 4 15 852.544 44.8516 5 2 4 -15 890.471 49.3711 5 2 4 -14 52.5826 10.5820 5 -2 4 14 70.3557 11.4274 6 -2 4 14 50.2826 8.81277 5 -2 -4 14 47.8799 8.31531 5 -2 4 14 71.1753 9.26780 2 2 -4 -14 81.5650 12.7370 3 2 4 -14 74.0555 8.05097 3 -2 -4 14 48.5782 8.68723 1 2 4 -14 54.0847 11.3590 4 2 4 -13 208.093 18.5398 2 -2 -4 13 217.010 17.1485 5 2 4 -13 182.916 17.3087 5 -2 4 13 204.252 15.2799 5 2 -4 -13 202.459 20.2978 3 -2 4 13 217.428 15.3225 2 -2 -4 13 242.892 18.5614 1 2 4 -13 194.214 18.2843 4 2 4 -12 487.858 30.8491 2 2 -4 -12 495.656 34.1606 3 -2 -4 12 536.971 31.3344 1 2 4 -12 496.176 30.6638 5 -2 4 12 483.754 26.8172 5 -2 4 12 513.684 26.9834 2 2 4 -12 506.219 31.7934 4 -2 4 12 469.129 29.3202 6 -2 -4 12 524.978 30.2348 5 -2 -4 11 3040.99 135.409 5 -2 4 11 3002.18 130.772 2 2 4 -11 3094.69 136.351 2 2 -4 -11 3258.67 141.687 3 -2 -4 11 3230.88 137.445 1 -2 4 11 3048.99 134.089 6 2 4 -11 3082.08 137.114 4 -2 4 11 3108.44 131.280 5 2 4 -11 2859.65 135.170 5 -2 -4 10 1160.28 57.1213 5 -2 4 10 1135.97 52.7181 2 2 4 -10 1150.85 57.9738 2 2 4 -10 1182.15 57.4877 5 -2 -4 10 1228.78 59.0547 1 -2 -4 10 1190.87 57.0929 4 2 4 -10 1073.99 58.8616 4 -2 4 10 1216.74 55.9195 6 -2 4 10 1175.80 53.1700 5 2 4 -9 41.7474 8.92601 2 2 4 -9 44.0658 8.39245 5 -2 4 9 39.3509 6.98033 6 -2 4 9 38.2431 5.62229 5 -2 -4 9 30.6283 6.09744 5 -2 -4 9 43.1941 7.04348 4 -2 4 9 30.5780 5.13709 2 -2 -4 9 42.4071 7.58926 1 2 4 -9 25.7261 8.92988 4 2 4 -8 4.41583 6.46368 2 2 4 -8 3.03216 4.95907 5 -2 4 8 2.32801 3.51283 5 -2 -4 8 1.02331 3.90915 5 -2 -4 8 2.52761 3.58067 1 -2 4 8 2.70579 4.51262 6 -2 -4 8 1.14487 3.24396 4 -2 4 8 3.82420 3.57497 2 2 4 -8 4.10198 8.09010 4 -2 -4 7 3997.10 166.457 5 -2 4 7 3896.49 160.799 5 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697.259 40.1817 4 -2 -4 1 772.435 37.9444 5 2 4 0 4648.93 194.494 3 2 4 0 4563.34 196.890 1 -2 -4 0 4639.30 197.261 5 2 4 0 4598.19 194.923 5 2 4 1 3451.15 141.954 3 2 4 1 3159.81 143.365 1 2 4 1 3275.63 141.528 5 2 4 2 1164.18 55.2640 5 2 4 2 1124.71 57.0921 1 2 4 2 1202.62 56.0570 3 -2 -4 -2 1288.71 61.1638 6 2 4 3 2286.98 101.475 5 -2 -4 -3 2438.25 107.771 6 -2 -4 -3 2231.69 107.333 4 2 -4 3 2315.47 96.6624 5 2 4 3 2310.93 102.469 3 2 -4 4 8011.38 325.823 5 2 4 4 7930.63 331.323 3 2 -4 4 7984.38 325.045 6 2 -4 4 7738.67 324.308 1 -2 -4 -4 8489.33 337.818 4 -2 -4 -4 7985.08 336.430 6 2 4 4 7874.27 330.122 5 2 4 5 207.004 15.7736 5 2 4 5 202.997 16.6163 3 2 -4 5 220.615 12.8920 6 -2 -4 -5 234.349 19.4425 6 -2 -4 -5 242.270 20.7781 4 2 4 6 95.8411 10.5556 5 2 4 6 104.767 12.0335 3 -2 -4 -6 97.1824 12.5610 6 2 -4 7 17.9527 3.64994 2 -2 -4 -7 20.2159 7.78022 6 2 4 7 28.1191 7.15953 5 2 4 7 3.51463 6.59931 3 -2 -4 -7 22.5216 9.83655 4 2 4 8 2002.87 91.9056 5 2 4 8 2028.90 93.6858 3 2 -4 8 2006.48 87.7753 2 -2 -4 -8 2017.60 97.0290 4 -2 -4 -8 2075.32 98.0688 6 2 4 9 1269.62 61.3033 5 2 -4 9 1250.86 57.4021 2 2 4 9 1254.34 63.0148 3 2 -4 9 1231.77 55.5888 3 -2 -4 -9 1360.87 66.4666 4 -2 -4 -9 1210.18 66.0971 6 2 -4 10 44.1556 5.18201 3 2 4 10 54.1684 11.3945 3 2 -4 10 51.7290 6.49743 2 -2 -4 -10 46.4228 9.83092 6 -2 -4 -10 60.3261 12.6297 4 2 -4 11 1465.11 69.1192 2 2 4 11 1562.32 75.4046 3 -2 -4 -11 1600.58 76.9727 4 2 -4 11 1506.89 66.7682 3 -2 -4 -11 1464.37 78.3400 6 2 -4 12 576.334 32.0102 2 2 4 12 650.648 37.9362 3 2 4 12 554.405 37.0984 6 -2 -4 -12 580.825 37.8496 4 2 -4 12 607.053 29.7926 3 2 -4 13 113.948 11.0633 4 2 -4 13 132.610 10.0707 3 2 4 13 134.284 16.3629 6 2 -4 13 102.280 10.8191 2 -2 -4 -13 119.186 16.4789 4 2 -4 14 11.2027 5.48042 5 2 -4 14 2.80611 3.38965 4 2 -4 14-1.52965 3.06430 3 2 4 14 5.39031 9.70433 6 2 -4 14 4.62638 3.69627 2 -2 -4 -14 3.48215 10.4077 4 2 4 15 634.743 43.0115 6 2 -4 15 748.775 41.7407 5 2 -4 15 692.662 36.2777 3 -2 -4 -15 715.545 43.9719 4 2 -4 15 754.381 36.6549 4 2 -4 15 736.478 39.6434 2 -2 -4 -15 749.042 43.7505 3 2 -4 16 489.752 30.6215 5 2 -4 16 397.544 27.2921 2 2 -4 16 423.320 24.6791 3 -2 -4 -16 501.033 33.2280 4 2 -4 16 449.630 23.3133 4 2 4 16 403.709 31.7697 6 -2 -4 -16 381.647 30.0246 3 2 -4 17 5.01983 5.89424 5 -2 -4 -17 3.53826 10.6841 4 -2 -4 -17 5.78112 5.93602 3 2 -4 17 5.37638 2.71097 4 2 -4 17 2.87626 4.43163 2 2 4 17-2.05605 11.2438 6 2 -4 18 52.9181 10.7457 5 -2 -4 -18 46.0548 12.9129 4 2 -4 18 47.5513 9.49104 2 -2 -4 -18 58.0543 11.1404 3 2 4 18 49.3831 13.6317 6 -2 -4 -19 1230.15 70.3348 3 2 4 19 1338.95 73.5377 6 -2 -4 -19 1444.27 71.0618 4 -2 -4 -20 81.9045 13.5697 3 2 4 20 77.0381 16.5426 6 -2 -4 -20 90.4687 16.9329 4 -2 -4 -21 151.853 18.5376 3 -2 -4 -22 88.2517 16.2269 4 2 4 22 81.1443 18.8642 6 -2 -4 -22 60.1123 12.9881 3 -2 -4 -23 916.114 57.4831 3 2 4 23 998.504 61.2311 6 -2 -4 -23 995.622 55.2534 4 -2 -4 -24 31.6050 13.5932 4 -2 -4 -24 9.89028 8.47092 3 2 4 24 16.4702 16.9162 6 2 4 25 22.8890 16.7759 6 2 4 26 11.8836 17.5834 6 2 4 27 337.165 35.2386 6 2 4 28 22.4677 19.2080 6 2 -4 30 98.8159 21.1858 6 -2 5 27 495.339 40.6206 6 2 5 -27 548.508 40.6364 2 2 5 -26-7.07331 14.7958 2 2 -5 -26-3.42964 9.71401 3 -2 5 26 7.77799 15.9657 6 2 5 -25-13.6141 14.1061 2 -2 5 25-2.46776 13.6571 6 2 -5 -25 9.96059 10.2227 3 2 5 -24 50.0134 16.0574 2 2 -5 -24 41.9806 13.3261 3 -2 5 24 28.2008 15.8864 6 2 5 -23 663.285 42.9861 2 2 -5 -23 569.401 45.5796 3 -2 5 23 606.680 42.3685 6 -2 5 22-6.33149 13.2487 6 2 5 -22-10.1830 13.0195 2 2 -5 -22-9.23818 9.11639 3 -2 5 21-5.99548 12.5415 6 2 5 -21 1.95859 11.3442 2 2 -5 -21-3.00546 7.26006 3 2 5 -20 5.66513 11.8502 2 2 -5 -20-2.91764 7.04753 3 -2 5 20-5.65851 10.4388 6 2 -5 -19 1150.04 69.2175 3 2 5 -19 1102.71 62.6940 2 -2 5 19 1243.22 63.6873 6 -2 5 18 16.7541 11.3562 6 2 5 -18-1.73969 10.5051 2 2 -5 -18-2.71575 8.03395 3 -2 5 17 75.6596 13.9174 6 2 5 -17 98.1766 15.6434 2 2 -5 -17 70.4909 14.4749 3 2 -5 -16 47.6378 13.2039 3 2 5 -16 43.5718 12.1311 2 -2 5 16 68.0128 12.0422 6 2 -5 -15 1284.58 68.7623 3 -2 5 15 1169.01 59.9448 6 2 5 -15 1311.66 63.0441 5 2 5 -15 1140.35 60.8222 2 -2 5 15 1095.79 55.8118 2 -2 -5 15 1169.73 60.2150 5 2 5 -14 89.9845 14.2165 5 -2 5 14 82.6295 9.63817 5 -2 -5 14 68.6338 10.3578 5 2 -5 -14 74.2510 13.4654 3 -2 5 14 64.4959 11.6084 6 -2 5 14 77.9122 10.0306 2 2 5 -14 48.3632 11.0862 2 2 5 -13 16.8922 9.17487 5 2 5 -13 24.1931 9.66497 2 -2 5 13 6.07619 5.90449 5 2 -5 -13 13.3302 6.86734 3 -2 -5 13 13.4348 5.53538 5 -2 5 13 12.3756 6.49994 2 -2 -5 12 856.270 45.7402 5 -2 5 12 932.413 45.5020 6 2 5 -12 830.839 46.5660 2 2 5 -12 893.334 46.8046 5 -2 5 12 812.795 41.0144 5 2 -5 -12 895.457 52.2391 3 -2 -5 12 907.402 48.2139 1 -2 -5 12 873.977 46.1909 4 -2 5 12 843.016 41.3408 2 -2 5 11 72.4699 7.94678 5 2 5 -11 76.0948 11.6843 5 -2 -5 11 88.2038 10.7340 5 2 5 -11 79.5373 11.6194 2 -2 5 11 84.2414 10.5534 6 -2 -5 11 86.3732 10.6937 4 2 -5 -11 105.652 14.3213 3 -2 5 11 61.6718 7.89596 2 2 5 -11 74.5036 4.67282 3 -2 -5 11 65.0118 10.3572 1 2 5 -10 111.359 12.4556 5 -2 -5 10 93.9445 11.5463 4 -2 -5 10 85.1328 10.3052 5 2 5 -10 87.2089 5.57224 3 -2 -5 10 77.5708 11.1458 1 -2 5 10 77.5182 8.05142 2 2 -5 -10 102.613 14.1950 3 -2 5 10 92.1542 10.4440 6 2 5 -10 98.0106 12.7302 2 -2 -5 9 1184.53 55.6034 5 2 5 -9 1131.93 56.3031 2 2 -5 -9 1204.31 61.1437 3 2 5 -9 1032.72 47.2676 3 -2 -5 9 1124.88 57.5990 4 -2 5 9 1161.53 52.3839 6 -2 5 9 1069.53 49.4070 2 2 5 -9 1164.26 55.6552 5 -2 5 9 1167.82 49.4004 5 -2 -5 9 1207.34 58.2801 1 -2 5 8 223.674 11.9238 5 -2 -5 8 252.458 17.1678 5 2 5 -8 200.401 11.3546 3 -2 5 8 200.304 12.0075 2 2 -5 -8 241.321 20.3920 3 -2 -5 8 197.795 17.8727 4 2 5 -8 212.097 16.7975 5 2 5 -8 236.890 18.1766 2 -2 -5 8 195.208 17.3823 1 2 5 -7-2.04554 5.85915 5 -2 5 7 2.78361 2.75099 5 -2 -5 7 1.57466 4.46010 4 -2 -5 7 2.16951 3.70570 5 2 5 -7 2.42028 3.37979 3 2 -5 -7 1.64459 4.21352 3 -2 5 7-0.60383 2.72903 2 2 5 -6 26.9384 7.23754 5 -2 -5 6 36.2839 6.52748 5 -2 -5 6 29.2447 7.54361 4 2 5 -6 23.0573 4.39777 3 2 -5 -6 40.2490 8.21523 3 -2 5 6 21.9565 3.08253 2 -2 -5 5 1916.92 86.3489 5 2 5 -5 1870.07 81.0369 3 2 5 -5 1889.89 85.1196 5 -2 -5 5 1880.92 91.2789 4 2 5 -4 833.014 39.4179 3 -2 -5 4 846.431 43.6538 5 -2 -5 4 824.829 48.0923 4 2 5 -4 897.676 42.7740 5 -2 -5 3 47.8919 7.35883 5 2 5 -3 43.7191 6.57428 3 -2 -5 3 57.8027 10.3289 4 -2 -5 2 1099.50 50.5815 5 2 5 -2 917.717 46.2434 3 2 5 -2 940.256 49.7120 1 -2 -5 2 1079.22 55.9533 4 2 5 -2 1035.66 48.1269 5 -2 -5 1 1522.13 70.3163 5 2 5 -1 1463.19 66.8718 3 -2 -5 1 1505.58 75.7992 4 2 5 -1 1404.96 69.7966 1 2 5 -1 1524.64 67.8713 5 2 5 0 95.8909 9.59066 5 2 5 0 65.8493 9.26414 3 2 5 0 66.1019 10.3271 1 -2 -5 0 99.4292 12.7023 4 2 5 1 1384.50 63.6986 5 2 5 1 1393.97 64.2103 3 2 5 1 1314.19 65.8960 1 -2 -5 -1 1454.33 70.6231 6 2 5 2 1132.20 53.3090 5 2 5 2 1093.80 54.0503 3 -2 -5 -2 1202.68 60.1304 6 2 5 2 1083.21 55.4969 1 2 5 3 2432.71 110.708 5 2 5 3 2665.89 112.896 3 2 5 3 2468.88 113.606 1 -2 -5 -3 2633.58 118.577 6 2 5 4 7.11314 6.15340 5 2 5 4 19.4925 8.49856 3 2 -5 5 3488.00 144.483 5 2 -5 5 3429.92 145.358 6 2 5 5 3278.30 150.026 5 2 5 5 3404.68 152.400 3 -2 -5 -5 3507.97 158.173 6 2 -5 5 3619.98 144.494 5 2 -5 6 1282.09 57.0169 5 2 5 6 1291.37 64.0511 3 -2 -5 -6 1463.65 72.4247 4 2 -5 6 1279.89 56.9074 1 2 5 6 1277.77 61.7283 5 -2 -5 -6 1306.21 68.5101 6 2 -5 6 1359.13 57.1305 5 2 5 7 893.863 47.2594 5 2 5 7 890.315 49.2029 3 2 -5 7 920.092 42.8424 1 -2 -5 -7 966.891 53.9139 6 2 -5 7 1010.34 43.6648 5 -2 -5 -7 1008.72 56.6175 4 2 -5 8 161.465 11.1536 5 2 5 8 152.412 14.2572 5 2 5 8 146.244 16.0972 3 -2 -5 -8 141.181 16.8039 6 -2 -5 -8 142.013 19.0469 4 2 -5 9 1356.91 59.4047 3 2 5 9 1269.91 66.0421 5 -2 -5 -9 1438.95 73.9931 6 2 5 9 1464.95 69.7468 3 -2 -5 -9 1460.62 74.9212 4 2 -5 9 1427.75 63.4092 5 2 -5 10 160.194 9.59514 3 -2 -5 -10 164.038 18.7554 6 2 5 10 141.259 15.4125 5 -2 -5 -10 198.294 22.3950 4 2 5 10 191.839 19.1090 3 2 5 11 883.132 47.1203 5 2 -5 11 860.801 39.4542 3 -2 -5 -11 987.938 55.4132 4 -2 -5 -11 945.874 54.9119 6 2 -5 11 913.245 44.8231 5 2 -5 12 20.2724 6.72231 4 2 -5 12 21.8706 5.60069 5 2 5 12 32.8852 9.76302 5 -2 -5 -12 17.1695 13.3742 4 2 -5 13 135.420 12.9925 5 -2 -5 -13 144.774 20.1268 4 2 -5 13 132.719 13.6113 4 2 -5 14 50.8219 8.75115 5 2 -5 14 44.0812 7.35517 2 2 -5 14 50.0773 8.09790 4 -2 -5 -14 28.2769 14.3903 4 2 -5 15 1056.66 51.1833 4 2 -5 15 911.665 49.4650 2 -2 -5 -15 1026.46 59.2498 4 2 -5 15 987.703 52.0687 5 2 5 16 50.8942 13.8210 6 2 -5 16 51.3169 7.97677 4 -2 -5 -16 24.1008 15.6584 4 -2 -5 -17 332.521 29.5619 4 2 5 17 328.504 29.2498 6 2 5 18 17.5639 14.3120 6 -2 -5 -18 30.8216 14.4739 4 2 5 19 27.2240 15.5550 6 -2 -5 -19 37.4035 14.8533 4 -2 -5 -20 2.19776 13.0030 4 2 5 20 2.34970 12.2055 6 2 5 21 43.7690 15.1257 6 -2 -5 -21 63.6314 16.8950 4 2 5 22 15.1624 14.1642 6 2 5 23 52.3660 16.8937 6 -2 -5 -23 63.0394 18.0527 4 -2 -5 -24 13.0001 13.9832 4 2 5 24 19.0079 16.4087 6 2 5 25 149.161 24.3169 6 2 5 26 23.2855 17.4247 6 2 5 27 3.01633 17.4703 6 2 6 -26 14.3430 16.7194 2 2 6 -25 154.483 22.5520 2 2 6 -24 79.6786 18.7946 2 2 -6 -24 104.990 19.9478 3 2 6 -23 132.819 20.6498 2 2 -6 -23 112.252 20.5280 3 2 6 -22 2.08423 14.0145 2 2 -6 -22-3.28793 9.31254 3 2 6 -21 10.0494 12.9672 2 2 -6 -21 12.7571 9.04586 3 2 6 -20 29.1506 13.4550 2 2 -6 -20 40.1622 12.7320 3 2 6 -19 9.41065 11.3710 2 2 -6 -19 9.04735 7.73494 3 2 6 -18 14.4415 11.6469 2 2 -6 -18 8.77965 9.36154 3 2 -6 -17 1053.52 62.6031 3 2 6 -17 947.578 54.7207 2 2 -6 -16 107.429 17.6902 3 2 6 -16 81.2502 15.4181 2 2 -6 -15 225.273 24.4114 3 2 6 -15 201.084 20.4187 2 2 -6 -14 56.0136 12.8083 3 2 6 -14 24.5452 11.4160 2 -2 -6 14 52.9993 9.67589 4 2 6 -13 720.335 43.8752 2 2 -6 -13 829.709 51.6227 3 2 6 -13 784.481 45.0147 5 -2 -6 13 850.093 45.5131 4 2 6 -12 167.608 17.3662 5 2 6 -12 154.712 17.2035 2 -2 -6 12 157.940 16.1944 4 2 -6 -12 149.253 18.9333 3 2 -6 -11 1291.10 69.2969 3 2 6 -11 1230.23 61.9761 5 -2 -6 11 1275.19 61.9321 5 -2 -6 11 1172.53 64.0076 4 -2 -6 10 463.685 29.0394 5 2 6 -10 450.531 30.4741 2 2 6 -10 479.930 29.8320 5 -2 -6 10 431.274 31.3483 4 -2 -6 9 209.219 17.2144 5 -2 -6 9 249.825 21.6526 4 2 -6 -9 247.439 22.3319 3 2 6 -9 184.616 18.1942 2 2 6 -9 244.539 18.9799 5 -2 -6 8 78.5083 13.2717 4 2 6 -8 120.170 14.2812 2 2 6 -8 133.020 14.3018 5 -2 -6 8 109.892 12.0616 5 2 -6 -8 134.922 16.0236 3 2 -6 -7 2416.35 110.934 3 2 6 -7 2314.83 105.539 2 -2 -6 7 2308.91 111.434 4 -2 -6 7 2286.92 104.588 5 2 6 -7 2283.46 104.183 5 -2 -6 6 478.558 29.0778 5 2 -6 -6 526.210 33.5239 3 -2 -6 6 472.127 34.2730 4 2 6 -6 475.609 28.6067 5 -2 -6 5 387.528 24.5260 5 2 -6 -5 391.252 27.3033 3 -2 -6 5 379.722 29.8434 4 2 6 -5 377.550 23.9699 5 2 -6 -4 3.04655 5.51888 3 -2 -6 4-1.15459 4.40942 5 -2 -6 4 2.12248 6.78175 4 -2 -6 3 1758.21 80.6937 5 2 -6 -3 1811.51 83.2287 3 2 6 -3 1665.72 75.9839 3 -2 -6 3 1598.93 87.7214 4 2 6 -3 1798.20 78.9222 5 2 6 -2 343.380 20.4361 3 2 -6 -2 369.522 24.3918 3 -2 -6 2 329.358 28.1753 4 2 6 -2 345.148 21.8922 5 2 6 -1 204.678 17.3520 1 2 6 -1 191.191 14.5173 3 2 -6 -1 199.522 16.2255 3 -2 -6 1 171.620 19.7684 4 2 6 -1 188.910 15.1228 5 2 6 0 60.9904 8.93530 5 2 6 0 50.3389 8.93144 3 2 6 0 46.5927 10.1848 1 2 -6 0 44.8794 7.86128 3 -2 -6 0 40.5256 9.12166 6 -2 -6 0 52.0563 11.6065 4 2 6 1 2109.54 96.2162 3 2 -6 1 2292.94 97.2137 3 -2 -6 -1 2198.25 103.597 6 2 6 1 2081.45 98.5292 1 -2 -6 -1 2033.62 106.434 4 2 6 1 2153.72 95.4911 5 2 6 2 263.572 19.9840 3 2 -6 2 320.423 19.3658 3 2 6 2 311.525 22.5353 1 -2 -6 -2 291.988 23.9068 6 2 6 2 289.652 19.1258 5 2 6 3 976.062 51.6904 1 2 6 3 937.108 49.6254 3 2 -6 3 1019.07 47.6602 3 2 6 3 1023.92 48.7584 5 -2 -6 -4 25.0008 8.72381 6 2 6 4 9.57448 8.29468 1 2 6 4 17.8287 7.55595 5 2 -6 4 17.9785 4.60007 3 2 6 4 30.3029 9.98225 3 2 -6 5 7.38645 3.11558 3 2 6 5 2.91189 6.53067 5 2 6 5 4.95403 8.05797 3 -2 -6 -5 7.85281 6.27712 6 2 6 5-1.41246 8.09455 1 -2 -6 -6 62.6154 11.8410 6 2 6 6 51.7112 8.97501 5 2 6 6 48.5736 11.4895 3 2 6 6 54.1402 11.2496 1 2 -6 6 58.6630 5.48398 3 -2 -6 -6 63.6246 16.1123 4 2 -6 6 71.2236 5.32026 6 2 6 7 203.802 16.5686 5 -2 -6 -7 193.111 25.6438 4 2 6 7 163.870 17.3363 3 -2 -6 -7 195.511 20.2193 6 2 6 8 42.6327 9.80409 5 -2 -6 -8 41.0595 10.6015 6 2 6 8 39.5614 11.8822 3 -2 -6 -9 65.5204 16.3887 4 2 6 9 48.4730 9.81640 5 2 6 10 16.3404 8.05723 5 -2 -6 -10 12.7461 15.0952 4 2 6 11 374.104 25.7865 5 2 -6 11 363.822 28.0363 4 -2 -6 -11 441.118 36.2203 4 2 6 12-1.36986 7.76066 5 2 -6 12 9.01336 6.71141 4 -2 -6 -12-5.16112 15.5828 4 2 6 13 1.43451 8.74834 5 -2 -6 -13-2.59528 15.1938 4 2 -6 13 1.74445 4.94095 4 2 6 14 34.8275 10.3324 5 -2 -6 -14 46.9601 17.1539 4 2 -6 14 23.4871 7.26150 4 2 6 15 159.756 17.6681 5 -2 -6 -15 180.918 25.2461 4 2 6 16 1.65252 10.0788 5 -2 -6 -16 7.90357 14.9238 4 2 6 17 48.2295 12.8331 5 -2 -6 -17 63.1907 19.7176 4 -2 -6 -18 148.010 24.1108 4 -2 -6 -19 327.210 33.3397 4 -2 -6 -20 26.3347 18.3011 4 2 6 22 92.5378 19.3118 6 -2 -6 -22 73.2637 20.7593 4 2 6 23 393.829 36.9739 6 -2 -6 -23 424.978 37.8394 4 2 6 24 62.5870 19.7106 6 -2 -6 -24 49.3305 18.8186 4 2 6 25 14.0274 16.6079 6 2 6 26 14.4520 17.8085 6 2 7 -23 109.941 20.1947 2 2 7 -22 31.9770 15.6990 2 2 -7 -22 24.6912 11.3245 3 2 7 -21 41.5574 15.2453 2 2 -7 -21 37.6577 14.4116 3 2 7 -20 20.1146 15.3849 2 2 -7 -20 19.9049 11.7088 3 2 7 -19 253.684 24.8442 2 2 -7 -19 237.518 27.8723 3 2 7 -18 100.326 17.0551 2 2 -7 -18 99.3109 18.8053 3 2 -7 -17 17.9478 8.85535 3 2 7 -17-5.46604 11.3323 2 2 -7 -16 14.3987 10.1667 3 2 7 -16 24.9869 13.2202 2 2 -7 -15 785.138 49.9114 3 2 7 -15 626.185 41.7837 2 2 7 -14 73.6494 15.3125 2 2 -7 -14 80.0774 15.9385 3 -2 -7 14 77.5631 12.3126 4 2 -7 -13 309.871 28.6608 3 -2 -7 13 330.779 26.3996 4 2 -7 -12 103.508 16.1490 3 2 7 -12 100.365 15.8714 2 2 -7 -11 362.420 29.6655 3 2 7 -11 279.820 24.1055 2 -2 -7 11 324.252 26.7457 4 2 -7 -10 52.2393 13.0382 3 -2 -7 10 51.7806 11.8428 4 2 7 -9 733.337 42.3603 2 2 -7 -9 752.541 46.6289 3 -2 -7 9 693.653 46.2324 4 2 7 -8 492.518 32.4465 2 2 -7 -8 570.854 36.9833 3 -2 -7 8 487.143 36.4003 4 2 -7 -7 150.743 17.0895 3 2 7 -7 108.157 15.1607 2 2 7 -6 6.72921 8.05258 2 2 -7 -6 7.38213 7.05674 3 -2 -7 6 12.0879 8.00342 4 2 -7 -5 883.456 48.3524 3 -2 -7 5 775.695 51.8593 4 2 -7 -4 279.816 21.8194 3 -2 -7 4 219.186 23.9474 4 -2 -7 3 59.1206 12.9459 4 2 -7 -3 41.9871 9.34907 3 2 -7 -2 6.86608 5.11619 3 -2 -7 2 2.60709 7.04366 4 -2 -7 1 763.345 50.7670 4 -2 -7 0 238.117 25.3583 4 2 7 0 250.690 20.5679 1 -2 -7 -1 46.1159 12.4160 4 2 7 1 50.4915 11.0476 1 2 7 2 5.63493 8.42099 1 -2 -7 -2-2.75215 7.79484 4 2 7 3 424.956 28.0216 1 -2 -7 -3 320.094 31.6757 4 2 7 4 4.50265 8.88158 1 2 7 5 334.184 25.6841 1 2 7 6 68.1555 13.0525 1 -2 -7 -6 129.081 24.1039 4 2 7 7 5.03850 9.07839 1 -2 -7 -7 28.9805 19.8018 4 2 -7 8 7.39701 6.66388 4 2 7 8 5.24496 9.44629 1 2 -7 9 260.529 26.0928 4 -2 -7 -9 305.164 33.1619 4 -2 -7 -10 74.5345 21.6244 4 2 -7 10 64.3930 12.5626 4 2 -7 11-4.43898 7.09309 4 -2 -7 -11 2.99957 15.7906 4 -2 -7 -12 281.727 32.0302 4 2 -7 12 211.725 21.6859 4 -2 -7 -13 197.989 29.6393 4 2 -7 13 156.273 18.5447 4 -2 -7 -14 128.531 26.1336 4 -2 -7 -15 55.3304 20.9562 4 -2 -7 -16 122.994 24.8591 4 -2 -7 -17 518.160 44.4692 4 -2 -7 -20 33.8830 21.0882 4 -2 -7 -21 261.219 33.3403 4 -2 -7 -22 6.12691 20.2652 4 -2 -7 -23 21.3856 20.7256 4 2 -8 -19 16.8359 12.8773 3 2 -8 -18-3.25747 11.4700 3 2 -8 -17 336.898 33.5809 3 2 -8 -16-3.04279 9.72303 3 2 -8 -15 2.93538 9.38230 3 -2 -8 15 8.27688 7.90612 4 -2 -8 14 4.30470 7.12255 4 2 -8 -14 8.46427 9.64037 3 -2 -8 13 189.913 21.2802 4 -2 -8 12 62.5205 12.7621 4 -2 -8 11 96.2438 15.5982 4 -2 -8 10 19.9501 9.55814 4 -2 -8 9 2.56959 8.21095 4 -2 -8 8 15.8642 10.3669 4 -2 -8 7 70.6969 14.9645 4 -2 -8 6 52.8562 12.9725 4 -2 -8 5 19.8779 10.6010 4 -2 -8 4 57.9289 13.7509 4 -2 -8 3 135.776 20.4465 4 -2 -8 2 21.0283 11.7867 4 -2 -8 1 39.5752 12.5709 4 -2 -8 0 120.202 18.8792 4 -2 -8 -1 576.707 44.9947 4 -2 -8 -2 9.48201 9.73918 4 -2 -8 -3 463.801 40.1186 4 2 -8 4 183.317 24.8716 4 -2 -8 -4 184.440 25.2238 4 2 -8 5 221.904 26.6783 4 2 -8 6 18.4144 11.4484 4 2 -8 7 142.556 20.3273 4 -2 -8 -7 183.540 28.7724 4 -2 -8 -8 397.096 39.8970 4 2 -8 8 305.543 30.3191 4 -2 -8 -9 267.740 34.7408 4 2 -8 9 236.898 25.9082 4 -2 -8 -10 109.459 26.5936 4 2 -8 10 56.1144 14.1500 4 -2 -8 -11 92.9538 26.2154 4 2 -8 11 87.5242 15.6537 4 -2 -8 -12 17.3104 21.3307 4 -2 -8 -13 271.444 36.7361 4 -2 -8 -14 3.49766 20.9082 4 -2 -9 11 13.3870 9.71550 4 -2 -9 10 8.32971 10.3407 4 -2 -9 9 194.364 23.4747 4 -2 -9 8 11.7636 10.0568 4 -2 -9 7 12.0737 10.6389 4 -2 -9 6 40.3216 12.8080 4 -2 -9 5 104.696 19.9956 4 -2 -9 4 77.7302 17.5591 4 -2 -9 3 95.6589 19.0857 4 -2 -9 2 221.347 28.0442 4 2 -9 -1 86.5042 21.0277 4 -2 -9 1 129.827 21.2924 4 2 -9 0 8.42365 11.9337 4 2 -9 1 57.5206 16.9883 4 2 -9 2 159.803 25.8993 4 2 -9 3 50.3574 17.9310 4 2 -9 4 3.73934 10.5917 4 2 -9 5 10.8321 10.6901 4 2 -9 6 247.539 29.5398 4 2 -9 7 23.6580 13.5711 4 2 -9 8-3.25791 8.34730 4 3 0 -33-8.74045 18.4546 3 3 0 -32 2.86373 19.5641 3 3 0 -31 5.65545 16.2001 3 3 0 -30 13.7494 16.4473 3 3 0 -29-2.66081 16.8513 3 3 0 -28 408.588 35.8159 3 3 0 -27 9.98002 14.9197 3 3 0 -26 621.799 44.8121 3 3 0 -25 2.33291 13.8026 3 3 0 -24 1687.69 87.4797 3 3 0 -24 1632.78 86.4903 2 3 0 -23 11.0370 7.05892 2 3 0 -23-4.33121 13.0798 3 3 0 -22 16.7567 7.39643 2 3 0 -22 8.27039 12.2456 3 3 0 -21 1.98061 4.47557 2 3 0 -20 33.9946 8.02100 2 3 0 -19 1.80719 4.63030 2 3 0 -18 43.6400 9.27291 5 -3 0 18 65.2286 10.9957 2 3 0 -18 53.0660 9.37762 2 -3 0 17-1.33926 8.40411 5 3 0 -17-1.77688 5.25631 5 3 0 -17 1.62709 4.60831 