#============================================================================== data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 11 _journal_issue 4 _journal_year 2020 _journal_page_first 377 _journal_page_last 384 #============================================================================== data_shelx _audit_creation_date 2020-11-21 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _shelxl_version_number 2013-4 _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C36 H42 N4 O6 Pd S2' _chemical_formula_sum 'C36 H42 N4 O6 Pd S2' _chemical_formula_weight 797.25 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.6726(2) _cell_length_b 20.8824(4) _cell_length_c 10.3351(2) _cell_angle_alpha 90 _cell_angle_beta 104.429(2) _cell_angle_gamma 90 _cell_volume 1812.70(7) _cell_formula_units_Z 2 _cell_measurement_reflns_used 14390 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 26.6100 _cell_measurement_theta_min 3.6570 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 0.677 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.81984 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details CrysAlisPro _exptl_crystal_colour YELLOW _exptl_crystal_density_diffrn 1.461 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 824 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0455 _diffrn_reflns_av_unetI/netI 0.0246 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 30464 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.362 _diffrn_reflns_theta_min 3.372 _diffrn_ambient_temperature 293(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Xcalibur, Eos, Nova' _diffrn_measurement_method ? _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3303 _reflns_number_total 3695 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2013/4 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _refine_diff_density_max 0.405 _refine_diff_density_min -0.263 _refine_diff_density_rms 0.058 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.093 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 231 _refine_ls_number_reflns 3695 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0394 _refine_ls_R_factor_gt 0.0344 _refine_ls_restrained_S_all 1.093 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0325P)^2^+1.5270P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0809 _refine_ls_wR_factor_ref 0.0840 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C9(H9) 2.b Me refined with riding coordinates: C11(H11A,H11B,H11C), C18(H18A,H18B,H18C), C8(H8A,H8B,H8C), C10(H10A,H10B,H10C) 2.c Aromatic/amide H refined with riding coordinates: C2(H2A), C3(H3), C13(H13), C16(H16), C17(H17), C14(H14) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group H2 H 0.800(3) 0.0019(13) -0.059(3) 0.031(8) Uiso 1 1 d . . . . . H7 H 0.759(3) 0.1417(12) 0.002(2) 0.024(6) Uiso 1 1 d . . . . . Pd1 Pd 0.5000 0.0000 0.0000 0.02906(10) Uani 1 2 d S . P . . S1 S 0.75556(10) 0.04840(4) -0.24010(8) 0.0495(2) Uani 1 1 d . . . . . O1 O 0.3589(2) 0.07268(8) 0.01559(19) 0.0387(4) Uani 1 1 d . . . . . N1 N 0.6696(2) 0.06066(9) -0.0167(2) 0.0319(4) Uani 1 1 d . . . . . C6 C 0.5599(3) 0.15623(11) 0.0618(2) 0.0314(5) Uani 1 1 d . . . . . C7 C 0.6764(3) 0.12101(12) 0.0145(3) 0.0329(5) Uani 1 1 d . . . . . N2 N 0.7943(3) 0.03887(12) -0.0733(2) 0.0386(5) Uani 1 1 d . . . . . O3 O 0.7328(3) 0.11555(10) -0.2625(2) 0.0651(6) Uani 1 1 d . . . . . C5 C 0.4059(3) 0.13121(12) 0.0543(3) 0.0334(5) Uani 1 1 d . . . . . C1 C 0.5986(3) 0.21989(12) 0.1105(3) 0.0384(6) Uani 1 1 d . . . . . O2 O 0.8836(3) 0.01545(13) -0.2749(3) 0.0720(7) Uani 1 1 d . . . . . C9 C 0.7629(3) 0.24842(14) 0.1238(3) 0.0496(7) Uani 1 1 d . . . . . H9 H 0.8368 0.2125 0.1287 0.059 Uiso 1 1 calc R U . . . C4 C 0.2887(3) 0.17122(13) 0.0860(3) 0.0458(7) Uani 1 1 d . . . . . C2 C 0.4839(4) 0.25576(13) 0.1464(3) 0.0499(7) Uani 1 1 d . . . . . H2A H 0.5089 0.2966 0.1811 0.060 Uiso 1 1 calc R U . . . C15 C 0.2898(4) -0.05834(16) -0.3778(3) 0.0536(8) Uani 1 1 d . . . . . C12 C 0.5747(4) 0.00876(13) -0.3074(3) 0.0434(7) Uani 1 1 d . . . . . C3 C 0.3295(4) 0.23193(14) 0.1316(3) 0.0536(8) Uani 1 1 d . . . . . H3 H 0.2528 0.2580 0.1534 0.064 Uiso 1 1 calc R U . . . C13 C 0.4329(4) 0.03942(15) -0.3095(3) 0.0519(7) Uani 1 1 d . . . . . H13 H 0.4327 0.0825 -0.2871 0.062 Uiso 1 1 calc R U . . . C16 C 0.4316(4) -0.08773(15) -0.3780(3) 0.0570(8) Uani 1 1 d . . . . . H16 H 0.4309 -0.1305 -0.4029 0.068 Uiso 1 1 calc R U . . . C17 C 0.5754(4) -0.05536(15) -0.3422(3) 0.0516(7) Uani 1 1 d . . . . . H17 H 0.6704 -0.0762 -0.3415 0.062 Uiso 1 1 calc R U . . . C11 C 0.1216(4) 0.14613(17) 0.0658(5) 0.0777(12) Uani 1 1 d . . . . . H11A H 0.1167 0.1029 0.0335 0.116 Uiso 1 1 calc R U . . . H11B H 0.0498 0.1724 0.0019 0.116 Uiso 1 1 calc R U . . . H11C H 0.0919 0.1471 0.1493 0.116 Uiso 1 1 calc R U . . . C18 C 0.1360(5) -0.0954(2) -0.4118(4) 0.0765(11) Uani 1 1 d . . . . . H18A H 0.0497 -0.0675 -0.4067 0.115 Uiso 1 1 calc R U . . . H18B H 0.1421 -0.1300 -0.3496 0.115 Uiso 1 1 calc R U . . . H18C H 0.1182 -0.1122 -0.5007 0.115 Uiso 1 1 calc R U . . . C14 C 0.2918(4) 0.00598(16) -0.3447(3) 0.0558(8) Uani 1 1 d . . . . . H14 H 0.1967 0.0268 -0.3462 0.067 Uiso 1 1 calc R U . . . C8 C 0.8227(5) 0.28777(19) 0.2502(4) 0.0779(12) Uani 1 1 d . . . . . H8A H 0.8180 0.2624 0.3266 0.117 Uiso 1 1 calc R U . . . H8B H 0.7571 0.3251 0.2466 0.117 Uiso 1 1 calc R U . . . H8C H 0.9307 0.3007 0.2572 0.117 Uiso 1 1 calc R U . . . C10 C 0.7683(5) 0.2864(2) 0.0019(4) 0.0942(15) Uani 1 1 d . . . . . H10A H 0.8730 0.3039 0.0125 0.141 Uiso 1 1 calc R U . . . H10B H 0.6920 0.3205 -0.0097 0.141 Uiso 1 1 calc R U . . . H10C H 0.7433 0.2589 -0.0750 0.141 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.02594(14) 0.02508(15) 0.03884(16) -0.00351(10) 0.01313(11) -0.00306(9) S1 0.0550(4) 0.0458(4) 0.0587(5) -0.0078(3) 0.0351(4) -0.0114(3) O1 0.0281(9) 0.0285(9) 0.0622(12) -0.0078(8) 0.0163(8) -0.0019(7) N1 0.0266(10) 0.0300(11) 0.0425(12) -0.0051(9) 0.0148(9) -0.0019(8) C6 0.0315(12) 0.0273(12) 0.0361(13) -0.0016(10) 0.0099(11) 0.0003(9) C7 0.0267(12) 0.0310(13) 0.0422(14) -0.0016(11) 0.0110(11) -0.0070(10) N2 0.0325(11) 0.0297(12) 0.0595(15) -0.0061(11) 0.0226(10) -0.0034(9) O3 0.0899(17) 0.0442(13) 0.0708(15) 0.0048(11) 0.0378(13) -0.0187(12) C5 0.0315(13) 0.0281(12) 0.0421(14) 0.0002(10) 0.0123(11) 0.0007(10) C1 0.0398(14) 0.0289(13) 0.0474(15) -0.0038(11) 0.0124(12) -0.0032(10) O2 0.0673(16) 0.0794(17) 0.0878(18) -0.0222(14) 0.0544(14) -0.0108(13) C9 0.0419(16) 0.0357(15) 0.072(2) -0.0148(14) 0.0167(14) -0.0089(12) C4 0.0358(14) 0.0352(15) 0.071(2) -0.0040(13) 0.0222(14) 0.0025(11) C2 0.0550(18) 0.0306(14) 0.068(2) -0.0132(13) 0.0234(15) -0.0010(12) C15 0.060(2) 0.058(2) 0.0426(16) -0.0001(14) 0.0117(14) -0.0089(15) C12 0.0567(18) 0.0391(15) 0.0395(15) -0.0030(11) 0.0214(13) -0.0045(12) C3 0.0498(17) 0.0369(16) 0.082(2) -0.0084(15) 0.0312(16) 0.0075(13) C13 0.0606(19) 0.0398(16) 0.0551(18) -0.0017(14) 0.0141(15) 0.0063(14) C16 0.075(2) 0.0419(17) 0.0556(19) -0.0085(14) 0.0182(16) -0.0060(16) C17 0.0602(19) 0.0464(17) 0.0521(17) -0.0084(14) 0.0215(15) 0.0018(14) C11 0.0385(17) 0.053(2) 0.153(4) -0.014(2) 0.044(2) 0.0046(15) C18 0.069(2) 0.081(3) 0.077(3) -0.006(2) 0.014(2) -0.022(2) C14 0.0517(19) 0.060(2) 0.0541(19) 0.0000(15) 0.0109(15) 0.0049(15) C8 0.082(3) 0.065(2) 0.082(3) -0.020(2) 0.011(2) -0.029(2) C10 0.085(3) 0.122(4) 0.081(3) 0.013(3) 0.031(2) -0.042(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 O1 1.9811(16) . ? Pd1 O1 1.9810(16) 3_655 ? Pd1 N1 1.9809(19) 3_655 ? Pd1 N1 1.9809(19) . ? S1 N2 1.684(3) . ? S1 O3 1.427(2) . ? S1 O2 1.427(2) . ? S1 C12 1.757(3) . ? O1 C5 1.319(3) . ? N1 C7 1.299(3) . ? N1 N2 1.427(3) . ? C6 C7 1.431(3) . ? C6 C5 1.418(3) . ? C6 C1 1.431(3) . ? C7 H7 0.87(3) . ? N2 H2 0.79(3) . ? C5 C4 1.415(4) . ? C1 C9 1.519(4) . ? C1 C2 1.368(4) . ? C9 H9 0.9800 . ? C9 C8 1.521(4) . ? C9 C10 1.498(5) . ? C4 C3 1.368(4) . ? C4 C11 1.506(4) . ? C2 H2A 0.9300 . ? C2 C3 1.401(4) . ? C15 C16 1.375(5) . ? C15 C18 1.505(5) . ? C15 C14 1.385(4) . ? C12 C13 1.382(4) . ? C12 C17 1.387(4) . ? C3 H3 0.9300 . ? C13 H13 0.9300 . ? C13 C14 1.376(4) . ? C16 H16 0.9300 . ? C16 C17 1.386(4) . ? C17 H17 0.9300 . ? C11 H11A 0.9600 . ? C11 H11B 0.9600 . ? C11 H11C 0.9600 . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C14 H14 0.9300 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Pd1 O1 180.0 3_655 . ? N1 Pd1 O1 90.24(8) . . ? N1 Pd1 O1 90.24(8) 3_655 3_655 ? N1 Pd1 O1 89.76(8) . 3_655 ? N1 Pd1 O1 89.76(8) 3_655 . ? N1 Pd1 N1 180.0 3_655 . ? N2 S1 C12 106.31(12) . . ? O3 S1 N2 105.46(13) . . ? O3 S1 C12 108.96(15) . . ? O2 S1 N2 103.41(15) . . ? O2 S1 O3 121.18(15) . . ? O2 S1 C12 110.31(15) . . ? C5 O1 Pd1 125.76(15) . . ? C7 N1 Pd1 126.01(17) . . ? C7 N1 N2 114.8(2) . . ? N2 N1 Pd1 119.16(15) . . ? C7 C6 C1 118.3(2) . . ? C5 C6 C7 121.8(2) . . ? C5 C6 C1 119.8(2) . . ? N1 C7 H7 115.5(16) . . ? N1 C7 C6 126.2(2) . . ? C6 C7 H7 118.2(16) . . ? S1 N2 H2 107(2) . . ? N1 N2 H2 105(2) . . ? N1 N2 S1 113.82(17) . . ? O1 C5 C6 125.0(2) . . ? O1 C5 C4 115.6(2) . . ? C4 C5 C6 119.4(2) . . ? C6 C1 C9 121.9(2) . . ? C2 C1 C6 118.7(2) . . ? C2 C1 C9 119.3(2) . . ? C1 C9 H9 106.9 . . ? C1 C9 C8 113.6(3) . . ? C8 C9 H9 106.9 . . ? C10 C9 C1 110.9(3) . . ? C10 C9 H9 106.9 . . ? C10 C9 C8 111.2(3) . . ? C5 C4 C11 119.0(2) . . ? C3 C4 C5 119.2(3) . . ? C3 C4 C11 121.8(3) . . ? C1 C2 H2A 119.5 . . ? C1 C2 C3 121.1(3) . . ? C3 C2 H2A 119.5 . . ? C16 C15 C18 120.7(3) . . ? C16 C15 C14 118.5(3) . . ? C14 C15 C18 120.8(3) . . ? C13 C12 S1 119.4(2) . . ? C13 C12 C17 120.3(3) . . ? C17 C12 S1 119.8(2) . . ? C4 C3 C2 121.6(3) . . ? C4 C3 H3 119.2 . . ? C2 C3 H3 119.2 . . ? C12 C13 H13 120.1 . . ? C14 C13 C12 119.9(3) . . ? C14 C13 H13 120.1 . . ? C15 C16 H16 119.1 . . ? C15 C16 C17 121.9(3) . . ? C17 C16 H16 119.1 . . ? C12 C17 H17 120.7 . . ? C16 C17 C12 118.6(3) . . ? C16 C17 H17 120.7 . . ? C4 C11 H11A 109.5 . . ? C4 C11 H11B 109.5 . . ? C4 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C15 C18 H18A 109.5 . . ? C15 C18 H18B 109.5 . . ? C15 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C15 C14 H14 119.6 . . ? C13 C14 C15 120.9(3) . . ? C13 C14 H14 119.6 . . ? C9 C8 H8A 109.5 . . ? C9 C8 H8B 109.5 . . ? C9 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Pd1 O1 C5 C6 15.4(4) . . . . ? Pd1 O1 C5 C4 -166.67(19) . . . . ? Pd1 N1 C7 C6 -2.7(4) . . . . ? Pd1 N1 N2 S1 90.35(19) . . . . ? S1 C12 C13 C14 -171.1(2) . . . . ? S1 C12 C17 C16 171.4(2) . . . . ? O1 C5 C4 C3 177.7(3) . . . . ? O1 C5 C4 C11 -3.5(4) . . . . ? C6 C5 C4 C3 -4.3(4) . . . . ? C6 C5 C4 C11 174.5(3) . . . . ? C6 C1 C9 C8 -139.5(3) . . . . ? C6 C1 C9 C10 94.4(4) . . . . ? C6 C1 C2 C3 -2.3(5) . . . . ? C7 N1 N2 S1 -86.9(2) . . . . ? C7 C6 C5 O1 6.2(4) . . . . ? C7 C6 C5 C4 -171.6(3) . . . . ? C7 C6 C1 C9 -5.2(4) . . . . ? C7 C6 C1 C2 175.0(3) . . . . ? N2 S1 C12 C13 81.9(3) . . . . ? N2 S1 C12 C17 -89.9(3) . . . . ? N2 N1 C7 C6 174.3(2) . . . . ? O3 S1 N2 N1 59.9(2) . . . . ? O3 S1 C12 C13 -31.3(3) . . . . ? O3 S1 C12 C17 156.8(2) . . . . ? C5 C6 C7 N1 -13.2(4) . . . . ? C5 C6 C1 C9 178.5(3) . . . . ? C5 C6 C1 C2 -1.3(4) . . . . ? C5 C4 C3 C2 0.8(5) . . . . ? C1 C6 C7 N1 170.6(3) . . . . ? C1 C6 C5 O1 -177.6(2) . . . . ? C1 C6 C5 C4 4.6(4) . . . . ? C1 C2 C3 C4 2.6(5) . . . . ? O2 S1 N2 N1 -171.96(18) . . . . ? O2 S1 C12 C13 -166.6(2) . . . . ? O2 S1 C12 C17 21.5(3) . . . . ? C9 C1 C2 C3 178.0(3) . . . . ? C2 C1 C9 C8 40.2(4) . . . . ? C2 C1 C9 C10 -85.8(4) . . . . ? C15 C16 C17 C12 -1.1(5) . . . . ? C12 S1 N2 N1 -55.8(2) . . . . ? C12 C13 C14 C15 0.2(5) . . . . ? C13 C12 C17 C16 -0.4(5) . . . . ? C16 C15 C14 C13 -1.6(5) . . . . ? C17 C12 C13 C14 0.8(5) . . . . ? C11 C4 C3 C2 -178.0(3) . . . . ? C18 C15 C16 C17 -177.5(3) . . . . ? C18 C15 C14 C13 177.9(3) . . . . ? C14 C15 C16 C17 2.0(5) . . . . ? _shelx_res_file ; TITL RED1 in P2(1)/n CELL 0.71073 8.6726 20.8824 10.3351 90 104.429 90 ZERR 2 0.0002 0.0004 0.0002 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O Pd S UNIT 72 84 8 12 2 4 L.S. 10 PLAN 2 CONF HTAB BOND MORE -1 BOND $H fmap 2 acta MERG 2 REM REM REM