#============================================================================== data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 11 _journal_issue 4 _journal_year 2020 _journal_page_first 377 _journal_page_last 384 #============================================================================== data_shelx _audit_creation_date 2020-11-21 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _shelxl_version_number 2013-4 _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C40 H50 N4 O6 Pd S2' _chemical_formula_sum 'C40 H50 N4 O6 Pd S2' _chemical_formula_weight 853.36 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.1561(6) _cell_length_b 12.1300(11) _cell_length_c 12.6117(17) _cell_angle_alpha 63.498(11) _cell_angle_beta 86.694(9) _cell_angle_gamma 81.451(7) _cell_volume 968.8(2) _cell_formula_units_Z 1 _cell_measurement_reflns_used 2488 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 24.6400 _cell_measurement_theta_min 3.6690 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 0.639 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.56514 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details CrysAlisPro _exptl_crystal_colour YELLOW _exptl_crystal_density_diffrn 1.463 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 444 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0653 _diffrn_reflns_av_unetI/netI 0.0913 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 11772 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.367 _diffrn_reflns_theta_min 3.399 _diffrn_ambient_temperature 298.15 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Xcalibur, Eos, Nova' _diffrn_measurement_method ? _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2843 _reflns_number_total 3939 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2013/4 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _refine_diff_density_max 1.449 _refine_diff_density_min -1.131 _refine_diff_density_rms 0.114 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.057 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 249 _refine_ls_number_reflns 3939 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1022 _refine_ls_R_factor_gt 0.0699 _refine_ls_restrained_S_all 1.057 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0881P)^2^+0.5697P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1623 _refine_ls_wR_factor_ref 0.1834 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C14(H14) 2.b Me refined with riding coordinates: C16(H16A,H16B,H16C), C19(H19A,H19B,H19C), C13(H13A,H13B,H13C), C15(H15A,H15B, H15C), C18(H18A,H18B,H18C), C17(H17A,H17B,H17C) 2.c Aromatic/amide H refined with riding coordinates: C5(H5), C10(H10), C6(H6), C12(H12A) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.0000 0.5000 0.0000 0.0367(2) Uani 1 2 d S . P . . S1 S 0.1718(2) 0.43440(15) -0.26896(14) 0.0458(4) Uani 1 1 d . . . . . O11 O 0.1142(5) 0.3826(3) 0.1573(3) 0.0420(10) Uani 1 1 d . . . . . N11 N 0.2314(6) 0.4649(4) -0.0828(4) 0.0348(10) Uani 1 1 d . . . . . C20 C 0.3850(8) 0.3904(5) -0.0301(6) 0.0349(13) Uani 1 1 d . . . . . N12 N 0.2415(7) 0.5208(5) -0.2080(5) 0.0413(12) Uani 1 1 d . . . . . O13 O 0.1561(7) 0.5198(5) -0.3932(4) 0.0662(14) Uani 1 1 d . . . . . O12 O 0.0093(6) 0.3798(4) -0.2110(4) 0.0617(13) Uani 1 1 d . . . . . C9 C 0.5381(8) 0.3522(5) -0.3026(5) 0.0406(14) Uani 1 1 d . . . . . C3 C 0.4173(8) 0.3157(5) 0.0937(5) 0.0359(13) Uani 1 1 d . . . . . C4 C 0.5969(8) 0.2369(5) 0.1286(6) 0.0421(14) Uani 1 1 d . . . . . C2 C 0.2824(8) 0.3171(5) 0.1817(5) 0.0365(13) Uani 1 1 d . . . . . C1 C 0.3336(9) 0.2444(5) 0.3049(5) 0.0419(14) Uani 1 1 d . . . . . C14 C 0.1934(9) 0.2511(5) 0.3979(5) 0.0439(15) Uani 1 1 d . . . . . H14 H 0.1378 0.3384 0.3691 0.053 Uiso 1 1 calc R U . . . C5 C 0.6321(9) 0.1644(6) 0.2464(6) 0.0538(17) Uani 1 1 d . . . . . H5 H 0.7439 0.1094 0.2701 0.065 Uiso 1 1 calc R U . . . C8 C 0.3691(8) 0.3167(5) -0.2434(5) 0.0391(13) Uani 1 1 d . . . . . C10 C 0.6788(9) 0.2593(6) -0.3013(5) 0.0463(15) Uani 1 1 d . . . . . H10 H 0.7918 0.2813 -0.3399 0.056 Uiso 1 1 calc R U . . . C6 C 0.5049(9) 0.1704(6) 0.3322(6) 0.0514(16) Uani 1 1 d . . . . . H6 H 0.5379 0.1219 0.4116 0.062 Uiso 1 1 calc R U . . . C7 C 0.3462(9) 0.1900(6) -0.1766(6) 0.0490(16) Uani 1 1 d . . . . . C16 C 0.7389(9) 0.2295(6) 0.0374(6) 0.0596(19) Uani 1 1 d . . . . . H16A H 0.6917 0.2864 -0.0406 0.089 Uiso 1 1 calc R U . . . H16B H 0.7585 0.1464 0.0445 0.089 Uiso 1 1 calc R U . . . H16C H 0.8565 0.2509 0.0504 0.089 Uiso 1 1 calc R U . . . C19 C 0.5807(10) 0.4853(6) -0.3643(6) 0.0538(17) Uani 1 1 d . . . . . H19A H 0.4731 0.5402 -0.3591 0.081 Uiso 1 1 calc R U . . . H19B H 0.6082 0.5070 -0.4461 0.081 Uiso 1 1 calc R U . . . H19C H 0.6878 0.4929 -0.3268 0.081 Uiso 1 1 calc R U . . . C12 C 0.4933(10) 0.1028(6) -0.1806(6) 0.0528(17) Uani 1 1 d . . . . . H12A H 0.4815 0.0188 -0.1384 0.063 Uiso 1 1 calc R U . . . C11 C 0.6552(10) 0.1354(6) -0.2443(6) 0.0530(17) Uani 1 1 d . . . . . C13 C 0.2818(11) 0.2117(6) 0.5188(6) 0.0580(18) Uani 1 1 d . . . . . H13A H 0.3830 0.2589 0.5099 0.087 Uiso 1 1 calc R U . . . H13B H 0.3302 0.1247 0.5527 0.087 Uiso 1 1 calc R U . . . H13C H 0.1877 0.2267 0.5701 0.087 Uiso 1 1 calc R U . . . C15 C 0.0326(11) 0.1780(7) 0.4092(6) 0.0630(19) Uani 1 1 d . . . . . H15A H -0.0540 0.1834 0.4682 0.095 Uiso 1 1 calc R U . . . H15B H 0.0823 0.0924 0.4320 0.095 Uiso 1 1 calc R U . . . H15C H -0.0323 0.2118 0.3344 0.095 Uiso 1 1 calc R U . . . C18 C 0.1797(11) 0.1403(7) -0.0987(7) 0.075(2) Uani 1 1 d . . . . . H18A H 0.0880 0.2085 -0.1030 0.113 Uiso 1 1 calc R U . . . H18B H 0.2225 0.0907 -0.0182 0.113 Uiso 1 1 calc R U . . . H18C H 0.1233 0.0900 -0.1255 0.113 Uiso 1 1 calc R U . . . C17 C 0.8065(12) 0.0353(7) -0.2501(7) 0.077(2) Uani 1 1 d . . . . . H17A H 0.9095 0.0736 -0.2978 0.116 Uiso 1 1 calc R U . . . H17B H 0.7533 -0.0095 -0.2846 0.116 Uiso 1 1 calc R U . . . H17C H 0.8520 -0.0212 -0.1716 0.116 Uiso 1 1 calc R U . . . H20 H 0.473(7) 0.393(4) -0.083(4) 0.024(13) Uiso 1 1 d . . . . . H12 H 0.167(10) 0.575(6) -0.229(6) 0.06(2) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.0313(4) 0.0375(4) 0.0402(4) -0.0198(3) 0.0006(3) 0.0066(3) S1 0.0382(9) 0.0580(10) 0.0445(9) -0.0296(8) -0.0023(7) 0.0075(7) O11 0.035(2) 0.044(2) 0.038(2) -0.0142(19) 0.0011(18) 0.0081(18) N11 0.035(3) 0.035(2) 0.033(3) -0.015(2) 0.003(2) -0.002(2) C20 0.028(3) 0.036(3) 0.048(4) -0.025(3) 0.002(3) -0.004(2) N12 0.037(3) 0.042(3) 0.038(3) -0.016(2) 0.003(2) 0.007(2) O13 0.069(3) 0.083(3) 0.042(3) -0.033(2) -0.008(2) 0.026(3) O12 0.034(3) 0.083(3) 0.083(3) -0.053(3) 0.004(2) -0.002(2) C9 0.036(3) 0.049(3) 0.040(3) -0.025(3) -0.005(3) 0.003(3) C3 0.030(3) 0.030(3) 0.049(4) -0.020(3) -0.001(3) 0.000(2) C4 0.026(3) 0.046(3) 0.059(4) -0.028(3) 0.000(3) 0.001(3) C2 0.031(3) 0.033(3) 0.051(4) -0.024(3) 0.002(3) -0.002(2) C1 0.046(4) 0.034(3) 0.040(3) -0.013(3) -0.008(3) 0.001(3) C14 0.055(4) 0.037(3) 0.032(3) -0.010(3) -0.005(3) 0.002(3) C5 0.041(4) 0.053(4) 0.064(5) -0.028(4) -0.012(3) 0.012(3) C8 0.037(3) 0.045(3) 0.040(3) -0.025(3) 0.001(3) 0.000(3) C10 0.040(4) 0.049(4) 0.051(4) -0.026(3) 0.009(3) 0.000(3) C6 0.051(4) 0.043(3) 0.049(4) -0.014(3) -0.012(3) 0.006(3) C7 0.043(4) 0.051(4) 0.057(4) -0.028(3) 0.001(3) -0.006(3) C16 0.032(4) 0.062(4) 0.080(5) -0.034(4) 0.000(3) 0.015(3) C19 0.056(4) 0.054(4) 0.056(4) -0.030(3) 0.012(3) -0.006(3) C12 0.053(4) 0.038(3) 0.069(5) -0.025(3) 0.000(4) -0.006(3) C11 0.052(4) 0.055(4) 0.057(4) -0.034(3) -0.006(3) 0.009(3) C13 0.069(5) 0.060(4) 0.044(4) -0.022(3) 0.000(3) -0.007(4) C15 0.062(5) 0.072(5) 0.058(4) -0.031(4) 0.016(4) -0.017(4) C18 0.060(5) 0.062(5) 0.091(6) -0.023(4) 0.014(5) -0.011(4) C17 0.085(6) 0.060(4) 0.083(6) -0.039(4) 0.015(5) 0.016(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 O11 1.988(4) 2_565 ? Pd1 O11 1.988(4) . ? Pd1 N11 2.001(4) 2_565 ? Pd1 N11 2.001(4) . ? S1 N12 1.690(5) . ? S1 O13 1.442(5) . ? S1 O12 1.423(5) . ? S1 C8 1.783(6) . ? O11 C2 1.310(6) . ? N11 C20 1.312(7) . ? N11 N12 1.416(7) . ? C20 C3 1.425(8) . ? C20 H20 0.88(5) . ? N12 H12 0.74(7) . ? C9 C8 1.403(8) . ? C9 C10 1.390(8) . ? C9 C19 1.518(8) . ? C3 C4 1.443(8) . ? C3 C2 1.433(8) . ? C4 C5 1.362(8) . ? C4 C16 1.515(8) . ? C2 C1 1.440(8) . ? C1 C14 1.521(8) . ? C1 C6 1.368(8) . ? C14 H14 0.9800 . ? C14 C13 1.525(8) . ? C14 C15 1.517(9) . ? C5 H5 0.9300 . ? C5 C6 1.394(9) . ? C8 C7 1.415(8) . ? C10 H10 0.9300 . ? C10 C11 1.379(9) . ? C6 H6 0.9300 . ? C7 C12 1.393(8) . ? C7 C18 1.516(9) . ? C16 H16A 0.9600 . ? C16 H16B 0.9600 . ? C16 H16C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C12 H12A 0.9300 . ? C12 C11 1.374(9) . ? C11 C17 1.528(8) . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C15 H15A 0.9600 . ? C15 H15B 0.9600 . ? C15 H15C 0.9600 . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O11 Pd1 O11 180.0(3) 2_565 . ? O11 Pd1 N11 88.72(16) 2_565 . ? O11 Pd1 N11 91.28(16) 2_565 2_565 ? O11 Pd1 N11 88.72(16) . 2_565 ? O11 Pd1 N11 91.28(16) . . ? N11 Pd1 N11 180.0 . 