2 3 0 -16 4135.45 191.166 5 3 0 -16 4192.23 190.100 2 -3 0 16 4650.60 189.157 5 3 0 -15 1.56980 3.54684 5 -3 0 15 1.20420 6.82120 5 3 0 -15-2.89920 3.50140 2 3 0 -14 22.1667 6.00317 5 3 0 -14 27.6282 6.64391 2 3 0 -13 1.39345 2.91501 5 -3 0 13-6.47328 6.18045 5 3 0 -13-1.27627 3.44670 2 3 0 -12 1532.46 73.7698 5 -3 0 12 1524.94 71.3228 5 -3 0 11-1.93726 5.48678 5 3 0 -11 1.13063 3.05323 2 3 0 -11-1.26667 3.24507 5 3 0 -10 5827.17 242.196 2 3 0 -10 5703.67 243.006 5 -3 0 10 5610.64 240.802 5 3 0 -9 7.81773 3.57237 5 -3 0 9 7.03814 4.75443 5 3 0 -9 1.00912 2.73020 2 -3 0 8 2956.35 126.059 5 -3 0 8 3010.50 125.643 1 3 0 -8 2865.76 126.696 2 3 0 -8 2763.94 127.212 5 3 0 -7-0.99522 1.70158 5 -3 0 7 4.85864 4.58760 5 -3 0 6 3112.87 131.577 5 -3 0 6 3078.92 131.027 1 3 0 -6 2952.76 132.491 5 3 0 -5 3.63700 1.90456 5 -3 0 5-0.77337 3.96377 5 -3 0 5 0.73496 3.87017 1 3 0 -4 4820.35 214.924 5 -3 0 4 5091.87 214.518 5 -3 0 4 5354.67 214.296 1 3 0 -3 6.05036 2.56934 5 -3 0 3-0.76671 3.99061 5 -3 0 3-2.90187 4.20933 1 -3 0 2 290.101 17.0140 5 3 0 -2 240.149 16.2564 5 3 0 -2 234.268 15.7027 1 3 0 -1 0.85063 1.25818 5 -3 0 1-0.81607 3.62112 5 3 0 -1-0.80278 1.93899 1 3 0 0 632.648 32.6616 5 -3 0 0 654.471 33.0084 5 3 0 0 604.334 32.0357 1 3 0 1 1.74040 2.10249 5 -3 0 -1-0.88758 4.15179 5 3 0 2 9451.44 398.995 5 -3 0 -2 9763.51 399.099 6 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12.4556 4 -3 -5 -19 418.999 33.6127 4 3 -5 19 457.183 34.7465 6 3 -5 20 258.590 25.4410 6 -3 -5 -20 226.525 24.7232 4 3 5 21 18.2493 16.0646 6 3 -5 21 16.6156 10.5919 6 -3 -5 -21 8.13785 13.4700 4 3 5 22 29.7164 17.5760 6 -3 -5 -22 2.02274 14.6651 4 3 5 23 209.091 27.3281 6 3 5 24 14.4069 18.5860 6 3 5 25 50.4709 20.5428 6 3 6 -25 70.3178 19.9778 2 3 6 -24 21.9057 15.2996 2 3 6 -23 319.105 30.6116 2 3 -6 -23 306.506 34.7434 3 3 6 -22-6.91743 15.8920 2 3 -6 -22-22.0987 13.3642 3 3 6 -21 117.853 19.6585 2 3 -6 -21 75.1179 18.7342 3 3 6 -20 306.613 28.8176 2 3 -6 -20 318.583 33.3738 3 3 6 -19 402.805 32.5176 2 3 -6 -19 421.949 37.7347 3 3 -6 -18-3.24459 11.0831 3 3 6 -18 2.01484 11.1508 2 3 6 -17 14.2402 13.1203 5 3 -6 -17 3.14242 9.68178 3 3 6 -17 15.4396 11.3041 2 3 6 -16 71.3963 15.6620 5 3 -6 -16 75.9016 16.6716 3 3 6 -16 75.0346 15.8202 2 3 6 -15 1034.68 57.6327 2 3 -6 -15 1104.33 65.8056 3 3 6 -15 987.063 57.6018 5 3 6 -14 50.9685 13.3851 5 3 -6 -14 45.2238 13.1306 3 3 6 -14 41.2393 13.1247 2 3 6 -13 137.368 18.0922 5 3 -6 -13 174.333 21.2922 3 3 6 -13 142.700 18.2993 2 3 6 -12 336.174 26.5564 2 3 -6 -12 322.520 30.0452 3 3 6 -11 1204.50 66.3830 2 3 -6 -11 1405.44 74.9269 3 3 6 -11 1331.40 66.5653 5 3 6 -10 102.485 15.8244 2 3 6 -10 81.6035 13.6567 5 -3 -6 10 100.343 13.6098 4 -3 -6 10 108.044 13.2871 5 3 -6 -10 82.0104 14.9289 3 -3 -6 9 1339.52 68.8419 5 3 6 -9 1316.56 69.7467 2 3 -6 -9 1503.65 76.7092 3 -3 -6 9 1343.86 71.0541 4 3 6 -9 1449.95 69.7757 5 -3 -6 8 111.337 14.6721 4 3 6 -8 91.2137 13.2837 5 -3 -6 8 103.755 13.0457 5 3 -6 -8 127.000 17.2686 3 3 6 -7 187.298 17.4974 5 -3 -6 7 173.631 16.9021 5 -3 -6 7 175.799 18.3321 4 3 6 -6 137.998 14.5763 5 -3 -6 6 101.153 13.0246 5 -3 -6 6 122.854 15.0860 4 -3 -6 5 948.044 50.0431 5 -3 -6 5 886.199 52.6138 4 3 6 -5 903.577 48.0913 5 3 6 -4 59.9195 10.2730 5 -3 -6 4 66.4299 10.3778 5 -3 -6 4 58.4929 10.9105 4 3 6 -3 8.35032 7.82769 5 -3 -6 3 6.18067 5.56783 4 -3 -6 3 3.06957 5.71714 5 3 6 -2 36.6691 10.4495 1 3 6 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3 7 -14 174.937 20.8858 2 3 7 -13 577.804 39.6115 2 3 -7 -13 639.240 45.7277 3 3 -7 -12 14.0629 8.68063 3 3 7 -12 16.1752 12.1965 2 3 7 -11 478.099 32.6088 2 3 -7 -11 441.591 35.8398 3 3 7 -10 46.7626 13.8175 2 3 -7 -10 38.9740 12.6626 3 -3 -7 10 39.3746 10.7493 4 -3 -7 9 161.822 18.5250 4 3 7 -9 138.107 18.3574 2 3 -7 -9 186.798 20.9857 3 3 7 -8 3.31594 10.4047 2 3 -7 -8 2.38004 7.04139 3 3 -7 -7 375.098 30.8080 3 -3 -7 7 399.777 31.2488 4 3 -7 -6 41.2260 11.1518 3 -3 -7 6 62.1772 12.6051 4 3 7 -5 86.3684 13.7890 5 3 -7 -5 94.8053 13.8982 3 -3 -7 5 89.7839 15.2753 4 3 7 -4 30.4323 10.7664 5 3 -7 -4 23.4371 9.03791 3 -3 -7 4 21.7000 9.70980 4 3 -7 -3 528.203 34.4104 3 -3 -7 3 493.627 36.9369 4 3 7 -3 472.536 30.8040 5 3 7 -2 40.5538 10.3609 5 3 -7 -2 29.5942 8.52404 3 -3 -7 2 35.0257 11.3905 4 3 7 -1 16.0616 10.2892 1 3 7 -1 16.2329 9.32378 5 -3 -7 1 20.3847 9.00052 4 3 7 0 92.9710 14.9772 1 3 7 0 111.805 13.6213 5 -3 -7 0 93.1585 16.1522 4 3 7 1 129.415 16.7014 1 -3 -7 -1 130.945 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15.5666 8.30205 4 -3 -8 6 87.7878 16.2981 4 -3 -8 5 362.737 32.1161 4 -3 -8 4 19.4866 10.3923 4 -3 -8 3 2.83318 8.72398 4 -3 -8 2 92.1836 16.9230 4 -3 -8 1 313.696 30.3528 4 3 8 1 45.0870 12.6808 1 -3 -8 -1 27.1602 9.73985 4 3 8 2 71.8670 15.2135 1 -3 -8 -2 27.4761 13.4293 4 3 8 3 964.214 55.3516 1 3 8 4 3.91349 10.9583 1 3 8 5 276.921 26.0573 1 -3 -8 -6 34.9168 22.6827 4 3 8 6 4.13069 11.3008 1 3 8 7 239.240 24.9136 1 -3 -8 -7 240.083 33.3350 4 3 8 8 158.601 21.8112 1 -3 -8 -8 171.074 28.3515 4 3 -8 9 11.4666 8.49485 4 3 8 9 20.4149 15.0125 1 -3 -8 -9 3.24506 19.6011 4 -3 -8 -10 6.52843 18.9074 4 -3 -8 -11 350.826 39.0969 4 -3 -8 -12 9.86880 20.0653 4 3 -9 6 63.1783 16.9886 4 3 -9 7 170.716 25.9901 4 4 0 -32 25.1638 20.4820 3 4 0 -31-3.07214 18.5509 3 4 0 -30 29.9364 20.9605 3 4 0 -29-5.83828 17.0913 3 4 0 -28 139.096 25.3606 3 4 0 -27-2.75821 8.16256 2 4 0 -27-13.8597 17.2342 3 4 0 -26 264.574 26.5640 2 4 0 -26 311.775 31.8281 3 4 0 -25-2.55381 6.54265 2 4 0 -25 5.15957 14.6131 3 4 0 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6.25354 5 -4 0 9 1.01224 5.25801 1 -4 0 8 1288.70 61.8051 5 -4 0 8 1284.65 61.2150 1 4 0 -8 1301.58 63.9179 5 4 0 -7 5.11640 3.94104 5 -4 0 7 7.15417 6.35545 5 -4 0 7-0.97828 5.15183 1 -4 0 6 7146.65 302.313 5 -4 0 6 7404.60 301.962 1 4 0 -6 7011.44 303.971 5 4 0 -5 2.42463 3.27547 5 -4 0 5-4.04362 5.32254 5 4 0 -4 157.454 13.7223 5 4 0 -4 149.348 12.8004 1 -4 0 4 142.459 13.4070 5 4 0 -3-3.51273 4.12314 5 4 0 -3 5.29913 3.00231 1 -4 0 3-4.12211 5.42514 5 4 0 -2 3198.31 140.726 5 -4 0 2 3196.45 140.216 5 4 0 -2 3218.35 139.977 1 4 0 -1 2.14605 2.74893 1 4 0 -1-1.15211 3.54729 5 -4 0 1-4.35957 5.50616 5 4 0 0 1605.31 79.2002 5 -4 0 0 1785.53 80.1191 5 4 0 0 1755.76 79.3271 1 4 0 1-2.32318 3.43647 5 -4 0 -1 1.17525 6.10481 5 4 0 1 4.32734 3.33122 1 -4 0 -2 2618.39 118.531 6 4 0 2 2707.08 119.011 5 4 0 3 2.41249 3.26590 5 -4 0 -3 21.0551 6.92450 6 4 0 4 8283.66 351.700 5 -4 0 -4 8445.56 351.905 6 4 0 5 3.87208 3.81911 5 -4 0 -5-2.57706 6.41662 6 4 0 6 478.762 28.6074 5 -4 0 -6 403.913 27.8818 6 4 0 7 1.41244 3.61844 5 4 0 7 0.84637 2.79922 4 -4 0 -7-4.24657 7.54884 6 4 0 8 1553.90 76.0856 5 4 0 8 1576.71 71.1742 4 -4 0 -8 1528.05 76.4498 6 4 0 9-1.55578 3.75777 5 4 0 9-1.51644 3.42621 6 4 0 9 0.87737 2.80345 4 -4 0 -9 1.57871 7.00516 6 4 0 10 6.27648 3.59225 4 -4 0 -10 5.05447 8.63285 6 4 0 10-1.60861 4.12176 6 4 0 11 3.38650 5.21369 6 -4 0 -11-3.56377 7.90682 6 4 0 12 3489.31 158.880 3 4 0 12 3572.47 161.453 6 4 0 12 3631.62 154.033 4 4 0 13 1.55125 4.77750 3 4 0 13 1.89557 4.57974 6 4 0 13 3.61759 3.18621 4 4 0 14-2.00117 5.12718 6 4 0 14-3.25572 5.56088 3 4 0 14-0.90787 3.10190 4 4 0 15-2.09865 5.37671 6 4 0 15-0.91169 3.21047 4 4 0 16 2137.83 95.0934 4 4 0 17 2.30790 7.10652 6 4 0 18 883.556 54.7079 6 4 0 19 2.52594 5.70786 6 4 0 20 1112.01 65.4562 6 4 0 21 2.73664 7.75156 6 4 0 22 31.2621 10.3748 6 4 0 23-2.94817 8.35073 6 4 0 24 335.703 32.2850 6 4 0 25-3.15857 8.53042 6 4 0 26 3.26322 8.36090 6 4 0 27-3.36732 9.53798 6 4 0 28 343.803 35.1199 6 4 0 29 3.57700 7.48354 6 4 1 -33 14.8637 19.8361 3 4 1 -32 95.4859 23.1095 3 4 1 -31 28.0863 19.9727 3 4 -1 -31 43.5806 23.1232 3 4 1 -30 257.782 30.1817 3 4 -1 -30 229.474 32.7266 3 4 1 -29 35.9639 12.4857 2 4 1 -29 79.9828 20.6180 3 4 -1 -29 105.447 25.1133 3 4 1 -28 11.6074 9.61312 2 4 -1 -28 12.4624 18.8210 3 4 1 -28 20.7291 17.2904 3 4 1 -27 13.9392 8.62409 2 4 -1 -27 42.5332 19.0828 3 4 1 -27 27.6988 17.3563 3 4 -1 -26 350.318 36.0459 3 4 1 -26 330.496 31.8732 3 4 1 -26 346.247 30.5470 2 4 1 -25-2.56893 6.58154 2 4 -1 -25-5.67532 17.8070 3 4 1 -25 7.02873 14.9722 3 4 -1 -24 33.8289 10.0081 2 4 1 -24 39.8212 10.3017 2 4 -1 -23 169.994 20.1230 2 4 1 -23 188.739 20.9781 2 4 -1 -22 727.938 46.3381 2 4 1 -22 742.422 47.1115 2 4 -1 -21 90.1130 13.6429 2 4 1 -21 137.286 16.5364 2 4 -1 -20 58.0768 11.6001 5 4 -1 -20 52.0429 10.3419 2 4 1 -20 50.6973 10.2745 2 4 -1 -19 154.316 17.5992 5 4 -1 -19 128.598 15.5559 2 4 1 -19 124.484 15.3709 2 4 -1 -18 16.6457 7.37150 5 4 -1 -18 16.4011 6.46824 2 4 1 -18 31.2906 8.55470 2 4 -1 -17 296.322 24.9017 5 4 -1 -17 315.746 24.0068 2 4 1 -17 292.136 24.0086 2 4 -1 -16 535.636 35.0481 5 4 -1 -16 507.864 33.2692 2 4 1 -15 544.256 35.8134 2 4 -1 -15 610.282 37.5605 5 4 -1 -15 554.732 35.1591 2 -4 1 15 626.509 34.9363 5 4 1 -14 710.230 41.9075 2 -4 -1 14 733.458 40.1385 1 4 -1 -14 719.532 42.0107 5 4 -1 -14 683.480 40.1701 2 -4 1 14 684.725 38.7460 5 4 -1 -13 700.924 39.2878 2 4 1 -13 658.111 39.9456 2 -4 -1 13 707.541 39.0400 1 4 -1 -13 662.226 40.2767 5 -4 1 13 716.129 38.2019 5 -4 1 12 1941.00 87.8306 5 4 -1 -12 1807.28 88.7439 2 4 1 -12 1876.66 90.7627 2 -4 -1 12 2011.88 89.3966 1 4 -1 -12 1921.77 91.2937 5 -4 1 11 1893.71 85.8191 5 4 -1 -11 1839.34 86.8032 2 -4 1 11 1800.22 84.1120 1 4 1 -11 1863.93 88.9136 2 -4 -1 11 1985.15 87.5885 1 4 -1 -11 1876.10 88.9373 5 -4 1 10 605.974 33.8242 5 4 -1 -10 601.552 34.2748 2 4 1 -10 641.378 36.3307 2 -4 1 10 574.536 32.1208 1 -4 -1 10 686.534 35.7662 1 4 -1 -10 598.495 35.6566 5 -4 -1 9 156.460 14.9406 1 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49.7741 6 4 1 10 556.546 32.1641 4 4 -1 10 554.865 34.2820 6 -4 -1 -10 566.524 37.3234 6 4 -1 