WGHT 0.032500 1.527000 FVAR 4.28584 H2 2 0.799817 0.001879 -0.059102 11.00000 0.03083 H7 2 0.759121 0.141679 0.001768 11.00000 0.02420 PD1 5 0.500000 0.000000 0.000000 10.50000 0.02594 0.02508 = 0.03884 -0.00351 0.01313 -0.00306 S1 6 0.755556 0.048399 -0.240097 11.00000 0.05501 0.04579 = 0.05872 -0.00785 0.03512 -0.01140 O1 4 0.358931 0.072682 0.015586 11.00000 0.02806 0.02845 = 0.06223 -0.00782 0.01626 -0.00193 N1 3 0.669591 0.060659 -0.016709 11.00000 0.02657 0.03002 = 0.04249 -0.00509 0.01480 -0.00192 C6 1 0.559894 0.156230 0.061847 11.00000 0.03149 0.02733 = 0.03614 -0.00158 0.00986 0.00031 C7 1 0.676428 0.121011 0.014482 11.00000 0.02671 0.03096 = 0.04224 -0.00158 0.01103 -0.00699 N2 3 0.794323 0.038873 -0.073329 11.00000 0.03254 0.02973 = 0.05955 -0.00612 0.02260 -0.00344 O3 4 0.732787 0.115554 -0.262519 11.00000 0.08985 0.04416 = 0.07084 0.00480 0.03780 -0.01866 C5 1 0.405916 0.131213 0.054332 11.00000 0.03155 0.02814 = 0.04212 0.00023 0.01232 0.00070 C1 1 0.598634 0.219890 0.110502 11.00000 0.03985 0.02890 = 0.04735 -0.00381 0.01243 -0.00318 O2 4 0.883630 0.015451 -0.274943 11.00000 0.06730 0.07944 = 0.08780 -0.02215 0.05443 -0.01079 C9 1 0.762938 0.248421 0.123818 11.00000 0.04187 0.03569 = 0.07243 -0.01484 0.01667 -0.00895 AFIX 13 H9 2 0.836840 0.212485 0.128687 11.00000 -1.20000 AFIX 0 C4 1 0.288734 0.171215 0.085955 11.00000 0.03585 0.03519 = 0.07103 -0.00403 0.02221 0.00250 C2 1 0.483935 0.255764 0.146388 11.00000 0.05503 0.03061 = 0.06820 -0.01318 0.02337 -0.00097 AFIX 43 H2A 2 0.508883 0.296618 0.181135 11.00000 -1.20000 AFIX 0 C15 1 0.289759 -0.058341 -0.377831 11.00000 0.05955 0.05828 = 0.04255 -0.00007 0.01173 -0.00886 C12 1 0.574708 0.008765 -0.307445 11.00000 0.05669 0.03911 = 0.03950 -0.00295 0.02138 -0.00453 C3 1 0.329524 0.231935 0.131623 11.00000 0.04980 0.03694 = 0.08193 -0.00842 0.03121 0.00750 AFIX 43 H3 2 0.252818 0.258035 0.153403 11.00000 -1.20000 AFIX 0 C13 1 0.432855 0.039416 -0.309483 11.00000 0.06055 0.03983 = 0.05514 -0.00171 0.01407 0.00634 AFIX 43 H13 2 0.432710 0.082549 -0.287109 11.00000 -1.20000 AFIX 0 C16 1 0.431558 -0.087727 -0.378033 11.00000 0.07468 0.04191 = 0.05558 -0.00852 0.01824 -0.00605 AFIX 43 H16 2 0.430910 -0.130546 -0.402906 11.00000 -1.20000 AFIX 0 C17 1 0.575410 -0.055363 -0.342234 11.00000 0.06017 0.04638 = 0.05207 -0.00845 0.02147 0.00184 AFIX 43 H17 2 0.670391 -0.076194 -0.341548 11.00000 -1.20000 AFIX 0 C11 1 0.121613 0.146128 0.065823 11.00000 0.03851 0.05272 = 0.15251 -0.01426 0.04402 0.00465 AFIX 33 H11A 2 0.116661 0.102888 0.033503 11.00000 -1.50000 H11B 2 0.049765 0.172425 0.001855 11.00000 -1.50000 H11C 2 0.091886 0.147080 0.149277 11.00000 -1.50000 AFIX 0 C18 1 0.136014 -0.095380 -0.411776 11.00000 0.06855 0.08147 = 0.07731 -0.00612 0.01408 -0.02163 AFIX 33 H18A 2 0.049685 -0.067510 -0.406697 11.00000 -1.50000 H18B 2 0.142078 -0.130000 -0.349595 11.00000 -1.50000 H18C 2 0.118230 -0.112250 -0.500685 11.00000 -1.50000 AFIX 0 C14 1 0.291849 0.005977 -0.344685 11.00000 0.05174 0.06041 = 0.05410 0.00000 0.01090 0.00487 AFIX 43 H14 2 0.196671 0.026845 -0.346241 11.00000 -1.20000 AFIX 0 C8 1 0.822695 0.287768 0.250221 11.00000 0.08176 0.06462 = 0.08210 -0.01983 0.01079 -0.02904 AFIX 33 H8A 2 0.818033 0.262406 0.326627 11.00000 -1.50000 H8B 2 0.757065 0.325070 0.246632 11.00000 -1.50000 H8C 2 0.930709 0.300665 0.257195 11.00000 -1.50000 AFIX 0 C10 1 0.768288 0.286351 0.001939 11.00000 0.08460 0.12233 = 0.08125 0.01349 0.03131 -0.04250 AFIX 33 H10A 2 0.872979 0.303921 0.012459 11.00000 -1.50000 H10B 2 0.691967 0.320506 -0.009710 11.00000 -1.50000 H10C 2 0.743345 0.258927 -0.075017 11.00000 -1.50000 AFIX 0 HKLF 4 REM RED1 in P2(1)/n REM R1 = 0.0344 for 3303 Fo > 4sig(Fo) and 0.0394 for all 3695 data REM 231 parameters refined using 0 restraints END WGHT 0.0325 1.5270 REM Instructions for potential hydrogen bonds EQIV $1 -x+1, -y, -z HTAB N2 O1_$1 REM Highest difference peak 0.405, deepest hole -0.263, 1-sigma level 0.058 Q1 1 0.0861 0.1307 -0.0384 11.00000 0.05 0.41 Q2 1 0.1206 0.1092 0.1324 11.00000 0.05 0.37 ; _shelx_res_checksum 74310 _shelx_hkl_file ; 0 0 -2 112517. 3140.12 2 0 0 -2 108285. 3102.77 7 0 0 -2 110272. 3110.62 9 0 0 -2 111032. 2840.68 5 0 0 -2 111309. 2956.74 4 0 0 2 107418. 3135.31 8 0 0 2 113304. 3123.51 9 0 0 2 111530. 2848.90 5 0 0 2 109144. 2954.89 4 0 0 -2 118204. 3020.98 1 0 0 2 107338. 2972.65 1 0 0 2 104926. 3104.33 7 0 0 2 109254. 3123.36 2 0 0 -3 190.139 106.281 9 0 0 -3 725.185 176.821 1 0 0 3 525.227 117.317 4 0 0 -3 722.533 125.743 5 0 0 3 1387.67 300.871 8 0 0 3 521.591 156.012 1 0 0 3 228.812 99.4423 9 0 0 3 1148.04 253.068 2 0 0 -3 441.629 131.647 4 0 0 3 574.570 121.385 5 0 0 3 494.765 123.544 7 0 0 -3 605.716 196.147 2 0 0 4 183232. 5358.90 9 0 0 -4 180560. 5401.67 2 0 0 4 185550. 5399.28 7 0 0 4 179048. 5099.27 1 0 0 -4 204575. 5337.59 1 0 0 4 180484. 5045.29 4 0 0 4 184424. 5400.66 2 0 0 4 183863. 4827.85 5 0 0 -4 177364. 5327.00 9 0 0 4 177833. 5394.14 8 0 0 -4 184161. 5037.25 4 0 0 -4 184093. 4824.39 5 0 0 5 5.07042 82.1313 4 0 0 -5 94.0667 93.8015 4 0 0 -5-16.3455 64.0754 5 0 0 5 47.5550 51.6773 5 0 0 -5 252.237 222.829 2 0 0 5 79.0401 89.2719 1 0 0 -5 161.020 163.380 9 0 0 -6 12939.5 1154.89 2 0 0 -6 14178.5 960.932 4 0 0 -6 13570.0 821.780 5 0 0 6 13696.7 981.860 4 0 0 6 12721.5 800.964 5 0 0 -6 13732.7 1159.11 9 0 0 6 11666.8 943.937 1 0 0 -7 142.421 175.660 9 0 0 -7 203.276 193.437 2 0 0 -7 282.913 156.120 5 0 0 7-23.4765 100.164 4 0 0 7-47.4401 58.1649 5 0 0 7 100.322 106.106 1 0 0 8 63959.9 2833.68 4 0 0 -8 74259.1 3543.55 2 0 0 -8 74853.7 3469.65 9 0 0 8 68956.2 3045.60 1 0 0 -8 70183.3 2571.78 5 0 0 -9-287.419 307.824 2 0 0 9-82.5483 132.512 1 0 0 9 157.742 157.006 4 0 0 -9-130.049 292.572 9 0 0 10 2512.14 560.433 1 0 0 -10 3423.86 785.669 2 0 0 -10 4501.16 880.372 9 0 0 10 3591.63 633.134 4 0 0 11-34.5444 126.810 1 0 0 -11 142.044 186.321 9 0 0 -11 223.453 284.064 2 0 0 -12 6285.37 1156.72 9 0 0 12 6946.79 1073.20 1 0 0 -12 7326.98 1291.03 2 0 1 -2 174062. 4713.09 7 0 -1 -2 183014. 4525.90 4 0 -1 2 179078. 4717.26 7 0 -1 2 179579. 4739.96 2 0 -1 2 183725. 4354.02 5 0 1 2 175130. 4499.22 4 0 1 -2 179569. 4642.34 1 0 -1 2 179960. 4604.89 4 0 1 -2 169692. 4715.40 2 0 1 -2 175148. 4348.58 5 0 1 2 183441. 4744.85 2 0 -1 2 181037. 4712.26 9 0 -1 -2 177869. 4739.88 2 0 -1 -2 174314. 4509.72 5 0 -1 -2 178812. 4714.96 9 0 1 2 184590. 4520.95 1 0 -1 2 180912. 4744.34 8 0 1 2 181781. 4524.69 5 0 1 2 176139. 4736.13 8 0 -1 2 172726. 4633.09 1 0 1 -2 180833. 4731.40 9 0 1 2 180539. 4722.87 9 0 1 3 904642. 22414.4 9 0 -1 3 919083. 22277.0 1 0 -1 -3 910165. 22468.3 2 0 -1 3 960651. 22486.7 2 0 -1 -3 999999. 22103.7 5 0 1 3 943663. 22471.0 2 0 1 -3 983994. 22312.9 1 0 1 3 952484. 22071.8 5 0 -1 3 906120. 22408.4 7 0 -1 -3 927006. 22431.3 9 0 1 3 912973. 22100.4 4 0 -1 3 935148. 22482.5 8 0 1 3 939494. 22473.4 7 0 1 -3 911807. 22447.6 9 0 1 -3 922649. 22426.9 7 0 -1 3 919182. 22220.1 4 0 -1 3 969705. 21889.1 5 0 1 -3 912086. 21879.3 5 0 -1 3 954170. 22440.3 9 0 1 3 941966. 22489.2 8 0 1 -3 918859. 22472.4 2 0 -1 -3 937047. 22114.9 4 0 1 3 930574. 22121.0 1 0 -1 4 7143.87 668.411 7 0 -1 4 7013.07 687.229 8 0 1 4 8265.61 737.963 8 0 -1 -4 6203.70 630.114 9 0 1 -4 6510.18 430.958 5 0 -1 4 7697.48 604.808 4 0 -1 -4 8995.74 566.852 5 0 1 4 6762.74 501.276 5 0 1 4 7431.43 690.047 7 0 1 -4 7057.02 665.801 9 0 1 4 7386.89 691.909 2 0 -1 -4 8902.15 780.409 2 0 1 4 7098.09 560.836 1 0 1 -4 6779.99 664.979 7 0 1 -4 8006.71 642.371 1 0 1 -4 6987.84 693.699 2 0 -1 4 7418.32 453.896 5 0 -1 4 6760.47 638.499 9 0 -1 4 6563.79 654.789 2 0 1 4 7574.67 687.576 9 0 -1 4 6655.06 590.747 1 0 -1 -4 7417.72 553.807 4 0 1 4 6091.01 512.125 4 0 1 -5 52140.8 2418.96 2 0 -1 -5 56335.9 2118.18 4 0 -1 -5 54135.1 1958.22 5 0 1 -5 58923.5 2463.48 9 0 1 -5 55051.3 1841.71 5 0 1 5 56209.6 2134.87 1 0 -1 -5 54985.8 2448.29 2 0 -1 -5 54288.3 2389.91 9 0 -1 5 56275.8 2243.39 1 0 -1 5 56114.5 1844.48 5 0 1 5 56659.7 1987.01 5 0 1 5 55690.1 2091.61 4 0 -1 5 57409.5 2204.37 4 0 -1 6-10.5288 75.7986 4 0 1 6 305.283 157.721 4 0 1 6 170.815 78.6543 5 0 -1 -6 152.152 112.908 5 0 -1 6 117.079 91.2840 5 0 1 6-59.6024 143.870 1 0 1 -6-42.2531 212.529 2 0 -1 6-71.9742 131.363 1 0 -1 -6 64.1288 104.963 4 0 1 -6 256.032 105.368 5 0 -1 -6-93.7463 174.642 2 0 1 -6-21.3336 151.401 9 0 -1 -6-152.989 194.151 9 0 -1 -7 16481.0 1417.05 2 0 1 -7 16491.7 1445.62 2 0 -1 7 18384.6 1262.00 4 0 -1 -7 18360.9 1484.48 9 0 1 -7 17787.7 1432.02 9 0 -1 7 17775.1 981.658 5 0 1 7 18042.2 1240.41 1 0 1 -7 17189.2 963.509 5 0 1 7 17598.7 1076.62 5 0 -1 7 16334.7 1248.15 1 0 1 7 17574.3 1185.90 4 0 -1 -7 17809.3 1076.41 5 0 -1 -8 763.603 379.374 2 0 -1 8 364.534 255.971 1 0 1 -8 1045.96 497.400 2 0 -1 -8 306.057 235.148 9 0 -1 -8 302.126 171.729 5 0 -1 8 486.275 212.604 5 0 1 8 158.721 200.271 1 0 1 -8 82.0736 167.869 9 0 -1 8 304.022 289.871 4 0 1 8 505.658 289.893 4 0 -1 9 12441.6 925.120 3 0 -1 -9 14319.8 1474.41 9 0 -1 9 14085.1 1249.07 4 0 -1 -9 16278.1 1611.02 2 0 -1 -9 15000.2 1075.85 5 0 -1 9 16138.6 1405.65 1 0 1 -9 15728.2 1590.59 2 0 1 -9 15570.8 1553.96 9 0 1 9 12388.6 1176.97 1 0 1 9 13653.9 1167.56 4 0 -1 -10 194.333 136.628 5 0 -1 -10-193.615 334.744 2 0 1 10 172.493 131.543 1 0 -1 -10 144.681 213.826 9 0 1 -10-184.674 370.257 9 0 -1 10-180.613 233.414 1 0 1 10-52.1321 104.849 4 0 -1 10 7.68944 130.352 4 0 1 -10 72.5640 280.685 2 0 -1 -11 4199.76 915.085 9 0 -1 11 4355.77 828.542 1 0 1 11 4343.17 779.147 1 0 1 -11 4204.41 900.280 9 0 1 -11 6073.35 1109.67 2 0 -1 -11 5403.74 1066.30 2 0 -1 -12 171.095 273.756 9 0 1 -12-28.3973 269.495 9 0 -1 -12 67.5244 368.188 2 0 1 -12 147.022 261.491 2 0 -1 12 306.054 348.315 1 0 -2 2 1446.00 215.618 9 0 2 2 1225.12 177.865 5 0 -2 2 1677.05 245.191 2 0 2 -2 1481.69 217.687 7 0 2 -2 1514.11 233.806 2 0 2 -2 1706.28 235.515 9 0 -2 -2 1380.75 184.562 5 0 -2 -2 1253.39 208.050 9 0 2 2 1435.75 166.147 4 0 -2 -2 1355.18 212.494 2 0 -2 2 1265.87 202.730 1 0 -2 2 1558.09 226.389 7 0 -2 2 1693.38 248.365 8 0 2 2 1124.00 203.330 9 0 2 2 1440.46 221.630 8 0 -2 -2 1492.02 176.666 4 0 2 2 1523.45 228.011 2 0 2 -2 1366.34 202.818 1 0 -2 3 489159. 11558.7 3 0 2 3 504573. 12228.4 9 0 2 3 500676. 11826.2 1 0 2 -3 470460. 12190.9 9 0 -2 -3 474035. 11895.7 5 0 -2 -3 477816. 12173.9 9 0 -2 3 476644. 12112.4 1 0 -2 -3 481104. 12199.1 2 0 2 -3 457509. 12193.3 2 0 -2 3 479826. 12038.5 4 0 2 -3 491156. 12110.7 1 0 2 -3 489055. 12220.7 7 0 -2 3 482821. 11573.8 5 0 2 3 496015. 11924.3 5 0 -2 3 499756. 12168.9 9 0 2 3 497822. 12237.7 2 0 -2 3 487783. 12203.7 8 0 2 3 491851. 12224.1 8 0 -2 -3 500164. 11875.5 4 0 2 3 487056. 11833.1 4 0 -2 3 498594. 12233.1 2 0 -2 3 491024. 12178.3 7 0 -2 4 282449. 7496.41 9 0 -2 4 267493. 7296.51 4 0 -2 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2 6 35347.7 1664.90 4 0 2 -6 38110.4 2096.70 2 0 2 6 39947.7 1777.81 1 0 2 6 39296.2 1692.97 5 0 -2 7 3249.31 559.309 1 0 2 -7 3197.80 604.936 9 0 -2 7 3348.14 379.864 3 0 2 -7 3138.29 646.549 2 0 -2 -7 3435.37 613.397 9 0 -2 7 2797.93 488.189 4 0 2 7 3093.21 468.366 4 0 -2 -7 2925.89 434.550 5 0 -2 7 2760.15 335.588 5 0 2 7 2638.54 451.172 1 0 -2 -7 3189.26 599.684 2 0 2 8 17835.0 1297.00 1 0 -2 8 17127.6 980.551 3 0 2 8 17315.9 1223.82 4 0 -2 -8 19869.8 1625.64 9 0 2 -8 18842.2 1639.83 2 0 2 -8 15430.2 1470.99 9 0 -2 -8 15512.0 1487.61 2 0 -2 8 17545.2 1411.15 1 0 -2 -8 16459.6 1142.77 5 0 -2 8 15982.1 1284.02 4 0 -2 -9 486.573 181.984 5 0 2 9 292.137 234.171 4 0 -2 9 532.902 251.741 1 0 2 9 975.304 380.303 1 0 -2 9 709.440 298.945 4 0 -2 9 289.105 153.711 3 0 2 -9 570.288 365.513 2 0 2 -9 122.779 182.818 9 0 -2 -9 1010.10 375.645 9 0 -2 -9 1412.10 494.404 2 0 2 10 7490.06 929.869 1 0 -2 -10 8793.87 1236.69 2 0 -2 -10 6735.15 777.757 5 0 2 10 4403.78 670.809 4 0 -2 10 6489.37 881.780 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3140.96 782.537 1 0 6 -12 3083.95 834.773 9 0 6 -12 4159.89 1034.09 2 0 7 0 411.792 142.598 10 0 7 0 812.462 217.249 5 0 -7 0 478.603 176.640 1 0 7 0 352.954 148.658 1 0 -7 0 310.401 145.803 10 0 -7 1 160350. 4047.57 8 0 7 -1 160874. 4551.16 10 0 7 1 164819. 