#============================================================================== data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 12 _journal_issue 2 _journal_year 2021 _journal_page_first 204 _journal_page_last 215 #============================================================================== data_20zs_diiso4cl_0m _audit_creation_date 2021-01-13 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Bourhis, L.J., Dolomanov, O.V., Gildea, R.J., Howard, J.A.K., Puschmann, H. (2015). Acta Cryst. A71, 59-75. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. ; _chemical_formula_moiety 'C19 H22 Cl N' _chemical_formula_sum 'C19 H22 Cl N' _chemical_formula_weight 299.85 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Cl 0.14873 0.16029 11.46040 7.19640 6.25560 1.64550 0.01040 1.16620 18.51940 47.77840 -9.55739974976 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2ybc (x-z,y,z)' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 _symmetry_Int_Tables_number 14 _cell_length_a 7.28280(10) _cell_length_b 9.94270(10) _cell_length_c 24.0413(2) _cell_angle_alpha 90 _cell_angle_beta 97.0120(10) _cell_angle_gamma 90 _cell_volume 1727.83(3) _cell_formula_units_Z 4 _cell_measurement_reflns_used 8305 _cell_measurement_temperature 150.0 _cell_measurement_theta_max 28.47 _cell_measurement_theta_min 6.21 _exptl_absorpt_coefficient_mu 0.215 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6829 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.0497 before and 0.0355 after correction. The Ratio of minimum to maximum transmission is 0.9158. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.1526 _exptl_crystal_density_meas . _exptl_crystal_description needle _exptl_crystal_F_000 640.8004 _exptl_crystal_size_max 0.31 _exptl_crystal_size_mid 0.19 _exptl_crystal_size_min 0.14 _diffrn_reflns_av_R_equivalents 0.0223 _diffrn_reflns_av_unetI/netI 0.0182 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 14038 _diffrn_reflns_theta_full 26.3711 _diffrn_reflns_theta_max 26.37 _diffrn_reflns_theta_min 6.21 _diffrn_ambient_temperature 150.0 _diffrn_measured_fraction_theta_full 0.9784 _diffrn_measured_fraction_theta_max 0.9784 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 8 _reflns_limit_h_min -9 _reflns_limit_k_max 12 _reflns_limit_k_min 0 _reflns_limit_l_max 29 _reflns_limit_l_min -7 _reflns_number_gt 2966 _reflns_number_total 3448 _reflns_threshold_expression I>=2u(I) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _refine_diff_density_max 0.2397 _refine_diff_density_min -0.2428 _refine_diff_density_rms 0.0380 _refine_ls_d_res_high 0.8000 _refine_ls_d_res_low 3.2827 _refine_ls_goodness_of_fit_ref 1.0495 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 36 _refine_ls_number_parameters 194 _refine_ls_number_reflns 3448 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0411 _refine_ls_R_factor_gt 0.0337 _refine_ls_restrained_S_all 1.0495 _refine_ls_shift/su_max 0.0002 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0427P)^2^+0.5336P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0856 _refine_ls_wR_factor_ref 0.0927 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C18(H18), C15(H15) 2.b Aromatic/amide H refined with riding coordinates: C1(H1), C7(H7), C5(H5), C10(H10), C2(H2), C4(H4), C12(H12), C11(H11) 2.c Idealised Me refined as rotating group: C17(H17a,H17b,H17c), C19(H19a,H19b,H19c), C16(H16a,H16b,H16c), C14(H14a,H14b, H14c) ; _atom_sites_solution_primary iterative loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Cl1 Cl 0.15484(5) 0.97803(4) 0.447958(15) 0.04315(13) Uani 1.000000 . N1 N 0.80833(14) 0.57958(10) 0.35726(4) 0.0264(2) Uani 1.000000 . C8 C 0.91106(17) 0.48143(12) 0.33087(5) 0.0250(3) Uani 1.000000 . C1 C 0.59772(18) 0.78046(13) 0.40866(5) 0.0274(3) Uani 1.000000 . H1 H 0.72846(18) 0.78793(13) 0.41612(5) 0.0329(3) Uiso 1.000000 R C6 C 0.51918(17) 0.67445(12) 0.37577(5) 0.0250(3) Uani 1.000000 . C9 C 1.03406(18) 0.39964(12) 0.36577(5) 0.0279(3) Uani 1.000000 . C7 C 0.63360(17) 0.57270(12) 0.35208(5) 0.0262(3) Uani 1.000000 . H7 H 0.57422(17) 0.49904(12) 0.33214(5) 0.0315(3) Uiso 1.000000 R C5 C 0.32765(18) 0.66604(13) 0.36458(5) 0.0292(3) Uani 1.000000 . H5 H 0.27367(18) 0.59525(13) 0.34159(5) 0.0351(3) Uiso 1.000000 R C13 C 0.90169(17) 0.47548(13) 0.27210(5) 0.0270(3) Uani 1.000000 . C10 C 1.1442(2) 0.30916(13) 0.34089(6) 0.0336(3) Uani 1.000000 . H10 H 1.2256(2) 0.25160(13) 0.36378(6) 0.0403(4) Uiso 1.000000 R C3 C 0.29561(19) 0.86193(13) 0.41926(5) 0.0299(3) Uani 1.000000 . C2 C 0.48633(19) 0.87440(13) 0.43037(5) 0.0303(3) Uani 1.000000 . H2 H 0.53959(19) 0.94666(13) 0.45264(5) 0.0363(3) Uiso 1.000000 R C4 C 0.21411(18) 0.75912(14) 0.38638(5) 0.0315(3) Uani 1.000000 . H4 H 0.08331(18) 0.75237(14) 0.37889(5) 0.0378(3) Uiso 1.000000 R C12 C 1.01888(19) 0.38454(14) 0.24947(6) 0.0329(3) Uani 1.000000 . H12 H 1.01714(19) 0.37968(14) 0.20995(6) 0.0395(4) Uiso 1.000000 R C18 C 0.77012(18) 0.56108(13) 0.23281(5) 0.0305(3) Uani 1.000000 . H18 H 0.71254(18) 0.62907(13) 0.25598(5) 0.0366(3) Uiso 1.000000 R C11 C 1.1370(2) 0.30168(14) 0.28314(6) 0.0356(3) Uani 1.000000 . H11 H 1.2134(2) 0.23946(14) 0.26670(6) 0.0427(4) Uiso 1.000000 R C15 C 1.0390(2) 0.41001(14) 0.42906(5) 0.0342(3) Uani 1.000000 . H15 H 1.0069(2) 0.50485(14) 0.43781(5) 0.0411(4) Uiso 1.000000 R C17 C 0.6148(2) 0.47342(16) 0.20313(7) 0.0429(4) Uani 1.000000 . H17a H 0.6683(2) 0.4031(7) 0.1815(4) 0.0643(5) Uiso 1.000000 GR H17b H 0.5455(10) 0.4318(9) 0.23108(7) 0.0643(5) Uiso 1.000000 GR H17c H 0.5312(9) 0.5294(3) 0.1778(4) 0.0643(5) Uiso 1.000000 GR C19 C 0.8685(2) 0.63671(16) 0.18983(6) 0.0447(4) Uani 1.000000 . H19a H 0.9673(11) 0.6924(9) 0.20928(7) 0.0670(6) Uiso 1.000000 GR H19b H 0.9218(14) 0.57206(16) 0.1655(3) 0.0670(6) Uiso 1.000000 GR H19c H 0.7795(4) 0.6943(9) 0.1671(3) 0.0670(6) Uiso 1.000000 GR C16 C 1.2296(3) 0.38041(17) 0.46089(6) 0.0474(4) Uani 1.000000 . H16a H 1.2594(8) 0.2851(3) 0.4567(4) 0.0711(6) Uiso 1.000000 GR H16b H 1.3229(3) 0.4358(9) 0.4457(3) 0.0711(6) Uiso 1.000000 GR H16c H 1.2286(5) 0.4014(12) 0.50069(11) 0.0711(6) Uiso 1.000000 GR C14 C 0.8911(3) 0.31941(16) 0.44936(6) 0.0448(4) Uani 1.000000 . H14a H 0.7690(3) 0.3457(8) 0.4309(4) 0.0672(6) Uiso 1.000000 GR H14b H 