11 6.39735 4.53095 6 4 1 11 4.44330 4.56149 3 4 1 11 1.77837 5.03788 6 -4 -1 -11 7.66305 9.10926 6 4 1 11 1.17835 3.33906 4 4 1 12-1.55241 4.39679 3 4 -1 12 3.40720 5.03954 6 4 1 12-1.86655 4.21716 6 4 -1 12 1.98746 2.59253 4 -4 -1 -12 2.03985 10.1571 6 4 1 12-1.19377 3.22370 4 4 -1 13 103.002 13.2201 6 4 -1 13 72.4222 10.8983 3 4 -1 13 103.086 8.54770 4 4 1 13 107.472 14.0076 6 4 1 13 95.4285 10.6678 4 4 -1 14 1091.96 56.0937 3 4 1 14 1075.95 59.3479 6 4 -1 14 1041.28 58.0052 6 4 1 14 999.786 52.2661 4 4 1 15 2.38630 3.94624 4 4 -1 15-3.24992 5.19212 3 4 -1 15 2.02985 5.74906 6 4 1 15-2.15204 4.86227 6 4 -1 15 2.63286 2.57595 4 4 1 16 293.074 26.1760 6 4 -1 16 311.732 17.8338 4 4 -1 16 320.703 26.5627 6 4 1 17 28.3436 9.49016 6 4 -1 17 8.98635 6.68785 6 4 -1 17 20.0483 4.06629 4 4 1 18 1164.95 67.9944 6 4 -1 18 1253.73 68.8219 6 4 1 19 145.961 19.0225 6 4 -1 19 132.963 17.4937 6 4 -1 20 82.1172 13.9155 6 4 1 21 11.0670 7.49128 6 4 -1 21 16.0266 7.92036 6 4 1 22 74.6973 14.9103 6 4 -1 22 94.4655 15.9282 6 4 1 23 247.606 26.3727 6 4 -1 23 225.079 25.1474 6 4 1 24 49.4980 13.5595 6 4 -1 24 29.9319 11.5356 6 4 1 25-3.19703 8.19035 6 4 -1 25 3.10306 7.94962 6 4 1 26 630.318 48.7184 6 4 -1 26 684.130 49.5119 6 4 1 27 30.7057 13.1583 6 4 -1 27 66.4088 15.8939 6 4 1 28 260.188 29.2186 6 4 -1 28 130.359 22.1144 6 4 -1 29 3.54024 8.55204 6 4 -2 -29 38.4804 22.9762 3 4 2 -29 24.5200 15.9902 3 4 2 -28 397.097 34.3873 3 4 -2 -28 409.421 42.1681 3 4 -2 -27 49.8173 22.6834 3 4 2 -27 80.5845 18.1289 3 4 -2 -26-3.23626 18.7439 3 4 2 -26-2.22979 14.8721 3 4 -2 -25 15.6610 19.1097 3 4 2 -25 12.7689 15.1064 3 4 -2 -24 1124.25 71.1528 3 4 2 -23 182.694 24.8303 5 4 2 -22 127.198 20.5285 5 4 2 -21 30.8434 13.6489 5 4 2 -20 43.1626 14.6959 5 4 -2 -20 25.5032 8.29566 2 4 2 -19 402.328 28.0862 4 4 -2 -19 472.865 32.1138 2 4 2 -19 514.011 36.2952 5 4 -2 -18 31.6495 8.80394 5 4 2 -18 62.1613 14.5810 5 4 -2 -18 35.3548 8.43820 2 4 2 -18 54.0637 10.3798 4 4 -2 -17 15.9100 7.03109 5 4 2 -17 9.98190 9.20268 5 4 -2 -17 16.5843 6.67307 2 4 2 -17 18.4675 8.36906 4 4 2 -16 477.762 29.9310 4 4 -2 -16 492.776 32.2052 2 4 -2 -16 519.052 34.2327 5 4 2 -16 519.052 35.1459 5 -4 2 16 505.577 30.9690 5 4 -2 -15 1.76731 4.53177 5 4 2 -15 3.73011 8.72552 5 -4 2 15 8.24386 8.35616 5 4 -2 -15 11.9164 6.36297 2 4 2 -15 1.18716 7.58890 4 4 2 -14 2747.11 129.154 4 4 -2 -14 2903.32 133.588 5 4 -2 -14 3017.83 131.929 2 4 2 -14 3120.45 135.860 5 -4 2 14 2918.77 129.575 5 4 2 -13 436.145 28.0935 4 4 -2 -13 450.762 30.4503 5 4 -2 -13 503.587 30.1294 2 4 2 -13 521.036 33.7563 5 -4 2 13 463.409 28.2610 5 4 -2 -12 68.9309 10.0340 5 4 2 -12 75.0719 12.6559 5 -4 2 12 101.825 11.6445 5 -4 -2 12 81.1719 10.4588 5 4 -2 -12 75.1291 9.55882 2 -4 -2 12 89.6545 13.0994 1 4 2 -12 77.2619 11.0954 4 -4 2 11-3.29131 5.06708 1 4 -2 -11-1.44250 3.89561 5 4 2 -11-1.57703 6.99780 5 -4 2 11 3.95995 6.65680 5 -4 -2 11 10.5810 5.29778 5 4 -2 -11 1.15781 3.95508 2 4 2 -11 1.14776 6.42729 4 -4 -2 11 8.34859 8.31757 1 4 -2 -10 2392.70 107.184 2 -4 2 10 2318.34 106.097 5 -4 -2 10 2342.84 108.897 5 -4 2 10 2444.69 104.864 1 4 2 -10 2287.05 107.703 4 -4 -2 10 2432.42 109.882 1 4 -2 -10 2425.03 109.966 5 4 2 -10 2625.85 112.639 5 -4 2 9 3024.69 133.555 5 -4 -2 9 3001.86 136.187 5 4 -2 -9 3005.39 133.695 2 -4 2 9 3051.78 131.837 1 4 2 -9 3049.14 135.620 4 -4 -2 9 3126.00 137.168 1 4 -2 -9 3130.13 136.696 5 4 2 -9 3303.33 139.379 5 -4 2 8 142.475 12.7695 5 -4 -2 8 140.830 13.4296 5 4 -2 -8 149.898 12.2626 2 4 -2 -8 144.166 13.2158 5 4 2 -8 179.331 16.6176 5 -4 2 8 138.291 11.3264 1 4 2 -8 119.782 13.4973 4 -4 -2 8 154.853 15.7279 1 -4 2 7 2324.85 104.580 5 -4 -2 7 2318.49 107.433 5 4 -2 -7 2363.84 104.741 2 4 2 -7 2590.03 108.396 4 -4 2 7 2327.66 103.023 1 -4 -2 7 2297.86 108.130 1 4 -2 -7 2414.74 107.256 5 4 2 -7 2477.49 109.483 5 -4 -2 6 3490.13 158.254 1 -4 2 6 3651.02 154.708 5 -4 -2 6 3403.73 157.311 5 4 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1419.80 66.4661 5 4 -2 1 1297.60 59.5757 1 4 2 1 1352.07 65.5586 4 -4 2 -1 1222.60 59.9692 6 4 -2 2 4674.99 193.417 1 4 2 2 4869.31 198.475 5 4 -2 2 4720.22 195.944 5 -4 -2 -2 4495.86 199.757 5 4 2 2 4674.65 199.803 4 -4 2 -2 4174.51 193.862 6 4 2 3 10.2348 6.19167 5 4 -2 3 18.0024 4.80003 5 -4 -2 -3 8.03878 9.31939 6 -4 2 -3 3.63262 5.27338 6 4 2 3 5.79805 4.47897 4 4 2 4 1271.70 60.6572 5 4 -2 4 1179.52 57.9888 5 4 2 4 1313.55 62.0967 4 -4 -2 -4 1069.78 61.5398 6 -4 2 -4 1156.52 57.0759 6 4 2 5 802.850 43.9702 5 4 -2 5 842.892 42.3101 5 4 2 5 815.177 44.7990 4 -4 -2 -5 710.176 45.2873 6 -4 2 -5 789.255 41.4921 6 4 2 6 1447.24 69.1145 5 4 -2 6 1357.26 66.4081 5 4 2 6 1430.67 69.4168 4 -4 -2 -6 1329.39 71.2609 6 -4 2 -6 1363.16 66.3617 6 4 2 7 195.287 18.3112 5 4 -2 7 205.694 16.1882 5 4 2 7 185.297 17.3182 4 -4 -2 -7 176.386 19.5870 6 -4 -2 -8 89.1017 14.9604 6 4 2 8 112.542 13.8321 3 4 2 8 112.242 14.2475 5 4 -2 8 95.7418 11.1262 5 4 -2 8 101.947 10.8583 6 4 2 8 95.2199 12.1457 4 4 2 9 11.5073 8.68917 3 4 -2 9 3.79747 3.59370 6 4 2 9 4.80611 7.86280 5 4 -2 9 5.59613 4.47706 5 -4 -2 -9 9.83066 9.93604 6 4 2 9 8.99183 4.96271 4 4 2 10 248.369 22.0367 3 4 2 10 308.969 24.2913 5 4 -2 10 254.734 19.6969 6 4 2 10 276.114 21.6714 4 -4 -2 -10 251.859 24.4372 6 4 2 11 3.52643 9.75799 5 4 -2 11-1.47944 3.34256 6 4 2 11 2.96068 4.89596 4 4 -2 12 1252.67 64.0443 6 4 2 12 1231.67 62.9763 4 4 -2 13 1201.97 59.3034 3 4 -2 13 1140.82 60.6035 6 4 2 13 1107.81 58.8272 4 4 -2 14 2.91572 5.13380 3 4 -2 14 1.81858 5.15142 6 4 -2 15 290.740 22.0745 3 4 -2 15 265.407 15.0585 4 4 -2 15 303.491 24.5470 6 4 -2 16 882.197 50.7153 3 4 -2 16 1004.11 55.2221 6 4 -2 17 105.659 14.8970 6 4 -2 18 29.4690 9.15837 6 4 -2 19 49.9811 11.4974 6 4 -2 20 651.406 44.3303 6 4 -2 21 10.4472 8.05279 6 4 -2 22 262.008 26.6672 6 4 -2 23 54.0629 12.8159 6 4 -2 24 181.116 22.8820 6 4 -2 25 24.7008 11.5367 6 4 -2 26 109.069 18.9046 6 4 -2 27 252.891 29.2706 6 4 -2 28 172.032 24.7003 6 4 -2 29 10.6864 11.3900 6 4 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1579.92 78.7001 1 -4 3 7 1680.81 73.6776 5 -4 -3 7 1556.99 77.5478 5 -4 3 7 1620.45 71.1630 1 4 3 -7 1638.63 79.8357 4 4 -3 -7 1621.15 72.4876 2 4 -3 -7 1673.01 75.7529 5 4 3 -7 1562.46 78.0669 5 4 -3 -6 51.7241 7.46396 5 4 3 -6 83.9622 11.4906 5 -4 -3 6 45.1319 8.47465 5 -4 3 6 56.3401 8.18380 5 4 -3 -6 53.6052 6.07648 2 4 3 -6 54.3667 11.7774 4 4 -3 -5 1304.54 59.7314 2 -4 -3 5 1286.58 66.1234 5 -4 3 5 1346.07 61.8201 5 4 3 -5 1383.81 67.6556 1 4 3 -5 1399.24 69.3844 4 4 -3 -5 1365.01 63.4460 5 4 3 -5 1387.82 66.6623 5 -4 -3 4 153.246 14.3742 5 -4 3 4 145.934 12.1347 5 4 3 -4 167.715 17.2498 4 4 3 -4 122.402 13.6395 5 4 3 -4 152.980 15.7996 1 4 -3 -4 138.957 9.86969 2 4 -3 -4 141.396 11.8899 5 4 3 -3 734.193 41.8601 5 -4 -3 3 761.902 43.0315 5 -4 3 3 786.289 38.6756 5 4 -3 -3 764.690 35.9668 2 4 3 -3 800.893 43.9136 1 4 3 -3 815.540 45.9787 4 4 -3 -3 796.264 39.4607 5 4 -3 -2-0.47249 1.84926 2 4 -3 -2 2.68198 2.53220 5 4 3 -2-5.11707 5.88298 5 -4 -3 2 2.93013 3.31023 5 -4 3 2 2.45664 5.04269 5 -4 3 2 2.64157 3.40628 6 4 3 -2 11.4870 8.22542 1 4 -3 -1 909.743 45.2422 5 4 3 -1 881.277 48.2089 5 -4 -3 1 888.946 49.5514 5 4 3 -1 931.356 49.9765 1 -4 3 1 983.750 43.2991 6 4 -3 0 16.2020 4.00057 5 4 3 0 11.4309 6.28198 5 -4 -3 0 46.8198 8.36139 5 -4 3 0 12.5450 4.28242 6 4 3 0 53.5787 10.3770 1 4 3 0 27.4874 7.52340 4 4 -3 1 26.3591 4.96044 5 4 3 1 8.91603 6.56490 5 4 -3 1 16.4623 3.03618 1 4 3 1 8.65314 7.91790 1 4 3 1 13.9344 5.99211 4 -4 3 -1 13.5184 4.62152 6 4 3 2 515.125 33.1715 1 4 -3 2 511.064 29.0858 5 4 3 2 527.068 32.1975 5 4 -3 2 543.488 26.5575 1 -4 -3 -2 592.566 36.3614 6 4 3 2 568.700 35.7436 4 -4 3 -2 540.091 28.1977 6 4 3 3 437.247 28.3076 5 4 -3 3 437.738 25.6159 5 -4 -3 -3 457.264 31.4090 6 4 3 3 467.587 31.4781 4 4 -3 3 444.155 23.0071 1 4 3 4 974.659 49.7709 5 4 -3 4 906.096 46.0755 5 -4 -3 -4 883.089 52.2262 6 4 3 4 971.364 52.9391 4 4 3 5 1220.37 61.9532 5 4 -3 5 1206.45 58.8855 5 -4 -3 -5 1309.97 66.9308 6 4 3 5 1207.53 65.0742 4 4 3 6 1986.22 87.6087 3 4 3 6 1761.18 86.4342 5 4 -3 6 1789.27 83.5079 5 -4 -3 -6 1856.10 84.6826 4 -4 -3 -6 1789.82 90.9264 6 4 3 6 1741.35 89.2662 4 4 3 7 476.011 29.8673 3 4 3 7 451.214 28.9942 5 4 -3 7 384.121 25.3008 5 -4 -3 -7 453.862 27.1489 4 -4 -3 -7 400.292 31.1660 6 4 3 7 379.960 29.4175 4 4 3 8 339.566 25.7210 3 4 3 8 358.884 26.0597 5 4 -3 8 344.858 23.0761 5 -4 -3 -8 384.038 24.0909 4 4 -3 8 351.268 21.8463 6 4 3 8 336.633 26.2734 4 4 3 9 531.669 32.7681 3 4 3 9 465.346 31.4532 5 4 -3 9 423.098 28.2163 5 -4 -3 -9 522.949 29.5140 4 4 -3 9 451.917 27.2698 6 4 3 9 404.854 30.8454 4 4 3 10 1409.31 73.6650 5 -4 -3 -10 1488.79 70.3642 4 4 -3 10 1462.25 70.2989 6 4 3 10 1518.64 75.6273 4 4 3 11 83.6667 14.6242 5 4 -3 11 103.998 11.5478 6 -4 -3 -11 108.635 13.0352 4 4 3 12 151.129 18.7050 5 -4 -3 -12 216.902 17.7469 4 4 -3 13 151.375 14.5752 3 4 3 13 158.588 19.1718 5 -4 -3 -13 194.339 16.7176 4 4 -3 13 161.479 15.1421 2 4 -3 13 144.786 15.2448 6 4 -3 14 1815.71 89.5739 3 4 3 14 1853.68 95.3446 5 -4 -3 -14 2042.64 89.5127 4 4 -3 14 1929.21 92.8594 6 4 -3 14 1946.41 90.9488 2 4 -3 15 13.4040 6.11919 2 4 -3 15 11.1285 6.07701 3 -4 -3 -15 22.4348 9.47169 4 4 -3 15 7.27320 6.23036 6 4 -3 16 143.353 15.4267 3 4 3 16 143.480 20.9321 6 -4 -3 -16 189.019 16.5702 4 4 -3 16 178.405 18.5413 6 4 -3 16 192.760 17.4790 2 4 3 17 45.7456 15.6131 6 4 -3 17 38.4610 8.77685 3 -4 -3 -17 35.3793 10.3576 4 4 -3 17 49.4537 10.5445 6 4 -3 18 1705.99 85.4532 3 -4 -3 -18 1793.53 82.7492 4 4 3 18 1924.42 94.6412 6 4 -3 18 1648.75 89.1748 6 4 3 19 147.596 22.7452 6 -4 -3 -19 169.613 16.8652 4 4 -3 19 189.805 20.8507 6 4 3 20 64.3321 18.1728 6 4 -3 20 53.8218 12.4013 6 4 3 21 133.226 21.9758 6 4 -3 