4091.17 8 0 -7 1 174770. 4546.21 10 0 7 -1 170485. 4435.67 3 0 7 1 164421. 4698.36 5 0 7 -1 164481. 4072.71 6 0 -7 -1 170880. 4623.20 10 0 -7 -1 164218. 4688.33 5 0 7 -1 169661. 4652.87 1 0 -7 1 156790. 4690.11 1 0 -7 -1 157322. 4309.20 1 0 7 1 160768. 4547.12 10 0 -7 1 162877. 4504.43 5 0 7 1 157821. 4384.90 1 0 7 -1 160501. 4509.39 5 0 -7 -2 7387.14 659.769 5 0 7 2 8123.92 691.608 5 0 7 -2 8786.85 519.239 3 0 -7 2 7195.51 453.676 6 0 -7 2 7564.13 526.801 5 0 7 2 7179.63 602.996 2 0 7 -2 7863.39 680.842 1 0 -7 2 8737.80 722.909 1 0 -7 -2 8736.51 594.813 4 0 -7 2 8625.11 534.305 8 0 7 2 7826.86 627.228 10 0 7 -2 7513.51 614.664 10 0 7 2 7836.80 524.100 8 0 -7 2 9367.64 645.000 10 0 7 2 8236.38 478.320 1 0 -7 3 116903. 3498.17 10 0 7 -3 113070. 3675.61 7 0 7 3 111174. 3567.50 10 0 -7 -3 109059. 3640.67 5 0 7 -3 109456. 3008.67 3 0 -7 -3 114117. 3370.98 4 0 -7 3 111022. 3773.93 1 0 -7 3 112464. 3147.71 5 0 7 3 110045. 3003.35 1 0 7 3 112586. 3434.84 8 0 -7 3 110118. 3414.51 8 0 -7 3 114531. 3305.61 6 0 7 -4 465.050 220.037 9 0 7 4 519.524 218.515 10 0 7 -4 256.953 152.848 7 0 -7 -4 162.948 120.970 4 0 7 -4 314.442 78.3825 3 0 -7 4 355.328 174.852 8 0 -7 -4 365.777 215.741 2 0 -7 4 227.542 144.409 6 0 -7 4 358.782 217.263 1 0 7 4 352.059 124.670 4 0 -7 -4 260.941 155.953 5 0 7 -4 318.173 155.013 2 0 -7 4 309.931 75.3952 3 0 -7 -5 5684.00 584.792 4 0 -7 -5 4973.72 643.068 2 0 7 5 6792.05 575.812 4 0 7 -5 6174.68 768.147 2 0 -7 5 5758.62 731.764 1 0 7 -5 6503.65 773.568 9 0 7 -5 6093.99 749.691 7 0 -7 5 5917.36 327.771 3 0 -7 -5 6523.69 719.897 5 0 7 5 6276.36 496.969 1 0 -7 5 5371.07 692.544 4 0 7 6 582.133 178.712 4 0 7 6 452.761 142.883 1 0 -7 -6 262.429 160.340 5 0 -7 6 344.837 213.401 1 0 -7 6 299.445 203.564 4 0 7 -6 396.097 230.701 2 0 -7 6 564.345 116.333 5 0 -7 -6 646.421 201.207 4 0 -7 -6 267.152 155.907 2 0 7 -6 467.428 226.134 7 0 -7 6 361.280 67.6734 3 0 7 -6 202.275 229.571 9 0 -7 -7 17407.5 1464.30 2 0 7 -7 16657.8 1471.41 9 0 -7 7 15485.2 1333.95 4 0 7 7 16746.9 1000.32 1 0 -7 7 17783.6 1503.10 1 0 -7 -7 16771.0 1303.64 5 0 7 -7 16559.4 1478.83 2 0 7 7 16694.1 1063.76 4 0 7 -7 15620.9 1445.31 7 0 -7 7 15216.6 681.805 5 0 7 -8 413.418 249.793 9 0 7 -8 436.105 218.655 7 0 -7 8 1124.95 365.267 4 0 7 8 885.189 275.691 1 0 -7 -8 986.654 363.445 2 0 -7 8 575.520 344.126 1 0 7 -8 419.081 263.080 2 0 7 8 954.702 270.087 4 0 -7 -8 976.282 315.916 5 0 7 9 2440.01 429.590 4 0 7 -9 3710.36 776.311 9 0 -7 9 3615.77 686.339 4 0 -7 -9 4401.78 835.548 2 0 7 -9 2516.61 662.686 7 0 7 9 2519.82 434.834 1 0 -7 -9 2333.24 515.868 5 0 -7 9 2319.06 610.674 1 0 7 -9 2940.49 702.627 2 0 7 -10 3117.08 794.957 7 0 7 -10 1641.78 543.336 2 0 7 -10 2285.12 679.156 9 0 -7 -10 3028.16 606.616 5 0 -7 10 2998.62 760.362 1 0 -7 -10 3119.26 769.824 2 0 -7 10 1615.51 509.717 4 0 -7 11 4735.12 977.328 1 0 -7 -11 4824.00 813.649 5 0 7 -11 4109.03 941.802 2 0 -7 -11 5470.22 1081.29 2 0 7 -11 4947.42 1009.67 9 0 -7 11 3729.42 806.723 4 0 7 -12-279.056 229.893 9 0 -7 -12 331.983 347.466 2 0 -7 12 295.876 220.951 1 0 8 0 104994. 3100.30 1 0 -8 0 93412.5 3110.40 1 0 -8 0 97386.3 3156.29 5 0 -8 0 104128. 3124.24 10 0 8 0 105146. 3218.88 5 0 8 0 94097.3 3063.25 10 0 -8 1 57764.6 1914.83 10 0 -8 1 48996.2 1351.65 8 0 -8 1 51561.6 1868.52 5 0 8 1 58744.8 2093.84 5 0 8 -1 54950.8 1908.59 5 0 8 1 52060.5 1898.85 10 0 -8 -1 54313.4 2030.44 5 0 8 1 53435.8 1800.04 1 0 -8 -1 53961.5 1728.97 1 0 8 -1 55526.3 1824.81 3 0 -8 -1 53966.9 1958.06 10 0 -8 1 52299.4 2050.90 1 0 8 -1 52130.9 1908.31 10 0 8 1 52556.0 1414.50 8 0 8 -1 54206.7 1994.06 1 0 8 2 37609.3 1384.90 1 0 8 2 38012.6 1637.49 10 0 8 -2 36971.1 1405.41 3 0 -8 -2 39302.7 1563.79 4 0 -8 2 36647.3 1349.21 8 0 -8 -2 38025.5 1741.73 5 0 -8 2 37020.5 1480.64 5 0 8 -2 37597.0 1634.79 10 0 -8 2 40231.6 1606.72 10 0 8 2 36672.4 1606.82 2 0 -8 2 39356.8 1291.11 6 0 8 2 39383.8 1396.86 8 0 -8 2 39063.5 1802.29 1 0 -8 -3 375.389 147.863 4 0 -8 3 413.980 159.227 8 0 -8 3 584.988 294.617 1 0 8 -3 124.521 98.2868 10 0 -8 -3 214.785 145.445 5 0 8 3 282.266 164.812 10 0 8 3 310.424 87.4049 1 0 8 -3-75.9686 182.432 7 0 -8 3 297.130 112.229 5 0 8 -3 120.854 70.9441 3 0 -8 3 187.181 101.341 6 0 8 3 173.891 121.687 8 0 -8 4 12198.6 682.462 5 0 -8 4 12646.4 851.327 6 0 -8 -4 11612.9 969.809 5 0 8 -4 12504.9 596.396 3 0 8 -4 12136.0 1007.62 2 0 8 4 12858.1 794.535 4 0 -8 4 11836.9 1039.45 1 0 -8 4 11334.8 879.115 8 0 8 4 11390.3 934.786 10 0 8 -4 12203.0 1010.45 9 0 -8 -4 12769.1 861.635 4 0 8 -4 10980.2 967.650 7 0 -8 -5 916.079 277.128 5 0 -8 5 362.046 201.266 1 0 8 -5 845.343 270.289 2 0 8 -5 634.207 289.804 9 0 8 -5 315.692 141.475 7 0 -8 -5 373.094 145.916 2 0 -8 -5 646.332 185.264 4 0 8 5 613.559 174.799 4 0 -8 5 912.750 162.715 5 0 8 5 465.595 208.214 10 0 8 -6 37469.5 2175.16 9 0 -8 -6 35392.6 1972.55 5 0 -8 -6 34939.0 2067.24 2 0 -8 6 37147.8 2084.61 4 0 -8 6 36252.3 2164.45 1 0 -8 -6 40712.1 1849.19 4 0 8 6 40221.0 1683.78 4 0 8 -6 39639.6 2223.79 7 0 8 6 37315.4 1480.86 1 0 8 -6 34522.3 2118.12 2 0 -8 6 34857.4 1270.50 5 0 -8 6 35983.9 1272.15 5 0 8 -7 771.211 332.278 2 0 8 7 1184.25 261.167 1 0 8 7 1732.24 338.964 4 0 8 -7 1916.63 503.646 7 0 -8 -7 1785.48 495.661 2 0 -8 -7 1411.34 409.746 5 0 -8 7 1202.16 165.816 5 0 -8 7 505.706 311.438 4 0 -8 7 1488.80 520.832 1 0 8 -7 1456.26 463.523 9 0 -8 8 4647.13 777.845 4 0 -8 -8 4681.34 813.753 2 0 8 -8 5070.31 872.407 7 0 -8 8 4484.33 832.145 1 0 8 -8 4720.25 831.037 2 0 -8 -8 5002.81 771.954 5 0 8 8 4741.71 541.007 1 0 8 -8 3714.95 746.297 9 0 8 8 5343.58 597.154 4 0 8 -9 223.726 172.319 7 0 8 -9 91.2932 144.194 9 0 8 9 113.380 97.5726 4 0 -8 9-26.4338 131.489 4 0 -8 -9-38.1004 179.346 2 0 -8 -9 70.4568 153.450 5 0 -8 9 107.886 181.261 1 0 8 -9 168.428 226.998 2 0 -8 -10 5851.11 1042.93 2 0 -8 -10 6818.88 926.548 5 0 -8 10 6382.73 1098.53 1 0 8 -10 6989.37 1150.64 2 0 8 -10 6573.51 1106.63 7 0 8 -10 6306.61 1092.19 9 0 -8 10 4599.02 842.404 4 0 -8 11 1119.54 467.180 1 0 -8 -11 504.006 253.795 5 0 -8 11 635.831 296.476 4 0 8 -11 319.319 410.862 2 0 -8 -11 593.083 364.399 2 0 8 -11 492.267 523.873 9 0 9 0 71.9218 92.8251 10 0 9 0 120.706 142.146 1 0 -9 0 59.8770 118.039 1 0 9 0 148.529 126.647 5 0 -9 0 98.5249 99.2894 5 0 9 1 10286.9 756.904 10 0 9 -1 12025.1 819.027 5 0 -9 -1 10737.0 839.159 5 0 9 -1 11976.8 844.733 1 0 9 1 11106.2 449.485 8 0 -9 1 11144.3 780.216 5 0 9 1 11813.8 744.755 1 0 9 -1 11165.9 798.088 10 0 -9 1 10599.7 855.432 1 0 9 -1 10551.3 715.876 3 0 -9 -1 10607.1 675.369 1 0 9 -1 9080.40 445.813 6 0 -9 2 62238.3 2563.54 1 0 -9 2 64473.6 2241.96 5 0 -9 -2 59544.1 2473.02 5 0 -9 -2 70325.2 2345.34 4 0 9 2 59800.3 2091.94 1 0 9 2 58779.3 2324.25 10 0 -9 2 66087.0 1911.24 6 0 9 2 62127.0 2010.23 8 0 9 -2 65919.4 2146.47 3 0 -9 2 68007.8 2003.82 8 0 9 -2 61167.0 2368.81 10 0 9 3 19894.6 1210.80 10 0 9 -3 18964.1 1179.15 10 0 -9 3 19280.7 1029.21 8 0 9 -3 20110.9 916.423 3 0 -9 3 18558.7 1313.95 1 0 9 3 21006.3 1080.07 8 0 -9 3 18506.4 974.202 5 0 -9 -3 18523.9 1243.17 5 0 -9 3 19483.1 943.342 6 0 -9 -3 20270.5 1111.05 4 0 9 -3 20134.4 1283.53 7 0 9 3 20904.9 893.312 1 0 -9 4 1199.65 224.156 5 0 -9 -4 1153.18 264.250 4 0 9 -4 1134.03 299.805 7 0 9 -4 1166.34 328.541 2 0 -9 -4 1230.80 323.641 5 0 9 -4 1042.81 172.429 3 0 9 4 560.515 178.287 10 0 9 -4 1614.59 377.297 9 0 -9 4 1257.00 343.000 1 0 -9 4 1531.94 290.547 6 0 9 4 1029.22 168.863 1 0 -9 4 1279.21 282.370 8 0 -9 5 9862.04 1031.89 1 0 -9 -5 9425.40 806.531 4 0 -9 5 9331.98 587.287 5 0 9 -5 9419.50 965.759 7 0 9 -5 8874.59 935.976 2 0 9 -5 8925.12 478.926 3 0 9 -5 9330.91 958.701 9 0 -9 -5 7893.47 862.809 5 0 9 5 9436.39 720.298 4 0 9 5 8192.34 857.256 10 0 -9 6 908.557 177.107 5 0 9 6 1192.42 274.034 4 0 9 6 1409.35 413.427 10 0 -9 -6 1367.28 405.604 2 0 9 -6 1249.49 417.520 9 0 -9 6 976.993 361.472 4 0 9 6 1151.88 222.754 1 0 -9 -6 1793.09 444.543 5 0 -9 6 1463.87 479.584 1 0 9 -6 1083.49 366.334 7 0 9 -6 1324.76 425.856 2 0 -9 -7 48257.3 2529.52 5 0 9 7 49889.3 2058.53 4 0 -9 7 46866.0 2601.89 4 0 -9 7 51763.8 1569.56 5 0 -9 -7 47364.9 2649.27 2 0 9 7 47378.4 1840.15 1 0 9 -7 43971.4 2637.72 9 0 9 -7 47393.2 2724.17 7 0 9 -7 45657.9 2686.91 2 0 -9 7 49454.5 2797.00 1 0 9 7 50839.4 2587.57 10 0 -9 8 189.706 182.901 4 0 9 8 84.1302 116.499 1 0 -9 -8 303.176 247.753 2 0 -9 -8 333.744 233.252 5 0 9 -8 142.618 191.288 9 0 9 -8 130.963 169.933 2 0 9 -8 667.974 301.037 7 0 9 8 40.3319 83.3370 4 0 -9 8-44.7233 242.462 1 0 9 -9 6392.96 1063.76 2 0 9 -9 4929.12 914.851 7 0 -9 9 6471.51 983.180 4 0 -9 -9 5882.08 1006.82 2 0 -9 9 6149.00 1054.27 1 0 9 -9 6809.54 1073.14 9 0 -9 -9 6579.37 928.915 5 0 -9 10 487.475 280.772 4 0 -9 -10 193.598 231.070 5 0 9 -10 471.027 352.985 9 0 -9 -10 19.2664 319.419 2 0 9 -10-39.5513 225.893 7 0 9 -10-56.8826 179.963 2 0 -9 10 72.4028 178.921 1 0 -9 11 4322.20 962.444 1 0 9 -11 3348.44 866.474 2 0 -9 -11 4777.40 844.827 5 0 9 -11 4398.39 965.117 7 0 9 -11 4416.71 963.448 9 0 9 11 3770.26 851.755 10 0 -9 -11 4987.35 1052.58 2 0 -9 11 4624.08 921.051 4 0 10 0 1033.16 242.746 1 0 10 0 1012.90 248.253 10 0 -10 0 769.291 248.995 1 0 -10 0 892.652 247.416 5 0 10 -1 54099.3 1573.61 6 0 10 -1 54388.3 2181.25 10 0 -10 1 53206.1 2147.81 5 0 10 1 57987.7 1527.58 8 0 10 -1 57798.9 2111.52 3 0 10 1 54436.1 2167.17 10 0 10 1 61674.2 2104.22 1 0 -10 -1 52999.6 2265.17 5 0 -10 -1 55355.9 1981.62 1 0 -10 1 50426.7 2276.18 1 0 10 2 27656.0 1460.06 10 0 10 2 29816.3 1293.60 1 0 -10 2 29764.1 1672.86 1 0 -10 -2 29595.4 1608.33 5 0 10 -2 29407.7 1304.70 3 0 -10 2 28973.9 1105.92 8 0 -10 2 30258.1 1417.75 5 0 -10 2 29228.9 1039.96 6 0 10 2 28990.6 1131.17 8 0 10 -2 28425.6 1483.86 10 0 10 -3 7330.31 548.078 3 0 -10 -3 7713.55 799.908 5 0 -10 3 7297.16 606.157 5 0 10 3 6765.53 517.475 1 0 10 3 7291.93 594.405 8 0 10 -3 7415.77 734.132 10 0 -10 3 7042.03 517.377 6 0 -10 3 8071.95 873.547 1 0 10 3 6857.62 697.892 10 0 10 -3 7679.69 804.842 7 0 -10 3 8381.69 619.151 8 0 -10 4 42440.6 1772.49 6 0 10 -4 36727.1 2043.12 2 0 10 -4 41173.1 2151.38 7 0 10 4 42051.9 2054.61 10 0 -10 4 43025.0 1678.72 5 0 -10 4 46014.6 2342.98 1 0 -10 4 49662.3 1987.14 8 0 10 4 45364.4 1534.54 1 0 -10 -4 41113.2 2143.94 5 0 10 -4 45851.2 2245.05 9 0 10 -4 43772.5 1532.90 3 0 10 -5 2641.16 533.877 2 0 10 5 1932.04 419.141 10 0 10 -5 3254.09 569.018 7 0 10 -5 2287.44 245.485 3 0 -10 5 2280.59 297.011 5 0 -10 -5 1436.77 354.410 5 0 10 -5 2082.64 475.593 9 0 10 5 2129.59 262.132 1 0 -10 5 2526.67 516.956 1 0 10 -6 42523.7 2399.56 9 0 -10 6 43152.0 2516.60 1 0 10 6 40184.4 1536.46 1 0 10 -6 40858.3 2379.21 7 0 10 6 41623.0 2251.55 10 0 -10 -6 43592.1 2333.60 5 0 10 -6 40209.8 2336.41 2 0 -10 6 38764.1 2288.74 4 0 -10 6 42241.9 1510.93 5 0 -10 -7 841.453 385.551 5 0 -10 7 464.923 298.186 4 0 10 -7 663.121 399.644 7 0 -10 7 1156.75 488.410 1 0 10 -7 436.370 300.083 2 0 10 7 163.821 105.830 4 0 -10 7 141.463 61.8948 5 0 10 -7 764.908 337.100 9 0 -10 -7 318.668 276.186 2 0 10 7 458.087 166.334 1 0 10 7 289.511 273.162 10 0 -10 8 8641.27 1110.61 4 0 10 -8 9452.43 1226.02 9 0 10 -8 7867.49 1120.92 7 0 -10 8 7622.05 1119.54 1 0 10 -8 8679.82 1177.64 2 0 10 8 9029.08 1071.25 10 0 -10 -8 7572.10 1057.03 2 0 -10 -8 11042.9 1190.85 5 0 10 8 5343.05 611.144 4 0 -10 -9-296.211 368.028 2 0 -10 -9 163.112 178.594 5 0 10 -9 651.053 368.504 2 0 10 9 470.546 190.481 10 0 -10 9 244.881 155.882 4 0 10 -9-139.362 200.435 9 0 -10 9 128.889 325.563 1 0 10 -9 11.7435 224.851 7 0 -10 -10 12808.6 1580.21 2 0 10 -10 14697.7 1700.30 7 0 -10 10 11025.1 1385.42 4 0 -10 10 15353.9 1775.35 1 0 -10 -10 15028.2 1489.33 5 0 10 10 11483.2 1389.92 10 0 10 -10 14132.0 1696.16 2 0 10 -10 13552.5 1628.34 9 0 -10 -11 271.434 255.816 5 0 10 -11 151.675 280.540 2 0 -10 11 588.853 379.934 4 0 10 11 358.776 267.279 10 0 10 -11 37.1397 243.977 7 0 10 -11 249.464 239.302 9 0 -10 11 632.703 476.712 1 0 -10 -11 250.113 340.401 2 0 -11 0 278.996 152.411 1 0 11 0 229.400 134.246 10 0 11 0 226.712 70.8244 6 0 11 0 36.8290 57.4775 1 0 -11 -1 2319.12 346.184 1 0 11 1 2048.59 361.384 10 0 11 1 1937.27 324.676 1 0 -11 -1 1545.36 354.598 5 0 11 -1 1774.18 346.159 10 0 -11 1 2063.19 360.163 5 0 11 -1 2043.90 