0.9158(9) 0.2256(2) 0.4402(4) 0.0672(6) Uiso 1.000000 GR H14c H 0.8937(11) 0.3288(9) 0.49003(9) 0.0672(6) Uiso 1.000000 GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl1 0.0426(2) 0.0443(2) 0.0437(2) 0.01646(16) 0.00958(15) -0.00576(15) N1 0.0271(6) 0.0260(5) 0.0259(5) 0.0013(4) 0.0025(4) -0.0020(4) C8 0.0227(6) 0.0228(6) 0.0289(6) -0.0017(5) 0.0015(5) -0.0041(5) C1 0.0258(6) 0.0326(6) 0.0234(6) 0.0007(5) 0.0011(5) -0.0001(5) C6 0.0267(6) 0.0252(6) 0.0235(6) 0.0004(5) 0.0047(5) 0.0034(5) C9 0.0298(7) 0.0244(6) 0.0287(6) -0.0014(5) 0.0007(5) -0.0024(5) C7 0.0281(6) 0.0244(6) 0.0262(6) -0.0027(5) 0.0033(5) -0.0010(5) C5 0.0276(6) 0.0290(6) 0.0313(6) -0.0033(5) 0.0044(5) -0.0003(5) C13 0.0246(6) 0.0273(6) 0.0282(6) -0.0002(5) -0.0001(5) -0.0034(5) C10 0.0326(7) 0.0292(7) 0.0372(7) 0.0063(5) -0.0024(5) -0.0011(5) C3 0.0341(7) 0.0310(6) 0.0256(6) 0.0087(5) 0.0077(5) 0.0034(5) C2 0.0347(7) 0.0315(7) 0.0243(6) 0.0011(5) 0.0020(5) -0.0032(5) C4 0.0239(6) 0.0359(7) 0.0348(7) 0.0013(5) 0.0042(5) 0.0032(5) C12 0.0338(7) 0.0363(7) 0.0284(6) 0.0028(6) 0.0025(5) -0.0067(5) C18 0.0307(7) 0.0326(7) 0.0270(6) 0.0041(5) -0.0008(5) -0.0037(5) C11 0.0331(7) 0.0345(7) 0.0390(7) 0.0090(6) 0.0039(6) -0.0087(6) C15 0.0448(8) 0.0289(7) 0.0278(6) 0.0035(6) -0.0009(6) -0.0006(5) C17 0.0370(8) 0.0471(9) 0.0409(8) 0.0013(7) -0.0099(6) -0.0038(7) C19 0.0470(9) 0.0453(9) 0.0417(8) 0.0048(7) 0.0052(7) 0.0092(7) C16 0.0582(10) 0.0463(9) 0.0338(7) 0.0074(8) -0.0104(7) 0.0017(7) C14 0.0627(10) 0.0390(8) 0.0340(7) -0.0006(7) 0.0114(7) 0.0009(6) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C3 1.7414(13) . ? N1 C8 1.4249(16) . ? N1 C7 1.2653(16) . ? C8 C9 1.4087(17) . ? C8 C13 1.4075(17) . ? C1 H1 0.9500 . ? C1 C6 1.3975(17) . ? C1 C2 1.3807(18) . ? C6 C7 1.4691(17) . ? C6 C5 1.3905(18) . ? C9 C10 1.3886(18) . ? C9 C15 1.5210(17) . ? C7 H7 0.9500 . ? C5 H5 0.9500 . ? C5 C4 1.3859(18) . ? C13 C12 1.3983(18) . ? C13 C18 1.5210(17) . ? C10 H10 0.9500 . ? C10 C11 1.385(2) . ? C3 C2 1.3876(19) . ? C3 C4 1.3810(19) . ? C2 H2 0.9500 . ? C4 H4 0.9500 . ? C12 H12 0.9500 . ? C12 C11 1.3799(19) . ? C18 H18 1.0000 . ? C18 C17 1.5337(19) . ? C18 C19 1.525(2) . ? C11 H11 0.9500 . ? C15 H15 1.0000 . ? C15 C16 1.530(2) . ? C15 C14 1.529(2) . ? C17 H17a 0.9800 . ? C17 H17b 0.9800 . ? C17 H17c 0.9800 . ? C19 H19a 0.9800 . ? C19 H19b 0.9800 . ? C19 H19c 0.9800 . ? C16 H16a 0.9800 . ? C16 H16b 0.9800 . ? C16 H16c 0.9800 . ? C14 H14a 0.9800 . ? C14 H14b 0.9800 . ? C14 H14c 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C7 N1 C8 119.71(11) . . ? C9 C8 N1 117.41(11) . . ? C13 C8 N1 120.80(11) . . ? C13 C8 C9 121.54(11) . . ? C6 C1 H1 119.82(7) . . ? C2 C1 H1 119.82(8) . . ? C2 C1 C6 120.36(12) . . ? C7 C6 C1 121.77(11) . . ? C5 C6 C1 119.10(11) . . ? C5 C6 C7 119.13(11) . . ? C10 C9 C8 118.43(11) . . ? C15 C9 C8 119.49(11) . . ? C15 C9 C10 122.05(11) . . ? C6 C7 N1 122.40(11) . . ? H7 C7 N1 118.80(7) . . ? H7 C7 C6 118.80(7) . . ? H5 C5 C6 119.42(7) . . ? C4 C5 C6 121.16(12) . . ? C4 C5 H5 119.42(8) . . ? C12 C13 C8 117.42(11) . . ? C18 C13 C8 123.33(11) . . ? C18 C13 C12 119.24(11) . . ? H10 C10 C9 119.55(8) . . ? C11 C10 C9 120.90(12) . . ? C11 C10 H10 119.55(8) . . ? C2 C3 Cl1 119.23(10) . . ? C4 C3 Cl1 119.00(10) . . ? C4 C3 C2 121.77(12) . . ? C3 C2 C1 119.16(12) . . ? H2 C2 C1 120.42(8) . . ? H2 C2 C3 120.42(7) . . ? C3 C4 C5 118.43(12) . . ? H4 C4 C5 120.78(8) . . ? H4 C4 C3 120.78(8) . . ? H12 C12 C13 119.19(7) . . ? C11 C12 C13 121.62(12) . . ? C11 C12 H12 119.19(8) . . ? H18 C18 C13 107.92(7) . . ? C17 C18 C13 110.12(11) . . ? C17 C18 H18 107.92(8) . . ? C19 C18 C13 112.59(12) . . ? C19 C18 H18 107.92(8) . . ? C19 C18 C17 110.22(12) . . ? C12 C11 C10 120.04(12) . . ? H11 C11 C10 119.98(8) . . ? H11 C11 C12 119.98(8) . . ? H15 C15 C9 107.27(7) . . ? C16 C15 C9 113.35(12) . . ? C16 C15 H15 107.27(8) . . ? C14 C15 C9 110.36(11) . . ? C14 C15 H15 107.27(8) . . ? C14 C15 C16 111.01(12) . . ? H17a C17 C18 109.5 . . ? H17b C17 C18 109.5 . . ? H17b C17 H17a 109.5 . . ? H17c C17 C18 109.5 . . ? H17c C17 H17a 109.5 . . ? H17c C17 H17b 109.5 . . ? H19a C19 C18 109.5 . . ? H19b C19 C18 109.5 . . ? H19b C19 H19a 109.5 . . ? H19c C19 C18 109.5 . . ? H19c C19 H19a 109.5 . . ? H19c C19 H19b 109.5 . . ? H16a C16 C15 109.5 . . ? H16b C16 C15 109.5 . . ? H16b C16 H16a 109.5 . . ? H16c C16 C15 109.5 . . ? H16c C16 H16a 109.5 . . ? H16c C16 H16b 109.5 . . ? H14a C14 C15 109.5 . . ? H14b C14 C15 109.5 . . ? H14b C14 H14a 109.5 . . ? H14c C14 C15 109.5 . . ? H14c C14 H14a 109.5 . . ? H14c C14 H14b 109.5 . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -6 0 0 262.87 3.8 -7 0 0 0.8 1 -8 0 0 83.69 3.2 -9 0 0 -0.1 1.5 -3 -1 0 1436.66 15.3 -4 -1 0 413.76 5.7 5 -1 0 49.9 3 -5 -1 0 52.09 1.9 -5 1 0 52.29 3.4 -6 -1 0 55.89 2.4 -7 -1 0 323.17 6.4 -8 -1 0 92.89 3.9 -9 -1 0 79.49 3.9 -9 1 0 84.19 3.3 -2 -2 0 63.59 2.2 -3 -2 0 8.2 1.3 -4 -2 0 272.97 5.1 4 -2 0 270.77 6.5 -4 2 0 276.77 7.1 -5 -2 0 39.4 2.2 5 -2 0 40.5 3 -5 2 0 41.4 3.3 -6 -2 0 17.3 2.1 -7 -2 0 161.68 5.1 -8 -2 0 3.8 1.7 -1 -3 0 3025.2 31.7 1 3 0 3027.2 31.7 -2 -3 0 268.27 5.2 2 3 0 268.17 4.5 3 -3 0 1526.35 21 -3 -3 0 1561.54 18.7 4 -3 0 3 1.7 -4 -3 0 7.7 1.5 -4 3 0 6.3 1.9 -5 -3 0 0.3 1.3 5 -3 0 0.7 1.8 -5 3 0 4.4 2.1 6 -3 0 867.71 15.8 -6 -3 0 850.71 13.2 -6 3 0 867.21 16.8 -7 -3 0 271.87 7 -8 -3 0 29.5 3.1 0 -4 0 17.8 1.3 0 4 0 18.5 1.5 1 -4 0 992 14.6 -1 -4 0 1003.5 12.7 1 4 0 1025.5 12.8 -1 4 0 1006 12.2 -2 -4 0 283.37 5.6 2 -4 0 261.97 6.7 -2 -4 0 269.77 5.8 -2 4 0 263.17 3.9 2 4 0 271.97 5.3 -3 -4 0 14 2 3 -4 0 13.9 2.6 -3 -4 0 14.8 2 3 4 0 12.1 1.5 4 -4 0 1363.76 20.8 -4 -4 0 1324.97 18 -4 4 0 1411.46 22.1 5 -4 0 10.2 2.5 -5 -4 0 10.5 2.1 -5 4 0 7.4 2.5 6 -4 0 110.69 5.6 -6 -4 0 106.29 4.5 -6 4 0 103.19 5.9 -7 -4 0 31.7 3.1 7 -4 0 31.4 3.8 -8 -4 0 0.3 1.8 0 -5 0 2.5 1 0 -5 0 0.7 1.4 0 5 0 0 1.1 0 5 0 -0.5 1 1 -5 0 561.54 10.3 -1 -5 0 545.15 8.6 -1 5 0 554.24 8.4 1 5 0 564.14 8.8 1 5 0 562.24 9.2 2 -5 0 1625.54 23 -2 -5 0 1641.44 20.1 -2 -5 0 1678.83 20.6 2 5 0 1643.44 19.8 -2 5 0 1594.64 18.4 -3 -5 0 60.69 3.3 3 -5 0 45.3 3.5 -3 -5 0 45.2 3 3 5 0 50.79 2.5 -3 5 0 54.39 1.6 -4 -5 0 112.39 4.4 4 -5 0 113.19 5.5 -4 -5 0 111.69 4.5 -4 5 0 114.79 6.1 -5 -5 0 1333.17 19.2 5 -5 0 1336.37 22.3 -5 5 0 