21 105.571 17.3984 6 4 3 22 189.585 26.0641 6 4 -3 22 189.830 22.7030 6 4 3 23 225.991 28.1689 6 4 -3 23 164.960 22.3796 6 4 -3 24-2.98465 8.83082 6 4 3 24-15.4052 16.4318 6 4 3 25 188.157 26.9878 6 4 -3 25 152.932 22.0553 6 4 -3 26 65.1791 15.2561 6 4 3 26 82.1943 23.4955 6 4 -3 27 10.1742 11.2240 6 4 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876.170 47.4305 1 4 -4 -3 836.703 41.2765 5 4 4 -2 357.203 25.3468 5 -4 -4 2 397.022 27.3609 5 4 4 -2 373.283 26.7169 1 4 4 -1 92.2415 12.6252 5 -4 -4 1 94.9566 12.5989 5 4 -4 -1 99.1356 8.73051 5 4 4 -1 89.0371 13.4171 1 4 4 0 120.545 14.9385 1 4 4 0 144.762 14.9988 5 -4 -4 0 147.369 15.7304 5 4 -4 0 148.267 11.0845 5 4 -4 1 133.833 10.6340 5 4 4 1 121.528 14.3655 5 -4 -4 -1 165.026 16.5377 4 4 4 1 135.585 15.9351 1 4 -4 2 1426.86 64.4030 5 4 4 2 1293.82 68.3351 5 -4 -4 -2 1394.84 69.7036 4 4 4 2 1344.03 70.2184 1 4 -4 3 11.3142 1.94595 1 4 4 3 17.6544 10.2460 3 4 -4 3 4.94074 3.52744 5 4 4 3 12.0956 7.70401 5 4 -4 3 4.16793 1.55054 2 4 4 3 4.75059 7.41205 1 -4 -4 -3 12.6274 8.89010 4 4 4 4 7.02815 9.06417 3 4 -4 4 5.51240 2.04207 1 4 -4 4 4.33600 3.05886 5 4 4 4 8.22324 7.85321 5 4 -4 4 3.15868 1.92783 2 -4 -4 -4 8.50595 8.30152 4 4 4 5 1113.28 58.2535 3 4 4 5 1102.49 57.1303 5 4 -4 5 1056.65 52.3102 5 -4 -4 -5 1156.38 57.8684 4 4 4 6 1081.29 55.2700 3 4 4 6 967.457 53.2955 5 4 -4 6 1012.87 49.6672 5 4 4 7 511.040 33.7625 5 4 4 7 597.949 36.2772 3 4 -4 7 542.402 30.7390 5 -4 -4 -7 586.813 35.1373 4 4 -4 8 5.83231 3.42142 2 4 4 8 18.5933 9.90545 5 4 -4 8 4.39418 4.40900 5 -4 -4 -8 16.1225 9.53613 4 4 4 9 1397.39 71.2317 5 4 -4 9 1389.65 67.4045 5 -4 -4 -9 1435.60 70.9911 4 4 -4 9 1396.14 65.2368 6 4 -4 9 1426.85 64.7621 2 4 4 10 525.178 35.3925 5 4 -4 10 557.841 32.8493 5 -4 -4 -10 599.079 35.8385 4 4 -4 10 569.266 31.3247 6 4 -4 10 559.093 30.4217 2 4 4 11 376.740 28.9528 5 -4 -4 -11 398.081 28.6336 4 4 -4 11 416.126 25.3238 6 4 -4 11 386.993 23.8649 2 4 -4 12 53.5935 8.06524 2 4 4 12 69.2900 13.6957 5 4 -4 12 62.6863 8.92881 6 -4 -4 -12 55.8213 12.1166 4 4 -4 13 273.745 19.5464 3 4 4 13 296.906 25.6370 5 -4 -4 -13 254.670 22.7022 4 4 -4 13 275.699 20.8619 6 4 -4 13 270.060 19.7042 2 4 4 14-1.94772 11.1578 5 4 -4 14-3.09958 4.95268 6 -4 -4 -14 6.08720 10.1501 4 4 -4 15 16.8630 6.79246 6 4 4 15 8.10359 10.9652 5 -4 -4 -15 30.5116 11.4543 4 4 4 16 105.492 18.1172 5 4 -4 16 112.971 14.6956 6 -4 -4 -16 108.568 15.0955 4 4 4 17 608.067 41.9968 5 4 -4 17 615.154 38.9508 6 -4 -4 -17 578.346 37.3278 4 4 4 18 149.928 21.4214 5 -4 -4 -18 152.011 18.1256 4 4 -4 18 130.386 16.7925 6 -4 -4 -19 446.384 31.2660 4 4 -4 19 427.097 33.1371 6 4 4 20 188.600 25.1916 6 -4 -4 -20 156.938 19.0321 4 4 -4 20 144.026 19.3308 6 4 4 21 72.3433 19.1992 6 -4 -4 -21 66.0093 14.2336 4 4 -4 21 63.9043 13.1931 6 4 4 22 367.980 35.3180 6 4 -4 22 306.147 29.4235 6 4 4 23 134.055 23.9049 6 4 -4 23 77.5364 16.1699 6 4 4 24 52.3491 20.2067 6 4 -4 24 6.06596 9.35626 6 4 -4 25 9.58779 11.5854 6 4 4 25 9.51260 18.7639 6 4 5 -25 239.840 29.4006 2 4 5 -24 15.9088 16.0233 2 4 -5 -24 15.7749 11.1880 3 4 5 -23 207.462 26.8829 2 4 -5 -23 141.900 23.9529 3 4 5 -22 108.716 21.4026 5 4 5 -22 82.6829 21.1815 2 4 -5 -22 127.016 22.5129 3 4 5 -21-9.98669 14.4602 5 4 5 -21 4.86211 15.9461 2 4 -5 -21 7.26501 8.77387 3 4 5 -20 140.329 21.7947 5 4 5 -20 130.183 22.3301 2 4 -5 -20 159.060 23.7072 3 4 5 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15.3252 2 5 -3 -8 990.523 47.1599 2 -5 3 8 923.495 47.6593 5 5 3 -8 897.943 52.1884 5 -5 3 7 426.616 27.7248 5 5 -3 -7 529.571 30.6027 5 5 3 -7 500.323 32.9624 5 5 -3 -6 164.509 12.4415 2 5 3 -6 162.671 17.6971 5 -5 3 6 160.363 14.7398 5 5 -3 -6 148.532 14.1765 5 5 -3 -5 5.11322 4.22869 5 5 3 -5 1.63150 8.24285 5 -5 3 5 3.17838 6.39797 5 5 -3 -5 0.80830 2.76240 2 5 -3 -4 9.30648 3.45610 2 5 -3 -4 11.1910 4.38975 5 5 3 -4-1.60110 9.95889 5 -5 3 4 2.12445 6.61142 5 5 3 -3 252.195 22.4656 5 -5 3 3 268.269 19.8816 5 5 -3 -3 289.630 17.1890 2 -5 3 3 285.855 18.1224 6 5 -3 -3 281.099 19.8317 5 5 3 -2 374.064 27.9101 5 -5 3 2 393.283 25.3903 5 -5 3 2 363.139 23.0589 6 5 -3 -1 330.885 22.0273 5 5 3 -1 320.856 25.3093 5 -5 3 1 325.032 20.6013 6 5 3 0 157.422 17.9068 5 -5 3 0 176.439 14.7478 6 5 -3 1 163.896 14.1485 5 5 -3 1 148.212 11.3400 1 5 3 1 120.833 16.1419 5 -5 3 -1 165.978 14.0134 6 5 -3 2 2473.25 110.377 5 5 3 2 2417.72 113.472 5 5 -3 2 2390.39 106.332 1 -5 3 -2 2516.91 109.386 6 5 -3 3 222.183 18.0857 5 5 3 3 250.379 21.8640 5 5 -3 3 250.660 16.3220 1 -5 3 -3 271.883 19.4339 6 5 3 4 336.573 26.3953 5 5 -3 4 343.398 23.4937 5 5 -3 4 371.469 21.3845 1 5 -3 5 212.237 17.3112 5 5 3 5 222.580 20.6947 5 5 3 6 2814.14 126.193 5 5 -3 6 2652.75 122.192 5 5 3 7 6.91391 8.60743 5 5 -3 7 1.39585 5.19704 5 5 3 8 1320.52 68.7391 5 5 -3 8 1304.97 65.3247 5 5 3 9 1074.07 58.8895 5 5 -3 9 1043.17 55.1699 5 5 3 10 126.631 17.8479 5 5 -3 10 144.775 14.9053 5 5 3 11 90.6363 16.6853 5 5 -3 11 54.1310 9.84252 5 5 3 12 871.753 51.2623 5 5 -3 12 809.962 47.1637 5 5 3 13 630.573 40.7776 5 5 -3 13 505.007 35.0623 5 5 -3 13 558.276 34.7961 6 5 3 14 57.2779 14.9302 5 5 -3 14 74.1345 12.0019 5 5 -3 14 61.8960 10.9143 6 5 3 15 25.2547 13.7553 5 5 -3 15 21.9763 8.17907 6 5 3 16 436.335 36.0183 5 5 -3 16 445.604 31.7097 6 5 3 17 501.426 40.0391 5 5 -3 17 556.566 37.1146 6 5 3 18 87.0360 19.0973 5 5 -3 18 79.1129 14.0620 6 5 3 19 140.602 22.8576 5 5 -3 19 130.534 17.5255 6 5 3 20 186.086 25.9924 5 5 -3 20 189.295 21.6421 6 5 3 21 202.801 27.2739 5 5 -3 21 214.614 23.6707 6 5 -3 23 125.576 18.9401 6 5 -3 24 11.9767 9.91465 6 5 -3 25 78.2268 16.1253 6 5 -3 26 3.27711 9.28246 6 5 -3 27 321.192 34.0352 6 5 -3 28-3.55892 10.0807 6 5 4 -25 104.667 23.0114 5 5 4 -24 2.96490 16.2125 5 5 4 -24-8.71229 16.4507 2 5 -4 -24-3.97183 8.97481 3 5 4 -23 290.642 31.0326 5 5 4 -23 279.400 30.4697 2 5 -4 -23 228.167 29.8441 3 5 4 -22 8.24333 15.2072 5 5 4 -22-2.72805 15.8006 2 5 4 -21 311.874 30.5255 5 5 4 -21 190.817 26.3496 2 5 4 -20 165.411 23.4646 5 5 4 -19 246.719 27.1417 5 5 4 -19 295.561 29.3585 2 5 4 -18 73.9014 17.1975 5 5 4 -18 116.691 20.1527 2 5 4 -17 411.783 34.4078 2 5 4 -17 383.611 33.1136 5 5 4 -16 15.9449 12.9152 5 5 4 -16 11.5484 14.3701 2 5 4 -15 608.387 41.7251 2 5 -4 -15 588.968 38.1415 5 5 4 -15 547.093 40.0680 5 5 4 -14 8.80923 11.9060 2 5 -4 -14 12.9510 7.08525 5 5 4 -14 17.0780 11.8259 5 5 4 -13 12.8470 12.2817 2 5 -4 -13 12.1690 6.32970 5 5 4 -13 32.6986 13.0749 5 5 -4 -12 18.0497 6.13291 5 5 4 -12 21.9295 11.8077 5 5 -4 -11 7.73593 5.29422 5 5 4 -10 200.516 20.5339 5 -5 4 10 160.221 15.1493 5 5 -4 -10 188.935 16.5922 5 5 -4 -9 33.7917 7.66831 5 5 4 -9 52.7341 12.8618 5 5 -4 -9 51.9594 6.40977 2 -5 4 9 61.7947 9.98915 5 -5 4 8 338.162 21.5079 5 5 -4 -8 281.225 17.3702 2 5 -4 -8 298.805 21.6203 5 -5 4 7 495.094 27.9988 5 5 -4 -7 439.678 23.8272 2 5 -4 -7 489.303 29.1152 5 -5 4 6 526.332 29.0941 5 5 -4 -6 449.019 24.2840 2 5 -4 -6 513.540 29.8754 5 5 4 -6 568.313 35.1163 5 -5 4 5 1141.88 54.4439 5 5 4 -5 1194.12 61.2608 1 5 -4 -5 1076.40 49.1788 2 5 -4 -5 1098.96 55.0114 5 5 4 -5 1089.70 58.9436 5 -5 4 4 454.593 27.0756 5 5 4 -4 482.433 32.9339 1 5 -4 -4 441.594 21.7940 2 5 -4 -4 454.226 27.0988 5 5 4 -4 409.583 30.3152 5 5 4 -3 246.131 21.5846 5 5 4 -3 275.394 24.0121 1 5 -4 -3 229.878 12.7556 2 5 -4 -2 263.688 14.0490 2 5 4 -2 267.519 23.0620 5 5 4 -2 278.013 24.6319 1 5 -4 -2 302.362 19.5227 5 5 4 -1 382.983 27.5038 5 5 -4 -1 337.221 17.0007 2 5 4 -1 324.498 26.8863 1 5 -4 -1 354.832 22.2226 5 5 -4 0 1126.73 54.4907 5 5 4 0 1182.53 59.8274 5 5 -4 0 1076.50 48.4651 2 5 4 0 1203.22 61.3693 1 5 -4 1 183.756 14.4429 5 5 4 1 156.711 17.6125 5 5 4 1 170.548 19.5068 1 5 -4 2 6.58986 4.30491 5 5 4 2 1.61565 9.25836 5 5 4 2 9.20683 10.3140 1 5 -4 3 354.283 21.7404 5 5 4 3 291.194 24.6572 5 5 -4 3 298.579 16.6627 1 5 4 3 337.332 27.4481 1 5 -4 4 1647.68 76.2481 5 5 4 4 1687.62 81.1450 5 5 -4 4 1588.82 71.1961 1 5 4 4 1664.08 82.5815 1 5 -4 5 23.4868 6.46797 5 5 4 5 10.0619 10.3559 5 5 4 5 22.7728 11.9339 1 5 -4 5 18.2295 4.26862 1 5 -4 6 339.034 19.8731 1 5 4 6 345.299 26.9722 5 5 -4 6 392.157 24.4493 5 5 4 7 1643.80 81.3668 5 5 -4 7 1587.44 76.2125 5 5 4 8 132.259 17.7089 5 5 -4 8 142.128 14.0423 5 5 4 9 18.4012 10.8948 5 5 -4 9 8.28265 5.41822 5 5 4 10 471.873 33.3140 5 5 -4 10 413.691 28.1785 5 5 4 11 1389.12 72.7494 5 5 -4 11 1341.19 68.1625 5 5 4 12 14.2653 12.3297 5 5 -4 12 20.5467 7.05561 5 5 4 13 12.5605 12.1299 5 5 -4 13 6.72536 6.43118 5 5 -4 13 9.77528 5.60508 6 5 4 14 487.351 35.7768 5 5 -4 14 457.028 31.6315 5 5 -4 14 468.813 30.3914 6 5 4 15 201.323 24.5783 5 5 -4 15 197.380 19.7054 5 5 -4 15 220.773 19.2285 6 5 4 16 251.495 25.9967 5 5 -4 16 183.816 20.2294 5 5 -4 16 202.889 19.5818 6 5 4 17 7.19768 13.7470 5 5 4 18 94.8092 20.4666 5 5 4 19 333.009 32.3815 5 5 4 20 45.2944 17.8655 5 5 4 21 154.058 25.4238 5 5 4 22 156.142 25.1785 5 5 4 23 5.88091 16.2748 5 5 5 -24-3.01586 16.6909 5 5 5 -23 14.4884 15.8553 5 5 5 -22 16.7509 17.3563 5 5 5 -22 8.27989 16.9956 2 5 -5 -22-4.07394 11.5383 3 5 5 -21 307.442 30.9833 5 5 5 -21 292.060 30.2374 2 5 -5 -21 281.031 33.2098 3 5 5 -20 5.19533 14.7158 5 5 5 -19 2.50524 15.1274 5 5 5 -19-2.53406 14.6766 2 5 5 -18 21.9370 14.2697 5 5 5 -18-14.9130 15.1576 2 5 5 -17 232.668 25.4735 5 5 5 -17 300.800 29.0293 2 5 5 -16-4.62462 12.6451 5 5 5 -16 16.5975 14.0294 2 5 5 -15 31.6451 14.3585 5 5 5 -15 23.2464 14.3583 2 5 5 -14 97.2956 18.5293 2 5 5 -14 91.9671 17.8601 5 5 5 -13 563.521 40.7657 2 5 5 -13 599.433 40.5862 5 5 5 -12 64.4284 16.8376 2 5 5 -12 71.4077 15.3416 5 5 5 -11 9.97808 11.5652 5 5 5 -9 897.242 52.1171 5 5 5 -8 203.733 21.5458 5 5 5 -6 43.8756 12.6654 5 5 -5 -5 1111.71 53.2578 5 5 5 -5 1046.94 58.9557 5 5 5 -4 230.119 22.8186 1 5 5 -4 204.626 