183.873 6 0 -11 1 1218.40 349.431 1 0 11 2 355.020 148.997 1 0 11 -2 332.737 189.934 10 0 -11 2 558.178 202.127 5 0 11 2 634.063 239.781 10 0 -11 2 11.8273 154.322 1 0 -11 2 646.142 128.680 8 0 -11 -2 193.396 100.593 1 0 11 -2 292.428 205.559 3 0 -11 -2 392.587 227.848 5 0 11 2 331.426 94.8534 8 0 11 -3 61279.5 2614.78 7 0 -11 -3 52158.5 2507.03 5 0 11 3 61921.1 2128.32 8 0 11 -3 60535.4 2095.66 3 0 -11 3 58285.1 2203.16 5 0 -11 3 60003.8 2746.31 1 0 11 3 57695.7 2442.77 10 0 -11 3 58818.3 1928.70 6 0 -11 3 56055.7 2043.71 8 0 11 -3 59906.9 2511.00 10 0 11 3 55970.6 2023.11 1 0 -11 4 15685.3 932.386 6 0 11 -4 15311.9 1249.17 7 0 11 4 15023.2 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650.721 10 -1 12 -9 3056.24 726.297 9 1 -12 9 1755.81 529.542 4 1 -12 9 2039.41 649.630 1 -1 12 -9 1959.49 616.760 7 -1 -12 -9 2633.14 628.580 5 1 12 10 414.178 295.928 10 -1 12 -10 7.32895 155.744 9 -1 -12 -10 209.565 250.270 5 -1 12 -10 211.775 201.980 7 1 -12 10-231.667 233.389 4 -1 12 -10 156.221 291.083 2 1 -12 10 934.400 512.379 1 1 -13 -11 131.249 189.539 5 -1 13 11 272.533 248.217 10 1 13 -11 261.149 234.097 9 -1 -13 11 289.402 288.570 4 -1 -13 11 591.226 424.984 1 1 13 -11 50.3671 168.851 2 -1 13 10 4415.13 903.108 10 1 13 -10 4236.42 910.597 2 1 13 -10 5414.88 1023.10 7 1 -13 -10 4652.28 905.708 5 -1 -13 10 4190.24 1016.43 1 1 13 -10 2971.56 831.130 9 -1 -13 10 3742.72 845.488 4 1 -13 -9 1338.89 475.612 5 1 13 -9 1180.30 455.231 7 -1 -13 9 1894.71 594.885 4 -1 13 9 1292.36 496.589 10 1 13 -9 1496.32 558.009 9 -1 -13 9 742.806 382.173 1 1 13 -9 1619.29 588.886 2 1 13 -8 3257.58 740.993 2 -1 13 8 3554.84 709.266 10 1 -13 -8 3534.47 715.950 5 -1 -13 8 2684.67 735.534 1 1 13 -8 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653.671 155.559 8 -2 3 0 1035.22 182.816 4 2 -3 0 813.695 169.965 4 2 3 0 1072.84 173.718 4 2 3 0 1035.93 165.891 10 -2 -3 0 1407.73 201.760 4 -2 -3 0 1228.52 180.258 10 -2 3 0 850.040 186.519 6 -2 -3 0 1282.67 178.501 6 -2 -3 0 1407.21 232.555 5 -2 3 0 978.633 112.396 10 -2 3 0 778.787 170.075 8 -2 3 -1 20613.6 1047.31 7 2 3 1 22254.4 985.904 6 -2 -3 -1 21755.2 768.984 4 -2 3 -1 23034.8 837.788 2 -2 3 -1 23142.6 1059.13 3 2 -3 1 23996.3 1071.42 6 2 3 1 23623.9 1079.34 8 -2 -3 -1 23116.0 912.692 10 2 3 1 22349.9 895.920 10 2 -3 1 22935.6 1040.14 8 2 -3 1 22625.3 965.143 4 2 -3 1 22178.8 1045.49 3 -2 3 -1 21162.6 1028.73 8 2 -3 1 21826.6 833.326 2 -2 -3 -1 20872.3 1050.84 8 2 -3 1 22685.1 1066.12 7 -2 3 -1 21067.8 1034.41 6 -2 -3 -1 20565.2 993.339 6 -2 -3 -1 21933.4 1102.97 5 2 3 1 23768.4 1119.71 5 -2 -3 -2 1996.52 326.636 5 -2 3 -2 2217.43 345.762 8 2 3 2 1975.10 325.414 5 2 3 2 1311.99 253.076 2 -2 3 -2 2067.01 343.511 7 2 -3 2 1691.21 160.973 10 -2 -3 -2 2081.54 348.702 8 2 -3 2 1979.50 270.830 2 2 -3 2 1869.06 303.119 8 2 3 2 1963.30 317.902 8 -2 3 -2 1710.68 203.692 9 2 -3 2 2067.34 317.964 6 2 -3 2 1680.28 300.915 7 2 3 2 2224.50 317.642 6 2 3 2 1973.08 244.236 10 2 -3 2 2079.42 301.316 3 -2 3 -2 1839.37 267.025 2 -2 3 -2 1477.79 274.196 6 -2 -3 -2 1881.86 318.945 6 -2 3 -2 1702.91 262.858 3 2 3 3 63011.7 2224.93 9 2 3 3 60066.9 2080.78 10 2 -3 3 65799.7 2329.04 2 -2 -3 -3 64989.7 2551.44 8 -2 3 -3 62259.9 2095.95 9 -2 3 -3 58299.3 2481.59 7 -2 3 -3 62450.6 2494.03 8 2 -3 3 68479.5 2594.66 1 -2 3 -3 57969.2 2257.53 2 -2 3 -3 66092.3 2526.06 6 -2 -3 -3 65340.4 2435.31 2 2 -3 3 63277.2 2211.22 3 -2 -3 -3 62295.0 2399.45 5 -2 3 -3 63921.5 2221.96 3 2 -3 4 1368.34 280.829 5 -2 3 -4 1747.07 409.778 6 2 -3 4 1167.53 301.898 1 2 3 4 1491.40 302.135 9 -2 3 -4 1773.03 306.928 9 2 -3 4 2205.03 326.403 9 -2 3 -4 1966.30 427.344 8 2 -3 4 1741.53 295.983 3 -2 3 -4 1332.27 364.223 7 -2 -3 -4 2296.95 471.033 8 -2 3 -4 1518.24 344.413 2 2 3 4 1656.74 290.310 10 -2 -3 -4 1628.34 335.967 5 -2 -3 -4 1105.94 311.458 2 2 3 5 13260.1 541.784 4 -2 -3 -5 17114.8 1271.08 2 -2 3 -5 15527.4 1196.24 2 -2 3 -5 14960.5 1040.92 9 -2 3 -5 14098.2 1246.03 8 -2 -3 -5 12962.1 1214.44 8 2 -3 5 14268.0 933.871 3 2 -3 5 15919.5 1033.16 9 -2 3 -5 16594.1 1329.33 7 2 -3 5 12766.5 1098.13 1 -2 -3 -5 15027.7 1113.21 5 -2 3 -6 1865.96 469.245 2 -2 -3 -6 1366.74 363.502 5 -2 -3 -6 1983.25 469.840 2 -2 3 -6 1043.75 306.851 9 2 -3 6 1868.67 365.944 4 -2 3 -6 2277.23 575.271 8 2 3 6 1644.10 440.528 1 -2 -3 -6 1596.65 507.130 8 -2 3 -6 1428.43 463.988 7 2 -3 6 1641.71 454.663 1 2 3 6 1082.54 161.980 4 2 -3 6 1653.78 330.570 3 2 3 7 47343.8 1634.56 4 2 -3 7 46568.3 2138.51 4 -2 -3 -7 48929.5 2687.38 2 2 -3 7 44382.4 2485.15 1 2 3 7 46510.0 2369.35 1 -2 3 -7 50750.5 2827.37 7 -2 3 -7 49782.3 2458.91 9 2 -3 7 47992.0 2104.84 3 -2 3 -7 47602.7 2629.70 2 -2 -3 -7 48944.0 2399.07 5 2 -3 8 661.099 257.220 3 2 -3 8 130.173 192.812 1 2 3 8 290.753 214.698 1 -2 3 -8 220.018 182.584 2 -2 3 -8 160.911 165.721 9 2 -3 8 618.017 257.016 4 -2 -3 -8-29.8599 196.810 2 -2 -3 -8 348.739 212.963 5 2 -3 9 6815.02 800.642 4 -2 3 -9 9342.54 1240.70 2 -2 -3 -9 11165.5 1368.60 2 -2 -3 -9 9414.67 1052.75 5 2 -3 9 9512.77 1195.20 1 -2 3 -9 10191.4 1197.48 9 2 3 9 8234.75 1006.09 1 2 -3 9 6622.09 745.847 3 -2 3 -10 245.014 365.778 9 2 3 10 144.465 222.443 1 2 3 10 513.458 295.529 3 -2 -3 -10 744.693 487.226 2 2 -3 10 594.936 429.661 1 -2 3 -10 1254.25 527.703 2 -2 3 -11 7270.19 1108.06 9 2 -3 11 7566.57 1165.58 1 -2 -3 -11 5522.84 1099.71 2 -2 3 -11 6231.65 1155.50 2 2 3 11 4517.22 836.405 1 -2 -4 12 4147.50 934.989 4 2 4 -12 7482.81 1323.55 9 2 -4 -12 5804.44 1142.78 2 2 -4 -12 6895.68 1240.99 9 -2 -4 12 3449.61 843.568 1 2 4 -12 4559.79 1035.85 2 -2 4 11 2049.04 525.813 4 2 4 -11 2924.35 786.895 9 -2 -4 11 1854.34 571.574 1 -2 -4 11 2416.68 638.403 4 2 4 -11 2684.80 741.733 2 2 -4 -11 2907.69 749.474 2 2 -4 -11 3941.67 910.666 9 -2 -4 10 14258.7 1517.90 1 -2 -4 10 13879.4 1473.22 4 2 -4 -10 15470.9 1630.77 2 -2 4 10 13852.2 1346.09 4 2 4 -10 13545.0 1586.17 2 2 4 -10 17381.1 1808.44 9 2 -4 -10 15487.5 1679.10 9 2 -4 -10 12548.9 1059.05 5 -2 -4 9 4689.59 828.278 4 2 4 -9 5406.85 942.196 2 2 -4 -9 4073.48 771.228 2 -2 4 9 5858.82 818.528 4 2 -4 -9 4099.32 820.462 9 2 4 -9 4201.05 810.538 9 -2 4 9 3777.96 564.079 1 -2 -4 9 4195.93 787.463 1 2 -4 -9 4716.07 605.395 5 -2 4 8 15680.1 1085.37 1 2 -4 -8 17621.4 1535.39 2 -2 4 8 15483.1 1304.00 4 -2 -4 8 17026.8 1496.73 4 2 4 -8 16232.8 1527.29 2 2 4 -8 16715.7 1587.47 9 2 -4 -8 19985.8 1691.12 9 -2 -4 8 17885.8 1534.28 1 2 -4 -8 17406.4 1164.90 5 2 -4 -7 8986.79 1005.36 2 2 -4 -7 8147.31 1006.25 9 -2 4 7 7083.31 826.126 4 -2 4 7 7253.98 639.699 1 2 4 -7 6333.05 889.056 2 2 4 -7 9079.35 927.686 7 -2 -4 7 6857.17 869.978 1 2 4 -7 9262.11 1108.84 9 2 -4 -7 6708.75 688.059 5 -2 -4 7 8653.59 987.496 4 2 -4 -6 51058.0 2605.51 9 -2 -4 6 53581.8 2585.30 4 2 4 -6 51914.4 2603.34 2 -2 4 6 56457.4 1928.51 1 -2 -4 6 48232.5 2484.22 1 -2 4 6 54234.6 2424.82 4 2 4 -6 52414.6 2686.64 9 2 4 -6 54964.0 2380.06 7 2 -4 -6 52741.7 2499.37 2 2 -4 -6 56422.5 2218.06 5 2 -4 -6 59681.5 1926.40 1 2 4 -5 1949.34 338.466 7 2 4 -5 2178.42 455.913 9 -2 -4 5 1830.85 411.278 4 2 4 -5 1873.10 417.304 2 -2 4 5 2322.95 427.946 4 -2 4 5 2247.50 245.979 1 -2 -4 5 1851.93 330.673 7 -2 -4 5 2066.15 426.075 1 2 -4 -5 1810.13 397.568 9 2 -4 -5 1215.02 314.575 2 2 -4 -5 2267.49 370.679 5 2 -4 -5 2055.96 229.753 1 2 4 -4 149413. 4794.00 2 -2 4 4 154383. 3874.36 1 -2 -4 4 156446. 4357.79 7 2 -4 -4 153979. 4842.12 9 2 -4 -4 165166. 4664.33 2 2 -4 -4 154483. 3908.95 1 -2 -4 4 160253. 4895.54 4 2 4 -4 156423. 4911.06 9 2 4 -4 158740. 4421.68 7 -2 -4 4 166418. 4853.25 1 -2 4 4 168974. 4557.74 3 2 4 -4 137391. 3771.31 3 -2 4 4 162178. 4648.16 2 -2 4 4 152111. 4656.31 4 2 -4 -4 158343. 4504.51 5 -2 -4 3 2499.78 394.538 1 2 4 -3 1676.02 319.503 9 2 -4 -3 1883.30 307.887 5 2 -4 -3 1719.39 315.930 9 2 4 -3 1985.42 189.842 5 -2 4 3 1519.39 304.183 9 -2 -4 3 1613.51 328.378 4 -2 4 3 2149.91 317.727 3 -2 4 3 1983.73 320.947 4 -2 -4 3 2122.37 345.554 10 2 4 -3 1875.36 251.316 7 2 4 -3 1514.79 317.889 1 2 4 -3 2305.65 380.746 4 2 4 -3 1527.76 170.736 3 2 -4 -3 1474.80 250.495 2 2 -4 -3 1238.56 271.132 4 2 -4 -3 1793.90 171.675 1 -2 4 3 2096.56 297.382 2 2 -4 -3 1793.26 300.579 3 2 4 -2 14484.7 888.964 9 -2 -4 2 14509.6 842.974 10 2 -4 -2 13431.5 651.346 2 -2 -4 2 13184.9 849.378 1 -2 4 2 13245.0 837.100 4 -2 4 2 14230.7 859.162 9 2 4 -2 14819.6 907.011 1 2 4 -2 14500.0 884.522 4 -2 4 2 13847.7 674.100 2 -2 4 2 14548.2 843.520 3 2 -4 -2 12795.1 804.691 3 -2 -4 2 13086.7 870.710 4 -2 -4 2 14659.6 681.389 5 2 4 -2 14176.1 668.591 3 2 -4 -2 13830.8 872.663 4 2 4 -2 13062.7 655.029 5 -2 4 1 76235.2 2469.05 3 2 4 -1 79899.6 2456.37 4 -2 4 1 75656.3 2346.77 9 -2 -4 1 78055.8 2384.62 10 2 -4 -1 76677.9 2488.25 4 2 -4 -1 74463.7 2467.23 3 -2 -4 1 73099.3 2462.83 1 -2 -4 1 74852.5 2453.06 4 2 4 -1 73580.2 2397.60 10 -2 4 1 75587.6 2438.06 4 2 4 -1 79403.1 2506.19 1 2 4 -1 74512.3 2328.27 5 -2 -4 1 75463.2 2350.03 5 2 4 0 37799.1 1396.72 10 -2 4 0 38028.0 1164.17 10 -2 -4 0 37365.4 1363.23 10 -2 -4 0 35648.6 1270.81 6 -2 -4 0 38328.1 1370.11 4 -2 -4 0 37776.3 1428.22 8 -2 4 0 39482.3 1518.10 3 2 4 0 37590.3 1290.68 6 -2 4 0 38206.7 1454.81 6 -2 4 0 37713.0 1379.04 8 2 -4 0 37515.6 1491.14 3 2 -4 0 38888.7 1471.76 4 2 4 0 39967.4 1513.13 5 -2 -4 0 39346.1 1519.61 5 -2 4 0 37234.2 1432.96 4 -2 4 -1 13415.8 532.262 10 2 -4 1 15326.8 639.377 2 2 -4 1 16172.6 818.396 8 -2 -4 -1 14982.7 846.499 8 -2 -4 -1 14212.4 613.786 4 2 -4 1 12898.2 768.258 6 2 4 1 14383.1 732.701 10 2 -4 1 14209.1 523.878 10 2 4 1 14977.6 886.984 5 -2 4 -1 14867.7 831.873 6 -2 4 -1 13878.9 620.790 2 2 4 1 13637.7 793.356 8 -2 -4 -1 14103.2 870.186 5 -2 -4 -1 14191.9 732.593 10 -2 4 -1 12489.7 813.445 7 2 4 1 14474.5 747.289 6 -2 -4 -1 14471.9 782.950 6 2 -4 1 13444.2 798.084 3 -2 4 -1 13350.9 772.969 8 2 -4 1 15491.7 804.397 4 -2 4 -1 14875.4 836.544 3 2 -4 2 70844.8 2504.45 1 -2 -4 -2 61489.5 2326.80 5 -2 -4 -2 60180.1 2297.10 8 2 -4 2 62840.6 2166.75 3 -2 4 -2 61579.3 1934.51 9 2 -4 2 64083.6 2085.04 2 -2 4 -2 60233.6 2270.78 6 2 -4 2 63709.1 2246.39 8 -2 4 -2 60579.3 2261.51 8 -2 4 -2 57754.9 2050.65 2 2 4 2 61415.6 2041.12 10 2 4 2 77771.3 2491.16 5 2 4 2 63971.7 2278.05 8 2 -4 2 62791.7 1771.67 10 2 -4 2 67313.1 2386.45 7 -2 4 -2 60602.7 2355.80 7 -2 -4 -2 63092.5 2105.36 10 2 4 2 65409.4 2229.91 6 -2 -4 -2 62701.7 2285.83 6 2 4 2 61771.8 2274.95 2 -2 4 -2 65397.3 2194.76 3 2 -4 2 63434.9 2237.97 6 -2 4 -3 19653.4 995.697 9 2 4 3 19099.0 1001.60 10 2 4 3 18970.3 1072.77 9 2 -4 3 20169.4 1249.04 1 -2 4 -3 19446.4 1093.71 2 2 -4 3 17751.1 1047.02 2 -2 4 -3 18409.5 1227.24 7 -2 4 -3 20510.6 1243.54 6 -2 -4 -3 19182.9 1235.38 8 -2 4 -3 18842.8 1206.12 8 2 -4 3 19480.9 1029.37 3 -2 -4 -3 20410.8 1204.75 5 -2 4 -3 20619.0 1051.84 3 2 -4 3 20138.2 857.681 10 -2 -4 -4 68092.4 2890.31 8 2 -4 4 63197.0 2728.52 1 -2 4 -4 66255.6 2463.20 9 -2 -4 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-4 -7 3261.48 649.042 2 -2 4 -7 3667.45 758.665 7 2 -4 7 3325.54 641.399 1 -2 4 -8 13021.8 1272.58 9 -2 4 -8 12825.9 1459.68 7 -2 4 -8 10879.8 1266.06 2 -2 -4 -8 12873.7 1383.93 2 2 -4 8 10662.2 893.448 3 2 -4 8 11232.6 1041.28 4 2 -4 8 11289.4 1244.28 1 -2 -4 -8 11539.1 1141.31 5 2 4 8 11828.7 1138.89 1 -2 -4 -9 230.453 181.425 5 2 -4 9 270.301 201.212 4 2 4 9 171.005 205.668 1 -2 -4 -9 731.823 411.338 2 -2 4 -9-91.1746 182.210 9 -2 4 -9 253.647 282.947 2 2 -4 9 897.137 455.619 1 -2 -4 -10 10041.0 1149.73 5 -2 4 -10 13568.9 1599.28 2 -2 4 -10 11074.1 1341.49 9 -2 -4 -10 10970.6 1456.20 2 2 4 10 10572.6 1184.37 1 2 -4 10 10875.5 1372.07 1 -2 -4 -11 422.635 391.408 2 -2 4 -11 184.975 159.456 9 2 -4 11 1008.85 539.171 1 -2 4 -11 191.030 210.383 2 2 4 11 116.145 154.557 1 2 5 -12 219.936 409.873 9 -2 -5 12 743.074 449.538 1 2 -5 -12 762.781 484.719 9 -2 -5 12 441.920 377.625 4 2 -5 -12 375.657 358.082 2 2 5 -12 328.123 395.675 2 2 5 -11 6117.48 1127.29 9 -2 -5 11 4236.03 900.690 1 2 -5 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2833.73 1 2 -5 -7 67899.4 3183.15 9 2 -5 -7 62316.1 2533.42 5 -2 5 6 7963.31 504.871 1 2 -5 -6 6855.15 797.752 2 2 -5 -6 6710.44 851.718 9 2 -5 -6 6610.78 679.905 5 2 5 -6 8343.24 979.171 9 -2 -5 6 5832.78 789.591 1 2 5 -6 6766.82 852.229 2 2 5 -6 6027.45 707.559 7 -2 5 6 6719.46 744.914 4 -2 -5 6 6937.27 861.604 4 2 -5 -5 141202. 