1304.67 23.5 6 -5 0 50.09 4.4 -6 -5 0 54.99 3.6 -6 5 0 49.3 5 7 -5 0 13.3 3.2 -7 -5 0 6.6 2.1 -7 5 0 7.6 3.3 -8 -5 0 0.7 2 0 -6 0 171.48 5.4 0 -6 0 166.68 3.6 0 6 0 169.98 4.8 0 6 0 166.58 4.4 -1 -6 0 4.5 1.4 1 -6 0 -0.4 1.5 -1 -6 0 1.8 1.3 1 6 0 3.8 1.5 -1 6 0 2.2 1.2 1 6 0 4.2 1.4 2 -6 0 2.7 1.8 -2 -6 0 5.5 1.6 -2 -6 0 7.7 1.8 -2 6 0 5.7 1.3 2 6 0 6.2 1.7 2 6 0 7.8 1.7 -3 -6 0 155.68 5.3 -3 -6 0 151.98 5 3 -6 0 162.58 6.4 -3 6 0 157.48 6.9 3 6 0 149.69 4.4 -3 6 0 149.49 3.8 4 -6 0 493.35 12.1 -4 -6 0 525.55 10.1 -4 -6 0 505.85 10.3 -4 6 0 490.45 12.9 -4 6 0 500.85 6.9 4 6 0 493.05 7.6 -5 -6 0 353.26 8.9 5 -6 0 352.06 10.7 -5 6 0 330.67 11.4 -6 -6 0 70.69 4.3 6 -6 0 71.49 5.4 -6 6 0 75.09 5.9 7 -6 0 16.6 3.6 -7 -6 0 14.1 2.8 -7 6 0 10 3.7 0 -7 0 0.4 1 0 -7 0 1.6 1.7 0 7 0 -0.9 1.3 0 7 0 0.7 1.2 -1 -7 0 26.6 2.4 -1 -7 0 24.8 2.8 1 -7 0 22.3 2.9 -1 7 0 26.5 2.6 1 7 0 24 2.6 1 7 0 18.2 2.6 -2 -7 0 347.77 7.6 2 -7 0 354.66 9.6 2 7 0 371.56 7.8 -2 7 0 339.77 7.1 -3 -7 0 136.69 5.3 3 -7 0 138.69 6.5 -3 -7 0 125.39 4.9 3 7 0 135.09 4.7 -3 7 0 130.79 4.1 -3 7 0 139.39 7.1 -4 -7 0 122.79 5.1 4 -7 0 123.79 6.3 -4 -7 0 126.59 5.4 -4 7 0 124.89 6.9 -4 7 0 128.39 3.7 4 7 0 131.59 4.4 5 -7 0 11.9 3.1 -5 -7 0 10.4 2.6 -5 -7 0 12.4 2.8 -5 7 0 16.7 1.7 -5 7 0 14.4 3.6 6 -7 0 7.9 3 -6 -7 0 14.5 2.8 -6 7 0 2.7 3.4 -6 7 0 10.8 1.5 7 -7 0 2.9 2.8 -7 -7 0 2 2.3 -7 7 0 -0.5 3.2 0 -8 0 43.4 3.6 0 -8 0 42 2 0 8 0 47.1 3.3 0 8 0 41.7 4 0 8 0 38.1 3 -1 -8 0 40.4 3.3 -1 -8 0 34.8 2.8 1 -8 0 26.8 3.6 -1 8 0 28.4 4 -1 8 0 30.7 2.8 1 8 0 34.3 3.2 1 8 0 33.7 3.6 1 8 0 33.6 3.2 2 -8 0 7.9 2.6 -2 -8 0 4.5 1.8 -2 8 0 3.8 1.6 2 8 0 3.2 2.1 -2 8 0 1.6 2.5 -3 -8 0 52.79 3.9 3 -8 0 55.09 4.7 -3 8 0 49 5.2 3 8 0 47.2 3.9 -3 8 0 57.69 3.4 4 -8 0 64.69 5.4 -4 -8 0 67.69 4.4 4 8 0 68.19 4.1 -4 8 0 75.99 3.5 -4 8 0 65.69 5.7 -5 -8 0 88.09 5.1 5 -8 0 66.19 5.5 -5 -8 0 77.39 4.8 -5 8 0 87.39 6.9 -5 8 0 70.89 3.2 -6 -8 0 0.7 2.3 6 -8 0 1 2.8 -6 8 0 2.1 1.4 -6 8 0 1.1 3 0 -9 0 -0.2 2.2 0 9 0 0.3 2.3 0 9 0 -2.9 1.6 0 9 0 -1.7 1.6 -1 -9 0 323.47 6.9 1 -9 0 313.27 9.7 -1 9 0 325.87 10.4 1 9 0 319.57 8.4 -1 9 0 310.27 8.3 1 9 0 316.57 8.6 2 -9 0 251.67 9.1 -2 -9 0 286.17 7.1 -2 9 0 284.57 7.6 2 9 0 259.37 7.6 -2 9 0 286.17 10.2 -3 -9 0 124.69 5.2 3 -9 0 118.39 6.8 -3 9 0 126.29 7.3 -3 9 0 121.79 4.9 3 9 0 119.99 5.3 4 -9 0 17.1 3.7 -4 -9 0 18.7 3 -4 9 0 21 4.1 4 9 0 21 3.1 -4 9 0 17.4 2.5 5 -9 0 4.1 2.9 -5 -9 0 -1.6 2.1 -5 9 0 5 1.8 -5 9 0 4 3.1 -6 -9 0 -2.4 2.1 6 -9 0 2.5 2.9 -6 9 0 1 1.5 -6 9 0 1 3.2 0 -10 0 94.59 5.8 0 10 0 92.39 5.2 0 10 0 85.49 6.2 0 10 0 85.39 4.8 -1 -10 0 -0.4 1.9 1 -10 0 9.9 2.9 -1 10 0 6.4 2.5 1 10 0 1.2 2.3 -1 10 0 3.7 2.7 2 -10 0 101.69 6.3 -2 -10 0 94.59 4.5 -2 10 0 94.79 4.9 2 10 0 87.39 5.2 -2 10 0 104.49 6.8 -3 -10 0 67.59 4.2 3 -10 0 63.29 5.4 3 10 0 58.59 4.8 -3 10 0 61.99 5.9 -3 10 0 58.79 4 4 -10 0 1.4 2.6 -4 -10 0 -1 1.9 -4 10 0 6.8 3.7 4 10 0 5.7 3.1 -4 10 0 4.6 2 -5 -10 0 41.2 4.3 5 -10 0 36.7 5 -5 10 0 40.7 3.3 -5 10 0 42.1 5.6 0 11 0 3.3 2.6 1 -11 0 -1 2.3 -1 11 0 0.5 2.5 1 11 0 -0.6 2.4 -1 11 0 2.7 2.2 -2 -11 0 35.3 3.4 2 -11 0 47.9 5.1 -2 11 0 41.3 5.4 2 11 0 38.4 4.8 -2 11 0 47 4 -3 -11 0 -4.3 1.7 3 -11 0 4 2.9 -3 11 0 -2.4 3 3 11 0 5.8 3.8 -3 11 0 -1.9 1.7 -4 -11 0 14 3 4 -11 0 16.2 4 -4 11 0 22 4.8 4 11 0 21.9 4.1 -4 11 0 25 3.2 1 -12 0 2 2.9 1 12 0 -0.7 3 -1 12 0 6 3.5 -1 12 0 2 2.3 2 -12 0 0.5 2.9 2 12 0 3.8 3.7 -2 12 0 4.2 3.1 -2 12 0 7.4 2.6 -9 0 1 185.18 5.2 -8 0 1 -1.6 1.2 -7 0 1 335.47 5.4 -6 0 -1 -0.4 0.7 -7 0 -1 478.45 7.4 -8 0 -1 -0.7 1.2 -9 -1 1 10.8 2.2 -8 -1 1 136.39 4.4 -7 -1 1 81.89 3.2 -6 -1 1 225.68 4.5 5 -1 -1 47.7 2.9 -5 -1 1 48.7 1.9 -5 1 1 48.1 3.3 -4 -1 1 0.5 0.6 -3 -1 1 166.38 2.8 -3 -1 -1 1 0.6 -4 -1 -1 921.01 10.9 -5 -1 -1 19.3 1.4 5 -1 1 15.8 2.1 -5 1 -1 21.6 2.5 -6 -1 -1 93.79 3.1 -7 -1 -1 94.39 3.6 -8 -1 -1 53.29 3.1 -8 1 -1 55.39 2.4 -8 -2 1 47.5 3.3 -7 -2 1 11.9 1.9 -6 -2 1 7.2 1.5 -5 -2 1 -1.5 0.8 5 -2 -1 -2.6 1.3 -5 2 1 -2.1 1.5 -4 -2 1 12.4 1.4 4 -2 -1 16 2.1 -3 -2 1 57.09 2.1 -2 -2 1 2400.36 25.6 -2 -2 -1 897.71 11.1 -3 -2 -1 524.15 7.6 4 -2 1 88.99 3.8 -4 -2 -1 90.29 2.8 -4 2 -1 88.99 4.1 5 -2 1 35.5 2.9 -5 -2 -1 34.9 2.1 -5 2 -1 36.6 3.3 -6 -2 -1 10 1.7 -7 -2 -1 251.47 6.2 -8 -2 -1 1.1 1.6 -8 -3 1 4.4 1.9 -7 -3 1 12.6 2.2 6 -3 -1 151.58 6.2 -6 -3 1 148.79 4.9 -6 3 1 139.99 6.7 5 -3 -1 294.87 7.9 -5 -3 1 281.37 6.2 -5 3 1 279.97 8.4 4 -3 -1 322.87 7.7 -4 -3 1 312.57 6.3 -3 -3 1 451.95 7.5 3 -3 -1 464.15 9 -2 -3 1 1124.09 14.1 2 3 -1 1133.29 13 -1 -3 1 546.25 7.6 1 3 -1 564.24 7.6 0 -3 1 2562.24 26.1 0 -3 -1 2496.85 26 1 3 1 9.3 1.5 -2 -3 -1 8.9 1.4 2 3 1 11.4 1.3 3 -3 1 1556.44 21.3 -3 -3 -1 1562.94 18.8 -4 -3 -1 153.28 4.3 4 -3 1 151.98 5.4 -4 3 -1 165.78 5.9 -5 -3 -1 46.2 2.8 5 -3 1 42.9 3.5 -5 3 -1 41.6 3.8 6 -3 1 379.56 9.8 -6 -3 -1 365.56 8 -6 3 -1 393.26 10.6 -7 -3 -1 25.9 2.8 -8 -3 -1 10.1 2.3 -8 -4 1 12.6 2.6 -7 -4 1 27.8 2.9 6 -4 -1 58.59 4.4 -6 -4 1 51.89 3.4 -6 4 1 57.19 4.9 5 -4 -1 500.85 11.4 -5 -4 1 487.55 9.4 -5 4 1 502.65 12.1 4 -4 -1 30.9 3.2 -4 -4 1 27.4 2.7 -3 -4 1 18.8 2.2 -3 -4 1 18.5 2.1 3 -4 -1 12.8 2.3 3 4 -1 19.7 1.8 2 -4 -1 1793.82 24.1 -2 -4 1 1858.51 21.2 -2 -4 1 1788.62 21.5 2 4 -1 1821.82 20.7 -2 4 1 1825.62 18.9 -1 -4 1 521.05 7.8 1 -4 -1 543.05 9.5 1 4 -1 524.25 7.9 -1 4 1 529.65 7.4 0 -4 -1 28.2 1.4 0 -4 1 27 1.4 0 4 1 31.4 1.8 0 4 -1 27.8 1.7 -1 -4 -1 682.33 9.5 1 -4 1 670.63 11 1 4 1 686.73 9.5 -1 4 -1 672.23 9 2 -4 1 607.64 11 -2 -4 -1 612.84 9.5 -2 -4 -1 624.24 9.3 2 4 1 609.74 8.8 -2 4 -1 631.64 7.6 -3 -4 -1 2013.3 23.4 -3 -4 -1 1975.5 23.9 3 -4 1 2001.5 26.9 -3 4 -1 1992 27.9 3 4 1 1988.6 21.7 4 -4 1 7 2.3 -4 -4 -1 8.4 1.9 -4 4 -1 11.4 2.7 5 -4 1 28.8 3.4 -5 -4 -1 31.3 2.8 -5 4 -1 32.1 3.9 6 -4 1 26 3.6 -6 -4 -1 29.7 3 -6 4 -1 25.8 4 -7 -4 -1 92.39 4.6 -8 -4 -1 60.19 4 -8 -5 1 2.2 2.1 -7 -5 1 -0.7 1.7 7 -5 -1 -0.3 2.1 -7 5 1 0.9 2.5 -6 -5 1 0.4 1.6 6 -5 -1 -1.4 1.8 -6 5 1 1.2 2.3 -5 -5 1 307.87 7.6 5 -5 -1 290.77 9 -5 5 1 304.67 9.9 4 -5 -1 187.38 6.8 -4 -5 1 192.58 5.6 -4 -5 1 186.78 5.7 3 -5 -1 79.39 4.5 -3 -5 1 91.59 3.8 -3 -5 1 81.69 3.7 3 5 -1 86.99 3.1 -3 5 1 83.79 2 -2 -5 1 616.54 9.7 2 -5 -1 602.94 11.7 -2 -5 1 603.34 10 2 5 -1 593.34 9.3 -2 5 1 596.64 8.3 1 -5 -1 56.19 3.2 -1 -5 1 54.69 2.6 1 5 -1 58.39 2.7 -1 5 1 56.59 2.5 1 5 -1 48.7 2.8 0 -5 1 596.74 10.3 0 -5 -1 622.44 10.5 0 -5 1 607.54 8.1 0 -5 -1 612.54 8.1 0 5 1 622.94 9.1 0 5 -1 616.34 9.1 0 5 -1 603.74 9.5 0 5 1 612.54 9.5 1 -5 1 145.39 4.9 -1 -5 -1 135.09 3.9 1 5 1 140.69 4.2 -1 5 -1 145.69 3.8 1 5 1 141.89 4 -2 -5 -1 23.5 2.5 -2 -5 -1 23.4 2.7 2 -5 1 24.1 3.1 -2 5 -1 29.1 1.8 -2 5 -1 36.1 3.6 2 5 1 29.6 2.4 3 -5 1 17.9 2.9 -3 -5 -1 18.5 2.3 -3 -5 -1 20.9 2.3 3 5 1 21.7 2.1 -3 5 -1 23.2 1.3 -3 5 -1 32.9 3.7 -4 -5 -1 86.59 4 4 -5 1 95.69 5.2 -4 -5 -1 88.99 4.1 -4 5 -1 90.99 5.6 -5 -5 -1 530.65 10.7 5 -5 1 530.35 12.6 -5 5 -1 555.84 13.9 -6 -5 -1 81.99 4.3 6 -5 1 74.49 5.1 -6 5 -1 74.39 5.4 -7 -5 -1 -0.5 1.8 7 -5 1 2.2 2.4 -7 5 -1 1.8 2.7 -8 -5 -1 10.9 2.6 -7 -6 1 7.2 2.4 7 -6 -1 7 2.9 -7 6 1 6.9 3.4 6 -6 -1 87.29 5.6 -6 -6 1 94.29 4.9 -6 6 1 93.29 6.4 5 -6 -1 -5.1 2.1 -5 -6 1 -2.6 2.1 -5 6 1 1.3 2.9 4 -6 -1 1640.24 25.9 -4 -6 1 1709.63 22.3 -4 -6 1 1699.93 23 4 6 -1 1656.53 19 -4 6 1 1686.53 27.7 -4 6 1 1674.83 18.2 -3 -6 1 7.5 1.8 -3 -6 1 8.8 1.9 3 -6 -1 8.9 2.2 3 6 -1 7.1 1.7 -3 6 1 8.4 1.3 -2 -6 1 157.38 4.7 2 -6 -1 159.98 5.8 -2 -6 1 164.58 5 2 6 -1 160.28 4.7 2 6 -1 166.28 5 -2 6 1 163.78 4.2 1 -6 -1 110.39 4.8 -1 -6 1 108.39 3.6 -1 -6 1 104.09 3.9 1 6 -1 102.49 3.7 1 6 -1 109.49 4.3 1 6 -1 109.69 4 -1 6 1 101.39 3.6 0 -6 -1 168.08 3.6 0 -6 1 162.28 5.1 0 -6 1 165.08 3.6 0 -6 -1 165.58 5.2 0 6 1 167.68 4.8 0 6 -1 165.58 4.5 0 6 -1 164.98 4.7 0 6 1 167.28 4.4 -1 -6 -1 142.29 4.5 -1 -6 -1 141.59 4.1 1 -6 1 152.78 5.4 -1 6 -1 146.19 4.3 -1 6 -1 142.59 5.7 1 6 1 148.19 4.7 1 6 1 141.79 4.4 -2 -6 -1 468.55 8.6 -2 -6 -1 451.15 8.8 2 -6 1 468.25 10.6 -2 6 -1 466.55 11.3 2 6 1 479.95 9 2 6 1 468.45 8.9 -2 6 -1 467.35 7.9 2 6 1 461.75 8.5 -3 -6 -1 898.01 14.2 -3 -6 -1 854.11 13.4 3 -6 1 893.11 16.4 -3 6 -1 866.31 11.6 3 6 1 856.11 12.4 -3 6 -1 837.12 16.9 -4 -6 -1 426.66 9.4 4 -6 1 396.86 10.9 -4 -6 -1 430.06 9.1 -4 6 -1 415.36 11.9 -4 6 -1 418.56 6.3 4 6 1 418.86 6.9 5 -6 1 844.62 17.3 -5 -6 -1 856.81 14.9 -5 6 -1 841.82 9.8 -5 6 -1 803.12 18.2 6 -6 1 -1.9 2.1 -6 -6 -1 -0.5 1.8 -6 6 -1 -2.1 2.5 7 -6 1 121.99 7 -7 -6 -1 114.39 5.6 -7 6 -1 121.59 7.6 -7 -7 1 5.4 2.5 7 -7 -1 4.7 2.8 -7 7 1 4 3.3 -6 -7 1 560.34 12.4 6 -7 -1 555.64 14.6 -6 7 1 537.95 15.6 5 -7 -1 1 2.3 -5 -7 1 7 2.4 -5 -7 1 5.1 2.3 -5 7 1 5.5 1.2 -5 7 1 4.9 2.8 -4 -7 1 37.9 3.5 4 -7 -1 35.6 4.2 -4 -7 1 33.4 3.4 -4 7 1 35.6 2.2 -4 7 1 29.5 4.2 4 7 -1 41.4 3.3 -3 -7 1 395.06 8.6 -3 -7 1 402.46 9 3 -7 -1 404.36 10.7 -3 7 1 398.66 7.4 3 7 -1 393.26 7.9 2 -7 -1 280.37 8.3 -2 -7 1 268.57 6.6 2 7 -1 279.27 6.6 -2 7 1 262.77 6.2 -1 -7 1 286.67 6.2 -1 -7 1 289.07 7.1 1 -7 -1 288.27 8 -1 7 1 290.17 6.6 1 7 -1 286.97 7.6 1 7 -1 282.67 7 1 7 -1 291.27 6.8 0 -7 1 373.06 8.9 0 -7 -1 365.16 8.7 0 -7 1 372.46 6 0 -7 -1 374.46 5.9 0 7 -1 373.96 7.6 0 7 -1 371.06 9.4 0 7 1 378.56 8 0 7 -1 365.26 8 0 7 1 376.06 7.6 -1 -7 -1 360.96 7.1 -1 -7 -1 366.26 8.1 1 -7 1 354.56 9.2 -1 7 -1 362.76 7.6 -1 7 -1 352.86 9.8 1 7 1 365.96 8.1 1 7 1 359.06 7.7 -2 -7 -1 49.4 3.4 2 -7 1 54.69 4.1 2 7 1 46 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3 7 4 2.1 2.1 -3 7 -4 4.5 1.5 -3 7 -4 6.8 2.9 -4 -7 -4 0.7 1.7 4 -7 4 0.5 2.1 -4 -7 -4 0.5 1.7 -4 7 -4 0.3 1.2 4 7 4 0.2 1.9 -4 7 -4 -1.5 2.2 -5 -7 -4 65.39 4.3 5 -7 4 58.09 5.3 -5 -7 -4 59.89 4.2 -5 7 -4 60.69 3 -5 7 -4 66.59 6.1 6 -7 4 45 4.7 -6 -7 -4 49.1 4.2 -6 7 -4 43.1 2.6 -6 7 -4 39.9 5.3 -7 -7 -4 59.99 4.7 7 -7 4 55.49 5.7 -7 7 -4 50.59 5.7 -7 7 -4 58.39 2.9 -6 -8 4 184.88 7.5 6 -8 -4 177.18 8.6 -6 8 4 185.78 4.7 -6 8 4 169.48 9.3 5 -8 -4 32.8 4.7 -5 -8 4 36.2 3.9 -5 -8 4 34.3 3.6 -5 8 4 33.5 2.5 4 -8 -4 7.2 2.7 -4 -8 4 4.8 2.2 4 8 -4 8.7 2.3 -4 8 4 7.6 1.8 -3 -8 4 154.58 5.5 3 -8 -4 160.98 7.1 3 8 -4 163.38 5.6 -3 8 4 160.28 5 2 -8 -4 83.19 5.3 -2 -8 4 81.09 4 -2 8 4 82.29 3.9 2 8 -4 81.49 4.2 1 -8 -4 64.09 4.6 -1 -8 4 66.79 4.1 -1 -8 4 64.49 3.3 1 8 -4 63.49 4 -1 8 4 60.59 3.7 1 8 -4 58.99 3.7 1 8 -4 55.69 4.4 0 -8 4 57.19 2.5 0 -8 -4 51.69 3.9 0 -8 4 51.49 3.9 0 8 4 50.29 3.4 0 8 -4 57.09 3.6 0 8 -4 55.69 3.4 0 8 -4 61.59 4.4 0 8 4 52.29 3.2 1 -8 4 37.9 3.9 -1 -8 -4 36.2 3.4 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-1 8 -5 81.69 5.6 1 8 5 80.89 4.3 1 8 5 95.59 4.6 2 -8 5 1.4 2.2 -2 -8 -5 3.7 1.8 -2 8 -5 3.6 1.7 2 8 5 2.6 2.1 -2 8 -5 4.4 2.7 3 -8 5 1.9 2.3 -3 -8 -5 4.2 1.9 -3 8 -5 2.4 1.6 -3 8 -5 -0.3 2.3 3 8 5 3 2.3 -4 -8 -5 64.19 4.2 4 -8 5 75.29 5.8 -4 8 -5 79.39 6.4 4 8 5 70.39 4.3 -4 8 -5 71.09 3.8 5 -8 5 2.6 2.8 -5 -8 -5 1.6 2 -5 8 -5 0.7 1.5 -5 8 -5 -0.6 2.8 6 -8 5 9.1 3.7 -6 8 -5 5.8 3.3 -6 8 -5 4.3 1.7 -6 -9 5 3.1 2.7 6 -9 -5 -2.2 2.5 -6 9 5 3.9 3.5 -6 9 5 -1.8 1.5 -5 -9 5 76.29 4.9 5 -9 -5 71.19 6 -5 9 5 78.09 3.7 -4 -9 5 40.1 3.7 4 -9 -5 43.7 4.7 -4 9 5 39.2 3 4 9 -5 39.2 3.9 3 -9 -5 10.2 3.2 -3 -9 5 14.6 2.6 3 9 -5 16 2.9 -3 9 5 13.5 2.3 2 -9 -5 8.8 2.7 -2 -9 5 8.6 2 -2 9 5 9.1 2.1 2 9 -5 8.2 2.5 -1 -9 5 2.7 1.7 1 -9 -5 -2.1 1.8 -1 9 5 3.9 2 1 9 -5 2.7 2 0 -9 5 165.28 6.9 0 -9 -5 156.58 6.7 0 9 -5 172.98 6.3 0 9 -5 157.18 7.3 0 9 5 156.88 6.1 0 9 5 164.98 5.8 0 9 -5 169.58 6 1 -9 5 31.7 4.1 -1 -9 -5 25.9 2.6 -1 9 -5 30.3 3.1 -1 9 -5 36.4 4.7 1 9 5 27.7 3.3 1 9 5 28.6 3.2 1 9 5 26.7 3.2 2 -9 5 -1.1 2.1 -2 -9 -5 -1 1.6 2 9 5 1.2 2.3 -2 9 -5 -1.2 2.4 -2 9 -5 2.2 1.8 -3 -9 -5 190.28 6.5 3 -9 5 188.38 8.5 3 9 5 185.88 6.8 -3 9 -5 177.38 9 -3 9 -5 184.38 6.2 -4 -9 -5 27.6 3.4 4 -9 5 30.6 4.3 4 9 5 28.3 4.2 -4 9 -5 28.3 3.1 -4 9 -5 23.6 4.7 5 -9 5 7.4 3.2 -5 -9 -5 9 2.7 -5 9 -5 9.5 2.1 -5 9 -5 9.5 3.7 5 -10 -5 12.2 3.9 -5 -10 5 18.1 3.2 -5 10 5 22 2.7 -5 10 5 26.6 5 -4 -10 5 36.3 3.7 4 -10 -5 31.1 4.4 4 10 -5 26 3.9 -4 10 5 27.5 3.1 -3 -10 5 1.1 1.9 3 -10 -5 0.5 2.5 3 10 -5 1.5 2.8 -3 10 5 2 1.8 -2 -10 5 87.59 4.3 2 -10 -5 93.99 6.1 2 10 -5 86.89 5.2 -2 10 5 75.29 4.6 1 -10 -5 22 3.4 -1 -10 5 17.5 2.7 1 10 -5 24.5 3.6 -1 10 5 25.9 3.4 0 -10 -5 32.9 4.2 0 -10 5 26.4 3.8 0 10 5 21.2 3.3 0 10 -5 26.4 3.4 0 10 -5 31.2 3.4 0 10 -5 25.7 4.1 -1 -10 -5 16.9 2.6 1 -10 5 29.2 4.3 -1 10 -5 25.7 3.4 1 10 5 29.8 3.8 -1 10 -5 27.8 4.5 -2 -10 -5 20.9 2.9 2 -10 5 21.5 4 2 10 5 25.2 3.8 -2 10 -5 23.1 3.1 -2 10 -5 12.7 3.9 3 -10 5 87.29 6.5 -3 -10 -5 87.99 4.7 3 10 5 85.59 5.6 -3 10 -5 85.79 4.8 -3 10 -5 94.99 7.3 4 -10 5 18.8 4.1 -4 -10 -5 19 3.3 4 10 5 22.6 4.2 -4 10 -5 24.1 3 -4 10 -5 25.3 5 4 -11 -5 35.4 4.9 -4 -11 5 31.5 3.9 -4 11 5 38.2 3.7 -4 11 5 36.8 5.5 4 11 -5 35.5 4.6 -3 -11 5 28 3.6 3 -11 -5 35.4 4.6 3 11 -5 24.1 4.3 -3 11 5 28.8 3.4 2 -11 -5 -0.4 2.1 -2 -11 5 -6.5 2.3 -2 11 5 1.3 1.9 2 11 -5 -2.1 2.7 1 -11 -5 -4.3 2 1 11 -5 -4.4 2.4 -1 11 5 1.1 2.1 0 11 5 46.8 4.8 0 11 -5 39.7 4.3 0 11 -5 51.89 4.6 1 -11 5 1.7 2.5 -1 11 -5 3.1 3 -1 11 -5 0.6 2.1 1 11 5 -3.7 2.3 2 -11 5 37.6 4.9 -2 -11 -5 24.5 2.9 -2 11 -5 25.7 3.3 -2 11 -5 26.4 4.9 2 11 5 33.2 4.7 3 -11 5 55.59 5.5 -3 -11 -5 61.19 4.3 -3 11 -5 54.39 4.3 3 11 5 54.49 5.7 -3 11 -5 52.69 5.9 1 -12 -5 9.4 3.2 1 12 -5 9.3 3.5 -1 12 5 6 2.6 0 12 -5 23.3 4 1 -12 5 14.8 3.6 -1 12 -5 11.1 3.8 1 12 5 13.4 3.7 -1 12 -5 14.5 3.1 -9 0 6 -1 1.2 -8 0 6 183.88 4.2 -7 0 6 -2.6 0.7 1 0 6 0.2 0.5 -2 0 -6 7.7 1 -3 0 -6 -0.7 0.6 -4 0 -6 3943.71 41.7 -4 0 -6 4044.9 46.7 -5 0 -6 0.7 1 -6 0 -6 3 1.3 -7 0 -6 -0.1 1.4 -8 0 -6 33.5 2.9 -9 -1 6 38.9 3 -8 -1 6 -1.1 1.3 -7 -1 6 74.59 2.9 -6 -1 6 72.59 2.6 5 -1 -6 407.26 8.4 -5 -1 6 414.46 6.1 -4 -1 6 118.49 2.7 4 -1 -6 119.59 4 -3 -1 6 42.3 1.6 -2 -1 6 3.1 0.8 1 1 6 292.67 4.6 -2 -1 -6 1884.01 21.6 2 1 6 1988 20.1 -2 1 -6 1975.5 21.1 -3 -1 -6 1170.58 14.5 -3 1 -6 1166.48 13.6 -3 1 -6 1180.98 17 -4 -1 -6 1.6 1 -4 1 -6 4.2 0.9 -4 1 -6 4.7 1.6 -5 -1 -6 34.4 2.4 -5 1 -6 36.8 3.2 -5 1 -6 35.1 1.9 -6 -1 -6 43.9 2.8 -6 1 -6 44.1 2.3 -7 -1 -6 49.6 3.2 -7 1 -6 45.6 2.7 -8 -1 -6 8.2 2.1 -8 1 -6 11.8 2 -8 -2 6 34.3 2.9 -7 -2 6 92.39 3.8 -6 -2 6 359.46 6.9 -5 -2 6 565.54 8.8 5 -2 -6 570.04 11 4 -2 -6 311.17 7.2 -4 -2 6 311.87 5.8 3 -2 -6 617.54 10.6 -3 -2 6 612.74 8.7 -2 -2 6 140.39 3.5 2 2 -6 142.29 2.5 -1 2 6 -0.6 0.7 1 2 -6 -0.8 0.7 -1 2 6 -1 0.7 0 -2 -6 86.39 2.3 0 -2 6 84.09 2.4 -1 -2 -6 2.5 1 -1 2 -6 2.8 0.9 1 2 6 3.6 0.9 -2 -2 -6 345.77 6.2 2 -2 6 345.37 7.4 2 2 6 336.57 5.2 -2 2 -6 337.37 5.3 -2 2 -6 335.77 7.5 -3 -2 -6 1445.16 18 3 -2 6 1476.95 20.7 -3 2 -6 1484.95 21.1 -3 2 -6 1487.55 16.4 -4 -2 -6 368.26 7 4 -2 6 380.96 8.8 -4 2 -6 375.06 9.1 -4 2 -6 366.16 5.6 -5 -2 -6 3.8 1.4 5 -2 6 6 2.3 -5 2 -6 5.6 1.1 -5 2 -6 5.3 2.1 -6 -2 -6 0.9 1.4 -6 2 -6 1.8 1 -7 -2 -6 6.5 2 -7 2 -6 7.3 1.5 -8 -2 -6 4 1.9 -8 2 -6 6.3 1.6 -8 -3 6 0 1.6 -7 -3 6 12.3 2.2 6 -3 -6 93.59 4.8 -6 -3 6 91.59 3.9 5 -3 -6 12.6 2.4 -5 -3 6 10.4 1.7 -4 -3 6 31.8 2.3 4 -3 -6 39.5 3.2 -3 -3 6 2.5 1 3 -3 -6 3.2 1.5 -2 -3 6 1374.76 16.9 -2 -3 6 1395.46 16.5 2 -3 -6 1366.06 19 -2 3 6 1367.86 14.6 2 3 -6 1384.06 15.8 -1 -3 6 1364.86 16.2 1 3 -6 1402.86 16.3 -1 3 6 1372.16 15.8 0 -3 -6 227.78 4 0 -3 6 230.98 4.2 0 3 -6 226.48 4.6 0 3 6 228.78 4.7 0 3 -6 236.48 4.5 -1 -3 -6 -1.3 0.9 1 -3 6 0.3 1.2 -1 3 -6 -1.8 1.1 1 3 6 0 0.7 2 -3 6 59.19 3.3 -2 -3 -6 59.19 2.8 2 3 6 57.99 2.4 -2 3 -6 57.59 2.2 -2 3 -6 57.59 3.5 -3 -3 -6 4.5 1.4 3 -3 6 4.5 1.8 -3 -3 -6 6.1 1.3 3 3 6 3.8 0.9 -3 3 -6 4.5 0.9 -3 3 -6 7 2 4 -3 6 160.98 5.9 -4 -3 -6 156.38 4.7 -4 3 -6 160.18 3.3 -4 3 -6 150.68 6.2 5 -3 6 208.18 7.2 -5 -3 -6 207.28 5.8 -5 3 -6 202.38 4 -5 3 -6 198.28 7.4 6 -3 6 -1 2.1 -6 -3 -6 -1.5 1.4 -6 3 -6 2.9 2.2 -6 3 -6 -1 0.8 -7 -3 -6 16 2.5 -7 3 -6 17 1.8 -8 -3 -6 16.2 2.8 -8 3 -6 15.9 2 -8 -4 6 180.78 6.5 -7 -4 6 19.5 2.7 -6 -4 6 1.2 1.5 6 -4 -6 4.4 2.1 5 -4 -6 93.09 5 -5 -4 6 96.69 4 4 -4 -6 380.96 9.3 -4 -4 6 379.76 7.7 3 -4 -6 351.06 8.4 -3 -4 6 358.76 7.1 -3 -4 6 347.17 6.7 3 4 -6 356.26 5.4 -2 -4 6 578.94 9 -2 -4 6 576.34 9.4 2 -4 -6 558.44 10.7 2 4 -6 569.54 8.5 -2 4 6 581.34 7.6 1 -4 -6 6.6 1.7 -1 -4 6 6.2 1.3 1 4 -6 6.4 1.5 -1 4 6 8.7 1.4 0 -4 -6 2.7 0.9 0 -4 6 1.4 1.3 0 -4 -6 3 1.2 0 -4 6 1.8 1.1 0 4 -6 3.8 1.5 0 4 6 3.2 1.1 0 4 -6 1.8 1 0 4 -6 1.2 1.1 0 4 6 2 1 0 4 6 2.3 1 1 -4 6 400.96 8.5 -1 -4 -6 407.56 7 -1 4 -6 405.26 7 1 4 6 406.56 7.1 1 4 6 408.96 7.3 -1 4 -6 400.96 8.9 -2 -4 -6 334.87 6.5 2 -4 6 332.77 8 -2 -4 -6 327.07 6.8 2 4 6 325.37 6.2 -2 4 -6 334.07 8.5 -2 4 -6 326.37 5.9 -3 -4 -6 18.9 2.4 -3 -4 -6 22.3 2.3 3 -4 6 21.4 2.7 -3 4 -6 24.3 1.7 -3 4 -6 18.8 2.9 3 4 6 22.1 1.9 -4 -4 -6 262.77 6.6 4 -4 6 257.87 7.9 -4 4 -6 265.07 4.8 -4 4 -6 267.37 8.5 -5 -4 -6 176.68 5.9 5 -4 6 170.08 7 -5 4 -6 181.58 3.9 -5 4 -6 181.58 7.5 6 -4 6 2.5 2.5 -6 -4 -6 -1.2 1.5 -6 4 -6 -0.5 0.9 -6 4 -6 -0.5 2.4 7 -4 6 12.8 3.4 -7 -4 -6 9.2 2.4 -7 4 -6 16.3 1.7 -8 -4 -6 155.38 6.6 -8 4 -6 168.78 4.6 -8 -5 6 30.2 3.6 -7 -5 6 36 3.5 7 -5 -6 36.9 4.2 6 -5 -6 36.6 3.7 -6 -5 6 35.9 3.1 -5 -5 6 38 3.1 5 -5 -6 45.5 3.8 -4 -5 6 125.59 4.8 -4 -5 6 127.39 4.5 4 -5 -6 127.19 5.7 -3 -5 6 -2.6 1.1 3 -5 -6 -0.9 1.5 -3 -5 6 1.4 1.3 -3 5 6 0.2 0.7 3 5 -6 -1.3 1 2 -5 -6 1.3 1.5 -2 -5 6 -0.9 1.2 -2 -5 6 -0.8 1.1 -2 5 6 0.1 0.9 2 5 -6 -0.7 1.1 -1 -5 6 1977.1 23.3 -1 -5 6 2033.4 25.6 1 -5 -6 2039.5 26.9 1 5 -6 2017.4 23.7 1 5 -6 2028.8 24.2 -1 5 6 1951.1 23.3 1 5 -6 2015.5 25.9 0 -5 -6 214.38 5.8 0 -5 -6 207.78 4 0 -5 6 200.48 4.3 0 -5 6 206.28 5.8 0 5 -6 202.98 5.2 0 5 6 204.58 4.9 0 5 -6 206.68 4.9 0 5 6 203.98 5.1 0 5 6 203.68 5.1 0 5 -6 202.78 6 -1 -5 -6 205.08 4.8 -1 -5 -6 192.18 5.3 1 -5 6 193.48 6 1 5 6 206.58 5.2 1 5 6 209.88 5 -1 5 -6 198.58 4.6 -1 5 -6 207.28 6.5 -1 5 -6 194.78 4.9 2 -5 6 49.3 3.5 -2 -5 -6 52.09 3 -2 -5 -6 49.2 2.8 -2 5 -6 45.6 2.5 2 5 6 48.7 2.7 2 5 6 52.09 3 -2 5 -6 47 3.7 3 -5 6 15.2 2.7 -3 -5 -6 16.7 2.4 -3 -5 -6 17.4 2.4 -3 5 -6 16 1.7 -3 5 -6 19.5 3.2 3 5 6 15.1 2.1 -4 -5 -6 217.08 6.3 4 -5 6 216.78 7.6 -4 -5 -6 226.38 6.1 -4 5 -6 212.08 8.1 4 5 6 226.28 4.2 -4 5 -6 214.98 4.8 -5 -5 -6 385.36 9.2 5 -5 6 366.46 10.7 -5 5 -6 376.96 11.4 -5 5 -6 386.86 6.7 6 -5 6 154.58 7.5 -6 -5 -6 151.58 6 -6 5 -6 166.28 8.1 -6 5 -6 152.48 4.1 7 -5 6 28.5 4.6 -7 -5 -6 21.6 3.2 -7 5 -6 24.4 2.1 -7 5 -6 27.9 4.6 -7 -6 6 86.29 5 7 -6 -6 82.69 5.9 -7 6 6 78.79 6.6 -6 -6 6 17.9 2.8 6 -6 -6 7.7 2.8 5 -6 -6 17.3 3.3 -5 -6 6 14.9 2.5 4 -6 -6 285.47 9 -4 -6 6 284.17 7.2 -4 -6 6 288.27 7.5 4 6 -6 279.97 5.1 -4 6 6 281.17 4.7 -3 -6 6 47.4 3.3 -3 -6 6 31.9 2.8 3 -6 -6 38.6 3.7 3 6 -6 36.1 2.7 -3 6 6 36.5 2.1 -2 -6 6 0.4 1.3 2 -6 -6 1.3 1.6 -2 -6 6 -0.2 1.2 -2 6 6 -0.6 1 2 6 -6 2.5 1.5 1 -6 -6 577.34 11.7 -1 -6 6 571.64 10.6 -1 -6 6 590.74 9.5 1 6 -6 570.94 10.2 1 6 -6 579.54 9.8 -1 6 6 578.84 9.7 1 6 -6 588.44 11.1 0 -6 6 4.3 1.7 0 -6 -6 4.4 1.8 0 -6 -6 3.9 1.1 0 -6 6 6.2 1.2 0 6 6 4.2 1.6 0 6 -6 4 1.5 0 6 -6 3.8 1.3 0 6 6 4.2 1.3 0 6 -6 2.2 1.7 -1 -6 -6 279.17 7 -1 -6 -6 276.17 5.9 