2_565 ? N12 S1 C8 103.4(3) . . ? O13 S1 N12 102.9(3) . . ? O13 S1 C8 110.1(3) . . ? O12 S1 N12 110.9(3) . . ? O12 S1 O13 118.1(3) . . ? O12 S1 C8 110.2(3) . . ? C2 O11 Pd1 128.7(4) . . ? C20 N11 Pd1 125.2(4) . . ? C20 N11 N12 113.5(5) . . ? N12 N11 Pd1 121.3(3) . . ? N11 C20 C3 127.6(5) . . ? N11 C20 H20 110(3) . . ? C3 C20 H20 122(3) . . ? S1 N12 H12 102(6) . . ? N11 N12 S1 113.5(4) . . ? N11 N12 H12 106(5) . . ? C8 C9 C19 124.3(5) . . ? C10 C9 C8 118.1(5) . . ? C10 C9 C19 117.5(5) . . ? C20 C3 C4 116.6(5) . . ? C20 C3 C2 123.2(5) . . ? C2 C3 C4 120.2(5) . . ? C3 C4 C16 121.4(6) . . ? C5 C4 C3 118.1(5) . . ? C5 C4 C16 120.5(5) . . ? O11 C2 C3 123.9(5) . . ? O11 C2 C1 117.2(5) . . ? C3 C2 C1 118.8(5) . . ? C2 C1 C14 118.6(5) . . ? C6 C1 C2 118.0(6) . . ? C6 C1 C14 123.4(6) . . ? C1 C14 H14 106.8 . . ? C1 C14 C13 114.3(5) . . ? C13 C14 H14 106.8 . . ? C15 C14 C1 110.9(5) . . ? C15 C14 H14 106.8 . . ? C15 C14 C13 110.7(5) . . ? C4 C5 H5 119.1 . . ? C4 C5 C6 121.7(6) . . ? C6 C5 H5 119.1 . . ? C9 C8 S1 118.3(4) . . ? C9 C8 C7 121.4(5) . . ? C7 C8 S1 119.8(5) . . ? C9 C10 H10 119.2 . . ? C11 C10 C9 121.7(6) . . ? C11 C10 H10 119.2 . . ? C1 C6 C5 123.0(6) . . ? C1 C6 H6 118.5 . . ? C5 C6 H6 118.5 . . ? C8 C7 C18 126.3(6) . . ? C12 C7 C8 116.7(6) . . ? C12 C7 C18 117.0(6) . . ? C4 C16 H16A 109.5 . . ? C4 C16 H16B 109.5 . . ? C4 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C9 C19 H19A 109.5 . . ? C9 C19 H19B 109.5 . . ? C9 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C7 C12 H12A 118.6 . . ? C11 C12 C7 122.9(6) . . ? C11 C12 H12A 118.6 . . ? C10 C11 C17 121.0(6) . . ? C12 C11 C10 118.9(6) . . ? C12 C11 C17 120.2(6) . . ? C14 C13 H13A 109.5 . . ? C14 C13 H13B 109.5 . . ? C14 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C14 C15 H15A 109.5 . . ? C14 C15 H15B 109.5 . . ? C14 C15 H15C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C7 C18 H18A 109.5 . . ? C7 C18 H18B 109.5 . . ? C7 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C11 C17 H17A 109.5 . . ? C11 C17 H17B 109.5 . . ? C11 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N12 H12 O11 0.74(7) 2.24(7) 2.803(6) 133(7) 2_565 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Pd1 O11 C2 C3 -2.6(8) . . . . ? Pd1 O11 C2 C1 176.4(3) . . . . ? Pd1 N11 C20 C3 3.1(8) . . . . ? Pd1 N11 N12 S1 -91.9(4) . . . . ? S1 C8 C7 C12 167.0(5) . . . . ? S1 C8 C7 C18 -14.8(9) . . . . ? O11 C2 C1 C14 -1.9(7) . . . . ? O11 C2 C1 C6 176.6(5) . . . . ? N11 C20 C3 C4 177.1(5) . . . . ? N11 C20 C3 C2 -3.4(9) . . . . ? C20 N11 N12 S1 87.9(5) . . . . ? C20 C3 C4 C5 180.0(5) . . . . ? C20 C3 C4 C16 -3.0(8) . . . . ? C20 C3 C2 O11 3.0(8) . . . . ? C20 C3 C2 C1 -175.9(5) . . . . ? N12 S1 C8 C9 -67.1(5) . . . . ? N12 S1 C8 C7 120.6(5) . . . . ? N12 N11 C20 C3 -176.7(5) . . . . ? O13 S1 N12 N11 168.3(4) . . . . ? O13 S1 C8 C9 42.2(5) . . . . ? O13 S1 C8 C7 -130.1(5) . . . . ? O12 S1 N12 N11 41.1(5) . . . . ? O12 S1 C8 C9 174.3(4) . . . . ? O12 S1 C8 C7 2.0(6) . . . . ? C9 C8 C7 C12 -5.1(9) . . . . ? C9 C8 C7 C18 173.1(6) . . . . ? C9 C10 C11 C12 -4.4(10) . . . . ? C9 C10 C11 C17 176.2(6) . . . . ? C3 C4 C5 C6 -3.8(9) . . . . ? C3 C2 C1 C14 177.1(5) . . . . ? C3 C2 C1 C6 -4.3(8) . . . . ? C4 C3 C2 O11 -177.5(5) . . . . ? C4 C3 C2 C1 3.6(8) . . . . ? C4 C5 C6 C1 3.0(10) . . . . ? C2 C3 C4 C5 0.5(8) . . . . ? C2 C3 C4 C16 177.4(5) . . . . ? C2 C1 C14 C13 -158.8(5) . . . . ? C2 C1 C14 C15 75.2(7) . . . . ? C2 C1 C6 C5 1.2(9) . . . . ? C14 C1 C6 C5 179.7(6) . . . . ? C8 S1 N12 N11 -77.0(4) . . . . ? C8 C9 C10 C11 0.2(9) . . . . ? C8 C7 C12 C11 0.8(10) . . . . ? C10 C9 C8 S1 -167.6(4) . . . . ? C10 C9 C8 C7 4.6(9) . . . . ? C6 C1 C14 C13 22.7(8) . . . . ? C6 C1 C14 C15 -103.3(7) . . . . ? C7 C12 C11 C10 3.9(10) . . . . ? C7 C12 C11 C17 -176.8(6) . . . . ? C16 C4 C5 C6 179.2(6) . . . . ? C19 C9 C8 S1 14.8(8) . . . . ? C19 C9 C8 C7 -173.0(6) . . . . ? C19 C9 C10 C11 178.0(6) . . . . ? C18 C7 C12 C11 -177.6(7) . . . . ? _shelx_res_file ; TITL SIR2014 run in space group P -1 CELL 0.71073 7.1561 12.13 12.6117 63.498 86.694 81.451 ZERR 1 0.0006 0.0011 0.0017 0.011 0.009 0.007 LATT 1 SFAC C H N O Pd S UNIT 40 50 4 6 1 2 EQIV $1 -X,1-Y,-Z L.S. 10 PLAN 2 TEMP 25 HTAB N12 O11_$1 CONF BOND $H MORE -1 fmap 2 acta MERG 2 REM REM REM WGHT 0.088100 0.569700 FVAR 5.16012 PD1 5 0.000000 0.500000 0.000000 10.50000 0.03128 0.03753 = 0.04024 -0.01978 0.00057 0.00661 S1 6 0.171778 0.434397 -0.268957 11.00000 0.03817 0.05801 = 0.04454 -0.02961 -0.00229 0.00753 O11 4 0.114175 0.382565 0.157327 11.00000 0.03456 0.04384 = 0.03846 -0.01423 0.00110 0.00807 N11 3 0.231389 0.464899 -0.082850 11.00000 0.03524 0.03452 = 0.03300 -0.01462 0.00293 -0.00175 C20 1 0.385045 0.390398 -0.030125 11.00000 0.02790 0.03603 = 0.04760 -0.02513 0.00233 -0.00361 N12 3 0.241454 0.520786 -0.208047 11.00000 0.03711 0.04204 = 0.03839 -0.01616 0.00293 0.00705 O13 4 0.156069 0.519820 -0.393208 11.00000 0.06917 0.08310 = 0.04158 -0.03342 -0.00848 0.02627 O12 4 0.009278 0.379818 -0.211031 11.00000 0.03402 0.08334 = 0.08316 -0.05283 0.00354 -0.00198 C9 1 0.538066 0.352170 -0.302569 11.00000 0.03593 0.04898 = 0.04010 -0.02458 -0.00528 0.00295 C3 1 0.417320 0.315724 0.093711 11.00000 0.03030 0.02972 = 0.04929 -0.01983 -0.00093 -0.00032 C4 1 0.596863 0.236867 0.128608 11.00000 0.02604 0.04564 = 0.05861 -0.02848 0.00024 0.00101 C2 1 0.282443 0.317134 0.181740 11.00000 0.03086 0.03275 = 0.05071 -0.02359 0.00218 -0.00213 C1 1 0.333646 0.244367 0.304915 11.00000 0.04554 0.03413 = 0.04045 -0.01266 -0.00768 0.00135 C14 1 0.193381 0.251056 0.397890 11.00000 0.05475 0.03679 = 0.03248 -0.01037 -0.00501 0.00174 AFIX 13 H14 2 0.137836 0.338396 0.369113 11.00000 -1.20000 AFIX 0 C5 1 0.632079 0.164360 0.246382 11.00000 0.04055 0.05342 = 0.06445 -0.02753 -0.01194 0.01170 AFIX 43 H5 2 0.743885 0.109427 0.270147 11.00000 -1.20000 AFIX 0 C8 1 0.369060 0.316704 -0.243352 11.00000 0.03650 0.04505 = 0.04019 -0.02470 0.00059 0.00019 C10 1 0.678814 0.259329 -0.301283 11.00000 0.04017 0.04920 = 0.05098 -0.02611 0.00865 -0.00036 AFIX 43 H10 2 0.791822 0.281332 -0.339868 11.00000 -1.20000 AFIX 0 C6 1 0.504893 0.170351 0.332215 11.00000 0.05147 0.04322 = 0.04929 -0.01362 -0.01235 0.00582 AFIX 43 H6 2 0.537907 0.121859 0.411617 11.00000 -1.20000 AFIX 0 C7 1 0.346179 0.189996 -0.176562 11.00000 0.04292 0.05146 = 0.05669 -0.02779 0.00085 -0.00600 C16 1 0.738918 0.229459 0.037356 11.00000 0.03211 0.06199 = 0.07992 -0.03354 -0.00046 0.01511 AFIX 33 H16A 2 0.691725 0.286441 -0.040645 11.00000 -1.50000 H16B 2 0.758509 0.146381 0.044515 11.00000 -1.50000 H16C 2 0.856516 0.250863 0.050386 11.00000 -1.50000 AFIX 0 C19 1 0.580708 0.485294 -0.364316 11.00000 0.05646 0.05352 = 0.05615 -0.03021 0.01156 -0.00621 AFIX 33 H19A 2 0.473086 0.540166 -0.359065 11.00000 -1.50000 H19B 2 0.608176 0.506995 -0.446105 11.00000 -1.50000 H19C 2 0.687832 0.492917 -0.326830 11.00000 -1.50000 AFIX 0 C12 1 0.493334 0.102763 -0.180597 11.00000 0.05289 0.03763 = 0.06898 -0.02461 0.00006 -0.00618 AFIX 43 H12A 2 0.481484 0.018780 -0.138362 11.00000 -1.20000 AFIX 0 C11 1 0.655218 0.135408 -0.244261 11.00000 0.05225 0.05549 = 0.05656 -0.03381 -0.00583 0.00936 C13 1 0.281763 0.211676 0.518839 11.00000 0.06881 0.06002 = 0.04371 -0.02201 -0.00004 -0.00732 AFIX 33 H13A 2 0.383038 0.258854 0.509869 11.00000 -1.50000 H13B 2 0.330170 0.124706 0.552727 11.00000 -1.50000 H13C 2 0.187713 0.226680 0.570051 11.00000 -1.50000 AFIX 0 C15 1 0.032574 0.177956 0.409179 11.00000 0.06195 0.07175 = 0.05803 -0.03066 0.01609 -0.01685 AFIX 33 H15A 2 -0.054030 0.183448 0.468213 11.00000 -1.50000 H15B 2 0.082345 0.092415 0.432044 11.00000 -1.50000 H15C 2 -0.032329 0.211760 0.334423 11.00000 -1.50000 AFIX 0 C18 1 0.179712 0.140256 -0.098670 11.00000 0.05957 0.06192 = 0.09069 -0.02252 0.01368 -0.01099 AFIX 33 H18A 2 0.087978 0.208520 -0.103021 11.00000 -1.50000 H18B 2 0.222452 0.090741 -0.018191 11.00000 -1.50000 H18C 2 0.123283 0.090006 -0.125470 11.00000 -1.50000 AFIX 0 C17 1 0.806548 0.035267 -0.250125 11.00000 0.08537 0.06040 = 0.08301 -0.03916 0.01544 0.01605 AFIX 33 H17A 2 0.909455 0.073617 -0.297824 11.00000 -1.50000 H17B 2 0.753272 -0.009511 -0.284642 11.00000 -1.50000 H17C 2 0.852018 -0.021237 -0.171594 11.00000 -1.50000 AFIX 0 H20 2 0.472845 0.393406 -0.083187 11.00000 0.02430 H12 2 0.166900 0.575264 -0.229279 11.00000 0.05887 HKLF 4 REM SIR2014 run in space group P -1 REM R1 = 0.0699 for 2843 Fo > 4sig(Fo) and 0.1022 for all 3939 data REM 249 parameters refined using 0 restraints END WGHT 0.0881 0.5697 REM Highest difference peak 1.449, deepest hole -1.131, 1-sigma level 0.114 Q1 1 0.0086 0.4594 0.0952 11.00000 0.05 1.45 Q2 1 0.1054 0.5661 -0.0194 11.00000 0.05 0.74 ; _shelx_res_checksum 14377 _shelx_hkl_file ; 0 0 -2 53407.3 1441.32 6 0 0 2 54949.9 1451.95 6 0 0 2 51376.5 1677.36 2 0 0 -2 56853.7 1768.25 2 0 0 2 52787.8 1179.81 4 0 0 -2 52058.4 1190.87 4 0 0 -3 29599.7 1145.50 4 0 0 -3 35428.0 1913.48 2 0 0 3 30112.5 1452.37 6 0 0 -3 29897.5 1372.73 6 0 0 3 32306.0 1149.95 4 0 0 3 29349.4 1597.97 2 0 0 4 46449.8 1565.03 4 0 0 4 49473.4 1978.19 6 0 0 -4 50746.7 1954.22 6 0 0 4 49347.9 2304.15 2 0 0 -4 47937.8 2342.52 2 0 0 -4 49828.6 1640.53 4 0 0 -5 32628.5 2221.91 2 0 0 5 33596.2 1823.77 6 0 0 -5 28626.8 1412.83 4 0 0 -5 30809.1 1711.63 6 0 0 5 30927.9 2055.16 2 0 0 5 31140.8 1444.65 4 0 0 6 1413.74 544.192 6 0 0 -6 1898.26 551.759 6 0 0 6 902.133 339.922 4 0 0 -7 15422.8 1901.76 2 0 0 7 14924.2 1230.95 4 0 0 7 16784.7 1582.35 6 0 0 -8 13918.7 2025.47 2 0 0 8 12624.5 1487.25 6 0 0 8 12876.8 1227.10 4 0 0 -9-349.067 869.110 2 0 0 9-213.491 381.770 4 0 0 9-685.188 440.252 6 0 0 10 9870.39 1260.55 4 0 0 -10 9587.04 1921.62 2 0 0 10 10082.0 1560.56 6 0 0 -11 7396.48 1927.20 2 0 0 11 5030.89 989.011 4 0 0 11 6277.17 1319.78 6 0 0 12 310.520 603.410 4 0 0 -12 4459.33 1632.96 2 0 0 12 5051.66 1352.18 6 0 0 13 2827.31 1017.13 6 0 0 -13 2963.34 1448.02 2 0 0 -14 2583.51 1463.68 2 0 0 14 355.334 711.112 6 0 1 -13 1578.59 1296.22 2 0 -1 13 1887.03 821.900 6 0 -1 12 3332.41 1158.49 6 0 1 -12 4476.07 1731.38 2 0 1 -11 6237.20 1863.48 2 0 -1 11 8058.12 1470.65 6 0 -1 10 2395.63 645.239 4 0 1 -10 3907.71 1302.06 2 0 -1 10 3243.00 955.579 6 0 -1 9 3709.30 736.602 4 0 -1 9 2398.60 721.625 6 0 1 -9 2840.68 1332.42 2 0 1 -8 7470.11 1551.02 2 0 -1 8 7456.21 1191.88 6 0 -1 8 7076.54 885.505 4 0 -1 7 12659.4 1074.45 4 0 1 -7 11908.5 1807.58 2 0 -1 7 12495.6 1363.22 6 0 1 -6 2975.16 649.654 6 0 -1 6 3089.62 506.352 4 0 1 -6 2824.18 979.565 2 0 -1 6 2990.28 636.941 6 0 1 -5 81636.0 3737.18 2 0 -1 5 78712.9 2090.10 4 0 -1 5 83906.7 2878.91 6 0 1 -5 78010.9 2705.48 6 0 -1 5 78777.3 3474.97 2 0 -1 4 25448.8 1015.09 4 0 -1 4 27222.3 1459.19 6 0 1 -4 25633.6 1391.89 6 0 -1 4 25184.8 1797.82 2 0 1 -4 25059.8 1870.03 2 0 1 -3-430.549 736.149 2 0 -1 3-393.042 444.968 6 0 -1 3 188.267 442.613 2 0 1 -3 341.764 268.500 6 0 -1 3 351.422 189.432 4 0 1 -2 21956.1 913.909 6 0 1 -2 19791.6 1261.00 2 0 -1 2 23050.4 946.458 6 0 -1 2 21341.1 1265.51 2 0 -1 -3 290674. 