4671.62 9 -2 -5 5 135143. 4620.30 4 2 -5 -5 133344. 4364.58 2 -2 5 5 142485. 3449.07 1 2 5 -5 141921. 4638.14 2 -2 5 5 134102. 4328.12 4 -2 -5 5 129501. 4554.38 1 -2 -5 5 149874. 4222.82 7 2 5 -5 144967. 4303.58 7 2 5 -5 139903. 4754.86 9 2 -5 -5 148216. 4294.32 5 2 -5 -4 443.411 205.720 5 2 -5 -4 604.960 249.582 9 2 5 -4 292.136 133.426 7 -2 -5 4 779.250 292.270 1 2 5 -4 210.349 51.3024 3 -2 -5 4 550.002 258.323 4 2 -5 -4 490.558 204.673 2 -2 5 4 538.797 231.607 4 2 5 -4 186.435 171.302 9 -2 5 4 425.978 174.657 2 -2 5 3 131793. 3931.49 2 2 -5 -3 133819. 3890.53 2 -2 5 3 129332. 4094.93 4 2 -5 -3 133882. 4079.87 3 -2 5 3 139050. 4275.38 9 -2 5 3 142370. 4123.60 3 2 -5 -3 142769. 4273.76 4 2 5 -3 130191. 4259.79 9 -2 -5 3 141125. 4289.05 1 -2 -5 3 135273. 4305.54 4 2 5 -3 133525. 3530.76 3 2 5 -3 136083. 4332.98 1 2 5 -3 134935. 3808.75 7 -2 -5 3 138003. 3548.95 5 2 -5 -3 135487. 4114.47 5 2 5 -3 138155. 3540.29 5 -2 -5 2 2251.60 318.874 10 -2 5 2 2193.90 332.535 3 2 -5 -2 1919.03 223.901 2 -2 5 2 1964.11 320.181 9 -2 5 2 2259.68 256.128 2 -2 -5 2 2375.83 362.032 1 2 5 -2 2017.48 336.448 1 -2 5 2 1685.49 295.226 4 -2 -5 2 1890.20 328.933 4 2 5 -2 1747.68 304.806 10 -2 -5 2 2016.34 241.552 5 2 5 -2 2309.12 257.356 5 2 -5 -2 2451.12 349.317 4 2 -5 -2 2242.09 331.670 3 -2 5 1 302516. 7483.81 2 2 5 -1 309762. 8039.59 10 2 5 -1 322168. 7929.38 5 2 -5 -1 325920. 8147.10 4 2 5 -1 318984. 8144.38 1 -2 -5 1 296349. 8075.58 1 -2 5 1 314451. 8048.42 4 -2 5 1 315336. 8108.13 3 -2 -5 1 311078. 8072.89 4 2 -5 -1 311897. 8112.13 3 -2 -5 1 320866. 7998.24 10 -2 -5 1 310346. 7925.47 5 -2 5 1 289379. 7778.53 10 2 5 0 117993. 2918.57 5 -2 5 0 109487. 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280.542 2 -2 5 -8 1156.22 466.926 2 2 5 8 1132.91 351.062 1 2 -5 8 281.910 327.685 1 -2 5 -9 6902.53 991.909 9 -2 -5 -9 8089.61 1170.70 2 2 -5 9 4669.62 751.749 4 2 -5 9 7454.46 1080.35 1 2 5 9 6937.44 893.800 1 -2 -5 -9 6433.85 903.615 5 -2 5 -10 204.797 206.175 9 2 -5 10 831.110 413.245 1 2 5 10 796.249 338.258 1 -2 -5 -10 1021.63 469.480 2 -2 5 -10 918.571 451.450 2 -2 -5 -10 814.918 383.047 5 2 5 11 4667.38 828.742 10 -2 5 -11 4762.48 1015.27 2 -2 -5 -11 4748.27 1012.85 2 -2 5 -11 5622.01 996.754 9 2 -5 11 5962.51 1075.82 1 2 -6 -12 4665.77 1058.99 2 2 6 -12 5353.46 1124.86 9 -2 -6 12 5532.12 1050.36 4 -2 -6 12 4564.28 990.737 1 2 6 -12 3917.20 969.570 2 2 -6 -11 415.642 340.883 9 -2 6 11 968.382 366.163 4 -2 -6 11 662.068 375.591 1 -2 -6 11 557.240 381.626 4 2 -6 -11 480.772 346.794 2 2 6 -11-194.387 230.158 9 2 6 -11 772.578 357.431 2 2 -6 -10 13640.6 1533.04 2 2 6 -10 11590.6 1499.53 9 2 -6 -10 14751.5 1658.76 9 -2 -6 10 8914.80 1274.95 1 2 6 -10 12758.1 1537.05 2 -2 -6 10 9560.64 1264.46 4 -2 6 10 10436.8 1140.58 4 2 -6 -10 14156.0 1191.32 5 -2 6 9 2120.36 467.493 4 -2 -6 9 3312.13 715.355 4 2 -6 -9 2270.76 624.056 2 2 -6 -9 3086.32 546.105 5 -2 -6 9 2796.51 653.666 1 2 6 -9 1850.35 578.713 9 2 -6 -9 2323.12 672.263 9 2 6 -9 3090.38 706.163 2 -2 6 8 38232.9 2148.96 4 2 -6 -8 45228.3 2709.21 9 2 6 -8 41066.7 2649.56 9 -2 6 8 42278.3 1669.19 1 -2 -6 8 41958.0 2524.87 4 -2 -6 8 37060.4 2459.23 1 2 6 -8 43218.2 2626.53 2 2 6 -8 43082.4 2384.96 7 2 -6 -8 40059.5 2423.31 2 2 -6 -8 41215.9 2107.24 5 2 6 -7 3676.77 681.905 2 -2 6 7 2534.02 501.637 4 2 -6 -7 2554.37 562.148 9 2 6 -7 2454.08 588.007 9 -2 6 7 3002.05 321.749 1 -2 -6 7 2946.13 617.387 1 2 -6 -7 2733.48 489.242 5 -2 -6 7 3068.34 631.139 4 2 6 -7 2871.86 536.978 7 2 -6 -7 2390.58 519.779 2 -2 -6 6 24323.9 1701.22 4 2 -6 -6 25263.6 1597.27 2 2 -6 -6 26939.0 1804.23 9 2 6 -6 27117.6 1841.88 9 -2 6 6 25965.2 923.189 1 -2 -6 6 20758.2 1607.25 1 2 6 -6 25831.8 1746.76 2 2 6 -6 25927.9 1559.11 7 -2 6 6 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112622. 3464.55 10 -2 -6 2 109910. 3578.98 4 -2 6 2 108672. 3131.16 2 -2 6 2 116043. 3539.69 3 2 -6 -2 104318. 3469.63 3 -2 -6 2 109015. 3568.71 1 -2 -6 2 108149. 3167.06 5 2 -6 -2 116527. 2944.50 1 2 6 -2 113136. 3169.74 5 -2 -6 1 10399.6 747.862 4 -2 6 1 12288.8 811.766 3 -2 6 1 10529.0 738.983 4 -2 -6 1 10443.7 768.289 1 -2 6 1 10981.0 651.981 10 -2 6 1 10580.3 494.757 2 2 -6 -1 10882.9 771.580 3 2 6 -1 10267.4 726.887 10 2 6 -1 11767.0 815.749 1 -2 -6 1 11526.1 743.784 10 -2 -6 1 10633.5 494.918 6 2 -6 -1 12226.4 812.175 4 -2 -6 1 10568.0 694.507 5 2 6 -1 10944.2 697.483 5 2 -6 -1 10536.5 619.364 1 -2 -6 0 175237. 4597.66 8 2 6 0 164905. 4691.27 10 2 -6 0 176084. 4798.93 4 2 -6 0 171501. 4449.65 10 -2 6 0 161928. 4391.30 10 -2 -6 0 169358. 4798.66 5 -2 6 0 161378. 4455.96 8 -2 6 0 160927. 4607.89 6 -2 -6 0 161946. 4333.29 6 -2 6 0 173252. 4805.46 3 -2 -6 0 173009. 4687.05 10 2 6 0 164663. 4309.82 6 2 -6 0 168094. 4793.63 3 2 6 0 171911. 4798.90 5 2 -6 0 175478. 4711.33 1 2 6 0 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3291.92 693.579 5 -2 -6 -10 4776.43 991.954 2 -2 -6 -11 622.458 361.232 5 2 6 11 125.621 152.346 10 -2 6 -11 503.462 402.427 9 -2 -6 -11 460.680 359.625 2 -2 6 -11 759.813 443.879 2 2 -6 11 968.188 476.937 1 2 7 -12 92.6469 229.344 9 -2 -7 12 270.056 341.245 1 -2 -7 12 110.738 301.425 4 2 7 -12 350.741 374.103 2 2 -7 -12 942.911 620.926 2 -2 7 11 1489.06 442.806 4 2 7 -11 1595.45 616.335 9 2 -7 -11 1501.12 439.723 5 -2 -7 11 2258.74 682.266 1 2 -7 -11 1304.31 487.889 2 2 7 -11 2332.53 696.437 2 -2 -7 11 1256.75 496.568 4 -2 7 10 2571.00 543.195 4 -2 -7 10 973.849 476.429 4 -2 -7 10 1723.08 628.966 1 2 -7 -10 2369.18 622.773 2 2 7 -10 1214.47 505.206 9 2 7 -10 3048.64 755.152 2 2 -7 -10 2698.99 549.890 5 2 7 -9 14725.2 1609.35 9 -2 7 9 13435.0 1250.74 4 2 7 -9 14097.8 1418.77 7 2 -7 -9 16076.1 1552.65 2 2 7 -9 14907.4 1604.77 2 -2 -7 9 12261.5 1449.03 1 2 -7 -9 15305.3 1272.03 5 -2 -7 9 14123.3 1500.44 4 2 7 -8 1573.74 482.348 2 2 7 -8 1061.92 439.212 9 -2 7 8 2707.75 307.711 1 2 -7 -8 2269.44 483.944 5 -2 7 8 2683.34 528.093 4 2 7 -8 2223.66 526.990 7 -2 -7 8 1876.85 571.984 1 -2 -7 8 2342.51 604.603 4 2 -7 -8 2655.47 585.818 2 2 7 -7 44500.4 2637.89 9 -2 -7 7 46727.8 2592.94 4 -2 7 7 44304.3 1394.27 1 2 -7 -7 44841.7 2402.08 2 -2 -7 7 40613.6 2487.25 1 2 7 -7 47308.5 2627.73 2 2 7 -7 41215.6 2260.85 7 -2 7 7 43363.7 2204.79 4 2 -7 -7 47365.8 2263.90 5 2 -7 -6 2676.67 474.779 5 -2 -7 6 2271.13 511.883 1 2 -7 -6 2848.36 502.194 2 -2 7 6 1842.58 390.815 4 -2 -7 6 2465.91 530.601 4 2 7 -6 2641.36 547.794 2 2 7 -6 1595.73 371.807 7 2 7 -6 1701.60 453.939 9 -2 -7 5 62511.3 2894.14 4 2 7 -5 64952.7 2959.16 9 -2 -7 5 60932.9 2879.31 1 -2 7 5 63992.9 2628.62 4 2 -7 -5 66618.0 2656.20 2 2 7 -5 71896.8 2667.07 7 2 7 -5 65209.9 2905.86 2 2 -7 -5 68939.2 2717.16 5 -2 -7 4 354.749 93.1271 5 -2 7 4 329.223 179.241 2 2 7 -4 267.264 72.4396 3 2 -7 -4 362.718 168.332 5 2 7 -4 372.538 192.301 9 -2 7 4 381.292 202.906 4 -2 -7 4 619.368 287.133 1 2 7 -4 377.250 173.926 7 2 7 -4 456.471 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421.057 1 -2 -7 -10 124.761 173.686 5 -2 7 -10-20.6297 217.475 9 -2 -7 -10 1026.10 498.411 2 2 7 10 14.8025 118.389 10 -2 7 -10 632.729 531.254 7 2 -7 10 278.853 390.173 1 -2 7 -10 24.4752 236.496 2 -2 -7 -11 2165.89 599.752 5 2 7 11 2148.31 588.147 10 -2 7 -11 2693.02 797.763 2 -2 -7 -11 1318.79 554.500 2 2 -7 11 1307.36 584.749 1 -2 7 -11 2350.36 650.223 9 2 8 -12 16543.8 1995.93 9 -2 -8 12 11850.9 1713.03 1 2 -8 -12 17020.3 1923.42 2 -2 -8 12 10971.2 1516.44 4 2 8 -12 11212.4 1650.08 2 2 -8 -11 887.831 328.922 5 -2 8 11 937.659 355.169 4 -2 -8 11 395.390 276.934 1 2 8 -11 293.905 249.762 9 2 -8 -11 1316.31 558.424 2 -2 -8 11 318.600 282.930 4 2 8 -11 786.591 402.405 2 2 -8 -10 10497.2 1344.99 2 2 8 -10 10355.0 1439.28 2 -2 -8 10 8912.49 1340.11 1 2 8 -10 10203.4 1284.10 7 2 8 -10 10179.5 1417.80 9 -2 8 10 10204.3 1129.36 4 -2 -8 10 11807.5 1446.44 4 2 -8 -10 10750.0 1131.24 5 2 -8 -9 1384.37 416.790 5 2 8 -9 1488.28 536.331 2 -2 -8 9 591.298 406.818 1 2 8 -9 1967.53 655.590 9 2 -8 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131888. 4205.10 7 2 8 -4 143408. 3644.44 5 -2 -8 4 127622. 4621.36 1 -2 8 4 126990. 4272.54 4 -2 -8 4 137452. 3621.99 5 2 8 -4 136473. 3547.50 3 2 -8 -4 132401. 4445.76 5 -2 8 3 2631.97 367.199 2 2 -8 -3 1840.14 359.543 5 -2 8 3 2184.58 371.322 4 -2 -8 3 2123.02 361.302 1 -2 -8 3 2403.40 423.861 4 -2 8 3 2307.86 377.462 10 2 8 -3 2243.29 401.707 10 -2 -8 3 2279.33 288.224 5 2 8 -3 2399.13 280.450 5 2 8 -2 65769.1 2564.07 10 -2 -8 2 66960.1 2613.35 1 -2 8 2 65329.3 2372.51 10 -2 8 2 68081.7 2493.72 4 -2 8 2 68398.1 2189.79 2 2 -8 -2 62936.1 2519.74 3 2 8 -2 65960.8 2248.87 5 2 -8 -2 65091.9 2581.26 5 -2 -8 2 66422.5 2256.55 5 2 -8 -2 67358.8 1986.41 1 -2 -8 2 65664.7 2606.82 4 -2 -8 1 1115.82 273.340 1 2 -8 -1 648.985 233.280 5 2 -8 -1 845.833 182.914 1 2 8 -1 1109.60 245.623 5 2 8 -1 594.744 204.179 10 -2 8 1 573.727 174.277 10 -2 -8 1 691.744 95.9889 6 -2 -8 1 1236.79 261.576 5 2 -8 -1 909.200 244.135 3 2 8 0 149630. 4252.35 1 2 -8 0 136389. 4175.97 3 -2 8 0 134184. 3825.71 10 -2 -8 0 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45987.5 1674.56 5 -2 -9 3 48370.7 2258.14 1 -2 9 3 40966.1 1911.09 4 2 9 -3 42173.5 2064.39 10 -2 9 3 43786.0 1960.61 10 -2 9 3 44070.3 1825.51 2 2 9 -3 42187.5 1634.82 5 2 -9 -3 44351.8 2095.54 5 2 -9 -2 786.899 153.903 1 -2 -9 2 784.321 287.247 1 -2 -9 2 1028.90 226.876 5 2 9 -2 960.912 206.243 5 -2 9 2 846.605 188.759 2 -2 9 2 754.200 208.034 10 2 -9 -2 851.609 245.396 5 2 9 -2 738.305 223.252 10 2 -9 -1 125755. 4152.64 5 2 9 -1 119236. 3994.96 10 -2 9 1 125653. 3762.18 10 -2 -9 1 127500. 4068.57 1 2 -9 -1 126077. 3655.19 1 2 -9 -1 121712. 4028.40 3 -2 -9 1 124509. 3895.92 5 2 9 -1 130919. 3909.73 5 -2 -9 0 763.502 234.190 1 -2 -9 0 478.409 219.577 5 -2 9 0 264.515 133.265 10 -2 9 0 292.243 99.3805 8 -2 -9 0 565.241 134.515 8 2 -9 0 263.735 158.487 3 -2 9 0 288.900 127.446 6 2 9 0 404.988 218.738 10 2 -9 0 248.334 108.071 1 2 -9 0 385.610 153.643 10 2 -9 1 82637.9 3018.26 1 -2 9 -1 84827.7 2820.95 6 2 9 1 88914.0 2558.74 6 -2 9 -1 88390.9 2784.15 10 2 9 1 81384.4 2955.33 10 2 9 1 89226.9 2748.73 8 -2 -9 -1 84690.2 2777.22 8 2 -9 1 90763.3 2744.26 10 -2 9 -1 86997.9 2661.94 8 2 -9 1 83817.6 2993.84 3 -2 -9 -1 91986.6 3213.46 5 2 -9 2 21706.5 1067.79 8 2 -9 2 22208.0 1036.10 10 -2 9 -2 18826.7 1032.60 10 2 9 2 18118.5 1139.72 10 2 -9 2 21149.7 1193.89 3 -2 9 -2 19893.3 1098.08 8 -2 -9 -2 20851.2 1183.04 8 2 9 2 21815.9 1139.17 8 -2 9 -2 21476.2 1376.07 7 -2 9 -2 20188.7 1091.37 2 2 9 2 21935.7 1079.86 6 -2 9 -2 19226.2 1130.76 6 2 -9 2 18769.0 1270.67 1 -2 -9 -2 18667.0 1287.78 5 2 -9 3 53382.9 1907.28 10 2 -9 3 48695.9 2014.30 8 -2 9 -3 50503.6 2113.19 2 -2 9 -3 53245.1 2473.17 7 2 -9 3 49145.1 2364.74 1 2 9 3 49128.3 2124.19 10 -2 9 -3 53794.0 2238.26 6 -2 9 -3 47511.8 1950.67 10 -2 -9 -3 50931.4 1745.92 4 -2 9 -3 52753.8 2201.21 8 -2 -9 -3 48637.5 2358.41 5 -2 -9 -3 50864.3 2266.35 8 2 -9 3 52267.4 2074.39 3 -2 -9 -4 4223.01 647.822 5 2 9 4 3754.91 526.285 10 -2 9 -4 3316.13 545.111 8 -2 -9 -4 4107.43 377.003 4 2 -9 4 4109.95 462.171 10 -2 9 -4 4043.20 565.523 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185.943 7 -2 9 -8 644.854 377.267 2 2 -9 9 1518.15 523.351 1 -2 -9 -9 2827.67 664.137 5 2 9 9 1535.87 458.630 10 -2 9 -9 2960.91 696.590 9 -2 9 -9 2702.02 742.819 7 2 -9 9 3124.75 630.412 4 -2 9 -9 1351.00 540.980 2 -2 -9 -10 240.463 257.397 5 -2 9 -10 209.106 269.193 9 2 9 10 122.640 150.457 10 2 -9 10-98.1326 218.455 1 -2 9 -10-709.305 413.576 7 -2 9 -10 123.812 236.919 2 -2 -10 11 707.487 447.726 1 2 10 -11 1616.07 638.892 9 2 -10 -11 779.347 407.088 2 -2 -10 11 514.189 303.706 4 2 10 -11 1617.98 581.146 7 2 -10 -11 1512.51 457.978 5 2 10 -11 1869.91 669.643 2 -2 10 10 12430.7 1213.29 4 2 -10 -10 9457.71 1287.79 2 2 10 -10 10421.0 1486.09 9 2 10 -10 9427.27 1374.89 2 -2 -10 10 10908.1 1432.79 4 2 10 -10 10252.1 1328.48 7 -2 -10 10 9380.34 1386.42 1 2 -10 -10 10134.3 1185.12 5 2 10 -9 4781.67 927.006 2 2 -10 -9 5405.25 839.798 5 2 10 -9 5948.72 1094.86 9 -2 10 9 4325.43 693.691 4 -2 -10 9 4295.25 