21.5519 5 5 -5 -4 259.261 17.2669 5 5 5 -3 218.702 21.9439 1 5 5 -3 167.193 19.9818 5 5 -5 -3 228.974 15.8869 5 5 5 -2 123.711 17.2157 5 5 5 -2 141.026 18.6720 1 5 -5 -2 150.876 12.2771 5 5 5 -1 1726.43 91.2571 5 5 5 -1 2013.87 94.9227 1 5 -5 -1 1959.19 85.7464 5 5 -5 0 21.0006 5.34351 5 5 5 0 13.3308 10.1933 5 5 5 0 21.1709 12.2148 1 5 5 1 310.108 25.4975 5 5 5 1 310.711 26.5400 1 5 -5 1 272.656 18.2999 5 5 5 2 133.302 18.3693 1 5 5 2 101.295 16.5441 5 5 -5 2 134.623 11.5811 5 5 -5 3 160.949 13.0823 5 5 5 3 169.500 19.2427 5 5 5 3 176.866 20.9094 1 5 5 4 3.98828 11.2989 1 5 -5 4 6.80149 4.62758 5 5 5 4 8.51943 10.2921 5 5 -5 5 207.339 15.7714 5 5 5 5 248.170 22.6732 5 5 5 5 230.260 23.5987 1 5 -5 6 275.311 19.0668 5 5 5 6 295.992 24.9788 5 -5 -5 -6 285.019 25.2237 4 5 5 6 293.927 26.5913 1 5 -5 7 7.72800 4.72536 5 5 5 7 7.14739 10.3542 5 -5 -5 -7 12.2348 11.9450 4 5 5 8 629.205 41.1193 5 5 -5 8 640.468 36.2272 5 -5 -5 -8 722.047 42.8025 4 5 5 9 609.367 40.6520 5 -5 -5 -9 659.523 41.2742 4 5 5 10 11.4345 10.5661 5 -5 -5 -10 21.2567 12.1182 4 5 5 11 43.0773 13.8553 5 -5 -5 -11 63.9651 14.5549 4 5 5 12 183.911 21.6110 5 -5 -5 -12 211.920 21.4031 4 5 5 13 119.608 18.8053 5 -5 -5 -13 115.983 17.4978 4 5 5 14-2.15359 12.3367 5 -5 -5 -14 1.78661 12.0131 4 5 5 15 190.810 22.4437 5 -5 -5 -15 196.618 21.7843 4 5 5 16 116.171 19.3348 5 -5 -5 -16 114.236 18.5087 4 5 5 17 79.4834 19.3659 5 -5 -5 -17 65.9772 15.5005 4 5 5 18 38.5050 16.4834 5 -5 -5 -18 21.3315 15.1505 4 5 5 19 265.972 29.1157 5 -5 -5 -19 284.918 25.8909 4 5 5 20 28.1392 16.5322 5 5 5 21 36.9234 18.0800 5 5 5 22 2.72367 16.7725 5 5 6 -22 37.7156 18.7673 5 5 6 -21 114.315 22.8144 5 5 6 -20 16.2150 18.1836 5 5 6 -19 294.593 29.9368 5 5 -6 -19 234.108 32.1693 3 5 6 -19 237.649 28.1825 2 5 6 -18 7.55532 16.1153 5 5 -6 -18 31.2138 14.5472 3 5 6 -18 20.2882 15.6389 2 5 6 -17 63.7240 17.5658 5 5 6 -17 102.021 19.9747 2 5 6 -16 64.1192 17.7023 5 5 6 -16 46.0814 16.7170 2 5 6 -15 386.601 33.9021 2 5 6 -15 344.199 31.9337 5 5 6 -14 13.7122 13.6679 5 5 6 -14 7.01982 14.8252 2 5 6 -13 2.29750 13.3105 2 5 6 -13 15.5800 14.3532 5 5 6 -12 80.4912 18.1400 2 5 6 -12 88.6048 17.0638 5 5 6 -11 165.663 21.8571 2 5 6 -11 139.563 19.3973 5 5 6 -10-4.08345 13.5063 5 5 6 -9 135.512 18.9879 5 5 6 -8 9.70613 11.9604 5 5 6 -7 706.386 44.0550 5 5 6 -6 11.1630 10.7851 5 5 6 -5 142.240 17.9463 5 5 6 -4 5.39640 9.95734 5 5 6 -3 321.048 27.8569 1 5 6 -3 311.786 26.0610 5 5 6 -2 52.3393 14.2454 1 5 6 -2 56.7520 13.7270 5 5 6 -1 382.423 30.8896 1 5 6 -1 384.630 29.0327 5 5 6 0-5.26402 10.5954 5 5 6 0 12.3155 12.0167 1 5 6 1 177.920 19.5380 5 5 6 1 165.093 21.4970 1 5 6 2 58.4451 14.0530 5 -5 -6 -2 98.9136 17.9617 4 5 6 2 56.2783 15.7614 1 5 6 3 516.986 36.4349 5 -5 -6 -3 569.062 39.3700 4 5 6 3 552.730 39.0702 1 5 6 4 18.0943 11.4939 5 5 6 4 15.0341 13.3818 1 -5 -6 -4 34.7933 13.7906 4 5 6 5 1.82336 11.5499 5 5 6 5 2.17961 12.0648 1 -5 -6 -5 18.5420 14.4027 4 5 6 6 114.414 18.8628 1 5 6 6 130.513 17.9769 5 -5 -6 -6 145.229 21.3159 4 5 6 7 965.583 57.8897 5 -5 -6 -7 1177.72 63.5707 4 5 6 7 1095.57 62.3361 1 5 6 8 22.7582 14.1313 1 5 6 8 71.7671 15.5753 5 -5 -6 -8 44.0351 16.4143 4 5 6 9 15.4198 12.3233 5 -5 -6 -9 4.21721 14.7439 4 5 6 9 6.94509 13.2672 1 5 6 10 80.4822 15.5969 5 -5 -6 -10 73.9922 18.9410 4 5 6 11 726.512 47.7534 5 -5 -6 -11 843.050 50.9845 4 5 6 12 106.481 18.2557 5 -5 -6 -12 123.085 20.7820 4 5 6 13 73.1521 16.6982 5 -5 -6 -13 65.8644 18.0022 4 5 6 14 10.6994 12.5322 5 -5 -6 -14 4.24907 15.0740 4 5 6 15 92.2128 18.7132 5 -5 -6 -15 131.654 21.3024 4 5 6 16 4.51907 13.9195 5 -5 -6 -16 16.9707 15.5882 4 5 6 17 25.6845 17.6129 5 -5 -6 -17-2.11234 16.8281 4 5 6 18 14.3212 14.9868 5 -5 -6 -18 10.5311 15.8929 4 5 6 19 142.061 23.8985 5 -5 -6 -19 211.456 25.2087 4 5 6 20 20.0946 15.7834 5 5 -7 -17 166.857 26.4249 3 5 -7 -16 7.92919 11.7289 3 5 7 -16-2.51023 16.3259 2 5 -7 -15 15.3002 12.2606 3 5 7 -15 44.3023 18.7064 2 5 -7 -14 47.9188 16.4143 3 5 7 -14 19.4360 16.7835 2 5 7 -13 143.091 22.6686 2 5 -7 -13 156.538 24.3042 3 5 7 -12 23.5874 15.7496 2 5 7 -12 13.8493 14.9003 5 5 7 -11-9.19586 14.5629 2 5 7 -11 31.4954 14.1207 5 5 7 -10 45.0411 16.7133 2 5 7 -10 72.5422 17.1640 5 5 7 -9 295.245 27.6786 5 5 7 -7 77.9380 16.1739 5 5 7 -6 42.2183 14.4659 5 5 7 -5 302.406 27.6896 5 5 7 -4 5.84358 11.1607 5 5 7 -3 257.255 24.1367 5 5 7 -2 7.62075 11.6227 5 5 7 -1 257.565 26.4784 1 5 7 -1 320.227 27.0027 5 5 7 0 15.3065 12.9558 1 5 7 0 18.9749 12.5707 5 5 7 1 373.849 32.2345 1 5 7 1 423.396 31.0475 5 5 7 2 68.3590 15.7325 5 5 7 2 47.2886 14.8351 1 -5 -7 -2 61.5504 19.2180 4 5 7 3 78.2426 15.6732 5 5 7 3 54.6262 16.9956 1 -5 -7 -3 97.7581 19.9747 4 5 7 4 148.171 19.7609 5 -5 -7 -4 108.019 20.9508 4 5 7 4 156.546 21.6351 1 5 7 5 442.163 33.1943 5 -5 -7 -5 437.871 37.5318 4 5 7 5 430.104 35.3072 1 5 7 6 47.8021 15.7253 1 5 7 6 19.7621 13.1293 5 -5 -7 -6 26.7904 17.4438 4 5 7 7 25.9817 13.7813 5 5 7 7 4.87139 15.7221 1 -5 -7 -7 34.2678 18.3576 4 5 7 8 72.6526 17.1066 5 5 7 8 59.1337 18.1446 1 -5 -7 -9 424.361 36.5104 4 5 7 9 413.021 35.4114 1 5 7 10 25.4026 16.5843 1 -5 -7 -10 51.8991 20.7289 4 5 7 11-5.17569 15.4724 1 -5 -7 -11 32.1829 18.9112 4 5 7 12 105.140 20.3307 1 -5 -7 -12 86.8018 20.7952 4 -5 -7 -13 114.047 22.2861 4 5 8 -10 16.9724 16.3178 2 5 8 -9 45.1825 17.4475 2 5 8 1 140.709 22.1136 1 5 8 2-16.9520 16.0336 1 5 8 3 31.9415 15.3302 1 5 8 4 142.929 23.0002 1 5 8 5 63.7335 18.2685 1 5 8 6 31.0719 17.4564 1 5 8 7 49.9234 18.2036 1 5 8 8-2.68342 14.6731 1 6 0 -27 3.12899 9.63483 2 6 0 -26 194.029 23.7698 2 6 0 -25 3.46686 7.83405 5 6 0 -24 788.757 54.4258 5 6 0 -24 722.071 50.7467 2 6 0 -23 6.39353 8.19828 5 6 0 -23 13.8295 10.3023 2 6 0 -22 83.0680 16.1088 5 6 0 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4.95550 15.2591 5 6 7 -12 13.0237 18.0781 5 6 7 -11 145.444 24.7843 5 6 7 -10 12.3997 15.7137 5 6 7 -8 12.0157 14.2261 5 6 7 -7 342.080 31.5803 5 6 7 -6 11.6218 16.6135 5 6 7 -5 110.004 21.0987 5 6 7 -4 13.5400 15.1838 5 6 7 -3 328.761 30.9162 5 6 7 -2-2.21859 15.5079 5 6 7 -1 43.7541 16.4886 1 6 7 -1 66.2519 18.8896 5 6 7 0 56.2982 17.4272 1 6 7 0 70.6398 18.1653 5 6 7 1 196.172 24.8224 5 6 7 1 162.902 23.6491 1 6 7 2 17.6038 13.8184 5 6 7 2 7.49444 14.9423 1 6 7 3 158.424 21.9556 5 6 7 3 126.634 22.0772 1 6 7 4-13.2825 14.6473 5 6 7 4-2.55561 16.7666 1 6 7 5 44.5687 16.2305 5 6 7 5 36.1397 16.2819 1 6 7 6-2.62832 15.0565 1 6 7 6-2.25051 14.6364 5 6 7 7 136.586 20.7714 5 7 0 -25 6.36218 9.41372 2 7 0 -24 118.059 19.3650 2 7 0 -23-3.53899 7.99574 5 7 0 -23 3.00245 7.25189 2 7 0 -22 41.0264 12.8259 5 7 0 -22 37.7670 12.0046 2 7 0 -21-6.65781 9.84963 5 7 0 -21-2.85501 6.89893 2 7 0 -20 109.676 18.5752 5 7 0 -20 103.662 17.3478 2 7 0 -19 3.15608 7.62382 5 7 0 -19 2.60642 7.71105 2 7 0 -18 92.9665 17.1586 5 7 0 -17-3.01434 9.28108 5 7 0 -17 4.93667 7.59997 2 7 0 -16-5.84347 7.05730 5 7 0 -16 2.41557 6.18872 2 7 0 -15-8.44740 8.67171 5 7 0 -15 7.03568 7.22323 2 7 0 -14 41.1686 11.7796 5 7 0 -14 22.9093 8.83062 2 7 0 -13 2.66943 6.03112 5 7 0 -13-2.23716 6.04127 2 7 0 -12 41.4643 10.3378 2 7 0 -12 38.8772 10.9657 5 7 0 -11-2.11098 5.70287 2 7 0 -11-5.03366 7.13009 5 7 0 -10 303.667 27.0979 5 7 0 -9-2.38008 6.74161 5 7 0 -7 9.10335 5.15519 5 7 0 -6 1639.73 85.1660 5 7 0 -5 22.0225 7.33846 5 7 0 -4 1315.43 71.3671 5 7 0 -3 1.85412 5.00789 1 7 0 -3 4.27516 7.74507 5 7 0 -2 180.209 19.3574 5 7 0 -2 159.523 17.1121 1 7 0 -1-4.22652 5.98537 5 7 0 -1 7.48391 5.97825 1 7 0 0 2091.04 101.545 5 7 0 0 1999.40 98.5705 1 7 0 1 11.3247 7.04224 1 7 0 1 12.6197 7.84393 5 7 0 2 672.074 42.9396 5 7 0 2 658.299 41.2652 1 7 0 3 14.7002 7.82549 5 7 0 3 5.76282 5.92584 1 7 0 4 2107.64 104.697 5 7 0 4 2163.42 103.543 1 7 0 5 3.91292 6.89185 1 7 0 5 6.42160 6.33567 5 7 0 6 13.0013 7.85661 5 7 0 6 3.97592 6.35929 1 7 0 7 8.82040 6.53289 5 7 0 8 1132.57 63.8897 5 7 0 9 11.4340 7.57746 5 7 0 10 159.250 19.1294 5 7 0 11-2.41087 6.17705 5 7 0 12 299.690 27.5342 5 7 0 13-2.55798 6.17922 5 7 0 14 415.784 34.1298 5 7 0 15 2.69434 6.08839 5 7 0 16-2.76187 6.67177 5 7 0 17-8.51838 8.04944 5 7 0 18 120.012 19.0061 5 7 0 19 3.00672 7.26322 5 7 0 20 37.1392 12.4881 5 7 -1 -25 12.1741 9.38392 2 7 -1 -24 232.195 28.4590 5 7 -1 -24 189.706 23.8868 2 7 -1 -23-3.50665 8.98359 5 7 -1 -23-2.87143 7.35628 2 7 1 -23 3.16417 8.10624 2 7 -1 -22 6.75940 7.63797 5 7 1 -22-3.45167 9.32267 5 7 -1 -22 11.1382 7.88849 2 7 1 -22 9.15776 7.82229 2 7 -1 -21-3.26214 7.88221 5 7 -1 -21-8.09526 8.31122 2 7 1 -21-2.93613 7.09513 2 7 -1 -20 294.927 30.0619 5 7 1 -20 261.315 28.7427 5 7 1 -20 265.597 27.7172 2 7 -1 -20 316.700 28.4060 2 7 -1 -19 6.13822 7.86689 5 7 1 -19 3.21909 8.69679 5 7 -1 -19 10.1625 7.82684 2 7 1 -19 5.52643 7.83039 2 7 -1 -18 80.9988 16.0702 5 7 1 -18 87.9363 16.7982 5 7 -1 -18 58.5118 12.4993 2 7 1 -18 75.9018 14.2046 2 7 -1 -17 20.6072 9.84276 5 7 1 -17 42.5595 13.0598 5 7 -1 -17 39.4735 10.7750 2 7 1 -17 47.7007 12.4786 2 7 1 -16 282.907 27.6673 2 7 -1 -16 354.614 31.3573 5 7 1 -16 345.741 32.0230 5 7 -1 -15-2.77015 7.48058 5 7 1 -15 11.3885 8.76620 5 7 -1 -15-4.35920 6.71090 2 7 1 -15 2.52096 7.45743 2 7 1 -14-2.45976 7.27635 2 7 -1 -14-2.66131 6.81784 5 7 1 -14 2.78555 6.72800 5 7 -1 -14 4.25358 5.44849 2 7 1 -13 9.63625 7.42111 2 7 -1 -13 2.59909 7.02255 5 7 -1 -13 6.17969 6.09804 2 7 -1 -12 549.649 36.9787 2 7 1 -12 535.792 38.4737 2 7 -1 -12 572.975 40.3460 5 7 1 -12 539.385 39.9920 5 7 -1 -11 2.44657 6.26918 5 7 1 -11-2.55557 6.90245 5 7 -1 -11 7.81880 5.53780 2 7 -1 -10 5.72036 4.89808 2 7 -1 -10 16.6559 8.38542 5 7 1 -10 9.94844 7.66611 5 7 -1 -9 126.700 15.2508 2 7 -1 -9 127.381 17.1185 5 7 1 -9 164.702 18.8705 5 7 -1 -8 1340.30 70.3361 5 7 1 -8 1191.10 69.3180 5 7 -1 -7 46.2643 10.6602 5 7 1 -7 51.1107 