4181.43 6 0 -1 -3 290237. 4327.18 2 0 1 3 281311. 4209.43 2 0 1 3 294301. 4180.97 6 0 1 3 292774. 3958.32 4 0 -1 -3 288673. 3931.01 4 0 1 3 305943. 4254.59 7 0 -1 -4 14359.7 1052.56 6 0 1 4 14148.3 948.748 4 0 -1 -4 11401.3 906.713 2 0 1 4 13288.8 1066.67 2 0 -1 -4 14708.3 982.680 4 0 1 4 12599.1 991.547 7 0 1 4 13937.5 1049.84 6 0 1 5 3142.85 666.220 2 0 1 5 3392.22 640.680 6 0 1 5 3045.35 552.510 4 0 -1 -5 2033.05 627.138 2 0 -1 -5 3438.91 657.491 6 0 -1 -5 2911.23 511.891 4 0 1 5 2709.17 559.238 7 0 -1 -6 11805.7 1098.90 4 0 1 6 9568.75 1083.21 7 0 1 6 13702.5 1316.68 6 0 -1 -6 11280.6 1171.55 6 0 -1 -6 13165.5 1560.05 2 0 1 6 11637.0 1093.52 4 0 1 6 11056.4 1289.60 2 0 1 7 9296.13 1061.26 4 0 -1 -7 10299.0 1576.80 2 0 1 7 8252.96 1149.65 6 0 1 7 7560.56 1041.15 7 0 1 8 23683.5 1742.42 4 0 -1 -8 25261.5 2520.77 2 0 1 8 22378.5 2005.97 6 0 -1 -9 29.2220 802.772 2 0 1 9 529.967 396.200 4 0 1 9 783.463 654.971 6 0 1 10 18180.6 1740.79 4 0 -1 -10 17931.2 2565.59 2 0 1 10 18787.2 2120.48 6 0 1 11 8915.63 1573.28 6 0 -1 -11 10551.8 2191.60 2 0 1 11 7851.28 1258.72 4 0 -1 -12 844.807 948.081 2 0 1 12-235.420 741.274 6 0 1 12 1487.44 637.666 4 0 -1 -13 2993.43 1444.05 2 0 1 13 2299.56 993.023 6 0 1 13 47.7168 677.455 4 0 1 14 3535.09 1352.24 6 0 -1 -14 3563.51 1701.86 2 0 2 -13 2577.48 1750.27 2 0 -2 13-776.398 850.913 6 0 -2 12 2648.14 956.122 6 0 2 -12 1747.99 1281.84 2 0 2 -11 9909.13 2331.99 2 0 -2 11 6438.81 1367.99 6 0 2 -10 4215.04 1562.52 2 0 -2 10 3510.02 973.342 6 0 -2 9 5528.81 1168.34 6 0 2 -9 6769.02 1846.00 2 0 2 -8 14479.9 2229.79 2 0 -2 8 17055.9 1765.89 6 0 -2 7 1571.31 521.295 6 0 -2 7 569.329 280.196 4 0 2 -7 889.447 791.751 2 0 2 -6-328.099 699.353 2 0 2 -6 413.790 394.437 6 0 -2 6 231.045 219.777 4 0 -2 6 415.606 395.870 6 0 2 -5 107535. 4565.44 2 0 2 -5 98608.2 3051.43 6 0 -2 5 101057. 3145.98 6 0 2 -4 110905. 4237.79 2 0 2 -4 101725. 2742.28 6 0 -2 4 101399. 3839.49 2 0 -2 4 107152. 2866.60 6 0 2 -3 5830.53 967.172 2 0 -2 3 4520.57 796.642 2 0 2 -3 4725.45 542.205 6 0 -2 3 5318.52 592.576 6 0 -2 2 15946.8 777.620 6 0 2 -2 14819.9 781.351 6 0 2 -2 14882.3 1338.62 2 0 -2 2 16047.3 1240.96 2 0 -2 1 78045.2 2286.71 2 0 2 -1 72472.7 2253.50 2 0 -2 0 5857.49 575.321 2 0 -2 0 5192.67 525.713 7 0 2 0 4059.72 508.526 7 0 2 0 5303.85 405.970 4 0 2 0 5817.46 549.442 2 0 2 1 18026.8 959.256 1 0 -2 -2 149232. 2845.90 1 0 2 2 160974. 2879.97 4 0 -2 -2 156252. 2924.41 7 0 2 2 147558. 2846.03 1 0 -2 -2 155594. 2578.49 6 0 2 2 155801. 2974.71 7 0 2 2 154687. 2605.74 6 0 -2 -2 153082. 2801.95 3 0 -2 -2 155563. 2882.03 4 0 2 2 152986. 2960.49 3 0 -2 -3 127056. 2754.15 3 0 -2 -3 125142. 3010.78 7 0 2 3 130667. 2974.43 4 0 2 3 128006. 3086.48 1 0 -2 -3 130505. 3006.10 1 0 2 3 129413. 2991.87 3 0 2 3 133476. 3143.23 7 0 -2 -3 127223. 2943.45 4 0 -2 -3 130076. 2517.87 2 0 2 3 124564. 2415.66 2 0 -2 -3 131033. 2879.21 6 0 2 3 136250. 2933.24 6 0 2 4-509.914 505.923 7 0 -2 -4-153.477 451.343 6 0 2 4-1008.56 678.970 4 0 2 4-722.751 659.475 6 0 -2 -4-895.162 649.889 3 0 -2 -4-631.014 529.845 1 0 -2 -5 4726.91 735.048 6 0 2 5 4197.43 769.755 7 0 2 5 4434.71 723.430 4 0 -2 -5 4983.69 851.657 1 0 -2 -5 4736.61 765.255 3 0 2 5 3624.49 612.243 2 0 -2 -5 3902.49 621.864 4 0 -2 -5 3799.08 732.654 2 0 2 5 3893.03 696.818 6 0 -2 -6 1065.75 436.629 4 0 2 6 1129.71 460.109 2 0 -2 -6 1723.41 708.264 2 0 -2 -6 1310.30 575.733 1 0 2 6 1313.30 596.019 6 0 -2 -6 336.445 551.877 3 0 -2 -6 476.179 356.761 6 0 2 6 515.955 365.363 4 0 2 6 1572.21 527.643 7 0 -2 -7 15855.3 1798.02 2 0 -2 -7 15327.2 1578.62 3 0 2 7 14491.2 1499.74 6 0 -2 -7 14564.5 1703.82 1 0 2 7 15129.6 1404.54 4 0 -2 -7 12324.7 1289.22 4 0 2 7 13212.3 1444.22 2 0 2 7 10258.2 1236.91 7 0 2 8 21092.0 1754.83 4 0 -2 -8 19296.5 1886.12 3 0 2 8 19768.2 1892.28 6 0 -2 -8 18950.0 2080.11 2 0 2 9 3352.86 824.798 4 0 2 9 2268.80 759.281 6 0 -2 -9 2510.34 906.411 2 0 -2 -9 3840.46 1036.13 3 0 -2 -10 337.769 652.797 3 0 2 10-123.557 671.808 6 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733.182 2 0 6 3 11449.4 1413.77 1 0 6 3 10409.0 1334.57 3 0 -6 -3 8716.74 1098.23 4 0 -6 -3 9989.37 1225.81 7 0 6 3 9486.97 1232.12 7 0 6 3 8882.09 1020.11 6 0 6 3 9147.94 1106.50 4 0 6 4 1930.00 745.313 1 0 -6 -4 466.622 444.941 1 0 6 4 577.273 432.972 7 0 -6 -4 990.046 471.853 3 0 -6 -4 549.920 427.353 7 0 6 4 716.353 405.893 6 0 6 4 729.621 547.606 4 0 -6 -4 1026.01 467.964 4 0 6 4 1187.39 517.214 3 0 -6 -4 776.240 349.248 6 0 6 5 53303.7 3134.13 3 0 6 5 43089.9 1376.12 2 0 6 5 50441.8 2801.65 4 0 -6 -5 58549.0 3065.40 1 0 6 5 56633.6 3048.55 1 0 -6 -5 50616.7 2731.01 3 0 -6 -5 51745.8 2924.27 7 0 -6 -5 49346.5 2395.71 6 0 6 5 52252.8 2508.42 6 0 6 6 44383.2 2857.80 1 0 -6 -6 37922.2 2528.27 1 0 6 6 36449.8 2505.60 4 0 -6 -6 37657.6 2411.77 3 0 6 6 38004.9 2322.04 6 0 -6 -6 36081.5 2533.00 7 0 6 6 33354.9 1364.12 2 0 6 6 37161.9 2688.27 3 0 -6 -7 2599.86 837.736 7 0 6 7 2614.38 780.804 6 0 -6 -7 2574.53 752.452 3 0 6 7 3608.91 903.226 4 0 6 7 2791.07 895.090 1 0 6 7 2780.02 501.651 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6597.94 1438.17 3 0 8 13 8072.10 1771.17 4 0 8 14 2531.25 1104.78 6 0 8 14 4113.70 1288.77 4 0 8 15 1554.12 1049.31 6 0 8 15-129.035 559.138 4 0 9 -7 2598.69 1503.90 2 0 9 -6 1986.48 1370.56 2 0 9 -5 6952.81 1976.94 2 0 9 -4 2515.45 1136.90 2 0 -9 4 1127.05 496.190 7 0 9 -3 5574.65 1455.15 1 0 9 -3 9223.09 1810.16 2 0 -9 3 7687.93 1201.67 7 0 9 -2 6979.78 1713.21 1 0 -9 2 7863.93 1199.13 7 0 9 -2 4808.63 1378.11 2 0 9 -1 1454.40 717.281 2 0 9 -1 2847.12 1226.75 1 0 -9 1 3092.44 753.885 7 0 9 -1 2603.77 539.599 4 0 9 0 5290.10 1438.37 1 0 -9 0 4272.58 931.751 7 0 9 0 4328.16 752.876 4 0 9 0 3922.54 1050.38 2 0 -9 -1 7624.65 1170.17 7 0 9 1 7613.83 1293.79 2 0 9 1 7916.51 1575.39 1 0 9 1 7220.81 1033.18 4 0 9 2 4229.64 514.812 5 0 -9 -2 7133.84 1187.57 7 0 -9 -2 5369.37 568.760 6 0 9 2 8218.16 1255.41 2 0 9 2 6181.03 975.268 4 0 9 2 6662.92 1479.35 1 0 9 3 8057.01 1451.68 1 0 9 3 7071.87 952.544 2 0 -9 -3 7431.86 1239.86 7 0 -9 -3 6917.80 743.407 6 0 9 3 7183.74 1085.02 4 0 9 4 1126.73 677.511 4 0 -9 -4 873.633 661.053 7 0 -9 -4 179.550 308.283 6 0 9 4 290.687 584.123 1 0 9 4 299.710 402.239 2 0 -9 -5 22859.4 1701.52 6 0 9 5 24997.3 1273.77 2 0 -9 -5 28011.2 2443.97 7 0 9 5 27844.7 2356.57 4 0 9 6 25541.2 2517.13 1 0 -9 -6 19665.7 2102.08 7 0 9 6 20799.0 1966.18 6 0 9 6 13431.5 700.944 2 0 9 6 21111.1 2125.80 4 0 -9 -7 2439.78 854.904 7 0 9 7 4034.89 1090.22 1 0 9 7 3764.75 939.529 4 0 9 7 3226.21 877.261 6 0 -9 -7 3794.88 1073.86 3 0 9 8 25302.9 2705.08 1 0 9 8 20065.6 2066.91 6 0 9 8 20905.2 2337.72 4 0 -9 -8 18056.4 2237.74 7 0 -9 -8 18976.8 2118.01 3 0 -9 -9 20399.7 2278.42 3 0 -9 -9 18575.5 2299.64 7 0 9 9 22207.1 2456.50 4 0 9 9 19413.4 2186.55 6 0 -9 -10 3212.02 907.471 3 0 9 10 4422.31 1330.44 1 0 9 10 2490.52 944.537 6 0 9 10 4024.85 1236.63 4 0 9 11 2637.76 1288.00 1 0 -9 -11 1396.65 762.817 3 0 9 11 1306.38 898.781 4 0 9 11 708.939 622.670 6 0 9 12 1955.00 909.535 6 0 9 12 1790.53 880.314 4 0 -9 -12 2509.51 1005.47 3 0 9 13 5678.76 1476.14 6 0 9 13 4952.91 1438.93 4 0 -9 -13 4982.17 1297.21 3 0 9 14 1263.70 922.594 6 0 9 14-944.319 960.781 4 0 9 15 390.916 631.258 4 0 9 15 255.449 709.685 6 0 10 -5 251.796 887.610 2 0 10 -5 1209.92 1062.35 1 0 10 -4 3930.68 1366.83 2 0 10 -4 1349.64 982.279 1 0 10 -3 2134.82 1010.22 2 0 10 -3 1006.87 901.289 1 0 10 -2 7784.52 1713.23 2 0 -10 2 10111.6 1376.16 7 0 10 -2 11036.0 2198.44 1 0 10 -1 740.229 753.452 1 0 -10 1 1927.70 708.423 7 0 -10 0 2695.36 758.860 7 0 10 0 1759.20 544.586 4 0 10 0 1310.79 944.535 1 0 10 0 1211.17 751.914 2 0 -10 -1 18147.9 1895.58 7 0 10 1 14354.6 1480.86 4 0 10 1 16406.2 1985.66 2 0 10 1 16669.8 2424.87 1 0 -10 -2 3487.56 426.393 6 0 -10 -2 5863.81 1112.67 7 0 10 2 5201.66 940.007 4 0 10 2 4559.56 969.090 2 0 -10 -3 1824.02 408.562 6 0 10 3 3131.11 1033.14 1 0 -10 -3 3810.58 999.037 7 0 10 3 1496.12 422.961 5 0 10 3 2324.10 712.989 4 0 10 3 2746.53 751.671 2 0 10 4 2578.51 712.378 2 0 10 4 5477.50 1644.06 1 0 -10 -4 1592.31 492.234 6 0 -10 -4 5319.74 1238.06 7 0 10 4 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681.920 4 0 10 15-1046.80 886.429 6 0 11 -4 998.087 1300.83 2 0 11 -4-1234.48 969.815 1 0 11 -3 4143.94 1570.29 1 0 11 -3 4614.66 1667.31 2 0 11 -2 1697.38 1059.73 2 0 11 -2 631.664 1022.75 1 0 11 -1 3605.45 1204.97 2 0 11 -1 3848.47 1217.11 1 0 -11 1 3847.89 937.068 7 0 -11 0 6737.17 1235.40 7 0 11 0 6394.23 1672.07 1 0 11 0 5779.54 1430.56 2 0 -11 -1 6205.80 1182.84 7 0 11 1 5012.52 901.041 4 0 11 1 5762.77 1577.29 1 0 11 1 5821.00 1295.93 2 0 11 2 4516.32 1034.36 2 0 -11 -2 5479.71 1189.53 7 0 11 2 5368.03 994.821 4 0 11 2 4099.73 1308.68 1 0 11 3 1062.37 653.656 4 0 -11 -3 192.488 504.712 7 0 11 3 293.693 569.023 2 0 11 3 1251.46 1010.44 1 0 11 4 6175.67 1075.74 2 0 11 4 9389.28 1818.23 1 0 11 4 6318.79 1260.72 4 0 -11 -4 7518.68 1354.95 7 0 11 5 8140.32 1712.21 1 0 11 5 5741.24 832.132 2 0 -11 -5 6659.31 1289.41 7 0 11 5 5402.91 1166.74 4 0 11 6 722.262 766.186 1 0 11 6-500.222 713.443 4 0 -11 -6 1144.18 788.467 7 0 11 7-70.5314 563.816 4 0 -11 -7 1636.45 922.614 7 0 11 7 2779.71 982.873 1 0 -11 -8 19618.0 2427.68 7 0 11 8 23029.5 2418.26 6 0 11 8 20570.4 2404.36 4 0 11 8 27411.5 2950.85 1 0 -11 -9 1660.54 820.249 7 0 11 9 5179.46 1278.28 6 0 11 9 5023.83 1306.98 4 0 11 9 6926.78 1670.51 1 0 11 10 255.696 512.073 6 0 11 10 457.333 619.946 1 0 11 10 141.343 604.263 4 0 11 11 1947.97 871.304 