904.419 4 2 10 -9 3922.63 795.774 7 2 -10 -9 5841.79 966.700 2 -2 -10 9 5575.69 1050.30 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12825.5 1184.87 1 -2 10 -8 20565.3 1731.48 9 2 -10 8 13499.4 1377.45 4 -2 10 -8 22636.3 1911.27 2 2 -10 8 22776.5 1989.15 1 -2 10 -8 20721.8 1975.42 7 2 10 8 16143.8 1425.33 10 -2 -10 -8 23259.9 1865.66 5 -2 -10 -9 437.253 274.298 5 2 -10 9-111.557 244.107 1 2 10 9 719.580 339.150 10 2 -10 9 840.009 352.655 4 -2 10 -9 367.002 293.634 2 -2 10 -9 75.2828 383.151 7 -2 10 -9 299.184 182.075 9 -2 -10 -10 3411.38 765.041 5 2 -10 10 3355.07 849.044 1 2 10 10 2600.32 622.473 10 2 -10 10 3623.51 766.066 4 -2 10 -10 3195.22 862.986 7 -2 10 -10 2820.15 773.470 2 -2 10 -10 2732.61 710.420 9 -2 -11 11 1180.39 569.851 1 -2 -11 11 1296.02 550.972 4 2 -11 -11 1759.39 673.366 2 2 -11 -11 911.255 349.777 5 2 11 -11 772.306 458.233 9 2 11 -11 1521.61 544.002 7 2 11 -11 1651.04 653.651 2 2 -11 -10 885.274 465.506 2 -2 11 10 969.075 340.906 4 2 11 -10 1239.46 513.665 9 -2 -11 10 1204.57 494.748 4 2 -11 -10 967.662 377.878 5 -2 -11 10 1156.81 545.906 1 2 11 -10 1247.37 504.370 7 2 11 -10 947.550 451.823 2 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25900.5 1708.94 7 2 -11 3 26255.6 1702.08 1 2 -11 3 26284.9 1415.05 3 -2 11 -3 25292.4 1452.31 6 2 11 3 25884.1 1521.55 10 -2 -11 -3 24248.1 1651.87 5 2 -11 4 434.916 202.311 3 -2 11 -4 623.860 246.495 2 -2 11 -4 631.559 375.989 7 -2 11 -4 629.898 258.348 9 -2 -11 -4 641.146 310.468 8 -2 -11 -4 705.325 187.869 4 -2 -11 -4 515.235 316.824 5 2 -11 4 587.756 310.751 1 2 11 4 726.899 288.762 10 -2 11 -4 626.944 276.301 6 -2 11 -5 47138.6 2420.20 2 -2 11 -5 47046.3 2389.49 9 -2 -11 -5 49575.7 1838.16 4 -2 11 -5 47841.3 2713.48 7 2 -11 5 45138.8 2606.92 1 2 -11 5 48180.7 2016.11 3 2 11 5 44892.9 2281.38 10 -2 -11 -5 47980.5 2599.42 5 -2 -11 -5 45370.3 2502.91 8 2 -11 6 841.871 263.935 3 -2 -11 -6 426.790 233.441 5 -2 11 -6 1283.88 404.030 9 2 -11 6 584.762 308.923 1 2 11 6 1062.49 325.678 10 -2 11 -6 696.384 324.904 7 -2 11 -6 180.475 231.114 2 2 11 7 7876.13 947.092 10 -2 11 -7 10221.1 1147.32 9 -2 11 -7 9956.89 1175.80 2 2 -11 7 9379.36 1229.04 1 -2 11 -7 9968.35 1306.48 7 -2 -11 -7 10109.4 1211.32 5 -2 -11 -8-134.031 174.202 5 2 -11 8 212.513 312.237 1 2 11 8 348.502 240.729 10 -2 11 -8 78.1063 296.408 7 2 -11 8 581.051 327.791 4 -2 11 -8-138.602 191.260 9 -2 11 -8 406.112 287.136 2 -2 -11 -9 1879.50 550.540 5 2 11 9 2321.18 576.243 10 2 -11 9 2353.30 598.684 4 -2 11 -9 2566.67 761.093 7 -2 11 -9 1218.08 441.652 9 -2 11 -9 2499.21 682.297 2 2 -11 9 853.542 354.863 1 -2 -11 -10 89.1733 296.038 5 -2 11 -10-80.1033 240.485 2 2 11 10 621.758 365.344 10 2 -11 10 65.0208 191.116 1 -2 11 -10 383.810 341.087 9 2 -11 10-184.794 211.425 4 -2 11 -10-31.3245 272.013 7 2 -12 -11 116.173 171.302 5 2 12 -11 901.726 488.271 7 2 12 -11-23.6989 196.693 9 -2 12 11 692.800 463.277 10 2 -12 -11 241.436 260.886 2 -2 -12 11 420.027 332.054 4 -2 -12 11-386.164 342.858 1 2 12 -11 249.509 202.489 2 2 12 -10 29.7306 346.628 9 2 -12 -10 132.381 173.159 5 2 12 -10 430.828 324.947 7 -2 12 10 51.2010 191.804 10 -2 -12 10 187.179 239.882 4 2 -12 -10 232.706 158.130 2 -2 -12 10-208.491 248.487 1 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906.956 10 2 12 -5 8483.04 1055.10 9 -2 12 5 8343.68 876.610 4 -2 -12 5 7458.22 999.238 1 -2 -12 5 8476.52 1043.84 4 2 12 -5 7678.74 866.832 7 2 12 -5 8427.80 503.920 3 -2 -12 5 9407.89 745.408 6 -2 -12 5 7965.56 570.861 5 2 -12 -5 7785.59 948.431 5 2 12 -4 113954. 3484.69 5 2 12 -4 106014. 4175.96 10 -2 12 4 109430. 3990.27 10 -2 -12 4 109659. 4331.38 1 -2 -12 4 111180. 4351.55 4 2 12 -4 103358. 3271.88 3 2 12 -4 111132. 3978.55 7 -2 -12 4 111911. 3234.06 6 2 -12 -4 101228. 4128.53 5 2 12 -3 1384.26 281.421 5 -2 -12 3 1450.90 299.799 5 -2 12 3 925.728 288.499 10 2 -12 -3 1700.49 196.748 1 -2 -12 3 1458.29 395.116 1 2 -12 -3 1653.74 368.717 5 -2 -12 3 1146.28 139.045 6 2 12 -3 1296.67 381.847 10 2 12 -2 3694.75 571.200 10 -2 12 2 4810.82 570.645 10 -2 12 2 4422.41 488.831 2 -2 -12 2 3834.16 505.766 5 -2 -12 2 4675.13 665.312 1 2 -12 -2 4150.36 441.643 1 2 -12 -2 4551.00 661.252 5 -2 -12 1-31.4900 101.067 1 -2 -12 1 77.2238 173.354 5 2 -12 -1 48.0418 107.660 5 -2 12 1 81.6641 106.631 1 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425.440 3 3 -1 -3 1741.68 276.596 3 -3 -1 3 1764.82 264.629 3 3 -1 -3 1402.79 261.025 1 3 1 -3 1419.26 303.089 9 3 1 -3 1477.83 242.286 3 -3 1 3 2003.08 291.856 3 3 -1 -3 1470.19 292.552 9 3 1 -3 1637.58 290.074 1 -3 -1 3 1574.04 299.917 9 3 -1 -3 1901.55 290.158 2 -3 1 3 1352.01 306.113 4 -3 -1 3 1788.62 335.469 4 3 1 -3 1612.15 326.231 4 -3 1 3 1580.68 298.347 9 -3 -1 3 1726.62 160.869 7 3 1 -2 64324.0 2234.13 1 3 1 -2 62952.7 2244.02 9 -3 1 2 63586.2 2208.84 9 -3 1 2 61276.3 2316.75 4 -3 -1 2 61371.5 2326.82 4 3 -1 -2 64053.4 2377.67 4 -3 -1 2 63923.2 2210.81 9 3 1 -2 66751.6 2393.13 4 3 -1 -2 61307.4 2177.00 3 3 -1 -2 59843.6 2155.51 9 3 1 -2 64408.5 2156.48 3 -3 1 2 64600.7 2227.77 3 -3 -1 2 61322.3 2140.70 3 3 1 -1 52746.0 1790.65 9 -3 1 1 50816.3 1590.99 7 -3 1 1 54157.7 1729.10 9 -3 1 1 52052.0 1954.05 4 3 -1 -1 55157.7 2015.90 4 3 1 -1 54900.2 1982.46 4 3 1 -1 52480.1 1442.27 7 3 -1 -1 56791.1 1750.49 9 -3 -1 1 55027.4 1777.47 10 -3 -1 1 48044.4 1906.34 4 3 -1 -1 51214.3 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1823.27 479.583 4 -3 -2 8 2234.85 281.957 3 3 -2 -8 3205.56 636.197 2 3 2 -8 1655.86 179.212 5 3 -2 -7 3918.27 701.231 9 -3 2 7 4881.61 541.503 1 3 2 -7 3416.89 678.608 9 -3 2 7 4136.44 677.019 4 -3 -2 7 4723.98 728.945 4 3 -2 -7 3486.39 467.204 1 -3 -2 7 4519.98 396.518 3 3 -2 -7 4174.36 670.425 2 3 2 -7 3830.37 304.405 5 3 -2 -7 4630.24 515.215 5 3 2 -7 4654.40 721.133 2 -3 -2 7 4519.52 630.331 1 3 2 -6 1679.52 411.643 2 -3 -2 6 1882.44 249.178 3 -3 2 6 2069.19 326.335 1 3 -2 -6 1978.05 457.948 9 -3 -2 6 2694.84 450.352 1 3 -2 -6 1917.79 320.195 1 -3 2 6 1199.92 340.143 4 -3 -2 6 2216.63 461.441 4 3 -2 -6 2462.47 360.619 5 -3 -2 6 1917.39 338.990 7 3 2 -6 1780.23 444.046 9 3 -2 -6 1902.73 421.163 2 3 2 -6 2528.10 255.179 5 3 -2 -5 35975.7 1588.32 5 3 2 -5 37539.0 1940.70 2 3 -2 -5 37893.9 1633.06 3 3 -2 -5 40898.3 2079.10 9 -3 2 5 38262.8 1515.60 1 -3 -2 5 38028.2 1788.43 1 -3 -2 5 36257.6 1984.73 4 -3 2 5 35926.1 1914.19 4 3 -2 -5 38117.4 1875.41 2 3 -2 -5 40652.6 1628.44 1 -3 -2 5 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54452.1 1886.90 9 3 -2 3 54702.1 1656.59 9 3 2 3 48850.5 1697.37 10 -3 2 -3 50734.0 2025.37 2 -3 2 -3 49290.6 2295.13 8 -3 -2 -3 50083.0 2334.19 8 3 -2 3 49501.1 2038.06 2 -3 2 -3 52197.5 2352.29 7 -3 2 -3 50676.1 2296.40 6 -3 -2 -3 51496.9 2315.24 6 3 -2 3 53161.5 1761.48 4 -3 2 -3 49419.6 1623.06 9 3 -2 3 54059.5 2166.90 3 3 2 3 48562.7 2171.68 3 3 2 4 28978.5 1252.46 10 3 2 4 29666.2 1420.11 9 -3 2 -4 27839.3 1240.51 9 3 -2 4 29359.3 1256.97 9 -3 2 -4 27322.8 1741.05 7 -3 2 -4 25095.2 1472.61 2 -3 -2 -4 28228.1 1786.84 8 -3 -2 -4 29502.1 1641.89 2 -3 -2 -4 27519.7 1608.78 5 -3 2 -4 30087.2 1798.70 6 -3 -2 -4 28914.9 1756.53 6 -3 2 -4 27638.0 1763.83 8 3 -2 4 26739.5 1487.47 3 3 2 4 26297.9 1564.70 3 3 2 5 29.1782 62.4699 10 3 2 5 40.5148 95.8660 3 -3 2 -5 235.203 120.859 9 3 -2 5 27.6899 60.7998 9 -3 2 -5 154.597 140.064 8 -3 -2 -5 129.448 168.316 8 -3 -2 -5 426.228 225.839 2 -3 2 -5 28.4036 159.010 7 3 -2 5 258.249 151.441 3 -3 2 -5 115.127 172.374 2 3 -2 5 165.508 194.806 1 -3 2 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10 -3 11 2 28694.0 1242.34 2 -3 -11 2 28263.8 1720.63 1 3 -11 -2 27219.2 1681.22 3 3 -11 -2 28834.2 1305.81 1 -3 -11 2 27230.9 959.988 6 -3 -11 2 29703.3 1762.63 4 -3 -11 2 27152.1 1495.58 5 -3 -11 1 668.666 253.929 1 -3 -11 1 342.799 192.828 5 -3 11 1 190.853 67.9442 10 -3 -11 1 573.683 170.508 8 -3 11 1 407.988 128.241 8 -3 11 1 485.004 113.707 2 -3 -11 1 208.964 127.423 4 -3 -11 1 500.678 112.595 6 3 -11 -1 624.007 253.936 5 3 -11 -1 574.166 186.246 1 3 -11 -1 470.404 243.392 3 -3 11 0 60448.5 2215.70 10 3 11 0 56418.7 2502.19 10 -3 11 0 59442.1 2101.31 8 -3 -11 0 61046.6 2269.82 8 3 -11 0 55021.5 2526.15 3 -3 11 0 60506.8 2368.42 6 3 -11 0 56515.8 2389.14 1 -3 -11 0 58972.2 2594.96 5 3 -11 1 1733.16 395.488 3 -3 -11 -1 1792.21 424.186 5 3 -11 1 1464.20 376.448 1 3 -11 1 1206.16 257.075 10 -3 11 -1 1695.25 259.958 2 -3 11 -1 1815.95 324.348 10 -3 11 -1 1660.61 306.941 8 -3 -11 -1 1470.29 304.911 8 3 11 1 1462.09 357.648 10 3 11 1 1400.01 240.017 6 -3 11 -1 1820.63 365.231 6 3 -11 2 52447.2 1906.89 10 -3 11 -2 52931.4 2548.26 7 -3 11 -2 46949.1 2071.84 8 -3 11 -2 49263.4 1928.70 2 3 -11 2 45934.6 2216.10 3 3 11 2 51531.2 1953.83 6 -3 11 -2 49784.0 2223.14 6 -3 -11 -2 48943.5 2208.13 8 3 -11 2 48625.5 2403.60 1 -3 11 -2 48554.2 1928.95 10 -3 -11 -2 45121.9 2405.79 5 3 11 2 47303.2 2198.69 10 3 -11 3 678.277 271.311 3 -3 -11 -3 970.067 271.940 8 -3 -11 -3 358.524 197.040 5 3 -11 3 1520.52 395.286 1 3 -11 3 785.415 195.124 10 -3 -11 -3 961.092 190.134 4 3 11 3 1112.91 320.665 10 -3 11 -3 1038.41 307.738 8 -3 11 -3 732.869 301.210 7 -3 11 -3 1178.31 316.598 6 -3 11 -3 1187.21 262.549 10 -3 11 -3 690.492 237.917 2 3 11 4 27284.8 1646.56 10 -3 11 -4 27153.8 1745.17 8 -3 11 -4 27358.7 1594.25 9 -3 -11 -4 30444.0 1924.37 8 -3 11 -4 29858.7 2040.07 7 3 -11 4 26464.7 1572.72 3 3 -11 4 27360.0 1907.08 1 -3 11 -4 29205.6 1820.20 6 -3 11 -4 27526.9 1599.34 2 -3 -11 -4 27825.6 1140.59 4 -3 -11 -4 28378.9 1938.12 5 3 -11 5 673.033 307.240 3 -3 -11 -5 1030.21 412.694 5 3 11 5 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5458.60 930.038 4 -3 -12 11 5345.53 1127.85 1 -3 -12 11 5241.53 1117.17 4 3 -12 -11 6927.69 1151.84 2 3 12 -11 5678.25 1051.13 7 3 12 -11 6451.57 1296.81 9 3 12 -11 4093.42 1000.58 2 3 12 -10 278.777 360.815 2 3 -12 -10 622.389 324.299 5 3 12 -10 173.281 200.081 9 -3 12 10 213.672 154.771 4 -3 -12 10 315.640 299.642 1 -3 -12 10 330.631 246.028 4 3 -12 -10 501.880 251.288 2 3 12 -10 49.3876 203.109 7 3 12 -9 1477.39 512.336 2 3 12 -9 2762.49 787.349 9 -3 12 9 1468.85 415.254 4 3 -12 -9 2771.34 623.520 5 -3 -12 9 2157.95 651.622 1 3 -12 -9 1172.21 429.086 2 -3 -12 9 2031.81 612.812 4 3 12 -9 2515.12 611.671 7 3 12 -8 739.082 410.322 9 3 -12 -8 375.110 261.086 5 -3 -12 8 1631.03 514.496 1 -3 -12 8 792.963 359.138 4 3 -12 -8 526.755 299.572 2 3 12 -8 1939.98 513.992 7 -3 12 8 773.281 340.615 4 3 12 -8 930.181 453.127 2 -3 12 7 50846.7 2634.38 4 3 12 -7 48397.6 3039.59 9 -3 -12 7 52434.2 3095.55 4 -3 -12 7 54653.3 3101.39 1 3 12 -7 50437.1 2990.38 2 3 12 -7 52953.1 2677.84 7 -3 12 7 49875.1 2787.60 10 3 -12 -7 52701.0 2817.21 5 3 12 -6 465.318 88.2634 3 3 -12 -6 1302.32 440.694 5 3 12 -6 586.817 97.0903 3 -3 12 6 817.870 364.350 10 -3 -12 6 1559.26 528.507 1 3 12 -6 1065.27 475.258 9 -3 12 6 1366.19 388.517 4 -3 -12 6 1109.43 465.702 4 3 12 -6 996.383 355.767 7 3 12 -5 17540.3 969.823 5 -3 12 5 17638.7 1377.82 4 -3 12 5 19150.7 1434.44 10 -3 -12 5 18301.4 1608.38 4 3 12 -5 16914.9 1569.25 9 3 12 -5 21469.3 1410.14 7 -3 -12 5 20174.5 1629.77 1 -3 -12 5 19939.7 1020.44 5 3 12 -5 20411.3 972.628 3 3 -12 -5 21033.9 1600.91 5 3 12 -4 6553.38 872.705 10 -3 12 4 7706.94 846.691 10 -3 -12 4 6957.71 934.603 4 -3 12 4 6811.22 817.069 4 3 12 -4 7995.61 800.407 7 -3 -12 4 10249.6 1083.91 1 -3 -12 4 8572.34 710.277 5 3 12 -4 7003.17 634.399 5 3 -12 -4 7911.12 950.787 5 -3 -12 3 107642. 4200.64 4 -3 12 3 104314. 3448.94 2 3 -12 -3 108606. 3113.78 1 -3 12 3 105088. 3719.11 10 3 12 -3 100527. 4042.16 10 -3 -12 3 106111. 4106.80 1 -3 -12 3 107039. 3582.49 5 3 -12 -3 106659. 