1 -6 6 275.77 7.7 -1 6 -6 261.27 6.3 1 6 6 262.17 6.2 -1 6 -6 281.07 8.2 1 6 6 272.77 6.6 -1 6 -6 274.27 5.9 2 -6 6 349.67 9.4 -2 -6 -6 349.37 7.5 2 6 6 346.87 7.4 -2 6 -6 333.27 9.8 -2 6 -6 348.07 7.1 3 -6 6 188.28 7.2 -3 -6 -6 177.88 5.6 -3 -6 -6 183.58 5.9 -3 6 -6 186.08 7.5 -3 6 -6 173.98 4.7 3 6 6 175.48 5.1 -4 -6 -6 72.49 4.4 4 -6 6 68.89 4.9 -4 -6 -6 71.99 4.1 -4 6 -6 72.79 3.1 -4 6 -6 73.59 5.4 4 6 6 77.99 3.4 5 -6 6 71.79 5.4 -5 -6 -6 69.19 4.4 -5 6 -6 73.89 5.9 -5 6 -6 66.99 3 -6 -6 -6 43.9 3.9 6 -6 6 52.09 5.1 -6 6 -6 44.9 2.6 -6 6 -6 36.2 5 -7 -6 -6 17 3 7 -6 6 15 3.9 -7 6 -6 13.1 2 -7 6 -6 15.3 4 -7 -7 6 47.5 4.2 7 -7 -6 45.6 5.2 -7 7 6 44.2 5.9 6 -7 -6 10.3 3.1 -6 -7 6 7.6 2.5 -5 -7 6 337.17 9.1 5 -7 -6 337.27 10.8 -5 7 6 331.87 5.8 -4 -7 6 83.19 4.3 4 -7 -6 78.09 5.3 -4 -7 6 69.79 4.3 -4 7 6 71.49 2.9 4 7 -6 70.59 3.4 -3 -7 6 60.89 3.9 -3 -7 6 59.69 3.5 3 -7 -6 58.39 4.4 3 7 -6 56.59 3.7 -3 7 6 65.49 3.1 -2 -7 6 643.54 11.2 2 -7 -6 636.14 13.6 2 7 -6 622.64 10.9 -2 7 6 632.04 10.6 -1 -7 6 521.95 9.1 -1 -7 6 507.05 10.5 1 -7 -6 497.25 11.2 -1 7 6 505.65 9.5 1 7 -6 512.25 10.1 1 7 -6 529.95 11 1 7 -6 506.95 9.6 0 -7 -6 4 1 0 -7 -6 3.6 1.7 0 -7 6 4.3 1.3 0 -7 6 1.9 1.8 0 7 6 3.8 1.7 0 7 -6 0 1.7 0 7 -6 3.8 1.5 0 7 -6 2.5 1.5 0 7 6 6.5 1.6 1 -7 6 224.88 7.4 -1 -7 -6 211.08 5.3 -1 -7 -6 213.98 6.5 1 7 6 220.88 6.3 1 7 6 215.38 6.3 -1 7 -6 220.78 6.2 -1 7 -6 217.38 7.7 1 7 6 226.38 6.1 2 -7 6 70.09 4.8 -2 -7 -6 67.39 3.6 2 7 6 75.49 3.9 -2 7 -6 73.59 5.4 -2 7 -6 70.99 3.6 -3 -7 -6 5.9 2 3 -7 6 7 2.5 -3 7 -6 7.5 1.7 -3 7 -6 7.9 2.9 3 7 6 4.4 2 -4 -7 -6 72.69 4.4 4 -7 6 68.49 5.1 -4 -7 -6 66.89 4.2 -4 7 -6 75.99 6 4 7 6 71.59 4 -4 7 -6 64.99 3.3 5 -7 6 18.5 3.7 -5 -7 -6 16 2.9 -5 -7 -6 13.3 2.7 -5 7 -6 16.9 4 -5 7 -6 14.9 2.2 6 -7 6 1.3 2.8 -6 -7 -6 7.4 2.7 -6 7 -6 1.2 2.7 -6 7 -6 3.3 1.5 7 -7 6 20.2 4.4 -7 -7 -6 26.5 3.8 -7 7 -6 26.7 4.9 -7 7 -6 23.8 2.5 6 -8 -6 40.5 4.8 -6 -8 6 29.8 3.9 -6 8 6 33.4 2.5 -5 -8 6 2.8 2.2 -5 -8 6 1.8 2.3 5 -8 -6 2.1 2.6 -5 8 6 2 1.4 -4 -8 6 -2.5 1.6 4 -8 -6 -1.1 2 4 8 -6 1.5 1.9 -4 8 6 2.6 1.4 3 -8 -6 111.69 6.1 -3 -8 6 107.99 4.7 -3 8 6 114.49 4.3 3 8 -6 109.39 4.8 2 -8 -6 6.7 2.4 -2 -8 6 6.9 1.9 2 8 -6 2.3 1.9 -2 8 6 4.1 1.7 -1 -8 6 2.9 1.9 -1 -8 6 1.9 1.8 1 -8 -6 4.9 2.4 1 8 -6 4 2.2 1 8 -6 1.1 1.9 -1 8 6 2.7 1.7 1 8 -6 2.4 1.9 0 -8 -6 189.28 6.9 0 -8 6 192.28 4.6 0 -8 6 196.88 7 0 8 -6 193.38 7.4 0 8 6 189.38 5.8 0 8 6 203.48 6.5 0 8 -6 201.08 6 0 8 -6 196.78 6.3 -1 -8 -6 436.66 10.2 1 -8 6 422.46 11 -1 -8 -6 434.26 8.1 1 8 6 450.65 9.9 1 8 6 453.05 9.9 -1 8 -6 442.76 11.9 1 8 6 435.06 9.4 -1 8 -6 437.66 9.5 2 -8 6 5.1 2.4 -2 -8 -6 8.5 2 -2 8 -6 12.7 2.2 -2 8 -6 9 3.2 2 8 6 8.6 2.5 -3 -8 -6 40.9 3.5 3 -8 6 46.4 4.8 -3 8 -6 43.7 3.2 -3 8 -6 46.7 5.2 3 8 6 46.8 4 -4 -8 -6 1.7 2 4 -8 6 6.1 2.9 4 8 6 4.1 2.6 -4 8 -6 3.5 3.1 -4 8 -6 3.6 1.7 5 -8 6 146.69 7.9 -5 -8 -6 155.58 6.4 -5 8 -6 160.38 8.7 -5 8 -6 157.18 5.2 6 -8 6 218.88 10.1 -6 8 -6 201.68 10.4 -6 8 -6 188.98 5.9 6 -9 -6 167.28 9 -6 -9 6 170.78 7.2 -6 9 6 175.98 10.1 5 -9 -6 4.3 3 -5 -9 6 8.4 2.7 -5 9 6 11.3 2.1 -4 -9 6 92.19 4.9 4 -9 -6 103.99 6.5 -4 9 6 99.09 4.4 4 9 -6 92.79 4.7 3 -9 -6 38.7 4.3 -3 -9 6 48.8 3.7 3 9 -6 48.2 4 -3 9 6 44.2 3.4 -2 -9 6 13.3 2.3 2 -9 -6 12.6 3 2 9 -6 14.2 2.8 -2 9 6 17.7 2.7 -1 -9 6 14.8 2.3 1 -9 -6 11.3 2.8 1 9 -6 12.7 2.6 -1 9 6 15.5 2.6 0 -9 6 274.37 8.9 0 -9 -6 282.57 8.9 0 9 6 267.87 7.4 0 9 -6 284.97 7.6 0 9 -6 289.87 9.5 0 9 6 257.87 7.9 0 9 -6 270.47 7.9 -1 -9 -6 16.4 2.2 1 -9 6 16.7 3.2 1 9 6 17.7 2.8 -1 9 -6 18.4 2.8 1 9 6 15.8 2.8 1 9 6 15 2.7 -1 9 -6 18.4 3.6 -2 -9 -6 -0.7 1.5 2 -9 6 -1 1.9 -2 9 -6 -2 2.2 -2 9 -6 -2.2 1.4 2 9 6 1 2.2 3 -9 6 103.09 6.6 -3 -9 -6 108.69 5.1 -3 9 -6 110.99 5 3 9 6 107.19 5.6 -3 9 -6 100.99 7 -4 -9 -6 43.3 3.8 4 -9 6 46.4 5.2 4 9 6 50.99 4.6 -4 9 -6 42.2 5.6 -4 9 -6 43.4 3.6 -5 -9 -6 2.9 2.4 5 -9 6 3.3 3.2 -5 9 -6 -1.2 3.1 -5 9 -6 5.3 2 -5 -10 6 -0.5 2.2 5 -10 -6 -2 2.4 -5 10 6 -0.5 1.7 4 -10 -6 49.6 5.1 -4 -10 6 46.4 4 4 10 -6 50.69 4.4 -4 10 6 41 3.6 3 -10 -6 97.79 6.5 -3 -10 6 95.99 4.9 -3 10 6 95.49 4.8 3 10 -6 105.19 5.6 2 -10 -6 30.7 4.3 -2 -10 6 37.2 3.4 2 10 -6 35.4 4 -2 10 6 38.2 3.6 -1 -10 6 12 2.6 1 -10 -6 16.2 3.2 -1 10 6 16.1 3 1 10 -6 15.8 2.9 0 -10 -6 4.2 2.3 0 -10 6 3.7 2.5 0 10 -6 2.9 2.2 0 10 -6 1.2 1.9 0 10 -6 1 2.6 0 10 6 1.2 2.2 -1 -10 -6 267.77 6 1 -10 6 281.47 9.7 1 10 6 276.17 8.3 -1 10 -6 283.07 8.6 -1 10 -6 258.87 10.2 2 -10 6 35.5 4.5 -2 -10 -6 37.2 3.2 2 10 6 28.6 4 -2 10 -6 31.2 4.9 -2 10 -6 29.6 3.5 -3 -10 -6 61.09 4.2 3 -10 6 54.59 5.3 -3 10 -6 62.09 4.2 -3 10 -6 65.29 6.1 3 10 6 69.29 5.6 4 -10 6 9.7 3.4 -4 -10 -6 12.3 2.9 -4 10 -6 12.9 4 -4 10 -6 11.5 2.5 4 10 6 13.9 4.1 4 -11 -6 -3 2.6 -4 -11 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647.04 12.1 -2 3 -7 652.43 9.3 -3 -3 -7 71.39 3.1 -3 -3 -7 73.19 3.1 3 -3 7 68.39 3.8 3 3 7 70.09 2.2 -3 3 -7 64.49 4 -3 3 -7 68.79 2.4 4 -3 7 4.9 2.1 -4 -3 -7 3.7 1.5 -4 3 -7 1.7 2 -4 3 -7 5.5 1.1 -5 -3 -7 2.7 1.6 5 -3 7 5.1 2.3 -5 3 -7 2.7 2.3 -5 3 -7 2.6 1 -6 -3 -7 3.4 1.8 -6 3 -7 2.3 2.2 -6 3 -7 2.2 1.1 -7 -3 -7 45.6 3.5 -7 3 -7 45.9 2.6 -8 -3 -7 1.9 2 -8 3 -7 -0.4 1.3 -8 -4 7 28.3 3.5 -7 -4 7 161.88 5.9 6 -4 -7 15.6 2.8 -6 -4 7 10.2 2 5 -4 -7 72.79 4.4 -5 -4 7 64.09 3.5 -4 -4 7 -1.9 1.1 4 -4 -7 -0.4 1.6 -3 -4 7 4.4 1.4 3 -4 -7 1.7 1.6 -3 -4 7 3.8 1.4 -3 4 7 4.7 0.7 3 4 -7 2.8 1 2 -4 -7 644.34 11.8 -2 -4 7 652.23 10.3 -2 -4 7 639.34 9.8 -2 4 7 627.24 8.5 2 4 -7 647.44 9.3 1 -4 -7 1078.39 16.3 -1 -4 7 1099.59 14.1 -1 -4 7 1119.89 14.7 1 4 -7 1114.59 14.7 -1 4 7 1081.39 13.9 1 4 -7 1100.89 14.2 0 -4 7 33.5 2.1 0 -4 7 32.8 2.6 0 -4 -7 36.9 2.5 0 -4 -7 36.9 1.7 0 4 7 38.8 2.2 0 4 -7 31 2 0 4 -7 38.2 2.8 0 4 -7 36.3 2.2 0 4 7 36.6 2.3 -1 -4 -7 227.88 5 -1 -4 -7 226.88 5.6 1 -4 7 229.98 3.2 1 -4 7 228.48 6.4 -1 4 -7 228.08 5.1 -1 4 -7 228.88 6.8 1 4 7 235.68 5.1 1 4 7 233.48 5.3 -2 -4 -7 90.49 3.5 2 -4 7 89.59 4.4 -2 -4 -7 91.29 3.5 -2 4 -7 93.89 3.1 -2 4 -7 91.59 4.7 2 4 7 93.19 3.3 -3 -4 -7 577.74 10.1 3 -4 7 582.14 12.1 -3 -4 -7 585.24 9.9 -3 4 -7 579.24 12.6 -3 4 -7 580.74 8.8 3 4 7 588.34 8.6 -4 -4 -7 53.09 3.3 4 -4 7 61.49 4.3 -4 4 -7 53.19 2.4 -4 4 -7 52.89 4.5 5 -4 7 367.76 10.3 -5 -4 -7 382.46 8.8 -5 4 -7 377.06 6.6 -5 4 -7 367.36 10.8 6 -4 7 139.79 6.8 -6 -4 -7 146.19 5.6 -6 4 -7 131.99 3.8 -6 4 -7 131.09 6.8 -7 -4 -7 -3.8 1.4 -7 4 -7 0.8 1.1 -7 4 -7 -0.7 2.4 -8 -4 -7 38 4 -8 4 -7 40.6 2.8 -8 -5 7 2 2.1 7 -5 -7 25.2 3.7 -7 -5 7 26 3.2 6 -5 -7 2.7 2.1 -6 -5 7 1 1.7 -5 -5 7 1.5 1.5 5 -5 -7 0.6 1.9 -4 -5 7 203.28 5.9 -4 -5 7 207.38 5.6 4 -5 -7 197.78 7.2 3 -5 -7 9.5 2.3 -3 -5 7 12.7 2 -3 -5 7 14 2.1 3 5 -7 13.5 1.8 -3 5 7 13.2 1.3 -2 -5 7 23.5 2.2 2 -5 -7 24.5 2.7 -2 -5 7 22 2.3 -2 5 7 23.3 1.8 2 5 -7 23.8 2.1 -1 -5 7 147.99 4.2 1 -5 -7 149.29 5.4 -1 -5 7 138.39 4.4 1 5 -7 147.89 5 -1 5 7 140.69 4.1 1 5 -7 136.79 4.4 1 5 -7 149.09 4.2 0 -5 7 6.8 1.7 0 -5 7 6.9 1.3 0 -5 -7 4.5 1.6 0 -5 -7 7.3 1.2 0 5 -7 3.7 1.6 0 5 7 5.8 1.3 0 5 -7 7.2 1.5 0 5 7 4.1 1.4 0 5 7 6.3 1.4 0 5 -7 5.5 1.3 -1 -5 -7 52.29 3.1 -1 -5 -7 53.29 2.7 1 -5 7 54.39 3.4 -1 5 -7 51.39 2.7 1 5 7 48.8 2.7 1 5 7 53.99 2.9 -1 5 -7 50.19 2.4 -1 5 -7 47.8 3.5 2 -5 7 5 2.1 -2 -5 -7 6.8 1.7 -2 -5 -7 6.5 1.6 -2 -5 -7 8.9 1.7 2 5 7 7.8 1.5 -2 5 -7 4.4 2.1 -2 5 -7 4.8 1.3 -3 -5 -7 192.98 5.5 3 -5 7 196.98 7.1 -3 -5 -7 192.28 5.8 3 5 7 186.98 4.8 -3 5 -7 184.68 4.6 -3 5 -7 186.18 7.4 4 -5 7 -1.1 1.9 -4 -5 -7 0 1.7 -4 -5 -7 -1.9 1.4 -4 5 -7 0.7 1 4 5 7 -0.4 1.4 -4 5 -7 2.4 2.3 -5 -5 -7 389.96 9.5 5 -5 7 393.36 11.2 -5 5 -7 390.56 7.1 -5 5 -7 392.36 11.7 -6 -5 -7 4.4 2.2 6 -5 7 6.2 3 -6 5 -7 0 2.6 -6 5 -7 5.4 1.5 -7 -5 -7 37 4 7 -5 7 33.4 5 -7 5 -7 36.8 2.6 -7 5 -7 41.2 5.1 7 -6 -7 126.99 6.9 -7 -6 7 109.79 5.7 6 -6 -7 92.29 5.8 -6 -6 7 104.79 5.1 -5 -6 7 34.4 3.2 5 -6 -7 29.8 3.7 4 -6 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20.2 1.7 -6 0 9 0.1 0.9 -5 0 9 8.3 1.1 -4 0 9 0.9 0.7 4 0 -9 1.2 1.2 -3 0 9 17.4 1.3 -2 0 9 -0.5 0.7 1 0 -9 1463.65 15.6 -1 0 9 1369.86 16.5 0 0 9 -0.2 0.8 0 0 -9 0.5 0.9 -1 0 -9 159.98 3.7 -1 0 -9 150.18 3.8 1 0 9 157.38 3.5 2 0 9 0.9 0.7 -2 0 -9 0.3 1 -2 0 -9 0.4 1.3 -3 0 -9 778.62 11.3 -3 0 -9 809.12 13.5 -4 0 -9 0 1.3 -4 0 -9 0.7 1.1 -5 0 -9 58.09 3 -6 0 -9 0.8 1.4 -7 0 -9 54.29 3.5 -8 0 -9 -0.9 1.6 -8 -1 9 9 1.8 -7 -1 9 68.79 3.1 -6 -1 9 584.84 9 5 -1 -9 8.3 1.8 -5 -1 9 7.1 1.2 -4 -1 9 851.01 11.3 4 -1 -9 862.71 13.7 -4 1 9 883.61 9 -3 -1 9 537.15 8 3 -1 -9 527.75 9.6 -3 1 9 545.35 6.8 2 -1 -9 289.17 6.6 -2 -1 9 296.77 5.4 -2 1 9 298.17 4.9 -1 -1 9 105.29 3.1 1 -1 -9 113.89 2.2 1 1 -9 112.99 2.8 -1 1 9 108.39 3 0 -1 -9 86.49 2.6 0 -1 9 92.29 2.8 0 1 9 93.99 2.8 0 1 -9 91.89 2.8 1 -1 9 254.67 4.5 -1 -1 -9 265.07 5.1 -1 -1 -9 254.37 5.2 -1 1 -9 257.77 5.1 -1 1 -9 276.77 6.6 -1 1 -9 265.67 5 1 1 9 251.97 4.8 -2 -1 -9 114.39 3.6 -2 -1 -9 111.59 4.1 -2 -1 -9 114.69 3.4 -2 1 -9 103.69 3.2 -2 1 -9 109.39 4.3 2 1 9 115.09 2.8 -3 -1 -9 295.67 7.1 -3 -1 -9 304.27 6.2 -3 1 -9 303.07 7.7 -3 1 -9 295.07 5.9 -4 -1 -9 2.9 1.2 -4 -1 -9 4 1.6 -4 1 -9 4.6 1.3 -4 1 -9 6.1 1.9 -5 -1 -9 16.2 2.3 -5 1 -9 14.7 2 -5 1 -9 14.6 2.5 -6 -1 -9 164.28 5.4 -6 1 -9 158.88 4.8 -7 -1 -9 68.29 4 -7 1 -9 66.89 3.6 -8 -1 -9 15.1 2.7 -8 1 -9 9 2.2 -8 -2 9 4.1 1.7 -7 -2 9 11.2 1.9 -6 -2 9 77.19 3.4 5 -2 -9 152.18 5.6 -5 -2 9 161.38 4.5 -4 -2 9 2.7 1.1 4 -2 -9 0.6 1.4 -3 -2 9 462.25 7.7 3 -2 -9 469.75 9.3 -3 2 9 476.65 5.9 2 -2 -9 313.17 7.1 -2 -2 9 309.67 6 2 2 -9 328.87 4.9 -2 2 9 315.57 5.1 1 -2 -9 200.18 5.3 -1 -2 9 192.98 4.5 -1 -2 9 189.38 4.2 1 2 -9 194.08 4.1 -1 2 9 190.88 4.2 0 -2 -9 736.03 9.7 0 -2 -9 714.33 11.7 0 -2 9 733.03 10 0 2 -9 731.63 9.9 0 2 9 734.63 10 0 2 9 704.23 10.1 1 -2 9 490.35 6.9 -1 -2 -9 496.45 7.9 1 2 9 493.95 7.7 -1 2 -9 492.95 7.9 -1 2 -9 507.05 7.7 -1 2 -9 509.75 9.9 -2 -2 -9 252.87 5.4 -2 -2 -9 252.67 5.6 -2 -2 -9 246.48 6 -2 2 -9 259.87 6.9 -2 2 -9 232.68 5 2 2 9 244.28 4.7 -3 -2 -9 619.04 10.2 -3 -2 -9 628.74 9.7 -3 -2 -9 608.74 10.7 -3 2 -9 621.54 9.4 3 2 9 610.24 7.3 -3 2 -9 614.04 12.2 -4 -2 -9 12.5 2 -4 2 -9 12.3 2.5 -4 2 -9 12.2 1.6 -5 -2 -9 157.18 5.3 -5 2 -9 152.38 4.3 -5 2 -9 154.18 6.5 -6 -2 -9 0 1.5 -6 2 -9 -1.9 1 -6 2 -9 4.5 2.3 -7 -2 -9 1.2 1.8 -7 2 -9 0.4 1.4 -8 -2 -9 19.6 3.1 -8 2 -9 22.1 2.6 -8 -3 9 -0.7 1.6 -7 -3 9 79.09 4.1 6 -3 -9 6.9 2.4 -6 -3 9 6.1 1.7 -5 -3 9 355.46 7.4 5 -3 -9 359.26 9.1 -4 -3 9 95.59 3.6 4 -3 -9 95.69 4.6 -3 -3 9 9.2 1.6 3 -3 -9 11.2 2.2 -3 -3 9 13.4 1.8 -3 3 9 12.7 1.1 -2 -3 9 47.1 2.6 -2 -3 9 51.99 2.5 2 -3 -9 51.99 3.2 -2 3 9 50.79 2.1 2 3 -9 46.5 2.2 -2 3 9 55.09 2.2 -1 -3 9 142.39 3.8 1 -3 -9 147.09 5 -1 -3 9 143.29 4 1 3 -9 144.99 3.9 -1 3 9 145.09 3.8 0 -3 -9 235.28 6.1 0 -3 -9 243.88 4.6 0 -3 9 240.88 5.1 0 3 -9 245.58 5.1 0 3 -9 238.98 5.3 0 3 9 247.18 5.1 0 3 -9 233.58 6.3 0 3 9 242.28 5.3 1 -3 9 159.98 3.3 -1 -3 -9 160.38 4.8 -1 -3 -9 155.08 4.2 1 3 9 158.88 4.1 1 3 9 158.28 4.4 -1 3 -9 152.28 5.5 -1 3 -9 165.18 4.3 -1 3 -9 160.88 3.9 -2 -3 -9 823.52 12.9 2 3 9 818.02 11.3 -2 3 -9 805.42 11.5 -3 -3 -9 11.3 1.8 -3 -3 -9 10.3 1.7 -3 -3 -9 7.1 1.6 3 3 9 8.4 1.3 -3 3 -9 7.1 2.1 -3 3 -9 6.6 1.3 -4 -3 -9 541.35 10.1 -4 3 -9 536.35 8.8 -4 3 -9 545.15 12.5 -5 -3 -9 50.09 3.4 -5 3 -9 40.7 2.5 -5 3 -9 47.7 4.4 -6 -3 -9 75.69 4.2 -6 3 -9 86.69 5.7 -6 3 -9 79.39 3.4 -7 -3 -9 -0.1 1.8 -7 3 -9 1.6 1.4 -8 -3 -9 -1.4 1.9 -8 3 -9 4.9 1.7 -8 -4 9 0.2 1.9 -7 -4 9 83.89 4.5 -6 -4 9 47.8 3.4 6 -4 -9 51.29 4.3 -5 -4 9 4 1.7 5 -4 -9 6.5 2.3 4 -4 -9 139.49 5.7 -4 -4 9 144.99 4.8 3 -4 -9 75.59 4.2 -3 -4 9 73.59 3.3 -3 -4 9 76.19 3.4 -3 4 9 79.79 2.3 3 4 -9 77.79 2.4 2 -4 -9 123.99 4.9 -2 -4 9 130.29 4 -2 -4 9 133.59 4.3 2 4 -9 130.39 3.7 -2 4 9 123.59 3.4 -1 -4 9 501.55 8.3 1 -4 -9 502.35 10 -1 -4 9 500.35 8.7 1 4 -9 501.25 9.6 1 4 -9 494.35 8.3 -1 4 9 492.95 8.2 1 4 -9 489.15 8.6 0 -4 -9 7.9 1.2 0 -4 -9 4.6 1.6 0 -4 9 4.9 1.4 0 4 -9 5.5 1.4 0 4 -9 4 1.3 0 4 -9 6.6 1.8 0 4 9 6.2 1.4 0 4 9 3.9 1.3 -1 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198.58 5 1 5 -9 190.68 5.3 -1 5 9 192.08 5.1 -1 5 9 195.58 5.1 1 5 -9 183.98 5.8 1 5 -9 197.78 5.2 0 -5 9 217.58 4.9 0 -5 -9 215.28 6.5 0 -5 -9 214.88 4.4 0 5 -9 239.68 7 0 5 9 219.28 5.3 0 5 -9 205.38 5.2 0 5 -9 209.98 5.6 0 5 9 222.78 5.7 -1 -5 -9 90.19 4 -1 -5 -9 87.49 3.4 1 -5 9 94.19 2.1 1 -5 9 90.79 4.7 -1 5 -9 82.79 4.6 1 5 9 91.89 3.5 -1 5 -9 92.19 3.7 -1 5 -9 92.39 3.5 1 5 9 88.09 3.8 -2 -5 -9 219.98 6.1 2 -5 9 215.28 7.3 -2 -5 -9 226.08 6 -2 -5 -9 232.68 5.9 -2 5 -9 226.78 5.6 -2 5 -9 231.28 7.7 2 5 9 225.38 5.7 -3 -5 -9 1.1 1.6 3 -5 9 1.7 2 -3 -5 -9 0.8 1.6 -3 5 -9 -0.1 1.2 -3 5 -9 -0.4 