1 0 11 11 752.144 689.172 6 0 11 11 473.861 653.957 4 0 -11 -11 1728.29 860.099 3 0 -11 -12 5378.18 1437.13 3 0 11 12 3624.40 1205.46 6 0 11 12 3748.14 1360.30 4 0 11 12 3887.37 1509.71 1 0 11 13-1063.54 930.123 4 0 11 13-17.3062 619.551 6 0 -11 -13 985.527 869.371 3 0 11 14 552.714 679.978 4 0 11 14-129.835 696.904 6 0 12 -2 3402.56 1527.13 2 0 12 -2-705.375 1126.63 1 0 12 -1-208.383 1082.28 2 0 12 -1 513.064 849.403 1 0 12 0 3523.58 1219.44 2 0 12 0 3799.56 1572.94 1 0 12 1 6628.39 1782.77 1 0 12 1 6294.83 1445.92 2 0 -12 -1 7669.45 1381.30 7 0 12 2 1406.15 881.590 2 0 12 2 4211.33 1472.63 1 0 12 2 2799.36 831.920 4 0 -12 -2 4799.77 1163.46 7 0 12 3 1537.51 1079.48 1 0 12 3 2559.90 857.927 4 0 -12 -3 2440.72 894.014 7 0 12 3 2319.15 836.281 2 0 -12 -4 1684.12 730.439 7 0 12 4 834.667 794.003 1 0 12 4 1853.45 833.702 4 0 12 5 3953.87 1248.22 1 0 12 5 2946.96 1045.96 4 0 -12 -5 2680.96 1002.02 7 0 12 6 1121.22 735.639 4 0 12 6 1479.14 908.713 1 0 -12 -6 1550.50 937.724 7 0 12 7 10366.3 1905.07 1 0 -12 -7 9571.85 1704.79 7 0 12 7 10816.8 1795.02 4 0 -12 -8 7576.08 1593.15 7 0 12 8 11222.0 2064.70 1 0 12 8 9226.79 1734.50 4 0 12 9 166.961 693.012 1 0 12 9 64.0675 657.902 6 0 -12 -9-467.552 963.170 7 0 12 9 988.322 629.123 4 0 12 10 1907.69 1057.76 1 0 12 10 1409.17 785.960 6 0 12 10-197.146 794.737 4 0 12 11 3389.12 1339.61 1 0 12 11 2809.98 1159.22 6 0 12 11 3434.19 1225.43 4 0 12 12 4948.00 1575.67 1 0 12 12 2814.41 1105.34 6 0 12 12 4482.16 1363.15 4 0 12 13-164.468 693.474 6 0 12 13 108.049 779.387 1 0 12 13 2254.83 1246.56 4 0 12 14 128.703 570.110 4 0 12 14-916.517 851.888 6 0 13 0 635.529 885.229 1 0 13 1 1023.36 800.029 1 0 -13 -2-86.3456 431.696 7 0 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770.356 7 0 14 5 2173.05 1172.37 1 0 14 6 1599.34 890.498 4 0 -14 -6 1682.87 604.607 7 0 14 6 2100.23 1048.90 1 0 -14 -7 2240.66 1072.10 7 0 14 7 3366.42 1239.63 4 0 14 7 3802.26 1398.55 1 0 14 8 1821.81 1070.72 1 0 -14 -8 4666.15 1432.38 7 0 14 8 5192.25 1377.19 4 0 14 9 393.354 525.956 4 0 -14 -9-535.653 722.084 7 0 14 10-128.126 594.951 4 0 14 10 428.128 895.667 1 0 14 11 2468.92 975.934 4 0 14 11 4503.86 1508.35 1 -1 14 10 3562.61 1364.08 4 1 -14 -10 4635.96 1590.06 7 -1 14 10 6160.13 1843.91 1 -1 14 9 2069.26 1123.89 1 1 -14 -9 1515.54 836.161 7 -1 14 9 1198.41 751.521 4 1 -14 -8-56.3499 643.328 7 -1 14 8 1240.64 1047.71 1 -1 14 8 1382.60 1058.88 4 -1 14 7 1798.69 1023.99 1 1 -14 -7 2158.63 1135.33 7 -1 14 7 2237.43 941.267 4 1 -14 -6 4030.47 1286.04 7 -1 14 6 2913.24 1019.58 4 -1 14 6 4151.96 1462.54 1 1 -14 -5 1422.30 906.531 7 -1 14 5 428.455 562.694 4 -1 14 5 2474.00 1301.64 1 1 -14 -4 2304.15 1072.57 7 -1 14 4 1457.66 967.152 1 -1 14 3 1533.34 1114.98 1 1 -14 -3 530.970 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1611.08 2 -2 4 13 9727.32 2059.02 6 -2 4 12 5678.70 1486.87 6 -2 4 12 5074.15 1349.08 4 2 -4 -12 4632.05 1430.46 2 -2 4 11 1127.15 891.808 4 2 -4 -11 1570.73 961.193 2 -2 4 11 2523.24 1043.33 6 -2 4 10 581.431 562.886 4 2 -4 -10 2096.83 794.815 2 -2 4 10 1919.76 1010.62 6 2 -4 -9 10871.5 1439.12 2 -2 4 9 13519.5 1859.80 4 -2 4 9 11915.1 1819.35 6 2 -4 -9 9202.86 1575.92 7 -2 4 8 7245.73 1360.37 4 2 -4 -8 6522.42 1016.29 2 2 -4 -8 7059.73 1415.80 7 -2 4 8 5263.63 1183.06 6 -2 4 7 6925.50 1282.84 4 2 -4 -7 6352.15 836.481 2 2 -4 -7 7798.32 1362.27 7 -2 4 7 7426.94 1432.13 1 -2 4 7 7611.69 912.457 3 -2 4 7 7593.19 1315.45 6 2 -4 -6 24201.2 1362.31 2 -2 4 6 26286.2 2266.46 4 2 -4 -6 28618.8 2339.58 7 -2 4 6 26469.6 2435.30 1 -2 4 6 26077.9 1654.87 3 -2 4 5 35016.6 2506.85 4 2 -4 -5 33746.9 1329.20 2 2 -4 -5 36441.4 2562.88 7 -2 4 5 35224.5 1919.45 3 -2 4 5 34873.8 2629.63 1 2 -4 -4-47.2850 332.734 4 -2 4 4-142.082 483.935 4 -2 4 4-242.666 492.424 1 2 -4 -4-105.676 544.991 7 2 -4 -4 250.975 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2 -4 1 5242.55 1022.83 2 -2 4 -1 4108.38 883.146 2 -2 4 -2 56871.4 3366.30 1 2 -4 2 66335.8 2558.84 4 -2 4 -2 63408.0 3569.43 2 2 -4 2 55604.0 2333.89 5 2 -4 3 16618.6 1393.31 5 -2 4 -3 16204.5 1917.53 1 -2 4 -3 16423.5 2004.67 2 2 -4 3 20023.4 1330.80 4 2 -4 4 1816.22 582.410 5 2 -4 4 1742.09 390.405 4 -2 4 -4 1845.21 986.409 2 2 -4 4 2766.31 752.895 6 2 -4 5 3970.45 467.185 4 -2 4 -5 7196.23 1653.05 2 2 -4 5 7765.37 1131.54 6 2 -4 5 7935.21 1175.14 5 -2 4 -6 30772.4 3268.51 2 2 -4 6 30082.6 2245.14 6 2 -4 6 23470.2 2159.01 5 2 -4 7 8425.75 1348.41 6 -2 4 -7 7543.81 1953.80 2 2 -4 8 5668.74 1215.00 6 -2 4 -8 4580.46 1595.08 2 2 -4 9 4482.58 1142.14 6 -2 4 -9 5070.37 1825.45 2 -2 4 -10 1725.09 1291.94 2 2 -4 10 2921.67 924.451 6 -2 4 -11 1896.33 1417.34 2 -2 3 14 194.194 668.079 4 -2 3 14 2041.81 989.128 6 2 -3 -14-906.685 1011.27 2 -2 3 13 3202.84 1255.66 4 2 -3 -13 2981.56 1291.90 2 -2 3 13 3772.79 1365.27 6 -2 3 12 5957.61 1500.67 4 2 -3 -12 5500.91 1376.19 2 -2 3 12 4731.75 1446.92 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1642.87 6 2 8 14 8705.63 1864.43 4 -2 -8 -14 10463.7 2450.73 3 2 8 15 930.439 802.138 4 2 8 15 3356.83 1305.11 6 -2 -8 -15 551.434 976.954 3 2 9 -7 1052.89 1240.01 2 2 9 -6 853.852 1150.42 2 2 9 -5 5182.73 1640.40 2 2 9 -4 2376.39 1143.35 2 2 9 -3-341.647 940.710 2 2 9 -2 1512.75 864.945 2 2 9 -2 923.678 431.768 4 2 9 -1 19798.7 2399.96 2 2 9 -1 15420.1 1390.75 4 2 9 0 31790.1 2824.75 2 2 9 0 20150.8 1765.91 4 2 9 1 1178.85 508.929 5 2 9 1 436.195 553.908 2 2 9 1 707.439 335.890 7 2 9 1 762.293 438.854 4 2 9 1 466.195 564.984 1 2 9 2 10681.2 1293.98 5 2 9 2 12570.7 1807.55 1 2 9 2 8978.59 1292.11 4 2 9 2 10613.6 1418.82 7 2 9 2 6353.42 519.681 6 2 9 3 12506.9 1700.69 1 2 9 3 11235.3 1475.28 4 2 9 3 11669.7 938.208 6 -2 -9 -3 11635.4 1790.76 3 2 9 3 9868.28 1281.50 5 2 9 4 5614.63 1140.93 1 2 9 4 3544.01 849.341 5 2 9 4 4582.14 1024.24 4 2 9 4 4394.63 734.598 6 -2 -9 -4 4162.96 1120.79 3 2 9 5 2847.92 818.960 1 2 9 5 2691.98 894.667 4 2 9 5 2094.51 561.960 6 -2 -9 -5 1706.16 845.444 3 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5811.36 867.188 4 2 10 -1 10956.2 1975.06 2 2 10 0 8030.87 1171.70 4 2 10 0 11846.3 1838.76 2 2 10 0 8588.91 1825.62 1 2 10 1 663.683 428.426 4 2 10 1 2247.20 990.749 2 2 10 1 824.985 789.200 1 2 10 2 2383.74 1061.80 2 2 10 2 1805.92 724.458 4 2 10 2 3437.81 1194.74 1 2 10 3 17201.3 1899.51 4 2 10 3 14371.8 1068.10 6 2 10 3 16459.0 1693.60 5 2 10 4 2223.60 872.338 1 2 10 4 2024.43 672.885 5 2 10 4 2343.24 914.490 4 2 10 4 2245.54 565.220 6 -2 -10 -4 2566.23 1064.65 3 2 10 5 2279.33 987.479 1 2 10 5 1373.71 583.269 4 2 10 5 26.0445 373.604 6 -2 -10 -5 1019.60 824.343 3 2 10 6 5705.20 1232.46 1 2 10 6 4976.88 1157.94 4 2 10 6 5543.75 969.837 6 -2 -10 -6 4853.09 1220.16 3 2 10 7 2315.17 951.505 1 2 10 7 3089.51 959.139 4 2 10 7 3247.21 802.342 6 -2 -10 -7 1828.92 924.476 3 2 10 8 1889.42 845.134 4 2 10 8 1595.48 792.119 1 2 10 8 1042.61 521.312 6 -2 -10 -8 2713.18 1126.36 3 2 10 9 2221.07 878.725 4 2 10 9 1051.02 878.132 1 2 10 9 3026.29 910.222 6 -2 -10 -9 705.967 682.544 3 2 10 10 5057.17 1222.21 4 2 10 10 5064.21 1313.05 1 2 10 10 5427.15 1264.90 6 -2 -10 -10 4749.05 1466.44 3 2 10 11 903.606 858.239 4 2 10 11 1967.69 858.844 6 -2 -10 -11 2330.14 1050.54 3 2 10 12 3100.34 1138.89 4 2 10 12 2814.69 1018.19 6 -2 -10 -12 4153.18 1462.41 3 -2 -10 -13 6244.86 1830.34 3 2 10 13 6757.96 1570.42 6 2 10 13 8334.74 1765.14 4 2 10 14 1240.21 742.620 6 -2 -10 -14 1627.49 1283.19 3 2 10 14 3169.37 1295.51 4 2 10 15-2470.42 1202.33 4 2 10 15-352.042 858.580 6 -2 -10 -15 416.679 1159.01 3 2 11 -4-84.2544 864.755 2 2 11 -3-343.307 719.418 2 2 11 -2 3382.29 1398.41 2 2 11 -1 5553.90 1499.14 2 2 11 -1 3706.32 1326.81 1 2 11 0 624.096 664.057 2 2 11 0 1947.43 1058.12 1 2 11 1 2308.71 1010.37 2 2 11 1 2167.33 1069.47 1 2 11 1 1329.91 568.616 4 2 11 2 9384.71 1564.42 2 2 11 2 7698.17 1252.03 4 2 11 2 6845.14 1501.30 1 2 11 3 8227.37 1353.25 4 2 11 3 10185.3 1621.26 2 2 11 3 10015.7 1806.41 1 2 11 4 52.3969 436.764 4 2 11 4-337.842 335.509 6 2 11 5 1870.65 999.411 1 2 11 5 609.516 449.671 4 2 11 5 447.729 492.430 6 -2 -11 -5 875.542 821.548 3 2 11 6 7615.94 1469.94 1 2 11 6 4577.31 1083.48 4 2 11 6 5628.78 974.706 6 -2 -11 -6 4986.60 1327.43 3 2 11 7 1249.98 692.737 4 2 11 7 1635.00 761.485 1 2 11 7 1103.90 514.775 6 -2 -11 -7 971.144 844.415 3 2 11 8 1597.90 832.488 1 -2 -11 -8 2035.64 937.988 3 2 11 8 1775.76 781.299 4 2 11 8 1560.55 726.466 6 2 11 9 4969.22 1402.11 1 2 11 9 3606.69 949.538 6 -2 -11 -9 3094.32 1151.22 3 2 11 9 3209.94 971.884 4 2 11 10 1117.35 790.626 1 -2 -11 -10-485.047 600.470 3 2 11 10 415.161 682.811 4 2 11 10 1530.70 786.199 6 2 11 11 879.166 752.154 4 2 11 11 3209.56 1126.09 1 2 11 11 2162.64 890.436 6 -2 -11 -11 2395.17 1183.68 3 2 11 12 745.101 707.966 4 2 11 12 746.469 639.791 6 -2 -11 -12 1412.04 1198.50 3 2 11 13 7690.03 1674.62 6 2 11 13 10816.6 2076.11 4 -2 -11 -13 9218.25 2245.30 3 2 11 14 7392.27 1745.55 4 2 11 14 7379.48 1799.40 6 -2 -11 -14 6357.12 1870.08 3 2 12 -2 2419.90 1376.97 2 2 12 -2 1168.24 1131.69 1 2 12 -1 4837.03 1519.65 2 2 12 -1 1817.83 1266.56 1 2 12 0-279.690 683.997 2 2 12 0 1380.17 951.436 1 2 12 1 3542.24 1229.46 2 2 12 1 2288.76 1220.27 1 2 12 2 4887.72 1031.24 4 2 12 2 8070.10 1518.99 2 2 12 2 6874.54 1745.71 1 2 12 3 2266.48 1011.97 1 2 12 3 1072.25 675.304 4 2 12 3 2137.69 813.627 2 2 12 4 2014.19 1074.31 1 2 12 4 1813.97 862.984 2 2 12 4-13.9604 460.853 4 2 12 5 1578.87 692.185 4 2 12 5 744.038 753.395 1 2 12 5 979.268 586.422 2 2 12 6 2137.42 763.019 4 2 12 6 2744.85 1013.90 1 2 12 6 2355.26 651.751 6 -2 -12 -6 805.228 653.638 3 2 12 7 3024.47 1109.66 1 2 12 7 2272.40 819.403 4 2 12 7 3371.25 898.079 6 -2 -12 -7 2833.97 1121.54 3 2 12 8 1941.32 847.388 4 2 12 8 2221.71 709.838 6 -2 -12 -8 2534.18 1084.65 3 2 12 8 3354.10 1120.99 1 2 12 9 3555.08 1155.03 1 2 12 9 3324.33 1180.69 4 2 12 9 3439.52 922.258 6 -2 -12 -9 4763.13 1518.95 3 2 12 10 576.521 838.681 4 2 12 10 516.047 680.827 1 2 12 10-11.0961 549.206 6 -2 -12 -10 379.047 655.824 3 2 12 11 2234.57 1035.91 1 2 12 11 2136.51 925.233 4 2 12 11 1360.21 818.813 6 -2 -12 -11 2236.48 1082.94 3 2 12 12 2655.87 1104.44 4 -2 -12 -12 477.029 836.612 3 2 12 12 1471.72 856.955 6 -2 -12 -13 1133.85 857.370 3 2 12 13 437.673 685.156 4 2 12 14 4179.14 1435.64 4 2 12 14 5280.31 1563.69 6 -2 -12 -14 5377.28 1777.24 3 2 13 -1 1941.12 1343.01 1 2 13 -1 310.166 1011.24 2 2 13 0 655.967 926.521 2 2 13 0 822.918 1039.15 1 2 13 1 2224.07 1083.11 2 2 13 1 12.0343 731.510 1 2 13 2 4330.42 1233.68 2 2 13 2 2971.58 1297.40 1 2 13 3 2634.89 1128.16 1 2 13 3 2193.74 851.817 4 2 13 3 2317.41 1071.02 2 2 13 4 4025.12 1322.07 1 2 13 4 1588.13 807.391 4 2 13 4 3823.72 1183.78 2 2 13 5 3404.99 953.550 4 2 13 5 5658.22 1511.07 1 2 13 6 3662.82 1298.69 1 2 13 6 2637.03 900.807 4 2 13 7 912.690 547.385 4 2 13 7 1100.23 774.837 1 2 13 8 1263.50 769.564 4 -2 -13 -8 2295.78 1058.67 3 2 13 8 1797.46 957.499 1 2 13 9 4498.99 1382.32 4 2 13 9 4969.74 1386.23 1 2 13 9 5332.46 1276.14 6 -2 -13 -9 2989.74 1315.49 3 2 13 10 6490.80 1593.23 1 2 13 10 5819.69 1382.47 6 -2 -13 -10 6408.34 1664.63 3 2 13 10 5489.83 1499.11 4 2 13 11 267.605 732.888 4 2 13 11 712.916 544.804 6 2 13 12-12.3611 676.374 4 2 13 12 613.435 584.175 6 2 13 13-56.0051 687.204 6 -2 -13 -13 2682.37 1246.93 3 2 13 13 1652.00 1001.66 4 2 14 2 430.062 971.572 1 2 14 3 884.789 848.878 1 2 14 4 752.703 969.615 1 2 14 4 1087.54 681.429 4 2 14 5 3487.17 1377.72 1 2 14 5 3339.18 1091.88 4 2 14 6 2399.93 960.618 4 2 14 6 330.340 900.256 1 2 14 7-27.7683 670.539 1 2 14 7 1398.24 746.660 4 2 14 8 1113.18 696.503 4 2 14 8 1931.41 1084.70 1 2 14 9 6487.18 1665.05 1 2 14 9 6405.15 1635.76 4 -2 -14 -9 3143.89 1129.96 3 2 14 10 3272.98 1190.99 4 -2 -14 -10 2491.26 1148.68 3 2 14 11 453.408 644.213 4 2 14 11 154.690 525.856 6 -2 -14 -11 144.036 694.749 3 2 15 6 1006.84 726.032 4 2 15 6 1127.71 848.075 1 2 15 7 1841.40 1208.84 1 2 15 7 614.836 687.454 4 2 15 8 323.314 613.248 1 2 15 8 714.902 706.576 4 -3 13 9 3039.71 1154.10 4 3 -13 -9 2625.37 1191.09 7 -3 13 9 2425.23 1384.36 1 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600.346 4 -3 12 4 2748.86 1211.04 1 3 -12 -4 2519.14 1153.24 7 3 -12 -3 5054.67 1558.24 7 -3 12 3 4642.37 1521.69 1 -3 12 2 3051.44 1428.72 1 3 -12 -2-154.586 991.944 7 -3 12 1-636.039 863.409 1 3 -12 -1-10.1454 670.489 7 3 -12 0 2739.78 1315.20 7 -3 12 0 2003.35 1335.91 1 -3 11 12 4337.63 1696.00 4 -3 11 12 1332.01 1141.18 1 3 -11 -12 2308.30 1388.23 7 -3 11 11 4561.43 1636.19 4 3 -11 -11 4884.97 1666.82 7 -3 11 11 3545.96 1393.06 1 -3 11 10 4661.68 1691.53 1 -3 11 10 3558.60 1388.50 4 3 -11 -10 3299.16 1373.01 7 3 -11 -9 717.827 804.382 7 -3 11 9 1007.91 899.536 5 -3 11 9 1498.24 895.325 4 -3 11 9 2319.83 1290.15 1 -3 11 8 427.923 688.778 5 -3 11 8 1017.93 761.613 4 -3 11 8 1482.52 1040.09 1 3 -11 -8-370.025 617.551 7 3 -11 -7 4232.85 1371.33 7 -3 11 7 3122.95 1262.52 1 -3 11 7 3655.10 1158.74 5 -3 11 7 3345.03 1238.82 4 -3 11 6 9286.15 2068.42 1 -3 11 6 9002.95 1666.02 5 -3 11 6 8986.53 1775.13 4 3 -11 -6 9324.96 1823.58 7 -3 11 5-157.373 579.521 5 -3 11 5 802.206 664.900 4 3 -11 -5 992.411 767.996 7 -3 11 5 1564.08 1031.97 1 3 -11 -4 6663.75 1533.65 7 -3 11 4 5988.53 1426.39 4 -3 11 4 7245.17 1783.38 1 -3 11 3 16296.6 2645.41 1 -3 11 3 11649.7 1860.07 4 3 -11 -3 15645.8 2472.19 7 3 -11 -2 3410.40 1260.79 7 -3 11 2 2230.25 1191.75 1 -3 11 1-425.476 707.036 1 3 -11 -1-1259.68 867.318 7 -3 11 0 667.093 951.489 1 3 -11 0 3015.53 1231.96 7 -3 11 -1 4183.01 1631.99 1 3 -11 1 3708.05 1581.80 7 -3 11 -2 924.279 861.606 1 3 -11 2 2596.75 1232.41 7 3 -10 -13 969.930 921.750 7 -3 10 13 760.001 883.545 4 -3 10 12-136.589 669.848 4 -3 10 12-459.659 855.265 1 3 -10 -12 1298.02 842.620 7 3 -10 -11 3038.97 1347.01 7 -3 10 11 4275.65 1605.89 1 -3 10 11 2717.73 1226.08 4 -3 10 10 4721.78 1559.49 4 -3 10 10 5116.22 1602.45 1 3 -10 -10 4524.57 1494.75 7 -3 10 9 3190.94 1381.07 1 3 -10 -9 4566.77 1427.97 7 -3 10 9 5393.74 1572.61 4 -3 10 8 1949.51 940.068 5 -3 10 8 2242.65 1017.04 4 3 -10 -8 2452.13 1068.24 7 -3 10 8 2916.79 1364.53 1 -3 10 7-338.734 592.144 5 -3 10 7 897.063 948.885 1 -3 10 7 36.0817 631.709 4 3 -10 -7-373.274 667.011 7 -3 10 6 69.2351 820.345 1 -3 10 6 600.153 580.281 5 -3 10 6 680.002 811.545 4 3 -10 -6 52.3011 791.543 7 -3 10 5 1105.63 654.544 5 -3 10 5 1271.93 831.374 4 3 -10 -5-385.711 788.465 7 -3 10 5 2447.88 1304.55 1 -3 10 4 3865.01 998.743 5 -3 10 4 5209.55 1369.87 4 -3 10 4 4215.06 1564.70 1 3 -10 -4 4619.58 1279.11 7 -3 10 3 18243.6 2009.79 5 -3 10 3 21354.5 2504.81 4 -3 10 3 25501.7 3161.16 1 3 -10 -3 23391.7 2790.63 7 -3 10 2 6629.73 1853.06 1 3 -10 -2 9997.61 1991.77 7 -3 10 1-169.031 712.790 2 -3 10 1 882.379 858.552 1 3 -10 -1-1045.12 854.668 7 -3 10 0 4122.42 1347.58 2 -3 10 0 5435.31 1564.67 1 3 -10 0 5888.67 1703.58 7 -3 10 -1 8801.59 1940.97 2 -3 10 -1 6610.23 1869.93 1 3 -10 1 7036.57 1826.88 7 -3 10 -2 2911.02 1224.42 1 3 -10 2 3831.54 1415.85 7 -3 10 -2 3188.18 1186.46 2 -3 10 -3 4258.51 1626.81 1 3 -10 3 3406.08 1351.36 7 -3 10 -3 1420.21 1051.57 2 -3 9 13 989.904 934.975 4 3 -9 -13 966.571 1043.57 7 -3 9 12 1333.98 1138.36 1 3 -9 -12 2845.84 1126.48 7 -3 9 12 2250.94 1099.98 4 -3 9 11 5408.61 1749.31 1 -3 9 11 6973.43 1854.23 4 3 -9 -11 2834.92 1283.16 7 -3 9 10 6450.95 1676.02 4 3 -9 -10 5812.93 1483.92 7 -3 9 10 9100.19 2226.88 1 -3 9 9 3783.65 1326.70 1 -3 9 9 1553.65 923.696 4 3 -9 -9 3034.72 1208.85 7 3 -9 -8 2901.94 1146.33 7 -3 9 8 4164.56 1315.97 4 -3 9 8 3452.48 1282.26 1 -3 9 7 14905.2 2245.22 4 -3 9 7 14377.6 2107.15 5 3 -9 -7 15901.5 2385.75 7 -3 9 7 16387.1 2510.99 1 -3 9 6 604.969 623.625 1 -3 9 6 376.796 553.319 5 -3 9 6-780.642 673.955 4 3 -9 -6 220.695 603.632 7 3 -9 -5 272.676 621.942 7 -3 9 5-254.372 563.746 5 -3 9 5 140.760 540.629 4 -3 9 5-1798.68 992.541 1 -3 9 4 6230.73 1217.14 5 -3 9 4 8234.76 1588.12 4 3 -9 -4 6080.80 1494.78 7 -3 9 4 9300.27 1920.19 1 -3 9 3 14188.5 2105.10 4 -3 9 3 15507.4 2457.88 1 3 -9 -3 16353.6 2326.59 7 -3 9 3 13994.0 1761.91 5 -3 9 2 7730.87 1269.67 5 -3 9 2 7026.57 1719.26 1 3 -9 -2 9765.22 1885.79 7 -3 9 1 4980.78 1258.31 2 -3 9 1 5541.08 1611.97 1 3 -9 -1 6176.12 1524.86 7 -3 9 0 11964.9 1899.88 2 3 -9 0 13195.8 2299.55 7 -3 9 0 14056.0 2381.23 1 -3 9 -1 8426.88 1791.69 2 -3 9 -1 5452.96 1575.91 1 3 -9 1 9175.21 2032.73 7 -3 9 -2 336.640 699.932 1 3 -9 2-1210.31 1040.47 7 -3 9 -2 1071.89 1071.63 2 3 -9 3 3504.69 1472.34 7 -3 9 -3 3585.31 1319.73 1 -3 9 -3 5363.72 1624.14 2 -3 9 -4 1698.31 1014.08 1 3 -9 4 1637.76 1005.26 7 3 -9 5 532.230 916.647 7 -3 9 -5 1480.65 1099.18 1 -3 8 14 6042.76 1854.43 4 -3 8 13 85.6684 774.253 4 3 -8 -13 844.714 862.985 7 -3 8 12 1287.11 932.339 4 3 -8 -12 776.035 1019.84 7 3 -8 -11 2254.59 1210.27 7 -3 8 11 3321.56 1493.91 1 -3 8 11 4359.13 1504.12 4 -3 8 10 1987.13 934.581 4 3 -8 -10 1828.49 1183.12 7 -3 8 10 3280.91 1444.96 1 3 -8 -9 2669.21 1082.64 7 -3 8 9 3750.38 1330.86 4 -3 8 9 677.740 835.090 1 -3 8 8 10256.3 2090.90 1 -3 8 8 12993.5 2142.56 4 3 -8 -8 11341.5 2044.29 7 -3 8 7 39805.6 3452.89 5 -3 8 7 48553.9 3908.15 4 3 -8 -7 47222.2 3854.04 7 -3 8 7 46082.3 4054.81 1 3 -8 -6 7050.51 1504.51 7 -3 8 6 7191.20 1453.07 5 -3 8 6 7458.38 1649.41 1 -3 8 6 6295.08 1381.94 4 -3 8 5 4130.96 1284.53 1 -3 8 5 2053.76 828.318 5 -3 8 5 2550.93 1005.81 4 3 -8 -5 3161.48 1153.97 7 -3 8 4 21271.2 2187.71 5 3 -8 -4 18258.3 1164.27 2 -3 8 4 20364.5 2382.51 4 -3 8 4 24938.7 2835.96 1 3 -8 -4 23552.8 2626.94 7 3 -8 -3 13171.0 1226.35 2 -3 8 3 15107.6 2023.90 4 -3 8 3 16266.5 2297.89 1 -3 8 3 14939.0 1795.28 5 3 -8 -3 16155.8 2194.21 7 3 -8 -2 5789.80 1000.28 2 -3 8 2 5613.51 1077.70 5 -3 8 2 7682.47 1685.69 1 3 -8 -2 7132.71 1651.29 7 -3 8 1 12937.6 1779.12 2 -3 8 1 12609.4 2102.76 1 -3 8 1 12117.3 1491.33 5 3 -8 -1 12859.2 2087.64 7 -3 8 0 17324.1 2454.99 1 -3 8 0 18214.8 2227.71 2 3 -8 0 17569.2 2575.88 7 -3 8 0 17592.2 1599.93 5 -3 8 -1 684.684 707.057 1 3 -8 1 296.926 622.954 7 -3 8 -2 944.289 945.987 1 3 -8 2 897.022 943.601 7 -3 8 -2 678.304 953.222 2 -3 8 -3 12307.0 2314.87 1 3 -8 3 16516.8 2751.61 7 3 -8 3 16466.0 1789.15 6 -3 8 -3 16711.4 2576.25 2 3 -8 4 7717.29 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2654.01 1 3 -7 -4 24427.6 2564.26 7 -3 7 3 10362.3 1448.72 5 3 -7 -3 10157.2 1074.37 2 -3 7 3 8321.81 1477.97 4 3 -7 -3 9522.51 1668.23 7 -3 7 3 10597.7 1787.83 1 -3 7 2 11411.9 1541.79 5 3 -7 -2 12851.5 1459.24 2 -3 7 2 8969.26 1524.60 4 -3 7 2 12658.6 1970.99 1 3 -7 -2 11243.3 1767.40 7 3 -7 -1 36521.0 2712.60 2 -3 7 1 39213.5 2678.04 5 -3 7 1 40473.4 3491.46 1 -3 7 1 39008.8 2837.71 2 3 -7 -1 38768.4 3412.23 7 -3 7 0 25776.9 2853.02 1 -3 7 0 27610.0 2611.97 2 3 -7 0 25463.1 2952.23 7 -3 7 0 25345.5 2063.12 5 -3 7 -1 4632.16 1437.34 2 -3 7 -1 4002.86 788.014 5 -3 7 -1 6211.01 1528.94 1 3 -7 1 5561.85 1561.99 7 -3 7 -2 5097.87 1469.80 1 3 -7 2 5322.87 1497.83 7 3 -7 2 4326.99 776.506 4 -3 7 -2 7832.62 1719.90 2 3 -7 3 10563.4 2072.35 7 3 -7 3 10061.8 1422.33 6 -3 7 -3 7761.53 1705.62 1 -3 7 -3 11917.6 2210.44 2 3 -7 4 8408.11 2021.26 7 3 -7 4 6589.00 1174.44 6 -3 7 -4 7513.38 1772.44 1 -3 7 -4 8477.60 2013.64 2 3 -7 5-244.677 665.678 7 3 -7 5 95.0500 449.740 6 -3 7 -5 208.961 667.189 1 -3 7 -5 1324.98 1140.09 2 -3 7 -6 204.066 582.678 1 -3 7 -6 1504.52 1274.87 2 3 -7 7 5002.76 1698.62 7 -3 7 -7 2388.91 1100.44 1 -3 7 -7 2658.19 1468.13 2 -3 6 14 418.293 606.452 4 -3 6 13 95.4870 616.761 4 -3 6 12 28026.2 3421.25 4 3 -6 -12 18989.2 2688.69 7 3 -6 -11 17865.1 1835.57 2 -3 6 11 20933.4 2805.68 4 3 -6 -11 18091.9 2525.55 7 -3 6 10 469.025 637.337 4 3 -6 -10 563.180 580.008 7 3 -6 -10-536.131 444.910 2 -3 6 9-511.357 613.113 4 3 -6 -9 122.626 588.772 7 -3 6 9 545.515 432.385 3 3 -6 -9 