4124.75 5 3 12 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480.920 510.471 7 5 11 -11-236.613 368.259 2 5 -11 -11 91.2093 154.546 5 -5 -11 11-162.991 297.982 1 5 11 -11 176.853 228.937 9 -5 11 11-70.0585 175.792 4 -5 -11 11 502.437 342.376 4 5 -11 -11 91.1861 184.209 2 5 11 -10 3526.64 870.013 2 5 -11 -10 3571.16 737.628 5 -5 -11 10 5113.06 985.207 1 5 11 -10 4606.70 1029.30 9 -5 11 10 3441.59 744.717 4 -5 -11 10 3412.20 870.718 4 5 -11 -10 5361.37 908.849 2 5 11 -9 645.395 418.640 2 5 -11 -9 917.448 437.742 5 -5 -11 9 552.503 384.963 1 5 11 -9 408.236 473.256 9 -5 11 9 871.083 404.636 4 -5 -11 9 287.615 318.101 4 5 -11 -9 1196.41 433.183 2 -5 -11 8 1675.19 523.272 1 5 11 -8 2539.73 667.335 2 5 -11 -8 1968.21 524.545 5 5 11 -8 2010.78 610.752 9 -5 11 8 1606.73 484.699 4 -5 -11 8 1736.90 584.886 4 5 -11 -8 2007.59 485.184 2 5 11 -8 1826.31 425.474 7 5 -11 -7 1570.97 483.638 5 5 11 -7 1599.08 497.480 9 -5 11 7 1428.79 468.526 4 -5 -11 7 1310.15 493.986 4 5 -11 -7 1588.84 379.243 2 5 11 -7 1796.86 382.455 7 5 11 -7 1435.44 512.427 2 -5 -11 7 2563.76 613.221 1 -5 11 6 23602.4 1790.36 4 -5 -11 6 21082.4 1776.41 1 5 11 -6 20919.5 1895.17 9 5 -11 -6 24000.1 1446.44 2 -5 -11 6 23501.7 2001.38 4 5 11 -6 22994.2 1342.56 7 5 11 -6 23341.2 1222.00 3 5 -11 -6 25459.6 1884.83 5 -5 -11 5 301.097 275.689 1 5 -11 -5-25.1320 142.747 5 5 11 -5 147.642 161.135 3 5 11 -5 166.623 187.768 9 -5 11 5 234.853 214.488 4 5 -11 -5 162.760 75.2833 1 -5 -11 5 79.2158 282.775 4 5 11 -5 124.362 102.305 7 5 -11 -5 180.449 233.448 3 5 -11 -4 8165.09 1035.46 5 -5 11 4 8670.55 879.641 10 -5 -11 4 8277.36 1039.34 1 -5 11 4 9206.93 1028.71 4 5 11 -4 7941.09 1034.43 9 -5 -11 4 9690.26 1151.46 4 5 11 -4 9740.52 732.457 7 -5 11 4 9335.44 658.437 2 5 -11 -4 9717.16 1085.54 3 5 11 -4 7965.17 791.599 3 5 -11 -4 10272.5 721.383 1 -5 -11 3 693.946 256.296 5 5 11 -3 338.086 224.142 10 -5 11 3 491.685 208.391 10 5 11 -3 719.077 241.668 3 -5 11 3 651.845 288.910 4 5 -11 -3 791.487 235.328 1 -5 -11 3 851.173 315.855 4 -5 -11 3 774.976 209.024 6 5 -11 -3 599.326 288.354 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5736.28 785.334 10 -5 -13 -2 5305.68 605.240 4 -5 13 -2 6236.50 792.190 8 -5 -13 -2 6869.63 886.057 8 5 -13 2 5533.93 861.835 1 -5 13 -2 5701.46 882.382 7 5 -13 2 6388.20 871.808 3 -5 13 -2 5766.85 832.914 6 5 -13 3 2154.26 528.119 3 -5 -13 -3 1204.56 462.474 5 5 -13 3 1493.42 453.610 1 -5 13 -3 1291.76 300.348 9 -5 13 -3 1849.71 471.416 8 -5 -13 -3 2246.28 570.676 8 -5 13 -3 1767.86 514.678 7 -5 13 -3 1598.81 462.541 6 5 13 3 1540.98 439.066 10 -5 -13 -4 7541.11 1130.95 5 5 13 4 4765.36 728.256 10 -5 13 -4 6466.72 936.735 8 -5 -13 -4 8610.87 1128.77 8 -5 13 -4 7699.11 1154.59 7 5 -13 4 5290.19 810.691 3 5 -13 4 9883.46 1260.37 1 -5 13 -4 6400.64 971.604 6 -5 -13 -5-284.833 214.795 5 5 -13 5 98.0206 124.127 3 5 -13 5-21.9759 120.868 1 5 13 5-77.2021 93.4923 10 -5 13 -5-298.436 232.637 8 -5 -13 -5-76.7478 222.118 8 -5 13 -5 448.727 318.322 7 -5 13 -5 84.6772 159.995 6 -5 -13 -6 1853.59 656.783 5 5 -13 6 832.673 347.752 3 5 13 6 1504.35 423.144 10 -5 13 -6 1507.30 501.169 8 -5 -13 -6 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1176.73 10 -5 14 6 12722.2 1345.91 4 -5 -14 6 11124.3 1339.11 1 5 14 -6 8552.40 1277.34 9 -5 -14 6 8769.77 1283.59 4 5 14 -6 12240.9 1065.53 7 5 -14 -6 11483.1 1344.28 5 -5 14 5 42145.1 2351.95 10 -5 14 5 41278.8 2502.90 4 -5 -14 5 41916.0 2666.88 1 5 14 -5 36711.5 2646.00 9 -5 -14 5 44767.2 2871.05 4 5 14 -5 45792.0 2134.34 7 5 14 -5 41372.0 1980.00 3 5 -14 -5 41714.9 2646.60 5 5 -14 -4 7369.43 1051.73 5 -5 14 4 7873.03 883.684 10 -5 -14 4 8235.59 1113.79 1 5 14 -4 6396.49 1015.21 9 -5 -14 4 7436.53 1084.99 4 5 -14 -4 6665.94 565.727 1 -5 -14 4 6583.72 778.796 5 5 14 -4 7012.06 781.777 3 5 -14 -4 6440.98 950.675 3 5 -14 -3 24065.3 1937.04 5 5 14 -3 22500.5 1823.83 10 -5 14 3 25847.8 1575.57 10 -5 -14 3 24521.1 1915.10 4 -5 -14 3 26179.1 1600.40 8 5 -14 -3 24051.4 1870.54 3 5 -14 -3 25323.2 1393.90 1 -5 -14 3 23715.6 1634.30 5 5 14 -3 25508.0 1655.90 3 5 -14 -2 7205.63 1068.41 5 5 14 -2 7051.77 956.823 10 -5 14 2 7721.89 776.957 10 -5 -14 2 7872.58 1005.31 4 -5 -14 2 9019.92 894.009 8 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6705.89 967.637 8 -6 -11 -3 8546.20 1147.42 8 -6 11 -3 11383.2 1356.61 7 -6 11 -3 9622.11 1207.80 6 6 -11 3 8996.30 1099.33 3 6 -11 3 9903.17 1222.80 1 6 11 3 8511.77 1146.83 3 -6 -11 -4 301.525 317.185 5 6 -11 4 75.0990 140.336 3 6 11 4 269.116 218.035 10 6 11 4 65.3717 198.755 3 -6 11 -4 414.116 286.058 8 -6 -11 -4 235.083 322.438 8 -6 11 -4 527.282 365.637 7 -6 11 -4 35.7161 331.095 6 6 -11 4 484.429 378.890 1 -6 -11 -5 7986.08 1238.26 5 6 -11 5 5635.49 890.526 3 6 11 5 9109.38 972.626 10 -6 11 -5 7802.23 1171.88 8 -6 -11 -5 10099.6 1387.59 8 -6 11 -5 11329.9 1501.77 7 -6 11 -5 11089.2 1440.33 6 6 -11 5 8895.39 1289.43 1 6 11 5 8761.40 1236.79 3 -6 -11 -6 520.039 335.470 5 6 -11 6 57.2274 146.799 3 6 11 6 156.163 294.110 3 6 -11 6 45.8230 176.954 1 -6 11 -6-65.6309 177.442 8 -6 -11 -6 120.915 238.643 8 -6 11 -6-76.8627 272.857 7 -6 11 -6 495.207 358.103 6 6 -11 7 1763.52 601.997 1 6 11 7 1708.44 581.602 3 -6 11 -7 1772.64 613.214 8 -6 -11 -7 2409.66 782.658 8 -6 11 -7 3385.65 919.296 7 6 12 -10 1918.33 684.050 2 6 -12 -10 1498.73 493.740 5 -6 -12 10 1502.48 571.649 1 6 12 -10 2789.88 914.472 9 -6 12 10 1596.84 552.138 4 -6 -12 10 2262.61 763.431 4 6 12 -9 451.343 308.845 2 -6 -12 9 889.346 404.630 1 6 -12 -9 594.446 369.463 5 6 12 -9 417.446 341.497 9 -6 12 9 338.314 298.909 4 -6 -12 9 196.413 207.444 4 -6 12 8 19921.8 1823.69 4 -6 -12 8 20078.8 1911.62 1 6 12 -8 19611.1 2074.06 9 -6 -12 8 22323.1 2203.30 4 6 12 -8 20744.0 2027.10 2 6 -12 -8 18784.9 1762.67 5 -6 -12 7 340.439 263.576 1 6 -12 -7 450.165 322.741 5 6 12 -7 711.603 401.136 9 -6 12 7 540.077 313.207 4 -6 -12 7 900.145 489.706 4 6 -12 -6 8401.22 1135.16 5 -6 -12 6 9423.44 1235.10 1 -6 12 6 10725.8 1249.53 4 6 12 -6 10571.4 1374.39 9 -6 -12 6 8483.21 1239.61 4 6 -12 -6 8062.34 1105.04 3 6 12 -6 8265.08 807.743 3 6 -12 -5 1471.53 467.756 5 6 12 -5 1732.83 394.826 3 -6 12 5 1768.31 435.372 10 6 12 -5 1897.26 570.714 9 -6 12 5 1023.31 409.226 4 -6 -12 5 1461.06 476.360 4 6 -12 -5 2414.93 563.602 3 -6 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1761.44 617.603 1 7 8 4 1782.75 557.821 3 -7 8 -4 2216.76 639.545 8 -7 -8 -4 3267.49 806.086 8 -7 8 -4 1479.96 514.179 7 -7 8 -4 3249.36 809.888 6 -7 -8 -4 2785.79 683.780 6 7 -8 5 3219.89 725.829 3 7 8 5 3200.11 769.433 3 -7 8 -5 2966.72 779.929 8 -7 -8 -5 1985.10 647.273 8 7 -8 5 1973.02 645.503 1 -7 8 -5 2057.17 674.526 7 -7 8 -5 2794.98 761.780 6 7 -8 6 860.572 360.692 3 7 -8 6 592.934 359.211 1 7 8 6 1142.30 511.145 3 -7 8 -6 314.543 260.201 8 -7 -8 -6 1478.91 672.967 8 -7 8 -6 1033.79 470.656 7 -7 8 -6 1203.36 612.123 6 -7 -9 10 3165.65 759.278 1 7 9 -10 1083.54 483.280 2 7 -9 -10 3179.17 700.682 5 7 9 -10 3126.66 887.343 9 -7 9 10 2003.53 614.260 4 -7 -9 10 1938.44 727.148 4 7 9 -9 417.320 353.783 2 7 -9 -9 193.891 277.171 5 7 9 -9 265.700 192.053 9 -7 9 9-95.5310 215.328 4 -7 -9 9-490.282 362.314 4 7 -9 -8 19407.9 1726.76 5 -7 9 8 15728.4 1665.32 4 7 9 -8 18707.5 2006.53 9 -7 -9 8 19065.2 2010.06 4 7 9 -8 16120.4 1774.94 2 7 -9 -8 18342.5 1680.06 3 7 9 -7 405.462 394.204 2 7 -9 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10637.9 1606.55 9 -8 -6 10 10525.4 1589.36 4 8 6 -10 10296.8 1467.99 2 8 6 -9 2314.83 652.643 2 8 -6 -9 1649.52 483.705 5 8 -6 -9 1842.49 635.052 9 8 6 -9 832.957 369.485 9 -8 6 9 1518.33 537.448 4 -8 -6 9 1814.96 672.878 4 8 -6 -9 2417.31 611.836 3 8 -6 -8 17685.9 1642.98 5 8 -6 -8 11305.0 1443.23 9 -8 6 8 13873.2 1629.78 4 8 6 -8 18825.7 1972.22 9 -8 -6 8 19386.2 2025.45 4 8 6 -8 16463.9 1703.98 2 8 -6 -8 18226.8 1679.40 3 8 6 -7 4472.48 846.326 2 8 -6 -7 4194.10 813.944 9 8 6 -7 4240.35 912.944 9 -8 6 7 5772.63 1020.41 4 -8 -6 7 7000.34 1161.07 4 8 -6 -7 7409.32 1055.24 3 8 6 -7 6067.97 806.506 3 8 -6 -6 20584.6 1721.18 9 -8 6 6 21406.5 1905.53 4 -8 -6 6 24615.6 2115.58 4 8 -6 -6 17964.6 1654.84 3 8 6 -6 21117.0 1578.69 3 8 -6 -5 706.579 412.906 3 8 6 -5 160.385 121.022 3 8 6 -5 308.618 236.735 9 -8 6 5-114.517 170.503 4 -8 -6 5 536.653 366.984 4 -8 6 4 19011.4 1699.21 4 8 6 -4 19752.0 1668.46 9 -8 -6 4 17153.4 1641.60 4 -8 -6 4 20499.5 1583.82 6 8 -6 -4 18574.5 1683.31 3 8 6 -4 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459.471 8 -8 -6 -1 2014.53 604.095 8 -8 6 -1 1249.17 409.906 7 -8 6 -1 2528.63 634.646 6 -8 -6 -1 1505.04 445.568 6 8 -6 2 4905.67 883.656 3 8 6 2 4868.31 923.626 3 -8 6 -2 4914.51 930.036 8 -8 -6 -2 7411.73 1137.68 8 -8 6 -2 6930.67 1021.25 7 -8 6 -2 7046.50 1089.00 6 -8 -6 -2 5939.41 984.569 6 8 -6 3 361.558 252.078 3 8 6 3 155.263 245.576 3 -8 6 -3 107.220 288.481 8 -8 -6 -3 218.360 246.618 8 -8 6 -3 131.694 274.420 7 -8 6 -3 95.8687 229.735 6 -8 -6 -3 688.637 419.652 6 8 -6 4 5128.28 944.720 3 8 -6 4 1243.83 539.809 1 8 6 4 4442.84 947.470 3 -8 6 -4 3538.94 893.686 8 -8 -6 -4 4868.33 1015.79 8 -8 6 -4 5413.36 992.778 7 -8 6 -4 4291.13 930.306 6 -8 -6 -4 7317.31 1203.96 6 8 -6 5-52.5079 131.712 3 8 6 5 656.593 437.625 3 -8 6 -5-65.8019 309.922 8 -8 -6 -5-209.828 183.938 8 -8 6 -5 420.041 377.797 7 8 -6 5-183.752 230.606 1 -8 6 -5 49.8367 298.307 6 -8 -6 -5 371.352 390.251 6 8 7 -10 609.554 426.350 2 8 -7 -10 10.1872 128.363 5 8 -7 -10 1122.67 561.860 9 8 7 -10 565.968 403.059 9 -8 7 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27050.6 2011.77 4 -8 -7 3 27282.6 2040.88 8 -8 7 3 26894.6 1996.86 8 -8 7 3 28024.6 2060.90 6 -8 -7 3 31243.0 1939.03 6 8 -7 -3 29073.9 2165.30 3 8 7 -3 29736.0 2075.62 3 8 -7 -2 11.2214 120.023 3 8 7 -2 244.211 344.942 3 8 7 -2 385.889 200.576 9 -8 7 2 527.371 281.298 4 -8 -7 2 8.08702 168.987 4 -8 -7 2 829.995 421.582 8 -8 7 2 155.654 161.084 8 -8 7 2-10.1080 123.946 7 -8 7 2 273.980 345.572 6 -8 -7 2 287.271 202.573 6 -8 7 1 18519.5 1538.31 4 -8 -7 1 18954.8 1427.94 4 -8 7 1 17573.6 1614.31 8 -8 -7 1 15877.4 1556.42 8 -8 7 1 21006.2 1497.93 7 -8 7 1 19579.1 1701.24 6 -8 -7 1 18116.3 1491.04 6 8 -7 -1 16222.5 1600.73 3 8 7 -1 18676.6 1699.52 3 8 -7 0 2782.45 664.514 3 8 7 0 1776.32 519.472 3 -8 -7 0 2322.37 449.773 4 -8 7 0 3173.09 699.450 8 -8 -7 0 1776.83 523.214 8 -8 7 0 2053.82 483.958 7 -8 7 0 3342.28 717.916 6 -8 -7 0 1751.40 471.693 6 8 7 1 6256.94 1029.35 3 -8 7 -1 5359.76 937.147 8 -8 -7 -1 6834.97 1068.02 8 -8 7 -1 6993.76 987.390 7 8 -7 1 7660.84 1086.20 3 -8 7 -1 7247.35 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9361.85 1314.66 4 -8 -8 8 10448.8 1504.75 4 8 8 -8 8302.52 1336.67 9 8 -8 -8 8894.44 1198.75 3 8 8 -7 1967.13 458.628 3 8 8 -7 2581.87 656.157 2 8 8 -7 2243.68 653.609 9 -8 8 7 2964.11 736.614 4 -8 -8 7 2587.90 724.338 4 8 -8 -7 2490.89 660.114 3 -8 8 6 21786.2 1963.13 4 -8 -8 6 25573.3 2227.43 4 8 -8 -6 23602.4 1957.44 3 8 8 -6 23806.7 1677.85 3 8 -8 -5 1984.46 540.835 3 8 8 -5 927.041 325.984 3 8 8 -5 894.561 404.859 9 -8 8 5 1276.79 463.255 4 -8 -8 5 340.347 252.349 4 8 8 -4 5979.44 864.772 3 8 8 -4 4531.24 814.826 9 -8 8 4 6545.24 996.843 4 -8 -8 4 6792.96 1026.39 4 -8 -8 4 6718.88 860.785 6 8 -8 -4 8761.11 1143.00 3 8 -8 -3 955.511 474.014 3 8 8 -3 697.171 294.756 3 8 8 -3 505.549 269.115 9 -8 8 3 870.558 348.371 4 -8 -8 3 986.302 398.598 4 -8 -8 3 667.719 327.292 8 -8 8 3 1285.59 476.267 8 -8 8 3 1050.01 299.311 7 -8 8 3 1084.94 386.970 6 -8 -8 3 1582.40 424.553 6 -8 8 2 21943.9 1741.72 4 8 8 -2 20196.9 1572.52 9 -8 -8 2 19826.9 1612.93 4 -8 -8 2 18098.2 1679.89 8 -8 8 2 18830.1 1672.27 8 -8 8 2 22515.8 1537.32 7 -8 8 2 20761.7 1752.18 6 -8 -8 2 23242.0 1661.96 6 8 -8 -2 20057.7 1814.06 3 8 8 -2 21550.6 1790.22 3 8 -8 -1 2877.66 686.556 3 8 8 -1 4366.95 817.357 3 8 8 -1 1911.40 447.713 9 -8 -8 1 2965.56 564.346 4 -8 8 1 4952.29 849.261 8 -8 -8 1 1931.84 562.317 8 -8 8 1 4668.25 720.046 7 -8 8 1 3811.43 739.987 6 -8 -8 1 3181.00 647.628 6 -8 -8 0 11869.8 1047.57 4 -8 8 0 10320.1 1274.05 8 -8 -8 0 11317.7 1335.63 8 -8 8 0 13750.8 1325.39 7 -8 8 0 11297.3 1324.34 6 -8 -8 0 12439.3 1276.66 6 8 -8 0 12017.8 1387.42 3 8 8 0 11938.8 1392.23 3 8 -8 1 123.487 143.529 3 8 8 1 382.765 248.334 3 -8 8 -1 214.428 291.448 8 -8 -8 -1 614.152 357.198 8 -8 8 -1 95.5818 152.240 7 -8 8 -1 197.101 302.955 6 -8 -8 -1 721.075 361.914 6 -8 8 -2 8106.42 1193.38 8 -8 -8 -2 6487.97 1111.30 8 -8 8 -2 8458.44 1164.37 7 -8 8 -2 10025.8 1335.84 6 -8 -8 -2 11090.2 1299.29 6 8 -8 2 10303.2 1292.53 3 8 8 2 10345.3 1352.78 3 8 -8 3 61.8780 244.567 3 8 -8 3 94.5286 234.015 1 8 8 3 82.0423 203.556 3 -8 8 -3 541.850 372.245 8 -8 -8 -3 705.548 474.291 8 -8 8 -3-106.509 253.134 7 -8 8 -3 862.254 395.365 6 -8 -8 -3-183.775 184.813 6 8 -8 4 799.263 