10.6830 5 7 -1 -6 38.8950 10.4027 5 7 1 -6 41.1770 9.70832 5 7 -1 -5 714.901 43.8623 5 7 1 -5 614.338 42.5151 5 7 1 -4 684.983 44.3535 5 7 1 -4 644.687 41.9448 1 7 -1 -4 714.059 43.8332 5 7 1 -3 2.03638 5.21949 1 7 -1 -3 6.17578 5.83274 5 7 1 -3 4.37626 4.94647 5 7 -1 -2 465.680 34.1331 5 7 1 -2 516.921 36.0500 5 7 -1 -2 512.907 32.9334 1 7 1 -2 538.228 35.7430 1 7 -1 -1 607.676 38.2696 5 7 1 -1 513.363 36.9289 5 7 -1 -1 499.483 33.6636 1 7 1 -1 592.465 37.7225 1 7 -1 0 227.577 21.2495 5 7 1 0 212.980 21.5496 5 7 -1 0 206.665 18.7913 1 7 1 0 208.130 20.3777 1 7 1 1 24.6800 7.93774 1 7 -1 1 16.2204 6.10664 5 7 1 1 38.8644 8.52688 5 7 -1 1 47.2271 8.95269 1 7 -1 2 1285.50 69.1699 5 7 1 2 1251.72 69.6662 5 7 -1 2 1337.66 67.0554 1 7 1 2 1283.11 69.1823 1 7 -1 3 266.403 23.6426 5 7 1 3 243.911 23.6776 5 7 -1 3 314.810 23.3585 1 7 1 3 260.607 23.8594 1 7 -1 4 6.97724 6.15173 1 7 1 4 4.20467 6.22908 1 7 -1 4 16.2192 7.35376 5 7 1 4 10.8626 6.95058 5 7 1 5 169.770 18.5273 1 7 -1 5 176.340 18.5768 5 7 1 5 167.324 18.7532 5 7 -1 5 166.189 17.2751 1 7 -1 6 422.026 30.1679 1 7 1 6 471.737 33.2487 1 7 -1 6 450.772 32.5051 5 7 1 6 413.010 32.1418 5 7 1 7 74.9571 13.0299 5 7 -1 7 95.0361 13.9247 5 7 1 8 39.3151 10.9191 5 7 -1 8 34.3461 10.1504 5 7 1 9 108.460 15.7909 5 7 -1 9 80.9803 13.7433 5 7 1 10 1177.60 65.6774 5 7 -1 10 1093.46 63.2793 5 7 1 11 12.4060 7.93740 5 7 -1 11 6.91996 7.63874 5 7 1 12 758.270 50.0090 5 7 -1 12 791.058 49.9290 5 7 1 13 5.27535 7.12585 5 7 -1 13 4.90116 8.10752 5 7 1 14 43.3182 11.0444 5 7 -1 14 63.0455 13.0896 5 7 1 15 19.4759 9.21816 5 7 -1 15 10.3480 6.65007 5 7 -1 16 334.231 30.0278 5 7 1 16 321.801 30.2889 5 7 1 17 75.8360 15.3206 5 7 -1 17 90.3727 15.7018 5 7 1 18 107.777 18.1289 5 7 -1 18 84.7773 16.2893 5 7 1 19 3.08047 7.89741 5 7 -1 19 14.5290 8.95186 5 7 -1 20 162.274 21.8681 5 7 -2 -24 57.7726 15.2922 5 7 -2 -24 59.1674 14.0250 2 7 -2 -23 65.8844 16.0934 5 7 -2 -23 46.0214 12.4239 2 7 -2 -22 293.333 31.5302 5 7 2 -22 311.343 30.9720 2 7 -2 -21 22.5247 11.3571 5 7 -2 -21 12.7250 8.45399 2 7 2 -21 27.3530 10.7299 2 7 -2 -20 204.412 24.4703 5 7 -2 -20 174.286 21.7950 2 7 2 -20 164.662 21.8640 2 7 -2 -19 113.793 18.6850 5 7 -2 -19 78.3527 14.5930 2 7 2 -19 111.464 18.1479 2 7 2 -18 436.518 36.1875 2 7 -2 -18 404.630 35.6252 5 7 -2 -18 445.008 33.9014 2 7 -2 -17 89.8362 16.3918 5 7 -2 -17 118.811 16.2829 2 7 2 -17 142.422 19.4893 2 7 -2 -16-11.0533 8.50851 5 7 -2 -16 12.8826 8.20011 2 7 2 -16 5.48048 8.43744 2 7 2 -15-2.67810 8.24679 2 7 -2 -15 2.69203 7.62556 5 7 -2 -15-6.13737 6.05322 2 7 2 -14 178.714 21.9382 2 7 -2 -14 187.305 21.8556 5 7 -2 -14 194.428 19.6526 2 7 -2 -13 287.654 24.1257 2 7 2 -13 297.573 27.6474 2 7 -2 -13 311.532 27.9575 5 7 2 -12 128.474 17.4120 2 7 -2 -12 138.591 17.6559 5 7 -2 -12 120.917 14.8514 2 7 -2 -11 33.1756 10.2439 5 7 -2 -11 44.5281 9.38935 2 7 -2 -10 366.616 26.7868 2 7 -2 -10 363.099 29.6515 5 7 -2 -9 493.532 33.6208 2 7 -2 -9 584.975 38.4551 5 7 -2 -8 6.53987 5.76666 2 7 -2 -8 10.8668 6.70032 5 7 -2 -7 573.675 35.0138 2 7 -2 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7 3 5 249.986 23.9178 1 7 3 5 243.530 25.7767 5 7 -3 6 81.6468 12.4327 5 7 3 6 73.0576 17.7993 5 7 3 6 64.9489 12.8478 1 7 3 7 141.863 17.6579 1 7 -3 7 135.891 16.3212 5 7 3 7 146.494 22.1354 5 7 -3 8 207.088 20.1845 5 7 3 8 245.690 26.6669 5 7 3 9 402.818 35.0452 5 7 -3 9 424.974 30.7171 5 7 -3 10 313.658 26.4947 5 7 3 10 366.650 32.5976 5 7 3 11 2.51172 14.7046 5 7 -3 11-2.04673 6.05484 5 7 3 12 7.72122 13.9029 5 7 -3 12 6.32488 5.97709 5 7 3 13 26.3876 16.6128 5 7 -3 13 34.8711 9.21536 5 7 3 14 97.7557 20.9059 5 7 -3 14 81.5016 13.4337 5 7 3 15 30.8523 17.4391 5 7 -3 15 4.67273 5.65058 5 7 3 16 8.65702 15.9704 5 7 -3 16 2.41931 6.19928 5 7 3 17-2.95722 16.5599 5 7 -3 17-2.49250 7.06006 5 7 -3 18 15.4679 8.82827 5 7 -3 19 13.4135 9.17977 5 7 -3 20 58.6188 13.2720 5 7 -3 21 2.89812 9.26075 5 7 4 -18 417.188 39.1746 5 7 4 -17 30.0668 16.8809 5 7 4 -16 14.6602 16.6190 5 7 4 -15 130.040 23.6287 5 7 4 -14 429.868 37.8582 5 7 4 -13 140.833 23.7143 5 7 4 -12 55.5100 17.7739 5 7 -4 -11 214.303 22.2488 5 7 4 -11 255.281 28.1945 5 7 -4 -10 135.421 17.0937 5 7 4 -10 181.060 23.4394 5 7 -4 -9 12.2876 7.43969 5 7 4 -9 17.2309 13.6337 5 7 -4 -8 88.6928 13.3315 5 7 4 -8 65.0377 17.2719 5 7 -4 -7 607.452 39.8589 5 7 4 -7 669.434 45.4866 5 7 -4 -6 86.2800 13.1556 5 7 4 -6 76.8714 18.3280 5 7 -4 -5 34.7215 8.78468 5 7 4 -5 23.0525 15.1761 5 7 -4 -4 101.758 13.5471 5 7 4 -4 114.031 18.9703 5 7 -4 -3 527.303 34.9354 5 7 4 -3 568.313 40.3396 5 7 -4 -2 5.17589 5.31427 5 7 4 -2-4.46921 12.6587 5 7 -4 -1 22.2479 7.20827 5 7 4 -1 15.6108 12.3703 5 7 -4 0 6.80802 5.63200 5 7 4 0-6.68557 13.1859 5 7 -4 1 545.097 35.2924 5 7 4 1 599.241 41.5754 5 7 -4 2 8.46409 5.97310 5 7 4 2 15.7618 13.7372 5 7 -4 3 18.7357 7.45487 5 7 4 3 18.0608 13.6531 5 7 -4 4 5.16533 5.88694 5 7 4 4 13.5733 14.3291 5 7 -4 5 370.714 27.1979 5 7 4 5 380.622 32.9869 5 7 -4 6 48.7560 10.1338 5 7 4 6 32.1763 15.6801 5 7 -4 7 98.6469 13.3105 5 7 4 7 102.464 18.9883 5 7 -4 8 114.635 14.7636 5 7 4 8 153.993 22.8334 5 7 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33.6949 15.6855 1 7 5 6 14.0444 15.7508 5 7 5 6 15.7755 14.5636 1 7 5 7 118.954 21.4224 1 7 5 7 184.095 24.0897 5 7 5 8 50.8910 18.1631 1 7 5 8 64.4171 17.6833 5 7 5 9 198.318 25.6837 5 7 5 9 203.491 26.3598 1 7 5 10 12.2980 15.0352 5 7 5 10 44.1655 17.9815 1 7 5 11 40.0854 18.1007 5 7 5 12 2.55016 15.8543 5 7 5 13 233.996 27.8536 5 7 6 -12 8.25012 16.6090 5 7 6 -11 137.954 23.2033 5 7 6 -9 85.9082 19.8179 5 7 6 -8 48.5281 17.4240 5 7 6 -7 158.410 24.0073 5 7 6 -6-2.47105 16.4811 5 7 6 -5 39.0481 16.4866 5 7 6 -4 21.7209 15.0299 5 7 6 -3 112.574 19.7262 5 7 6 -2 15.3754 15.0373 1 7 6 -2 35.7706 15.5428 5 7 6 -1-5.14467 14.7356 1 7 6 -1 2.37338 13.8948 5 7 6 0 14.1719 14.5553 5 7 6 0 12.9082 15.2838 1 7 6 1 56.4435 17.6613 5 7 6 1 10.4147 14.2842 1 7 6 2 2.35769 13.8027 5 7 6 2-2.62992 15.3965 1 7 6 3-14.1909 14.8530 5 7 6 4 19.0369 15.6278 5 7 6 5 220.595 25.9172 5 7 6 6 157.930 23.3444 5 7 6 7 53.6250 18.3949 5 7 6 8 2.45399 17.4074 5 7 6 9 135.830 23.3765 5 7 7 -6 15.8057 17.1440 5 7 7 -5 166.707 25.4879 5 7 7 -4-5.13654 16.7040 5 7 7 -3-10.1811 16.5582 5 7 7 -2 22.7236 15.7237 5 7 7 -1 55.2410 17.5641 5 7 7 0-7.52116 16.8602 5 7 7 1 10.0064 14.8058 5 7 7 2 17.4839 16.3985 5 7 7 3 104.538 20.7170 5 8 0 -21 3.08739 8.33818 2 8 0 -20 71.0982 14.8174 2 8 0 -19 3.57551 9.16084 5 8 0 -19 2.85455 7.70961 2 8 0 -18 115.337 20.1815 5 8 0 -18 125.802 18.5312 2 8 0 -17 6.78130 10.0301 5 8 0 -17-2.74059 7.76203 2 8 0 -16 348.836 31.4299 2 8 0 -16 356.597 34.0513 5 8 0 -15-3.18745 9.02850 5 8 0 -14 15.3488 9.54252 2 8 0 -13 12.1767 8.62647 5 8 0 -13 2.50611 8.01251 2 8 0 -12 1107.08 66.0340 2 8 0 -12 1215.87 70.4582 5 8 0 -11 7.14629 7.34653 2 8 0 -11 14.4281 8.18363 5 8 0 -10 166.878 19.8161 2 8 0 -10 174.533 22.3314 5 8 0 -9 2.74136 8.11013 5 8 0 -8 925.589 57.8765 5 8 0 -7 23.6567 8.45354 5 8 0 -6 266.416 25.8609 5 8 0 -5 17.8483 8.17922 5 8 0 -4 520.050 38.4536 5 8 0 -3 34.6392 9.31693 5 8 0 -2 1091.89 63.5489 5 8 0 -2 1092.66 61.1510 1 8 0 -1 18.9595 7.02082 1 8 0 -1 24.3875 8.11207 5 8 0 0 55.9607 10.6597 5 8 0 0 61.5766 10.8393 1 8 0 1 12.1863 6.58415 5 8 0 1 2.13144 3.64484 1 8 0 2 331.094 29.6554 5 8 0 2 436.372 30.9921 1 8 0 3 2.16628 4.89593 1 8 0 3 4.86790 6.89461 5 8 0 4-10.9446 7.00817 1 8 0 5 2.44735 7.24030 5 8 0 5 2.22380 6.29904 1 8 0 6 29.0610 8.85868 1 8 0 6 41.9324 10.6239 5 8 0 7 2.49704 6.39702 5 8 0 7-2.26843 6.42472 1 8 0 8 5.07357 7.19300 5 8 0 8 11.5590 6.84738 1 8 0 9-7.05055 6.34883 1 8 0 9-2.57355 6.95180 5 8 0 10 39.3472 10.6279 5 8 0 11 8.00963 7.56869 5 8 0 12 2.71913 6.96686 5 8 0 13-8.33738 8.56350 5 8 0 14 110.862 17.7473 5 8 0 15-2.91877 7.47836 5 8 -1 -22 84.3819 17.2211 2 8 -1 -21-5.82414 7.86737 2 8 -1 -20 151.025 20.7015 2 8 -1 -19 20.6815 11.4003 5 8 -1 -19-2.77849 8.87809 2 8 1 -19 6.09173 8.22545 2 8 -1 -18 132.604 21.0184 5 8 1 -18 134.450 21.6072 5 8 -1 -18 162.216 20.6341 2 8 1 -18 104.735 18.4965 2 8 -1 -17 46.5145 14.2541 5 8 1 -17 51.5996 15.0431 5 8 -1 -17 20.4072 9.84065 2 8 1 -17 35.1399 12.0730 2 8 -1 -16 257.635 28.1883 5 8 1 -16 232.772 27.3016 5 8 -1 -16 171.781 21.6637 2 8 1 -16 225.852 24.9886 2 8 -1 -15 9.40644 9.65446 5 8 1 -15-3.24288 9.59342 5 8 -1 -15 4.87473 8.06172 2 8 1 -15 2.80679 7.95004 2 8 -1 -14 602.332 40.7060 2 8 1 -14 518.427 40.7283 2 8 -1 -14 541.900 42.7632 5 8 1 -14 561.053 43.7209 5 8 1 -13 37.7235 10.8556 2 8 -1 -13 23.7306 10.8102 5 8 -1 -13 25.4559 9.75140 2 8 1 -12 5.22491 7.41813 2 8 -1 -12 25.9890 11.3127 5 8 1 -12 21.0382 10.5953 5 8 -1 -12 11.3326 7.76016 2 8 -1 -11 92.9614 14.2161 2 8 -1 -11 103.918 17.4963 5 8 1 -11 70.2828 15.0128 5 8 -1 -10 534.168 38.3450 2 8 1 -10 529.112 41.7055 5 8 -1 -9 31.4921 8.91600 2 8 -1 -9 34.7502 10.8160 5 8 1 -9 55.7818 13.1351 5 8 -1 -8 75.5251 14.8543 5 8 1 -8 103.802 16.2241 5 8 1 -7 227.756 24.2585 5 8 -1 -6 537.914 37.6675 5 8 1 -6 417.283 35.2678 5 8 -1 -5 54.2336 11.9485 5 8 1 -5 59.9083 11.9966 5 8 -1 -4 500.839 37.0298 5 8 1 -4 515.855 38.1457 5 8 1 -3 151.518 18.0285 1 8 -1 -3 172.601 19.7178 5 8 1 -3 128.999 17.3986 5 8 1 -2 59.6511 11.8038 1 8 -1 -2 42.5613 10.3398 5 8 1 -2 67.8825 12.5339 5 8 -1 -1 17.0595 6.70612 1 8 -1 -1 23.5183 8.06013 5 8 1 -1 10.0074 6.78787 5 8 1 -1 16.0982 7.37734 1 8 -1 0 648.554 43.1675 5 8 1 0 671.799 44.6869 5 8 -1 0 631.823 40.1899 1 8 1 0 648.737 43.1135 1 8 -1 1 21.0704 8.49166 5 8 1 1 15.0156 7.09950 5 8 -1 1 5.76233 5.45514 1 8 1 1 4.63791 6.87179 1 8 -1 2 16.4703 8.04977 5 8 1 2 15.0209 6.77561 5 8 -1 2 5.80041 5.49474 1 8 1 2 11.6497 6.90719 1 8 1 3 14.1368 7.00866 1 8 -1 3 16.4008 8.28227 5 8 1 3 25.0499 7.74786 