634.670 407.619 2 -3 6 9 348.704 754.786 1 3 -6 -8 10878.5 987.262 2 -3 6 8 12801.5 2228.13 1 -3 6 8 16148.2 2245.22 4 3 -6 -8 16833.4 2297.82 7 -3 6 8 11399.8 1437.08 3 3 -6 -7 16851.6 999.685 2 3 -6 -7 23025.6 2614.10 7 -3 6 7 20672.4 2669.95 1 -3 6 7 20439.0 1884.64 3 -3 6 6 2379.50 917.354 5 3 -6 -6 523.866 192.786 2 -3 6 6 1352.10 708.382 4 3 -6 -6 1224.86 758.339 7 -3 6 6 889.719 468.024 3 -3 6 6 1441.86 731.860 1 3 -6 -6 714.208 199.332 2 -3 6 5 23838.0 2403.09 5 3 -6 -5 23019.3 1446.62 2 -3 6 5 24938.1 2571.70 4 3 -6 -5 25404.6 2594.29 7 -3 6 5 28838.2 2764.76 1 -3 6 4 24985.8 2302.01 5 -3 6 4 28150.3 2640.80 1 3 -6 -4 32315.3 1806.20 2 -3 6 4 25501.9 2514.36 4 3 -6 -4 28490.0 2706.98 7 -3 6 3 8986.95 1357.59 5 3 -6 -3 11815.4 1283.12 2 -3 6 3 9970.83 1558.56 4 3 -6 -3 12302.0 1786.53 7 -3 6 3 10768.3 1742.11 1 -3 6 2 21938.3 2045.55 5 3 -6 -2 25605.1 1955.39 2 -3 6 2 22961.7 2440.12 1 3 -6 -2 23606.6 2455.22 7 -3 6 1 52933.1 3087.48 5 3 -6 -1 53681.4 3794.51 7 3 -6 -1 55031.9 3143.50 2 -3 6 1 52384.0 3742.44 1 -3 6 0 37593.5 3241.40 1 -3 6 0 35688.6 2809.59 2 3 -6 0 31756.5 3068.57 7 -3 6 0 34770.9 2439.71 5 -3 6 -1 11329.9 1729.94 2 -3 6 -1 9456.97 1765.11 1 3 -6 1 10069.8 1357.31 4 3 -6 1 8231.36 1610.23 7 -3 6 -1 8966.05 1231.59 5 -3 6 -2-1315.89 908.190 2 -3 6 -2 719.416 648.881 1 3 -6 2 450.489 334.965 5 3 -6 2 647.981 339.832 4 3 -6 2-673.666 654.316 7 3 -6 3 979.124 475.857 5 3 -6 3 1167.95 482.845 4 3 -6 3 162.526 901.604 7 -3 6 -3-479.618 778.768 1 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1239.21 3 -3 5 6 2805.63 1035.97 1 -3 5 6 3065.67 996.151 4 3 -5 -6 4620.85 1118.14 7 -3 5 6 3173.57 703.664 3 -3 5 5 11767.1 1695.79 5 -3 5 5 9555.81 1518.76 4 3 -5 -5 11257.7 1692.39 7 -3 5 5 11430.9 1760.53 1 -3 5 4 33150.8 2628.60 5 -3 5 4 30745.5 2668.77 4 3 -5 -4 36772.9 1949.46 2 3 -5 -4 34939.3 2841.93 7 -3 5 4 32401.0 2713.61 1 -3 5 3 1543.81 636.748 5 -3 5 3 1099.14 517.891 4 3 -5 -3 1588.27 649.651 2 3 -5 -3 1419.63 758.418 7 -3 5 3 2351.28 814.872 1 -3 5 2 27658.5 2265.88 5 3 -5 -2 31120.1 2154.61 2 -3 5 2 27674.5 2486.79 1 3 -5 -2 26024.4 2462.25 7 -3 5 1 65879.2 3410.68 5 3 -5 -1 76128.7 3616.93 2 -3 5 1 65985.1 3892.50 1 3 -5 -1 69117.4 4048.62 7 3 -5 0 19053.7 2001.39 2 -3 5 0 21363.1 2346.79 1 -3 5 0 20494.1 2043.76 2 3 -5 0 19743.5 2267.46 7 -3 5 0 20297.0 1858.94 5 -3 5 -1 2893.36 887.549 2 -3 5 -1 1050.27 491.684 5 -3 5 -1 854.832 507.690 1 3 -5 1 1839.33 555.213 5 3 -5 1 2521.53 748.034 4 3 -5 1 1131.22 639.707 7 -3 5 -2 1750.50 818.113 2 -3 5 -2 2282.51 795.156 1 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2196.30 5 3 -4 0 36032.8 2620.16 2 3 -4 0 35006.7 2550.12 4 -3 4 0 34842.9 2688.00 1 3 -4 0 32594.7 2751.66 7 -3 4 0 34692.4 2385.95 5 3 -4 1 20292.8 1711.52 5 -3 4 -1 20238.4 2129.13 1 3 -4 1 20777.4 1969.94 4 -3 4 -1 17659.3 1976.18 2 -3 4 -1 18710.3 1775.18 5 3 -4 1 17264.8 2174.41 7 3 -4 2 15450.8 1549.65 5 -3 4 -2 15323.2 1946.89 1 3 -4 2 17314.9 1736.25 4 -3 4 -2 18694.6 2166.44 2 -3 4 -2 14875.1 1537.65 5 3 -4 3 29390.4 2251.04 5 -3 4 -3 28042.8 2634.06 1 3 -4 3 30624.1 2278.98 4 -3 4 -3 30799.4 2956.42 2 3 -4 4 503.094 500.097 5 3 -4 4 932.934 472.822 4 3 -4 4 1.40000 497.379 6 -3 4 -4 222.612 484.915 1 -3 4 -4-208.235 822.608 2 -3 4 -5 17461.2 2227.24 1 3 -4 5 21235.2 1741.25 4 -3 4 -5 20930.3 2745.68 2 3 -4 5 19196.3 1953.22 6 3 -4 5 16008.9 1934.47 5 -3 4 -6 4962.08 1302.27 1 3 -4 6 5738.42 1173.33 6 -3 4 -6 6520.52 1777.11 2 -3 4 -7 9065.07 1833.99 1 3 -4 7 12937.4 1793.80 6 -3 4 -7 13846.2 2564.56 2 3 -4 8 4659.01 1245.00 6 -3 4 -8 3026.66 1600.10 2 3 -4 9 612.010 571.562 6 -3 4 -9 4391.16 1866.91 2 3 -4 10 1378.73 786.028 6 -3 4 -10 4830.97 1934.30 2 3 -3 -14-3058.95 1302.48 2 -3 3 13 2734.68 1296.88 4 3 -3 -13 4042.17 1392.26 2 -3 3 12 12264.4 2211.26 4 3 -3 -12 11776.7 1932.54 2 -3 3 11 2771.31 1179.91 4 3 -3 -11 3439.19 1106.87 2 -3 3 10 716.023 693.109 4 3 -3 -10 39.5003 538.969 2 3 -3 -10-506.877 751.849 7 -3 3 9 7858.40 1599.35 4 3 -3 -9 6412.41 1184.95 2 3 -3 -9 7852.25 1519.10 7 -3 3 8 7365.43 1519.28 4 3 -3 -8 7684.99 1174.44 2 3 -3 -8 7778.60 1352.79 7 3 -3 -7 5319.37 1235.51 7 -3 3 7 5162.56 1237.43 4 3 -3 -7 6006.04 927.909 2 -3 3 6 10656.9 1666.20 4 3 -3 -6 9537.58 1422.71 7 -3 3 6 6430.48 674.224 3 -3 3 6 9250.79 1685.62 1 -3 3 5 32845.5 2712.60 4 3 -3 -5 35950.2 2649.29 7 -3 3 5 30922.4 2625.91 1 -3 3 5 30543.2 2678.75 5 -3 3 4 51489.7 3281.70 5 -3 3 4 48658.6 3192.95 4 3 -3 -4 55417.1 3238.21 7 -3 3 4 51744.5 3226.03 1 3 -3 -3 19953.8 1957.95 7 -3 3 3 17113.6 1768.42 1 -3 3 3 17957.9 1897.01 5 -3 3 2 22564.7 2010.36 5 3 -3 -2 24747.2 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3423.74 1238.50 1 3 13 4-530.480 672.879 1 3 13 4 1138.40 710.028 2 3 13 4 45.0065 564.272 4 3 13 5 3257.47 1302.03 1 3 13 5 970.106 741.918 4 3 13 6 3819.56 1106.70 4 3 13 6 4446.95 1301.03 1 -3 -13 -6 2955.79 1147.34 3 3 13 7 1872.01 826.601 1 3 13 7 1457.76 671.576 4 -3 -13 -7 2417.23 1116.17 3 3 13 8 280.446 685.945 4 -3 -13 -8 652.149 1033.15 3 3 13 9-360.124 620.655 4 3 13 9 603.162 538.983 6 -3 -13 -9 254.123 764.081 3 3 13 10 459.704 513.316 6 -3 -13 -10-130.711 700.191 3 3 13 11-210.430 529.428 4 3 13 11-18.9640 521.971 6 -3 -13 -11 638.545 816.177 3 3 13 12 176.873 606.116 4 3 13 12 1254.07 876.591 6 -3 -13 -12 1109.21 1075.41 3 3 14 2 1339.33 899.167 2 3 14 2 1724.16 972.758 1 3 14 3 1852.51 1221.13 1 3 14 3 1485.16 865.214 2 3 14 4 2609.25 1229.78 1 3 14 4 1373.73 834.737 4 3 14 5 1337.48 962.996 4 3 14 5 1573.67 1004.63 1 3 14 6 2358.68 1066.97 1 3 14 6 745.645 653.044 4 3 14 7 212.728 613.764 4 -3 -14 -7 849.127 636.082 3 -3 -14 -8 297.516 756.893 3 3 14 8 92.8199 599.161 4 3 14 9 1184.50 843.329 4 -3 -14 -9 1596.10 1105.29 3 3 14 10 2949.30 1263.63 4 -3 -14 -10 3438.54 1468.88 3 3 14 11 369.287 793.631 4 -3 -14 -11-409.260 967.401 3 -4 12 8 1501.36 1140.55 4 -4 12 8 1159.45 897.119 1 4 -12 -8 694.164 707.416 7 -4 12 7 8568.69 2174.86 1 -4 12 7 7563.74 1906.96 4 4 -12 -7 5843.11 1812.25 7 -4 12 6 7222.46 1886.01 1 -4 12 6 7493.82 1873.64 4 4 -12 -6 8434.10 1944.22 7 4 -12 -5 7871.56 1910.46 7 -4 12 5 7741.27 2031.54 1 4 -12 -4 849.870 795.436 7 -4 12 4 3643.71 1590.58 1 4 -12 -3 1498.58 1060.52 7 -4 12 3 215.332 712.835 1 -4 11 10 6094.92 1730.24 5 -4 11 10 9395.50 2202.36 4 -4 11 10 7548.02 2029.96 1 4 -11 -10 3833.69 1483.82 7 -4 11 9 6430.35 2107.15 1 -4 11 9 4206.50 1406.10 5 -4 11 9 3557.81 1438.05 4 4 -11 -9 4302.06 1422.65 7 -4 11 8 436.123 561.685 5 -4 11 8 862.026 664.460 4 4 -11 -8 713.163 758.562 7 -4 11 8-1589.70 1150.59 1 -4 11 7 3878.42 1327.24 5 -4 11 7 6010.81 1674.95 4 -4 11 7 7793.71 1980.58 1 4 -11 -7 3895.66 1397.70 7 -4 11 6 18508.7 2894.63 1 -4 11 6 14647.3 2218.16 5 -4 11 6 12097.9 2178.58 4 4 -11 -6 15310.5 2542.94 7 -4 11 5 5200.59 1655.65 1 4 -11 -5 5596.31 1598.89 7 4 -11 -4 1725.64 1027.96 7 -4 11 4 2420.09 1427.85 1 4 -11 -3 562.180 829.001 7 -4 11 3 1230.69 951.553 1 4 -11 -2 5761.02 1717.98 7 -4 11 2 7115.19 1886.09 1 -4 11 1 3487.91 1317.03 1 4 -11 -1 3672.77 1462.89 7 -4 11 0 698.143 895.389 1 4 -11 0-2027.93 1187.88 7 -4 10 11 1393.34 982.902 5 -4 10 11 3079.99 1393.73 4 -4 10 11 4518.51 1652.64 1 4 -10 -11 2178.31 1108.01 7 -4 10 10 7005.59 1849.78 5 -4 10 10 7876.19 2037.39 4 4 -10 -10 6928.45 2028.89 7 -4 10 10 8124.20 2123.91 1 -4 10 9 6558.87 1771.04 1 -4 10 9 3642.69 1264.90 5 -4 10 9 3297.33 1547.33 4 4 -10 -9 4637.44 1594.36 7 -4 10 8 1306.73 837.132 5 -4 10 8 62.7879 663.057 4 4 -10 -8 2377.25 1003.34 7 -4 10 8 2182.66 1238.37 1 -4 10 7 6299.48 1501.26 5 -4 10 7 9073.30 1866.11 4 -4 10 7 8765.23 2131.59 1 4 -10 -7 8102.96 1897.89 7 -4 10 6 13854.4 2095.80 5 -4 10 6 14443.4 2505.18 1 -4 10 6 14182.8 2338.18 4 4 -10 -6 12809.5 2249.48 7 -4 10 5 891.905 655.699 1 -4 10 5 1551.30 672.387 5 -4 10 5 105.498 688.739 4 4 -10 -5 1721.36 1052.15 7 -4 10 4 1867.55 822.738 5 4 -10 -4 3760.45 1247.68 7 -4 10 4 4375.96 1602.19 1 4 -10 -3 3961.92 1295.01 7 -4 10 3 4727.04 1537.05 1 4 -10 -2 765.015 796.839 7 -4 10 2 1897.45 1145.84 1 -4 10 1 119.765 879.375 1 4 -10 -1 227.053 729.591 7 -4 10 0 223.490 900.921 1 4 -10 0 924.252 802.248 7 -4 10 -1 2688.04 1106.99 1 4 -10 1 4399.26 1564.40 7 -4 10 -2 1582.98 1134.83 2 -4 10 -2 1530.74 1173.17 1 4 -10 2 3252.14 1572.44 7 -4 9 12 1373.62 1037.39 5 -4 9 12 2375.30 1278.49 4 4 -9 -12 1661.71 1060.88 7 -4 9 11 3877.21 1546.20 5 -4 9 11 6056.30 1806.99 1 -4 9 11 4427.07 1572.77 4 4 -9 -11 2911.82 1377.75 7 -4 9 10 13351.8 2578.62 1 -4 9 10 11032.4 2226.87 5 -4 9 10 13235.1 2531.22 4 4 -9 -10 10538.8 2202.06 7 -4 9 9 3341.24 1441.95 5 -4 9 9 4546.52 1529.32 4 4 -9 -9 3822.22 1471.04 7 -4 9 9 5615.25 1733.71 1 -4 9 8-81.7305 731.968 1 -4 9 8-773.515 807.305 5 -4 9 8 624.754 587.392 4 4 -9 -8-16.8981 682.796 7 -4 9 7 5551.04 1605.74 1 -4 9 7 6861.07 1569.09 5 -4 9 7 6267.36 1713.26 4 4 -9 -7 5339.81 1525.74 7 -4 9 6 7169.57 1499.22 5 -4 9 6 11288.7 2156.83 1 -4 9 6 8442.06 1873.51 4 4 -9 -6 8861.48 1921.28 7 -4 9 5 5458.40 1503.39 1 -4 9 5 2796.48 983.800 5 -4 9 5 3750.11 1155.30 4 4 -9 -5 5144.03 1475.01 7 -4 9 4 5036.57 1275.35 5 4 -9 -4 2764.99 1237.22 7 -4 9 4 5795.11 1634.75 1 -4 9 3 9299.96 1663.99 5 4 -9 -3 11500.9 2051.39 7 -4 9 3 15252.4 2516.95 1 -4 9 2 4545.75 1129.13 5 4 -9 -2 5940.99 1614.41 7 -4 9 2 5318.13 1612.23 1 -4 9 1 1337.19 1003.45 1 4 -9 -1-131.592 625.064 7 -4 9 0 2272.68 1235.34 1 4 -9 0-1190.56 1071.06 7 -4 9 -1 7224.75 1787.71 2 -4 9 -1 9232.30 2127.21 1 4 -9 1 6729.10 1956.09 7 -4 9 -2 2643.30 1126.87 2 4 -9 2 1180.00 977.767 7 -4 9 -2 2001.83 1254.47 1 -4 9 -3-1448.10 1198.16 2 -4 9 -3 1450.25 1175.02 1 4 -9 3-969.511 963.284 7 -4 9 -4 1587.55 1023.09 2 -4 9 -4 1876.23 1215.29 1 4 -9 4 1158.35 1113.89 7 -4 8 13 703.737 784.206 4 4 -8 -13 734.151 910.406 7 -4 8 12 2412.21 1058.40 5 -4 8 12 2947.30 1369.91 4 4 -8 -12 