363.776 3 8 8 4 239.501 199.960 3 8 -8 4 453.008 327.295 1 -8 8 -4 200.173 269.160 8 -8 -8 -4 508.065 315.640 8 -8 8 -4 708.131 409.942 7 -8 8 -4 1565.97 559.151 6 -8 -8 -4 1263.49 477.310 6 8 -8 5 1192.05 497.381 3 8 8 5 1391.41 601.952 3 -8 8 -5 1144.94 507.245 8 -8 -8 -5 1911.42 694.131 8 -8 8 -5 1149.33 426.528 7 8 -8 5 1673.51 645.601 1 -8 8 -5 1713.31 548.663 6 8 9 -9 4484.00 975.952 2 8 -9 -9 4255.74 851.159 5 8 9 -9 5077.41 1107.36 9 -8 9 9 3955.18 902.759 4 -8 -9 9 4062.07 1021.42 4 8 9 -8 388.967 285.859 2 8 -9 -8 363.468 271.213 5 8 9 -8 19.9246 283.995 9 -8 9 8-248.460 330.624 4 -8 -9 8-117.047 177.660 4 8 -9 -8 316.842 245.997 3 8 -9 -7 13098.3 1518.47 5 -8 9 7 14720.4 1611.58 4 8 9 -7 10975.4 1511.45 9 -8 -9 7 12949.8 1653.23 4 8 9 -7 11594.9 1478.56 2 8 -9 -7 12185.3 1440.68 3 8 9 -6 92.5849 133.658 3 8 9 -6 128.028 146.544 9 -8 9 6 256.454 320.455 4 -8 -9 6 343.073 357.405 4 8 -9 -6 417.272 320.042 3 -8 9 5 15350.6 1573.47 4 8 9 -5 9636.03 1284.63 9 -8 -9 5 13302.0 1534.65 4 8 -9 -5 14011.9 1504.70 3 8 9 -5 15389.2 1379.97 3 8 -9 -4-284.037 237.475 3 8 9 -4 239.905 215.987 3 8 9 -4 75.0327 228.155 9 -8 9 4 294.888 275.760 4 -8 -9 4 279.787 298.110 4 -8 -9 4-104.141 302.253 8 -8 -9 4 30.3802 147.923 6 -8 9 3 7228.67 749.695 10 -8 9 3 13107.6 1376.10 4 8 9 -3 13417.0 1358.89 9 -8 -9 3 13209.2 1390.79 4 -8 -9 3 14765.8 1457.49 8 -8 9 3 8455.84 1098.88 8 -8 9 3 13717.3 1159.48 7 -8 9 3 14870.6 1486.27 6 -8 -9 3 13726.0 1221.15 6 8 -9 -3 9974.15 1290.18 3 8 9 -3 12777.0 1330.63 3 8 -9 -2 175.247 278.933 3 8 9 -2 354.330 269.790 3 8 9 -2 44.7455 129.509 9 -8 9 2 428.204 295.506 4 -8 -9 2 327.818 200.131 4 -8 -9 2 923.777 406.878 8 -8 9 2 164.808 206.126 8 -8 9 2 300.455 229.060 7 -8 9 2 104.193 172.080 6 -8 -9 2 49.8017 123.437 6 -8 -9 1 10775.2 1097.63 4 8 9 -1 11829.2 1168.83 9 -8 9 1 8639.89 1134.11 8 -8 -9 1 13682.2 1445.47 8 -8 9 1 14517.0 1307.42 7 -8 9 1 13142.6 1413.79 6 -8 -9 1 11841.9 1202.42 6 8 -9 -1 11633.8 1377.96 3 8 9 -1 11580.3 1349.37 3 8 -9 0 1365.39 497.125 3 8 9 0 2141.86 590.942 3 -8 -9 0 916.844 298.467 4 -8 9 0 1093.82 420.998 8 -8 -9 0 1719.94 513.782 8 -8 9 0 1461.88 447.336 7 -8 9 0 1202.16 460.543 6 -8 -9 0 2190.09 552.892 6 -8 -9 -1 8880.21 1233.01 8 -8 9 -1 6269.38 1008.02 8 -8 9 -1 9208.72 1145.19 7 -8 9 -1 8872.01 1217.96 6 -8 -9 -1 8577.31 1095.17 6 8 -9 1 7924.03 1143.28 3 8 9 1 8932.32 1229.10 3 8 -9 2 434.075 324.223 3 8 9 2 898.723 473.338 3 -8 9 -2 77.7475 259.177 8 -8 -9 -2 340.409 309.055 8 -8 9 -2 585.633 340.106 7 8 -9 2 29.2816 250.074 1 -8 9 -2 797.417 437.897 6 -8 -9 -2 658.131 358.348 6 8 -9 3 9521.36 1501.14 1 -8 9 -3 9358.15 1324.39 8 -8 -9 -3 11437.1 1494.84 8 -8 9 -3 9300.37 1308.71 7 -8 9 -3 11010.5 1497.61 6 -8 -9 -3 11811.6 1440.71 6 8 -9 3 9825.11 1309.12 3 8 9 3 10953.0 1436.29 3 8 -9 4 383.083 326.431 3 8 9 4 179.268 198.201 3 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296.694 3 9 7 -3-50.2824 152.851 3 -9 7 3-47.1320 160.452 4 -9 -7 3 191.645 178.640 4 -9 -7 3-156.850 200.314 8 -9 7 3 2.40787 195.403 8 -9 7 3-255.242 239.747 6 -9 -7 3-126.398 167.332 6 -9 7 2 10660.5 1247.92 4 -9 -7 2 13040.1 1300.97 4 -9 7 2 11244.2 1371.75 8 -9 -7 2 12256.4 1454.34 8 -9 7 2 11627.2 1372.99 6 -9 -7 2 13653.9 1365.46 6 9 -7 -2 10888.7 1389.84 3 9 7 -2 10285.6 1309.21 3 9 -7 -1 2213.00 631.457 3 9 7 -1 2442.63 689.411 3 -9 -7 1 1980.61 470.902 4 -9 7 1 3057.24 728.453 8 -9 -7 1 1892.63 611.949 8 -9 7 1 2992.51 780.429 6 -9 -7 1 2045.64 545.894 6 -9 7 0 11042.6 1408.10 8 -9 -7 0 10150.6 1367.93 8 -9 7 0 10340.3 1355.97 6 -9 -7 0 10881.9 1285.04 6 9 -7 0 9444.08 1305.94 3 9 7 0 11301.0 1444.29 3 9 -7 1 161.362 171.656 3 9 7 1 161.181 303.327 3 -9 7 -1 86.0483 199.144 8 -9 -7 -1 578.839 393.867 8 -9 7 -1 636.238 330.248 6 -9 -7 -1-214.364 199.792 6 9 -7 2 6071.55 1043.96 3 9 7 2 4446.35 946.431 3 -9 7 -2 5865.15 1104.10 8 -9 -7 -2 4976.78 1022.58 8 -9 7 -2 5138.83 1037.83 6 -9 -7 -2 5480.96 994.183 6 9 -7 3 105.946 366.276 3 9 7 3 260.049 240.608 3 -9 7 -3 825.045 485.194 8 -9 -7 -3 463.591 301.527 8 -9 7 -3 271.329 367.749 7 -9 7 -3 84.3314 208.055 6 -9 -7 -3 496.875 454.472 6 9 8 -8 1932.55 632.445 2 9 -8 -8 1358.62 533.887 5 9 8 -8 1500.43 645.279 9 -9 8 8 424.894 310.914 4 -9 -8 8 1613.25 697.781 4 9 -8 -8 2010.77 617.974 3 9 8 -7 3373.59 793.319 2 9 8 -7 3085.04 768.867 9 -9 8 7 2558.28 706.070 4 -9 -8 7 3295.18 854.933 4 9 -8 -7 3919.14 838.869 3 9 -8 -6 650.483 436.301 3 9 8 -6 241.963 184.357 3 9 8 -6 290.661 227.191 9 -9 8 6 404.669 378.532 4 -9 -8 6 1164.39 586.000 4 -9 8 5 32252.9 2391.11 4 9 8 -5 27234.0 2203.58 9 -9 -8 5 29506.4 2367.88 4 9 -8 -5 26465.7 2206.44 3 9 8 -5 29604.7 2111.85 3 9 -8 -4 664.461 389.486 3 9 8 -4 985.268 472.041 3 9 8 -4 803.759 357.140 9 -9 8 4 470.481 382.609 4 -9 -8 4 892.215 430.000 4 -9 -8 4 1440.37 522.731 8 -9 8 4 700.350 359.497 8 -9 8 4 1167.11 470.616 6 -9 -8 4 1187.51 401.106 6 9 -8 -3 7907.89 1186.72 3 -9 8 3 8354.86 1136.99 4 -9 -8 3 6915.82 1016.70 4 -9 -8 3 7225.06 1119.91 8 -9 8 3 7433.38 1091.23 8 -9 8 3 6668.98 1057.23 6 -9 -8 3 4366.55 760.127 6 9 8 -3 9096.83 1202.92 3 9 -8 -2 289.621 289.250 3 9 8 -2 627.479 334.676 3 -9 8 2 729.194 364.401 4 -9 -8 2 267.628 195.011 4 -9 8 2 29.5271 189.868 8 -9 -8 2 124.040 169.974 8 -9 8 2 187.532 328.879 6 -9 -8 2 281.648 218.638 6 -9 8 1 15820.7 1645.46 8 -9 -8 1 12264.7 1494.37 8 -9 8 1 14190.2 1583.14 6 -9 -8 1 18187.4 1613.16 6 9 -8 -1 11746.9 1471.70 3 9 8 -1 17216.1 1733.88 3 9 -8 0 617.107 365.414 3 9 8 0 657.002 384.188 3 -9 8 0 397.515 316.008 8 -9 -8 0 211.841 414.954 8 -9 8 0 378.441 286.059 6 -9 -8 0 716.418 377.680 6 9 -8 1 3780.26 826.756 3 9 8 1 3750.92 828.054 3 -9 8 -1 2822.01 739.216 8 -9 -8 -1 4143.99 911.441 8 -9 8 -1 3611.64 885.733 6 -9 -8 -1 3884.30 823.242 6 9 -8 2 713.878 385.930 3 9 8 2 711.039 423.029 3 -9 8 -2 173.175 291.498 8 -9 -8 -2 1503.43 594.276 8 -9 8 -2 515.076 336.062 7 -9 8 -2 118.092 189.185 6 -9 -8 -2 1115.80 429.277 6 9 8 3 8866.24 1375.96 3 -9 8 -3 6367.61 1183.60 8 -9 -8 -3 9027.91 1413.90 8 -9 8 -3 6537.92 1113.93 7 -9 -8 -3 10395.3 1449.15 6 9 -8 3 9356.37 1345.62 3 -9 8 -3 9057.69 1422.62 6 9 -8 3 6781.62 1454.02 1 9 -9 -8 8268.16 1256.40 5 9 9 -8 7764.16 1257.89 2 9 9 -8 5724.23 1146.84 9 -9 9 8 6187.22 1113.47 4 -9 -9 8 5985.65 1209.58 4 9 -9 -8 5936.99 1083.93 3 9 9 -7-20.6218 218.353 2 9 9 -7 28.7562 386.198 9 -9 9 7 237.173 243.852 4 -9 -9 7-54.7075 169.548 4 9 -9 -7 349.456 288.739 3 -9 9 6 11776.8 1478.96 4 9 9 -6 9383.71 1372.16 9 -9 -9 6 13257.7 1661.61 4 9 -9 -6 11746.7 1467.32 3 9 9 -6 12520.4 1308.64 3 9 -9 -5 13.5029 413.534 3 9 9 -5 467.859 313.197 3 9 9 -5 35.7439 239.382 9 -9 9 5 39.2179 134.170 4 -9 -9 5-117.873 140.079 4 -9 -9 5 275.560 228.723 6 -9 9 4 13766.4 1509.85 4 9 9 -4 11963.9 1397.00 9 -9 -9 4 9958.55 1330.62 4 -9 -9 4 14083.4 1541.72 8 -9 9 4 13438.9 1485.58 8 -9 9 4 12599.0 1459.28 6 -9 -9 4 13647.5 1317.74 6 9 -9 -4 14439.7 1625.36 3 9 9 -4 10688.4 1307.32 3 9 -9 -3 2062.92 664.951 3 9 9 -3 1458.52 484.892 3 -9 9 3 1460.73 496.074 4 -9 -9 3 840.859 404.733 4 -9 -9 3 1282.11 460.305 8 -9 9 3 1692.75 505.288 8 -9 9 3 1245.21 459.546 6 -9 -9 3 1898.67 484.856 6 -9 9 2 13970.6 1470.81 4 -9 -9 2 15732.6 1467.50 4 -9 9 2 11717.5 1423.89 8 -9 -9 2 12075.8 1462.49 8 -9 9 2 15415.4 1619.91 6 -9 -9 2 11435.6 1260.50 6 9 -9 -2 14063.6 1607.64 3 9 9 -2 15424.4 1626.36 3 9 -9 -1 21.9899 211.063 3 9 9 -1 715.342 458.956 3 -9 9 1 346.435 304.938 8 -9 -9 1 467.267 320.983 8 -9 9 1 1242.74 535.157 6 -9 -9 1 266.310 236.811 6 -9 9 0 10410.3 1375.25 8 -9 -9 0 11601.8 1473.17 8 -9 9 0 14695.9 1628.37 6 -9 -9 0 8336.74 1137.31 6 9 -9 0 13534.9 1573.11 3 9 9 0 11567.6 1477.81 3 9 -9 1 297.632 395.767 3 9 9 1-171.620 196.546 3 -9 9 -1-4.25096 225.852 8 -9 -9 -1-88.0070 186.614 8 -9 9 -1 115.788 254.708 6 -9 -9 -1-114.094 194.336 6 9 -9 2 6815.18 1147.27 3 9 9 2 8642.96 1324.48 3 -9 9 -2 7462.83 1235.25 8 -9 -9 -2 8164.21 1327.06 8 -9 9 -2 10074.0 1341.66 7 9 -9 2 4433.00 1052.00 1 -9 9 -2 9341.22 1386.46 6 -9 -9 -2 11471.1 1454.21 6 9 10 -7 1997.85 605.841 9 -9 10 7 1718.06 590.152 4 -9 -10 7 1597.98 610.063 4 9 -10 -7 2986.07 770.101 3 9 10 -6 39.3683 147.141 3 9 10 -6 137.527 201.740 9 -9 10 6 96.5224 172.762 4 -9 -10 6 276.848 244.828 4 -9 -10 6 722.792 362.313 6 9 -10 -6 221.313 236.056 3 -9 10 5 17998.6 1793.99 4 9 10 -5 14983.9 1670.35 9 -9 -10 5 13033.5 1618.09 4 -9 -10 5 13783.5 1562.43 8 -9 -10 5 15192.3 1416.32 6 9 -10 -5 14266.8 1639.86 3 9 10 -5 16431.7 1555.52 3 9 -10 -4 181.839 292.162 3 9 10 -4 51.7887 144.482 3 9 10 -4 621.091 398.693 9 -9 10 4 298.707 292.087 4 -9 -10 4-387.480 279.655 4 -9 -10 4-404.780 292.643 8 -9 10 4 1.19704 180.027 8 -9 10 4 50.5196 226.496 6 -9 -10 4 669.508 277.477 6 9 -10 -3 4918.91 948.755 3 9 10 -3 4261.35 843.256 3 -9 10 3 4701.10 871.079 4 -9 -10 3 3884.24 785.871 4 -9 -10 3 5194.69 937.314 8 -9 10 3 4496.27 866.472 8 -9 10 3 6144.42 1016.60 6 -9 -10 3 4527.58 756.236 6 9 -10 -2 146.621 291.512 3 9 10 -2 556.722 345.040 3 -9 -10 2 182.700 152.544 4 -9 10 2 121.539 176.391 8 -9 -10 2 163.013 184.317 8 -9 10 2 33.1075 228.199 6 -9 -10 2 41.8599 198.708 6 -9 10 1 18891.7 1847.47 8 -9 -10 1 22411.8 2042.54 8 -9 10 1 24099.5 2099.54 6 -9 -10 1 26024.1 1942.88 6 9 -10 -1 22081.0 2068.13 3 9 10 -1 22282.6 2032.55 3 9 -10 0 361.367 375.135 3 9 10 0 233.895 236.259 3 -9 10 0 247.373 313.664 8 -9 -10 0 564.840 406.314 8 -9 10 0 360.714 448.497 6 -9 -10 0 16.7406 106.225 6 9 -10 1 8738.45 1302.97 3 -9 10 -1 9414.15 1338.12 8 -9 -10 -1 9099.44 1340.91 8 9 -10 1 4572.61 1020.98 1 -9 10 -1 11139.1 1483.66 6 -9 -10 -1 8547.21 1174.38 6 9 10 1 9670.13 1366.45 3 9 -10 2 43.9351 310.719 3 9 10 2 133.779 266.250 3 -9 10 -2-143.962 287.864 8 -9 -10 -2 521.126 415.206 8 -9 10 -2 149.960 272.976 7 9 -10 2 361.934 285.644 1 -9 10 -2 443.303 290.381 6 -9 -10 -2 90.7499 307.725 6 9 -11 -7 430.805 291.404 5 9 11 -7 519.893 367.359 9 -9 11 7 791.919 350.282 4 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2954.71 689.844 3 9 12 -3 2273.84 606.447 9 -9 -12 3 2679.29 651.859 4 -9 12 3 2400.36 656.279 8 -9 -12 3 1854.72 574.212 8 -9 12 3 2910.22 697.407 6 9 -12 -2-280.411 254.991 3 9 12 -2 67.3180 241.434 3 -9 12 2-12.2716 173.399 8 -9 -12 2 635.974 450.100 8 -9 12 2 23.8379 200.526 6 9 -12 -2 3.75313 137.283 1 9 -12 -1 11953.4 1773.22 1 -9 12 1 16421.3 1678.43 8 -9 -12 1 13710.0 1590.17 8 -9 12 1 14259.6 1631.73 6 9 -12 -1 13606.7 1670.24 3 9 12 -1 12802.0 1563.90 3 9 -12 0-81.2492 163.637 3 9 12 0 539.860 367.845 3 9 -12 0 748.517 417.127 1 -9 12 0 472.000 334.434 8 -9 -12 0 606.711 368.369 8 -9 12 0 254.920 301.766 6 9 -12 1 3387.17 842.310 3 9 12 1 4080.10 917.871 3 -9 12 -1 3483.46 787.931 8 -9 -12 -1 3153.78 800.479 8 -9 12 -1 3947.00 924.901 6 9 -12 1 4620.25 959.624 1 9 13 -5 349.148 291.386 3 9 13 -5 282.709 165.524 9 -9 13 5 401.553 292.403 4 -9 -13 5-38.8928 211.037 4 -9 -13 5 161.682 194.837 8 -9 13 5 450.533 326.234 8 9 -13 -5 925.785 449.025 3 9 -13 -4 5193.03 1024.47 3 9 13 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4 -10 -9 3 9654.53 1258.23 4 -10 9 3 11438.9 1471.68 8 -10 -9 3 12685.4 1588.42 8 -10 9 3 11044.2 1443.51 6 -10 -9 3 12376.4 1375.86 6 10 -9 -3 12546.4 1637.92 3 10 9 -3 12691.7 1553.89 3 10 -9 -2 817.791 502.087 3 10 9 -2 833.648 448.585 3 -10 9 2 312.610 291.472 8 -10 -9 2 612.886 309.126 8 -10 9 2 1011.37 475.888 6 -10 -9 2 806.495 362.476 6 -10 9 1 11646.7 1522.15 8 -10 -9 1 9587.69 1389.25 8 -10 9 1 10592.5 1461.95 6 -10 -9 1 12019.8 1395.51 6 10 -9 -1 10776.3 1485.08 3 10 9 -1 11883.8 1558.69 3 10 -10 -3 609.183 372.235 3 10 10 -3 223.445 301.543 3 -10 10 3 383.581 413.106 4 -10 10 3-233.923 197.376 8 -10 -10 3 32.3874 201.451 8 -10 10 3 179.112 223.685 6 0 0 0 0.00 0.00 0 TITL RED1 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.71073 8.672553 20.882371 10.335061 90.0000 104.4289 90.0000 ZERR 2.00 0.000168 0.000403 0.000242 0.0000 0.0022 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O S Pd UNIT 72.00 84.00 8.00 12.00 4.00 2.00 TREF HKLF 4 END ; _shelx_hkl_checksum 29827 _olex2_submission_special_instructions 'No special instructions were received'