5 8 -1 3 17.5088 8.00125 1 8 -1 4 518.976 36.4519 5 8 1 4 513.768 36.9864 5 8 -1 4 438.946 32.4076 1 8 1 4 419.007 33.7861 1 8 -1 5 2.34813 6.65562 5 8 1 5 15.1260 7.76650 5 8 -1 5 6.01568 6.41245 1 8 1 5 4.81384 6.50501 1 8 1 6 12.1375 7.76196 1 8 -1 6 11.8251 7.28784 5 8 1 6 5.08778 6.15149 5 8 -1 6 4.06037 5.49037 1 8 -1 7-2.06049 6.34415 1 8 -1 7 2.38881 7.06648 5 8 1 7 5.15053 6.59742 5 8 1 7-2.45816 6.96206 1 8 -1 8 152.890 17.7282 1 8 -1 8 133.505 18.0272 5 8 1 8 133.576 18.2468 5 8 1 8 142.634 18.7733 1 8 -1 9-2.46097 6.30474 5 8 1 9-2.65779 6.80894 5 8 -1 9-2.14047 6.06241 1 8 1 9 7.62195 7.51574 1 8 1 10 48.7724 12.1733 5 8 -1 10 45.1304 11.6866 5 8 1 11 5.52052 7.07462 5 8 -1 11 5.10294 6.54000 5 8 1 12 219.337 25.0688 5 8 -1 12 252.368 24.9067 5 8 1 13 14.3557 10.4072 5 8 -1 13 5.31524 6.81622 5 8 1 14 8.80694 8.31759 5 8 -1 14 2.72070 8.05155 5 8 -1 15 19.5747 8.97035 5 8 -1 16 186.904 23.6275 5 8 -2 -20 89.1206 18.6358 5 8 -2 -19 230.815 27.2212 5 8 -2 -18 106.748 18.8309 5 8 -2 -17-3.19369 9.04656 5 8 2 -17 15.4757 10.5735 2 8 -2 -16 140.945 21.5876 5 8 2 -16 127.863 19.8646 2 8 2 -15 235.190 26.4472 2 8 -2 -15 252.994 27.2402 5 8 2 -14 8.78667 9.01790 2 8 -2 -14-5.91933 8.75516 5 8 2 -13-11.3610 9.70295 2 8 -2 -13 22.8169 9.11432 5 8 -2 -12 308.868 26.0665 2 8 2 -12 287.799 28.1756 2 8 -2 -12 273.599 28.1803 5 8 -2 -11 155.084 20.2783 5 8 -2 -11 151.464 17.5045 2 8 -2 -10 37.1030 12.0532 5 8 -2 -10 31.4760 9.45284 2 8 -2 -9 74.8435 14.5107 5 8 -2 -9 90.6883 14.0015 2 8 -2 -8 218.690 21.8182 2 8 -2 -8 347.880 29.0751 5 8 -2 -7 109.700 14.6829 2 8 -2 -7 149.796 19.1951 5 8 -2 -5 267.146 25.1331 5 8 -2 -4 291.525 26.3060 5 8 2 -3 41.7801 10.9224 1 8 -2 -3 69.0759 12.3163 5 8 2 -2 211.247 22.4029 1 8 -2 -2 190.993 20.6020 5 8 -2 -1 4.49284 7.43089 5 8 2 -1 2.45785 6.63863 1 8 -2 0 8.94613 6.92012 5 8 2 0 34.6732 10.3836 1 8 -2 1 102.836 12.8857 1 8 -2 1 80.3264 13.4046 5 8 2 1 76.8147 14.1679 1 8 2 2 204.091 23.1910 1 8 -2 2 246.182 20.6038 1 8 -2 2 227.806 22.9394 5 8 2 3 32.7058 10.7909 1 8 -2 3 24.7384 9.06624 5 8 -2 3 22.4605 6.99602 1 8 -2 4 29.0869 9.22552 5 8 2 4 15.2455 8.74499 1 8 -2 4 34.8887 8.75180 1 8 -2 5 118.994 14.8337 1 8 -2 5 105.229 15.3797 5 8 2 5 151.847 18.7877 1 8 -2 6 360.623 29.3701 5 8 -2 6 365.267 27.0262 1 8 2 6 340.932 30.1847 1 8 -2 7 2.27134 7.25858 5 8 2 7 7.85109 8.36295 1 8 -2 7 1.84100 5.66993 1 8 2 8 31.8482 10.4687 1 8 -2 8 44.8989 9.67492 1 8 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14.7859 5 8 3 -3 374.844 32.5895 1 8 -3 -3 489.006 33.6698 5 8 3 -3 397.278 35.6706 5 8 3 -2 315.484 28.4545 1 8 3 -2 311.995 31.8538 5 8 -3 -2 297.679 26.0680 5 8 -3 -1 45.1691 9.88876 5 8 3 -1 35.6962 16.3953 5 8 3 -1 49.1409 12.0327 1 8 -3 0 10.6303 7.26554 5 8 3 0 2.54658 13.9263 5 8 3 0 2.60588 6.67953 1 8 -3 1 137.699 17.3263 5 8 3 1 112.286 20.8259 5 8 3 1 117.235 17.2486 1 8 -3 2 294.048 26.0802 5 8 3 2 343.932 32.5283 5 8 3 2 321.446 28.8434 1 8 3 3 2.64119 7.48045 1 8 -3 3-2.12146 6.77845 5 8 3 3 2.57758 14.9287 5 8 3 4 173.023 21.0204 1 8 -3 4 192.226 20.0534 5 8 3 4 212.192 26.3495 5 8 -3 5 23.5308 9.17579 5 8 3 5 15.5643 16.1506 5 8 3 5 21.5619 10.0707 1 8 -3 6 145.742 18.0676 5 8 3 6 146.571 23.4425 5 8 3 6 144.302 19.5187 1 8 3 7-2.74801 8.12955 1 8 -3 7 2.15667 8.02821 5 8 -3 8 152.345 18.7541 5 8 3 8 203.614 26.3633 5 8 3 8 191.882 22.4136 1 8 3 9 31.0360 10.6177 1 8 -3 9 50.7356 11.4097 5 8 3 9 29.9693 16.8496 5 8 3 10 34.5042 11.0394 1 8 -3 10 20.2306 9.07474 5 8 3 10 41.6097 18.5360 5 8 3 11 72.9162 15.1229 1 8 -3 11 98.4142 15.1430 5 8 3 11 76.2689 20.3243 5 8 -3 12 128.534 17.2675 5 8 -3 13-2.38901 6.12103 5 8 -3 14 80.6523 14.3798 5 8 -3 15 2.50844 6.42703 5 8 -3 16 10.3234 8.25697 5 8 -3 17 23.9936 10.2279 5 8 4 -11 76.1183 21.5837 5 8 4 -10 22.9210 17.8364 5 8 4 -9 95.6544 20.7537 5 8 4 -8-8.26377 16.1299 5 8 4 -6 235.254 28.1063 5 8 4 -5 396.874 35.5145 5 8 4 -4 167.870 24.6689 5 8 4 -3-2.68023 8.25234 1 8 4 -3 39.0183 16.9170 5 8 4 -2-5.35863 8.56278 1 8 4 -2 2.57713 15.4062 5 8 4 -1 138.258 22.4763 5 8 4 -1 104.554 16.7087 1 8 4 0 46.0831 17.2016 5 8 4 0 53.8524 12.5562 1 8 4 1 33.3166 16.6682 5 8 4 1-8.13726 8.97269 1 8 4 2-10.2887 15.9925 5 8 4 2 10.8744 8.37382 1 8 4 3 142.415 23.6413 5 8 4 3 150.097 19.8545 1 8 4 4 99.5679 16.8661 1 8 4 4 102.040 21.9309 5 8 4 5-11.1608 9.53651 1 8 4 5 7.86097 15.5062 5 8 4 6 229.220 27.3503 5 8 4 6 132.894 19.4094 1 8 4 7 26.5763 17.6125 5 8 5 -4 5.30191 17.5364 5 8 5 -3 160.798 23.9760 5 8 5 -2 44.5392 17.9899 5 8 5 -1 7.81366 14.7568 5 8 5 0-15.5424 16.7126 5 8 5 1 90.6819 21.1962 5 9 0 -16 14.6882 9.73410 2 9 0 -14 338.155 31.3466 2 9 0 -13-2.76956 8.52807 2 9 0 -12-2.71131 6.94701 2 9 0 -12-3.33615 10.2726 5 9 0 -11 2.65754 9.07761 2 9 0 -11-3.25616 9.22220 5 9 0 -10 542.356 39.9717 2 9 0 -10 515.175 41.9805 5 9 0 -9 3.10922 10.2840 5 9 0 -8 39.5493 13.0889 5 9 0 -6 252.376 27.4276 5 9 0 -5 2.89585 8.56718 5 9 0 -4-2.86295 9.77990 5 9 0 -3-16.9760 9.98573 5 9 0 -2 167.702 21.2375 5 9 0 -1 2.33505 6.90749 1 9 0 -1-2.77061 7.48184 5 9 0 0-2.34058 7.74175 1 9 0 0-2.76046 9.13032 5 9 0 1-5.50811 9.11035 5 9 0 1-2.34806 7.50467 1 9 0 2 118.526 17.8435 5 9 0 2 125.806 17.4395 1 9 0 3-11.0737 8.19168 5 9 0 3 9.56367 8.66437 1 9 0 4 16.6644 8.90841 5 9 0 4 21.6794 9.00005 1 9 0 5 2.44193 6.25596 1 9 0 5-5.56742 7.88419 5 9 0 6 180.301 20.7132 1 9 0 6 170.004 21.5496 5 9 0 7-8.41742 9.58755 5 9 0 7-5.02028 7.73295 1 9 0 8 62.2465 13.7935 5 9 0 8 35.6284 10.8074 1 9 0 9-2.57153 8.50550 1 9 0 10 196.171 22.6430 1 9 0 11-2.66174 8.80389 1 9 0 12 212.194 24.1212 1 9 1 -14-3.01817 8.15123 2 9 1 -13 71.1916 15.2632 2 9 1 -12 197.029 23.2682 2 9 -1 -12 104.045 19.4982 5 9 1 -11 5.64147 8.68665 2 9 -1 -11 6.34766 8.57245 5 9 -1 -11 2.46816 7.60135 2 9 -1 -10 2.42227 6.54282 2 9 -1 -10 6.19554 8.77481 5 9 1 -10 3.23755 9.17064 5 9 -1 -9 23.6231 9.68986 2 9 -1 -9 6.05439 8.19278 5 9 -1 -8 195.195 21.7953 2 9 -1 -8 228.095 25.5148 5 9 1 -8 223.413 25.3735 5 9 -1 -7 5.79557 9.25894 5 9 1 -7-3.04437 8.22108 5 9 -1 -6 8.54129 8.43265 5 9 1 -6 11.9871 8.10347 5 9 -1 -5-5.59978 8.62075 5 9 1 -5 2.96132 8.76010 5 9 -1 -4 160.456 21.7974 5 9 1 -4 240.071 25.2422 5 9 -1 -3-8.20807 9.05055 5 9 1 -3 2.89596 7.82218 5 9 1 -2 33.0230 10.9344 1 9 -1 -2 27.0531 10.1649 5 9 1 -2 45.7800 12.2952 5 9 1 -1 27.9734 10.2204 1 9 -1 -1 21.3841 9.72074 5 9 1 -1 14.2224 9.12744 5 9 -1 0 33.8489 9.68068 1 9 1 0 33.1810 10.7864 1 9 -1 0 39.8767 12.3202 5 9 1 0 48.2307 13.1359 5 9 -1 1 10.6304 6.02394 1 9 -1 1 2.64972 7.50652 5 9 1 1-2.83186 8.02225 5 9 1 1 2.56859 7.60019 1 9 -1 2 15.9000 8.77071 5 9 1 2 2.84102 8.75367 5 9 -1 2 8.54437 6.83328 1 9 1 2 7.76872 7.00082 1 9 -1 3 23.8883 10.4380 5 9 1 3 19.9770 11.2155 5 9 -1 3 32.4368 9.65066 1 9 1 3 23.4075 9.98598 1 9 -1 4 157.823 20.7087 5 9 1 4 203.467 23.8206 5 9 -1 4 209.422 21.3883 1 9 1 4 186.099 21.7762 1 9 1 5 31.8675 11.8605 1 9 -1 5 26.7102 10.7831 5 9 1 5 25.8715 11.5926 5 9 -1 5 48.4551 11.3652 1 9 -1 6 120.756 16.4023 1 9 1 6 88.5479 15.8772 1 9 -1 6 120.593 18.1672 5 9 1 6 129.603 19.2846 5 9 -1 7 8.06406 8.89237 5 9 1 7 2.72996 8.07812 1 9 -1 8 205.830 24.1788 5 9 1 8 258.997 26.5935 1 9 1 9 13.9654 10.1377 1 9 -1 9 2.73606 8.76350 5 9 -1 9 32.7726 10.2112 1 9 -1 10 157.152 19.0919 1 9 1 10 144.532 20.3151 1 9 -2 -14 63.0652 14.9500 5 9 -2 -13 6.40944 10.2430 5 9 -2 -12 9.44043 10.0619 5 9 -2 -11 9.23034 9.83802 5 9 -2 -10 147.320 21.3960 5 9 -2 -9 38.1271 13.1059 5 9 -2 -8 5.73215 9.48189 5 9 -2 -7 2.80366 8.95892 5 9 -2 -6 129.021 18.9016 5 9 -2 -5 53.9938 13.1739 5 9 2 -5 38.9242 12.1368 5 9 -2 -4 7.97271 7.86270 5 9 2 -4-2.96348 9.12543 5 9 -2 -3 10.5182 8.40348 5 9 2 -3-2.93659 8.68844 5 9 2 -2 204.307 24.0286 1 9 -2 -2 273.160 26.2116 5 9 2 -2 209.189 24.9094 5 9 2 -1 21.7901 10.9616 1 9 -2 -1 25.7426 9.88856 5 9 2 -1 31.7327 11.6037 5 9 -2 0 38.1988 11.2503 5 9 2 0 48.9786 14.0467 5 9 2 0 57.3436 13.7289 1 9 -2 1 2.53593 8.93579 5 9 2 1 2.87982 9.20833 5 9 2 1-16.5390 11.5371 1 9 -2 2 98.6589 15.9459 5 9 2 2 99.7214 17.0426 1 9 -2 3 17.7187 9.44794 5 9 2 3 16.6911 9.52798 1 9 -2 4 121.805 18.2839 5 9 2 4 98.1314 17.0033 1 9 2 5-2.83902 8.04087 1 9 -2 5 5.12011 7.88243 5 9 2 6 97.5106 17.0730 1 9 -2 6 135.716 19.2519 5 9 -2 7 43.5913 12.3200 5 9 -2 8 98.0723 15.9350 5 9 -2 9 70.3088 14.8597 5 9 -2 10 86.8248 15.4803 5 9 -3 -7 2.71024 8.34542 5 9 -3 -6 10.6291 8.50145 5 9 -3 -4 207.209 23.3133 5 9 -3 -3 2.51730 8.32614 5 9 -3 -2 9.94997 8.23688 5 9 -3 -1 4.93523 8.94239 5 9 -3 0 100.303 16.5576 5 9 -3 1 2.42445 8.53684 5 9 -3 2 31.3035 10.1538 5 9 -3 3 14.4454 8.49720 5 9 -3 4 36.1395 10.3916 5 9 -3 5 9.68498 8.27983 5 9 -3 6 77.9818 14.7626 5 10 0 1 2.55531 7.55972 1 10 0 2 2.56691 7.90407 1 10 0 3-12.9158 9.11023 1 0 0 0 0.00 0.00 0 TITL exp_1 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 7.435472 7.295155 26.272863 90.0000 93.4607 90.0000 ZERR 6.00 0.000279 0.000281 0.001102 0.0000 0.0036 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 66.00 60.00 6.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 75764 _publcif_info_exptl_table_max_cols 4 _publcif_info_exptl_table_use_headnotes n _publcif_funding_html ; ; loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure '{289c58f7-101e-443d-b2ff-5cad87d27cb5}' y y y loop_ _publcif_info_exptl_table_extra_item sin_theta_over_lambda_max loop_ _publcif_info_exptl_table_header_item ? loop_ _publcif_info_tables.block_id _publcif_info_tables.reference_item "{289c58f7-101e-443d-b2ff-5cad87d27cb5}" "_geom_bond_atom_site_label_1" "{289c58f7-101e-443d-b2ff-5cad87d27cb5}" "_publcif_info_datablock.publ_exptl" "{289c58f7-101e-443d-b2ff-5cad87d27cb5}" "_geom_hbond_atom_site_label_D" loop_ _publcif_info_cif.paper_type EE