2386.53 1324.05 7 -4 8 11 4517.65 1675.48 1 -4 8 11 4657.91 1493.31 5 -4 8 11 6343.00 1765.42 4 4 -8 -11 6407.73 1704.41 7 -4 8 10 7058.64 1795.32 1 -4 8 10 7016.81 1879.50 5 -4 8 10 6722.52 1829.47 4 4 -8 -10 8851.96 2077.40 7 -4 8 9 4995.89 1592.76 5 -4 8 9 5370.75 1678.89 4 4 -8 -9 6067.74 1687.37 7 -4 8 9 6577.11 1816.29 1 -4 8 8-125.836 588.163 5 -4 8 8 1665.09 1100.89 1 -4 8 8 923.286 948.042 4 4 -8 -8 370.175 930.216 7 -4 8 7 3845.64 1287.94 5 -4 8 7 5654.77 1519.28 4 4 -8 -7 4679.85 1327.65 7 -4 8 7 4749.79 1496.27 1 -4 8 6 2640.06 1015.63 5 -4 8 6 795.185 682.740 4 -4 8 6 3433.10 1216.16 1 4 -8 -6 1979.52 893.782 7 -4 8 5 6245.47 1333.86 5 -4 8 5 5985.90 1475.39 1 -4 8 5 4882.00 1363.85 4 4 -8 -5 6840.99 1580.82 7 -4 8 4 14425.8 2260.96 1 -4 8 4 13274.4 1894.19 5 4 -8 -4 16797.9 2439.18 7 -4 8 3 5409.75 1302.51 5 4 -8 -3 6711.07 1623.45 7 -4 8 3 6383.15 1614.07 1 -4 8 2 11092.9 1798.32 5 -4 8 2 15717.3 2437.35 1 4 -8 -2 13039.1 2205.32 7 -4 8 1 6648.74 1330.57 5 -4 8 1 9210.22 1928.24 1 4 -8 -1 7793.90 1849.02 7 -4 8 0 2690.20 816.016 5 -4 8 0 874.717 649.244 1 4 -8 0 2913.44 1348.83 7 -4 8 -1 10270.7 1928.40 2 -4 8 -1 7809.98 1840.39 1 4 -8 1 9520.13 2212.44 7 -4 8 -2 1573.95 970.675 2 -4 8 -2-323.252 667.750 1 4 -8 2-1145.17 989.407 7 -4 8 -3 720.233 766.619 2 -4 8 -3 2251.59 1212.03 1 4 -8 3 2841.89 1475.70 7 4 -8 3 3354.63 973.174 6 -4 8 -4 6369.26 1904.12 2 -4 8 -4 4334.37 1508.76 1 4 -8 4 5829.38 1893.51 7 -4 8 -5 1898.81 1240.24 2 -4 8 -5 2136.59 1120.57 1 4 -8 5 67.5619 746.877 7 -4 7 13 651.973 610.532 4 4 -7 -13 140.752 873.959 7 -4 7 12 6.22765 850.819 4 4 -7 -12 1493.70 900.610 7 -4 7 11 2093.43 1137.13 5 -4 7 11 4860.64 1608.07 4 4 -7 -11 3828.38 1340.22 7 -4 7 10 6884.34 1811.63 5 -4 7 10 6088.79 1849.76 1 -4 7 10 10972.1 2233.15 4 4 -7 -10 6947.14 1767.51 7 -4 7 9 2461.67 1093.10 5 -4 7 9 3856.79 1352.64 4 4 -7 -9 4441.90 1460.88 7 -4 7 9 4387.01 1574.51 1 -4 7 8 1906.68 841.158 5 -4 7 8 1059.42 679.892 4 4 -7 -8 4058.02 1452.06 7 -4 7 8 2845.52 1064.13 1 -4 7 7 14442.2 2293.25 5 -4 7 7 12423.5 2181.76 1 4 -7 -7 8352.94 708.019 2 -4 7 7 14618.6 2364.98 4 4 -7 -7 16620.0 2394.84 7 -4 7 6 3451.10 1203.65 5 -4 7 6 6114.22 1481.64 4 4 -7 -6 7400.48 1652.28 7 -4 7 6 7976.41 1723.96 1 -4 7 5 5828.82 1316.67 5 -4 7 5 5984.18 1444.07 4 -4 7 5 6785.00 1652.70 1 4 -7 -5 6922.77 1523.77 7 4 -7 -5 7093.15 1093.08 2 -4 7 4 5248.87 1333.95 1 -4 7 4 3489.08 1104.45 5 4 -7 -4 3098.21 822.924 2 4 -7 -4 5505.56 1491.97 7 -4 7 3 9130.82 1577.75 5 4 -7 -3 6600.82 1524.30 7 4 -7 -3 8917.99 1332.21 2 -4 7 3 9905.92 1836.63 1 -4 7 2 8851.44 1537.83 5 4 -7 -2 11416.6 1952.50 7 -4 7 2 11239.0 1991.60 1 -4 7 1 15038.0 2334.25 1 4 -7 -1 18840.2 2652.01 7 -4 7 1 15065.4 2012.92 5 -4 7 0 8635.98 1486.98 5 -4 7 0 11670.0 2033.28 1 4 -7 0 7691.15 1774.16 7 -4 7 -1 11049.6 1888.41 2 -4 7 -1 9615.55 1974.14 1 4 -7 1 12605.8 2353.96 7 -4 7 -1 10142.0 1518.11 5 -4 7 -2 1211.02 919.550 2 -4 7 -2 382.160 918.939 1 4 -7 2 558.487 874.406 7 -4 7 -3 3834.39 1307.98 2 -4 7 -3 2953.32 1205.19 1 4 -7 3 2881.05 1528.45 7 -4 7 -4 20263.3 2974.62 1 -4 7 -4 25785.1 3383.69 2 4 -7 4 21582.3 3476.06 7 4 -7 4 19261.1 2226.44 6 -4 7 -5 2803.41 1159.40 1 -4 7 -5 2866.47 1429.95 2 4 -7 5 2243.63 1337.59 7 4 -7 5 1540.95 703.437 6 -4 7 -6-755.490 980.355 2 4 -7 6-1134.69 1056.05 7 -4 7 -6 1394.59 946.165 1 -4 6 13 42.8528 603.654 4 4 -6 -13-197.980 932.026 7 -4 6 12 2344.33 1214.89 4 4 -6 -12-153.476 833.174 7 -4 6 11 3279.96 1422.50 5 -4 6 11 4266.54 1347.03 4 4 -6 -11 5210.02 1419.61 7 -4 6 10 8568.91 2057.28 5 -4 6 10 10560.2 2107.86 4 4 -6 -10 2759.87 926.962 2 4 -6 -10 6289.81 1668.62 7 -4 6 9 2288.19 1286.84 5 -4 6 9 3516.83 1331.55 4 4 -6 -9 2961.03 639.416 2 4 -6 -9 4246.79 1361.85 7 -4 6 9 531.547 851.238 1 -4 6 8 2043.98 1017.95 5 -4 6 8 982.419 845.378 4 4 -6 -8 1105.34 452.115 2 -4 6 8 667.970 786.923 1 4 -6 -8 991.320 784.542 7 -4 6 7 15679.9 2305.29 5 -4 6 7 17768.2 2504.59 4 4 -6 -7 16303.9 2292.16 7 -4 6 7 16927.8 2386.06 1 -4 6 6 16098.4 2306.53 5 -4 6 6 17774.2 2444.48 4 4 -6 -6 14802.5 1420.05 2 4 -6 -6 17189.8 2290.93 7 -4 6 6 15682.4 2304.35 1 -4 6 5 399.502 467.073 5 -4 6 5 1224.01 783.321 4 4 -6 -5 1400.62 930.991 7 -4 6 5 1201.04 844.186 1 4 -6 -5 480.332 550.960 2 -4 6 4-589.758 688.968 5 -4 6 4 1479.79 867.278 1 4 -6 -4-835.302 781.406 7 4 -6 -4 1157.45 600.725 2 -4 6 3 8491.01 1565.57 1 -4 6 3 8957.33 1546.15 5 4 -6 -3 7653.00 1557.63 7 4 -6 -3 7047.28 1194.35 2 -4 6 2 1333.76 662.111 5 4 -6 -2 2300.51 964.412 7 4 -6 -2 1011.38 736.312 2 -4 6 2 549.533 812.786 1 -4 6 1 12478.8 1779.85 5 4 -6 -1 11522.5 1943.75 7 -4 6 1 13421.1 2062.34 1 -4 6 0 37345.7 3439.78 1 4 -6 0 36729.0 3546.71 7 -4 6 0 32799.9 2873.07 5 -4 6 -1 13673.5 2194.31 1 4 -6 1 11281.3 2145.96 7 -4 6 -1 9380.11 1515.13 5 -4 6 -2 1166.19 641.334 5 -4 6 -2 935.401 793.852 2 -4 6 -2-897.038 912.689 1 4 -6 2 656.317 665.833 7 -4 6 -3 8685.83 1832.67 2 -4 6 -3 5363.62 1469.79 1 4 -6 3 5672.51 1811.17 7 -4 6 -4 20499.7 2846.49 1 -4 6 -4 19074.4 2887.69 2 4 -6 4 17874.2 3054.67 7 4 -6 4 21347.9 2298.57 6 -4 6 -5 693.939 639.339 1 -4 6 -5 669.873 980.095 2 4 -6 5-361.631 1210.44 7 4 -6 5 1114.49 705.181 6 -4 6 -6-264.472 803.958 2 4 -6 6 1460.52 686.355 6 -4 6 -6 1019.38 604.049 1 -4 6 -7 4730.33 1700.45 2 4 -6 7 3596.74 1062.37 6 -4 6 -7 3175.43 1422.17 1 -4 5 13 1050.08 960.826 4 -4 5 12 2966.48 1325.44 4 4 -5 -12 3205.28 1281.88 7 -4 5 11 14371.9 2684.32 5 4 -5 -11 13418.4 1808.76 2 -4 5 11 14466.8 2471.09 4 4 -5 -11 14192.6 2323.26 7 -4 5 10 4105.94 1428.11 5 -4 5 10 4310.50 1405.95 4 4 -5 -10 2680.35 788.601 2 4 -5 -10 4431.69 1444.93 7 -4 5 9 619.320 721.404 5 -4 5 9 1091.78 727.202 4 4 -5 -9 270.874 356.311 2 4 -5 -9 630.019 767.650 7 -4 5 8 2671.21 1132.03 5 -4 5 8 1414.60 964.938 4 4 -5 -8 958.809 459.829 2 4 -5 -8-89.8258 696.682 7 -4 5 8 674.389 749.583 1 -4 5 7 40063.3 3670.58 5 -4 5 7 45546.1 3904.07 4 4 -5 -7 52413.4 3925.09 7 -4 5 7 43474.6 3755.67 1 -4 5 7 40838.6 2400.71 3 -4 5 6 27195.7 2967.50 5 -4 5 6 29322.8 3044.63 4 4 -5 -6 29488.0 2875.58 7 -4 5 6 28145.3 2903.92 1 -4 5 6 24259.3 1928.47 3 -4 5 5 13368.3 2023.95 1 -4 5 5 12259.2 1874.67 5 4 -5 -5 17285.0 2193.72 7 -4 5 4 7661.10 1472.14 5 4 -5 -4 8077.46 1236.16 2 4 -5 -4 9874.17 1698.03 7 -4 5 4 8888.96 1571.99 1 -4 5 3 1224.64 561.491 5 -4 5 3 2114.47 887.272 1 4 -5 -3 1615.04 743.398 7 4 -5 -3 771.611 508.940 2 -4 5 2 4026.37 994.793 5 4 -5 -2 6861.95 1481.31 7 4 -5 -2 4599.11 1037.69 2 -4 5 2 4834.07 1214.77 1 -4 5 1 31651.7 2764.03 5 -4 5 1 35903.5 3103.35 1 4 -5 -1 34568.2 3162.94 7 -4 5 0 34051.1 3061.79 1 4 -5 0 31327.2 3239.56 7 -4 5 0 31794.6 2781.38 5 -4 5 -1 16216.7 2260.50 1 4 -5 1 16170.5 2370.54 7 -4 5 -1 14560.0 1899.73 5 -4 5 -2 389.908 531.255 5 -4 5 -2 1340.53 1057.07 2 -4 5 -2 957.815 756.133 1 4 -5 2 841.316 1013.31 7 -4 5 -3 12679.5 2186.00 2 -4 5 -3 8519.51 1733.36 1 -4 5 -4 15855.2 2346.94 1 -4 5 -4 19371.6 2826.06 2 -4 5 -5 6433.48 1882.31 2 4 -5 5 5487.93 1231.43 6 -4 5 -5 3576.63 1414.92 1 -4 5 -6 4574.12 1596.38 2 4 -5 6 3966.95 1081.04 6 -4 5 -6 1475.47 1039.70 1 -4 5 -7 4881.09 1781.92 2 -4 5 -7 2881.76 1194.10 1 4 -5 7 4690.49 1197.80 6 -4 5 -8-890.103 1062.40 2 -4 5 -8 508.663 734.641 1 4 -5 8 960.087 818.549 6 -4 4 13 182.688 681.173 5 -4 4 12 5509.92 1754.98 5 4 -4 -12 5811.49 1362.35 2 4 -4 -12 6291.24 1578.57 7 -4 4 11 12797.2 2505.40 5 -4 4 11 15597.9 2486.42 4 4 -4 -11 12084.3 1757.07 2 4 -4 -11 11112.7 1983.09 7 -4 4 10 1251.58 788.924 5 -4 4 10-282.019 918.529 4 4 -4 -10-1345.24 674.745 2 4 -4 -10 199.662 669.395 7 -4 4 9-308.207 569.380 5 -4 4 9-638.558 733.308 4 4 -4 -9 137.674 488.177 2 4 -4 -9-704.383 842.178 7 -4 4 8 22928.4 2909.18 5 4 -4 -8 22339.5 1871.49 2 -4 4 8 23222.2 2837.25 4 4 -4 -8 22417.7 2613.72 7 -4 4 7 31700.2 3279.66 5 4 -4 -7 32234.8 2992.12 7 -4 4 7 29813.7 3131.61 1 -4 4 7 24507.7 1539.05 3 -4 4 6-844.067 802.163 5 -4 4 6 567.327 691.145 1 4 -4 -6-570.158 675.972 7 -4 4 5 2387.13 896.685 5 4 -4 -5 2979.35 1049.97 7 -4 4 5 3648.64 1100.48 1 -4 4 4 101071. 5172.76 5 4 -4 -4 104093. 5138.65 7 -4 4 4 99521.4 4879.93 1 -4 4 3 13787.7 1890.08 5 4 -4 -3 12515.1 1507.61 2 4 -4 -3 15307.3 2023.62 7 -4 4 3 14882.6 1870.41 1 4 -4 -2 2491.81 794.598 2 -4 4 2 2601.07 987.940 1 -4 4 2 1851.74 800.440 5 4 -4 -2 3563.02 1201.97 7 -4 4 1 54575.5 3559.26 5 -4 4 1 61213.9 3691.10 1 4 -4 -1 57818.9 3932.69 7 -4 4 0 39290.0 3027.18 1 4 -4 0 39147.6 3366.90 7 -4 4 0 34852.0 2834.82 5 -4 4 -1 24270.0 2477.36 1 4 -4 1 23216.6 2744.25 7 -4 4 -1 19959.1 2167.10 5 -4 4 -2 7187.13 1390.54 5 -4 4 -2 6891.02 1457.36 1 -4 4 -3 12124.6 1894.40 1 -4 4 -3 16055.4 2304.46 2 -4 4 -3 10625.9 1611.68 5 -4 4 -4 15613.4 2271.85 1 -4 4 -4 17488.7 2635.94 2 -4 4 -5 9436.10 1974.69 2 4 -4 5 8420.65 1494.49 6 -4 4 -5 4772.72 1365.88 1 -4 4 -6 2919.85 1153.12 2 -4 4 -6 2290.77 1043.57 1 4 -4 6 1481.71 722.422 6 -4 4 -7 393.699 883.214 2 -4 4 -7 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7223.39 1572.11 4 -4 -12 -5 7662.10 1864.56 3 4 12 6 11126.3 1865.56 4 -4 -12 -6 10433.8 2081.30 3 4 12 7 5205.66 1387.59 4 4 12 7 4889.86 1051.64 6 -4 -12 -7 7404.39 1843.03 3 4 12 8 2329.80 931.836 4 4 12 8 1447.45 665.709 6 -4 -12 -8 1743.50 1135.79 3 4 12 9 1140.49 910.618 4 4 12 9 1055.64 744.564 6 -4 -12 -9-1140.16 838.019 3 4 12 10 119.998 708.918 4 4 12 10 1319.10 660.484 6 -4 -12 -10 66.4040 933.615 3 4 12 11 2579.89 985.539 4 4 12 11 517.712 640.192 6 -4 -12 -11 3798.10 1545.37 3 4 12 12 1016.57 939.050 4 4 12 12 1236.30 791.527 6 -4 -12 -12 179.343 844.228 3 4 13 1 708.868 854.565 2 4 13 1 2095.37 1077.89 1 4 13 2-1041.42 944.513 2 4 13 2 515.260 665.111 1 4 13 3 1314.74 925.799 2 4 13 3 1000.76 769.597 4 4 13 3 2511.39 1183.56 1 4 13 4-276.379 627.719 1 4 13 4 954.626 752.211 4 -4 -13 -4 689.050 992.319 3 4 13 5-70.8689 637.955 4 -4 -13 -5 1288.12 823.927 3 4 13 6 4468.84 1262.67 4 -4 -13 -6 2900.65 1241.66 3 4 13 7 9267.80 1847.60 4 -4 -13 -7 5906.25 1845.41 3 4 13 8 2478.57 986.367 4 -4 -13 -8 1695.59 801.698 3 4 13 9 694.691 600.847 4 -4 -13 -9-155.164 712.443 3 4 13 10 90.3921 775.661 4 4 13 10 1648.72 859.663 6 -4 -13 -10 682.462 918.742 3 4 13 11 1559.43 828.452 4 4 13 11 265.713 490.190 6 -4 -13 -11 513.789 882.032 3 4 14 4-657.672 781.901 2 4 14 4 1589.55 818.701 4 4 14 5 101.898 637.376 4 4 14 6 2294.07 1079.07 4 -4 -14 -6 1466.46 921.283 3 4 14 7 4802.46 1390.85 4 -4 -14 -7 5494.16 1785.67 3 4 14 8 1913.83 1151.87 4 -4 -14 -8 966.794 1103.25 3 4 14 9-70.2584 665.072 4 -4 -14 -9 695.244 1101.74 3 -5 11 7 1070.76 931.914 5 5 -11 -7 300.602 641.688 7 -5 11 7 1179.92 1165.02 1 -5 11 6 7135.82 2057.16 1 5 -11 -6 4534.37 1582.21 7 -5 11 5 5441.97 1846.87 1 5 -11 -5 3140.89 1155.32 7 -5 11 4 3722.15 1664.85 1 5 -11 -4 1029.45 901.808 7 -5 10 9 5429.08 1644.19 5 -5 10 9 8107.30 2161.22 1 5 -10 -9 5578.16 1643.64 7 -5 10 8 976.124 825.784 1 -5 10 8 1269.38 971.330 5 5 -10 -8 2053.92 1204.37 7 -5 10 7-56.5244 753.850 5 5 -10 -7 1138.34 858.579 7 -5 10 7 859.906 860.679 1 -5 10 6 13244.2 2377.06 5 -5 10 6 13498.3 2589.26 1 5 -10 -6 15681.7 2774.19 7 -5 10 5 8601.70 1860.28 5 -5 10 5 12685.7 2519.44 1 5 -10 -5 9021.08 1998.22 7 -5 10 4 3684.24 1527.64 1 5 -10 -4 2913.75 1297.66 7 5 -10 -3 2021.14 953.705 7 -5 10 3 3425.33 1482.78 1 5 -10 -2 3043.66 1254.67 7 -5 10 2 4122.24 1647.71 1 5 -10 -1 3063.28 1366.42 7 -5 10 1 3043.32 1327.77 1 5 -10 0 664.937 1197.37 7 -5 10 0 303.634 855.594 1 -5 9 10 7895.34 2073.21 5 -5 9 10 7958.54 2100.06 4 5 -9 -10 8950.69 2143.69 7 -5 9 10 7498.08 2183.17 1 -5 9 9 7221.68 1854.60 5 5 -9 -9 5288.05 1659.96 7 -5 9 9 8055.92 2105.29 1 -5 9 8 883.362 783.415 5 -5 9 8 2478.11 1217.55 1 5 -9 -8 641.740 865.218 7 -5 9 7 2089.17 945.566 5 5 -9 -7-645.897 625.612 7 -5 9 7 1882.22 1151.37 1 -5 9 6 12623.8 2209.04 5 5 -9 -6 17746.8 2693.05 7 -5 9 6 20617.7 3110.52 1 -5 9 5 10487.9 1965.11 5 -5 9 5 15421.9 2655.44 1 5 -9 -5 11221.5 2158.87 7 -5 9 4 3908.66 1300.40 5 -5 9 4 4795.61 1576.00 1 5 -9 -4 6560.20 1955.33 7 -5 9 3 7301.84 1662.55 5 5 -9 -3 6254.83 1739.39 7 -5 9 3 7816.86 2015.10 1 5 -9 -2 6264.17 1726.37 7 -5 9 2 7015.94 1867.05 1 5 -9 -1 1429.92 1053.69 7 -5 9 1 4108.58 1554.58 1 5 -9 0 1861.09 1272.94 7 -5 9 0 1354.20 938.352 1 -5 9 -1 681.276 829.037 1 5 -9 1 5111.03 1773.72 7 -5 9 -2 4140.91 1715.60 1 5 -9 2 8460.71 2290.63 7 -5 8 11 1150.95 967.897 5 5 -8 -11 581.481 858.873 7 -5 8 10 8576.01 2189.65 5 -5 8 10 7925.71 2173.60 1 5 -8 -10 6941.88 1893.06 7 -5 8 9 7455.78 2029.96 5 -5 8 9 7428.24 1997.53 1 5 -8 -9 11822.5 2336.75 7 -5 8 8 216.670 572.961 5 5 -8 -8 884.268 755.645 7 -5 8 8 1160.10 896.300 1 -5 8 7 3064.44 1274.79 1 -5 8 7 3448.25 1245.28 5 5 -8 -7 468.114 815.972 7 -5 8 6 11873.4 2172.66 5 5 -8 -6 12400.6 2318.94 7 -5 8 6 12689.4 2335.15 1 -5 8 5 6004.45 1537.90 5 -5 8 5 8537.11 1948.20 1 5 -8 -5 7018.96 1734.31 7 -5 8 4 6255.08 1596.18 5 -5 8 4 6411.50 1743.36 1 5 -8 -4 7971.92 1914.10 7 -5 8 3 14173.1 2402.12 1 -5 8 3 13729.1 2127.07 5 5 -8 -3 15325.4 2460.56 7 -5 8 2 5150.89 1419.98 5 5 -8 -2 5412.05 1641.63 7 -5 8 2 5837.98 1701.69 1 -5 8 1 124.175 595.688 5 5 -8 -1-473.356 1066.45 7 -5 8 1 679.258 1024.90 1 5 -8 0 2713.21 1357.54 7 -5 8 0 3747.21 1332.54 1 -5 8 -1 7679.52 1946.70 1 5 -8 1 6879.65 1971.66 7 -5 8 -2 4167.19 1394.09 1 5 -8 2 145.253 1006.46 7 -5 8 -3-524.801 874.997 1 5 -8 3 1753.50 1334.08 7 -5 8 -4 1671.25 1082.38 2 5 -8 4-405.461 966.590 7 -5 7 12-52.1492 571.319 5 5 -7 -12 73.6996 654.208 7 -5 7 11 125.255 888.757 5 5 -7 -11 1395.67 1193.01 7 -5 7 10 5819.48 1777.34 5 5 -7 -10 7838.15 1964.39 7 -5 7 10 8687.13 2235.07 1 -5 7 9 6022.52 1777.63 5 -5 7 9 5617.19 1807.77 1 5 -7 -9 6070.19 1615.44 7 -5 7 8 3572.86 1304.49 1 -5 7 8 2662.36 1198.52 5 5 -7 -8 2856.53 1348.16 7 -5 7 7 3368.08 1294.82 5 -5 7 7 3961.96 1309.90 1 5 -7 -7 5688.63 1480.83 7 -5 7 6 16251.9 2509.17 5 5 -7 -6 17777.8 2632.80 7 -5 7 6 17970.0 2664.45 1 -5 7 5 6795.38 1684.44 5 5 -7 -5 6822.61 1649.74 7 -5 7 5 6274.98 1595.50 1 -5 7 4 3533.24 1281.10 5 -5 7 4 4262.19 1321.21 1 5 -7 -4 3863.82 1249.41 7 -5 7 3 10460.9 1973.96 1 -5 7 3 11293.1 1977.39 5 5 -7 -3 12498.4 2289.60 7 -5 7 2 2782.59 1021.66 5 5 -7 -2 2395.64 1145.83 7 -5 7 2 2728.29 1208.35 1 -5 7 1-48.2924 570.193 5 5 -7 -1 442.850 763.979 7 -5 7 1 823.167 863.623 1 -5 7 0 1366.33 833.965 5 5 -7 0 256.921 669.620 7 -5 7 0 841.977 859.948 1 -5 7 -1 6891.05 1489.45 5 -5 7 -1 6570.18 1795.60 1 -5 7 -2 2749.41 1353.11 1 5 -7 2 2037.20 1341.11 7 -5 7 -3 824.785 906.560 1 5 -7 3 1311.60 1211.60 7 5 -7 4 637.922 1157.80 7 -5 7 -4 2828.73 1449.38 2 -5 7 -4 2988.99 1359.74 1 5 -7 4 3106.13 1027.39 6 -5 7 -5 4617.46 1566.39 2 -5 7 -5 4116.83 1613.57 1 5 -7 5 6835.17 2246.20 7 5 -7 5 4947.57 1373.45 6 -5 6 12 795.241 1024.31 5 5 -6 -12 2142.68 1144.70 7 -5 6 11 3873.79 1495.93 5 5 -6 -11 3539.20 1385.73 7 -5 6 10 7495.21 1998.52 5 5 -6 -10 7978.11 1822.71 7 -5 6 9 2210.35 1072.12 5 -5 6 9 1256.20 1226.64 1 5 -6 -9 1549.84 1187.29 7 -5 6 8 8520.59 1995.97 1 -5 6 8 7280.74 1759.92 5 5 -6 -8 7539.64 1866.34 7 -5 6 7 7191.23 1727.15 1 -5 6 7 4230.63 1332.08 5 5 -6 -7 7107.28 1768.04 7 -5 6 6 8685.18 1836.96 5 -5 6 6 9689.38 1944.05 1 5 -6 -6 9593.13 1982.66 7 -5 6 5 3661.95 1222.71 5 5 -6 -5 3117.82 1128.08 7 -5 6 5 3143.42 1215.67 1 -5 6 4 8518.60 1764.51 5 5 -6 -4 10395.6 1945.96 7 -5 6 4 9078.99 1707.42 1 -5 6 3 11436.8 1913.54 5 -5 6 3 12523.2 2024.36 1 5 -6 -3 12546.5 2151.29 7 -5 6 2 6339.66 1501.41 1 -5 6 2 8647.05 1715.77 5 5 -6 -2 6378.69 1647.02 7 -5 6 1 10219.5 1793.28 5 5 -6 -1 10705.2 2115.75 7 -5 6 1 8122.54 1754.57 1 -5 6 0 2904.73 1085.66 5 5 -6 0 3016.32 1254.37 7 -5 6 0 2715.48 1027.64 1 -5 6 -1 819.153 665.141 5 5 -6 1 476.876 801.866 7 -5 6 -1 892.833 825.459 1 -5 6 -2 1038.19 578.077 5 -5 6 -2 341.914 670.766 1 -5 6 -3 1656.18 953.224 1 5 -6 3 601.248 933.441 7 -5 6 -4 6180.55 1914.29 2 -5 6 -4 4516.17 1442.33 1 5 -6 4 8722.08 2393.17 7 -5 6 -5 5479.26 1681.40 2 -5 6 -5 2151.10 1200.90 1 5 -6 5 4049.84 1733.89 7 5 -6 5 3778.08 1175.79 6 -5 6 -6 277.904 787.959 2 -5 6 -6 60.5765 681.366 1 5 -6 6-1105.95 1137.26 7 5 -6 6 323.701 527.527 6 -5 5 12-422.112 693.974 5 5 -5 -12 160.679 834.572 7 -5 5 11 6081.88 1886.64 5 5 -5 -11 6774.51 1698.05 7 -5 5 10 2752.26 1353.19 5 5 -5 -10 453.936 695.047 2 5 -5 -10 3673.74 1302.99 7 -5 5 9 4405.54 1499.19 5 5 -5 -9 1617.87 580.022 2 5 -5 -9 3480.33 1184.86 7 -5 5 8 4627.38 1498.58 1 -5 5 8 4142.92 1396.56 5 5 -5 -8 7380.27 1684.44 7 -5 5 7 10435.3 1930.50 1 -5 5 7 9557.84 1988.38 5 5 -5 -7 11025.6 1980.62 7 -5 5 6 5489.95 1519.21 5 5 -5 -6 7612.60 1641.14 7 -5 5 6 7009.05 1603.52 1 -5 5 5-374.148 677.705 5 -5 5 5-1303.60 872.417 1 5 -5 -5-394.302 715.453 7 -5 5 4 5058.30 1442.40 5 5 -5 -4 3983.39 1340.45 7 -5 5 4 3882.98 1193.38 1 -5 5 3 29718.1 3083.50 5 5 -5 -3 37372.3 3481.96 7 -5 5 3 34823.2 3187.68 1 -5 5 2 8248.61 1605.89 5 -5 5 2 7823.47 1555.03 1 5 -5 -2 8130.67 1741.43 7 -5 5 1 4304.67 1237.08 5 5 -5 -1 3914.71 1288.97 7 -5 5 1 6488.08 1472.78 1 -5 5 0 14598.9 2183.26 1 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5 -8 -4 -3 996.241 1208.69 3 -8 -4 -3 1442.63 941.475 5 -8 -4 -4 4571.27 1411.63 5 -8 -4 -4 5541.62 2081.28 3 -8 -4 -5 961.584 847.354 5 -8 -4 -5 3579.02 1727.76 3 8 4 5 1951.01 1210.82 6 -8 -4 -6-1367.66 1606.74 3 8 4 6 2024.75 1099.44 6 -8 -4 -7 2016.16 1609.89 3 8 4 7 169.192 750.660 6 -8 -5 3 2576.15 1320.90 5 -8 -5 2 261.289 550.569 5 -8 -5 1 55.2419 594.500 5 -8 -5 1 470.544 661.659 3 -8 -5 0-1255.87 812.708 5 -8 -5 0 175.761 663.938 3 -8 -5 -1 161.893 540.048 5 -8 -5 -1 336.731 995.310 3 -8 -5 -2 1320.34 982.195 3 -8 -5 -2 13.5909 653.503 5 -8 -5 -3 346.556 950.170 3 -8 -5 -3 998.520 816.402 5 -8 -5 -4 2869.59 1394.44 3 -8 -5 -4 3382.04 1257.40 5 -8 -5 -5 1258.61 993.818 5 -8 -5 -5 1763.23 1316.01 3 8 5 5 2692.08 1340.74 6 -8 -5 -6 1364.88 1305.72 3 8 5 6 135.618 714.464 6 -8 -5 -7-1333.59 1465.43 3 8 5 7 1696.97 1292.26 6 -8 -6 2 129.494 713.277 5 -8 -6 1 3213.94 1456.49 5 -8 -6 1 2779.04 1156.61 3 -8 -6 0 2474.32 1132.36 5 -8 -6 0 2206.92 1226.42 3 -8 -6 -1 1028.23 882.693 5 -8 -6 -1 414.253 739.091 3 -8 -6 -2-469.223 704.852 5 -8 -6 -2-809.719 1104.30 3 -8 -6 -3 222.796 1005.07 3 -8 -6 -3 6.68400 582.202 5 -8 -6 -4 466.358 1270.27 3 -8 -6 -4 4055.22 1330.44 5 -8 -6 -5 326.440 935.672 3 -8 -6 -5 1105.90 609.353 5 8 6 5 469.351 762.113 6 -8 -6 -6 3.31417 1253.10 3 8 6 6 861.565 944.345 6 -8 -6 -7-711.921 1559.58 3 8 6 7 1554.75 1035.52 6 -8 -7 1 398.706 676.921 5 -8 -7 1 1.00476 651.657 3 -8 -7 0 4237.91 1427.66 5 -8 -7 0 2198.70 1001.79 3 -8 -7 -1 544.377 731.630 5 -8 -7 -1 845.358 853.492 3 -8 -7 -2-210.873 504.120 5 -8 -7 -2 662.606 1168.20 3 -8 -7 -3 712.579 776.116 5 -8 -7 -3 1624.74 1226.78 3 -8 -7 -4-298.813 636.535 5 -8 -7 -4-1789.05 1253.04 3 -8 -7 -5 292.855 1021.97 3 -8 -7 -5 916.051 907.162 5 8 7 5-124.784 946.419 6 -8 -7 -6 595.123 1149.36 3 8 7 6 444.789 752.275 6 -8 -7 -7 2920.14 2124.89 3 8 7 7 4671.69 1627.23 6 -8 -8 -1 2203.02 1153.59 5 -8 -8 -1 1414.63 827.906 3 -8 -8 -2 2363.39 1133.49 5 -8 -8 -2 2829.60 1500.98 3 -8 -8 -3 703.378 900.004 5 -8 -8 -3 1699.14 943.560 3 8 8 3 1332.22 751.480 6 -8 -8 -4 550.808 709.950 5 -8 -8 -4 566.702 905.679 3 8 8 5 1256.76 1172.41 6 -8 -8 -5 813.404 959.129 3 8 8 6 2276.69 1000.64 6 -8 -8 -6-759.208 1224.08 3 0 0 0 0.00 0.00 0 TITL RED1 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 7.156059 12.129985 12.611680 63.4978 86.6941 81.4511 ZERR 1.00 0.000601 0.001099 0.001707 0.0111 0.0087 0.0072 LATT 1 SFAC C H N O S Pd UNIT 40.00 50.00 4.00 6.00 2.00 1.00 TREF HKLF 4 END ; _shelx_hkl_checksum 30185 _olex2_submission_special_instructions 'No special instructions were received'