1.9 3 5 9 1 1.9 -4 -5 -9 2 1.8 -4 -5 -9 3.3 1.8 4 -5 9 5.5 2.5 -4 5 -9 1.5 2.2 -4 5 -9 4 1.5 4 5 9 1.4 1.6 -5 -5 -9 40 3.7 5 -5 9 36 4.6 -5 5 -9 30.1 4.5 -5 5 -9 37.5 2.6 -6 -5 -9 157.38 6.5 6 -5 9 157.68 8 -6 5 -9 163.38 8.2 -6 5 -9 164.08 5 -7 -5 -9 -0.4 2.1 -7 5 -9 -0.2 2.6 -7 5 -9 0 1.5 -7 -6 9 51.29 4.1 7 -6 -9 48.9 4.7 -6 -6 9 48.9 3.8 6 -6 -9 55.29 4.8 5 -6 -9 43.5 4.3 -5 -6 9 39.4 3.6 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207.38 6.9 -5 -6 -9 197.98 7.1 5 -6 9 193.68 8.6 -5 6 -9 200.58 5.7 -5 6 -9 191.78 8.9 6 -6 9 2.2 3.1 -6 -6 -9 3.7 2.4 -6 6 -9 1.4 1.5 -6 6 -9 2 2.9 -7 -6 -9 11.1 3 -7 6 -9 2.3 3.2 -7 6 -9 5.3 1.8 7 -7 -9 3.1 2.7 -7 -7 9 3.7 2.5 6 -7 -9 9.5 3.2 -6 -7 9 6.8 2.4 -6 7 9 10.7 1.5 -5 -7 9 37.4 3.7 5 -7 -9 50.19 4.7 -5 7 9 46.1 2.5 -4 -7 9 0.5 1.8 4 -7 -9 0.5 2 -4 -7 9 0.1 1.7 4 7 -9 -0.2 1.7 -4 7 9 0.1 1.2 3 -7 -9 8.4 2.7 -3 -7 9 6.7 2 3 7 -9 5.3 1.9 -3 7 9 6.3 1.6 2 -7 -9 3.2 2.4 -2 -7 9 2 1.7 2 7 -9 1.8 2 -2 7 9 2.2 1.6 1 -7 -9 387.46 10.3 -1 -7 9 401.46 8 -1 7 9 403.16 8.7 -1 7 9 384.46 8.4 1 7 -9 399.16 8.9 1 7 -9 383.46 9.7 1 7 -9 394.56 8.6 0 -7 9 420.76 7.5 0 -7 9 407.56 10.2 0 -7 -9 423.36 6.4 0 -7 -9 409.46 10.2 0 7 9 445.86 8.9 0 7 -9 427.36 8.8 0 7 9 412.86 9.1 0 7 -9 408.06 10.6 0 7 -9 435.36 9.3 -1 -7 -9 97.49 4.8 1 -7 9 95.99 5.4 -1 -7 -9 93.89 3.8 -1 7 -9 96.09 4.4 1 7 9 93.79 4.5 -1 7 -9 109.19 6 1 7 9 97.19 4.2 -2 -7 -9 106.09 4.6 2 -7 9 100.69 5.8 2 7 9 109.69 4.8 -2 7 -9 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5.8 2 -1 27 108.39 6.5 2 1 27 108.99 7.1 -2 1 -27 113.89 5.9 -2 1 -27 103.59 7.5 -4 -2 27 47.9 4.7 4 -2 -27 49.1 5.3 -4 2 27 64.59 4.9 4 2 -27 41.1 5.2 -3 -2 27 31.7 3.9 3 -2 -27 31.3 4.8 -3 2 27 36.9 4 3 2 -27 25.8 4.7 -2 -2 27 214.28 8.1 2 -2 -27 208.88 9.6 2 2 -27 221.58 9.8 -2 2 27 219.08 7.7 1 -2 -27 125.59 7.5 -1 -2 27 120.59 6.2 1 2 -27 130.29 5.4 -1 2 27 132.49 6.2 1 2 -27 121.29 7.9 0 -2 -27 2.9 2.8 0 -2 27 2.6 3 0 -2 -27 1.4 1.9 0 2 -27 0.1 2.1 0 2 27 0.7 2.5 0 2 -27 4.2 3.6 -1 -2 -27 43 5.4 1 -2 27 38.9 5.4 -1 2 -27 41.7 4.2 1 2 27 40.2 4.9 -1 2 -27 41 5.6 -2 -2 -27 67.39 5.9 -2 2 -27 67.09 6.9 -2 2 -27 68.19 5.2 2 2 27 73.49 6.4 4 -3 -27 84.29 6.7 -4 3 27 79.59 5.3 -3 -3 27 25.3 3.9 3 -3 -27 31.6 5 -3 3 27 30.1 3.8 3 3 -27 16.8 4.6 2 -3 -27 8.1 3.3 -2 -3 27 5.7 3.1 2 3 -27 1.2 3.7 2 3 -27 11 2.6 -2 3 27 10.9 2.9 1 -3 -27 -3.2 2.3 -1 -3 27 1.2 2.9 1 3 -27 2.6 2.4 1 3 -27 -1.4 3.5 -1 3 27 -0.2 2.3 0 -3 27 111.89 6.4 0 -3 -27 121.99 7.6 0 -3 -27 124.29 4.7 0 3 -27 118.59 5.8 0 3 -27 123.89 8.5 0 3 27 116.79 6.2 -1 -3 -27 203.18 9.6 -1 -3 -27 188.18 6.6 1 -3 27 190.88 7.7 1 3 27 188.78 7.9 -1 3 -27 194.18 7.4 -2 -3 -27 17.5 4 -2 -3 -27 16.5 3.2 2 3 27 14.9 4.8 -2 3 -27 15.4 3.4 -2 3 -27 11.5 4.5 3 -4 -27 2.4 3 -3 -4 27 0.5 2.7 -3 4 27 0.4 2.1 2 -4 -27 -0.5 2.3 -2 -4 27 0.5 3.2 -2 4 27 -1.2 2.1 2 4 -27 2.3 4.3 2 4 -27 -1 2.4 1 -4 -27 6.7 3.3 -1 -4 27 2 3.5 -1 4 27 5.6 2.7 1 4 -27 3.8 2.7 1 4 -27 1.7 4.8 0 -4 27 4.1 4 0 -4 -27 2.6 2.9 0 4 27 7.7 3.3 0 4 -27 1.7 2.5 0 4 -27 6.8 4.4 -1 -4 -27 -1.9 2.4 1 -4 27 -1.4 4.1 -1 -4 -27 0.1 1.9 1 4 27 -4.4 3.7 -1 4 -27 2.4 2.5 -1 4 -27 0.3 4 2 -5 -27 2 2.8 -2 -5 27 4.3 3.9 -2 5 27 3.8 2.6 2 5 -27 2.8 5 2 5 -27 5.4 2.9 -1 -5 27 3.8 4.2 1 -5 -27 10.4 3.4 1 5 -27 2.6 2.8 -1 5 27 1.3 2.5 1 5 -27 -5.2 4.4 0 -5 -27 3.1 3 0 -5 27 3 4.3 0 5 -27 4.1 5.1 0 5 -27 0.7 2.5 0 5 27 1.6 3 4 0 -28 227.18 10 -4 0 28 240.08 8.8 -3 0 28 -0.8 2.2 3 0 -28 -1 2.8 -2 0 28 17.4 3.2 2 0 -28 13.1 3.6 1 0 -28 2.9 2 1 0 -28 1.7 2.9 -1 0 28 1.2 2.5 0 0 -28 28.7 4.7 0 0 28 26.2 4 0 0 -28 27.8 3.7 -1 0 -28 -0.9 2.9 -1 0 -28 -2.2 2.3 1 0 28 -2.2 3.9 -2 0 -28 72.59 5.2 -2 0 -28 78.29 7.2 2 0 28 81.19 6.4 -4 -1 28 -2 2.3 4 -1 -28 5.9 3.4 -4 1 28 -3.3 2.1 4 1 -28 -3.2 2.7 -3 -1 28 3.1 2.5 3 -1 -28 1.8 3 3 1 -28 -2.9 2.3 -3 1 28 -2.2 2 -2 -1 28 69.19 4.8 2 -1 -28 52.59 5.4 -2 1 28 67.29 4.9 2 1 -28 63.09 6.2 -1 -1 28 145.59 6.7 1 -1 -28 159.98 8.7 1 1 -28 155.28 8.7 -1 1 28 145.79 6.6 0 -1 28 2.1 3.1 0 -1 -28 2.1 2.8 0 1 28 6.1 3 0 1 -28 6.6 2.7 0 1 -28 0.1 3 -1 -1 -28 13.4 3.8 1 -1 28 5 4.1 1 1 28 5.9 4 -1 1 -28 4.4 3.4 -1 1 -28 12.4 3.2 -2 -1 -28 30.2 4.1 -2 -1 -28 31.7 5.2 -2 1 -28 26.5 5.1 -2 1 -28 24.8 4 2 1 28 26 5 -3 -2 28 2.9 2.5 3 -2 -28 0.1 2.6 -3 2 28 4.8 2.5 3 2 -28 -3.4 2.4 2 -2 -28 14.9 4.1 -2 -2 28 11.4 3.3 -2 2 28 13.4 3 2 2 -28 6.5 3.7 1 -2 -28 13.2 3.5 -1 -2 28 19.7 3.9 1 2 -28 17.8 3.1 -1 2 28 20.4 3.5 1 2 -28 13.9 4.2 0 -2 -28 7.7 2.3 0 -2 -28 5.5 3.3 0 -2 28 7.4 4 0 2 -28 5.4 4.1 0 2 28 5.9 3.2 0 2 -28 12.6 3.1 1 -2 28 1.6 4.3 -1 -2 -28 9.2 2.9 -1 -2 -28 4.9 3 -1 2 -28 0.9 3.6 1 2 28 5.1 3.8 -1 2 -28 10 3 -3 -3 28 126.29 6.7 3 -3 -28 133.19 8.2 3 3 -28 119.49 8 -3 3 28 131.79 6.7 -2 -3 28 2.9 2.9 2 -3 -28 -1.3 2.6 2 3 -28 -11 3.3 -1 -3 28 0.1 3.4 1 -3 -28 3.8 2.9 1 3 -28 -1.5 3.9 -1 3 28 4.6 2.8 1 3 -28 1.2 2.5 0 -3 28 10.2 4 0 -3 -28 16.3 2.5 0 -3 -28 4.1 3.1 0 3 -28 8.1 4.4 0 3 -28 12.3 3.1 0 3 28 8.1 3.5 1 -3 28 1.2 4.4 -1 -3 -28 3.4 3 -1 -3 -28 7.9 2.5 -1 3 -28 -1.2 2.4 1 3 28 -1.7 3.8 -1 3 -28 -1.7 3.6 -2 -4 28 12 3.9 2 -4 -28 9.1 3.5 2 4 -28 9.7 5 2 4 -28 14.4 2.9 -1 -4 28 7.7 4.1 1 -4 -28 6.3 3.3 1 4 -28 1.7 4.8 1 4 -28 4.4 2.8 -1 4 28 9.8 2.9 0 -4 28 218.48 8.8 0 -4 -28 212.68 9.9 0 4 -28 205.68 7.6 0 4 28 204.48 8.3 0 4 -28 224.08 10.9 3 0 -29 51.69 5.6 -2 0 29 0.2 2.5 2 0 -29 5 3.2 -1 0 29 30.4 4.4 1 0 -29 28.8 4.7 1 0 -29 37.9 3.3 0 0 -29 4.8 3 0 0 29 1.4 3.4 -1 0 -29 70.59 6.9 1 0 29 56.29 5.9 -1 0 -29 55.39 4.7 -3 -1 29 -1.1 2.3 3 -1 -29 1.1 2.9 3 1 -29 -4.1 2.4 -3 1 29 -2.3 2 2 -1 -29 104.89 7.2 -2 -1 29 104.89 6.1 2 1 -29 99.19 7.2 -2 1 29 94.39 5.8 1 -1 -29 0.5 2.7 -1 -1 29 4.9 3.2 -1 1 29 0.5 2.7 1 1 -29 5.5 3.5 0 -1 -29 79.79 4.5 0 -1 29 71.39 6.2 0 -1 -29 85.29 6.8 0 1 -29 76.49 7.2 0 1 -29 80.19 5.1 0 1 29 73.59 6.1 1 -1 29 5.1 4.3 -1 -1 -29 15.3 4.2 1 1 29 7.8 4.1 -1 1 -29 12.6 4.5 -1 1 -29 9.2 3 -2 -2 29 9.9 3.4 2 -2 -29 9.1 3.5 2 2 -29 2.7 3.3 -2 2 29 8.2 2.8 1 -2 -29 -2.8 2.5 -1 -2 29 0.9 3.2 1 2 -29 -3.9 3.4 1 2 -29 0.4 2.6 -1 2 29 1.8 2.9 0 -2 29 13.1 4.2 0 -2 -29 18.9 2.8 0 -2 -29 24.1 4.5 0 2 -29 8.6 4 0 2 29 15.4 4 0 2 -29 8.3 3.2 1 -3 -29 96.09 7.2 -1 -3 29 96.19 6.5 1 3 -29 91.79 8 1 3 -29 96.69 5.4 -1 3 29 97.49 6 -1 0 30 1.2 3.1 1 0 -30 -1.6 2.8 _iucr_refine_fcf_details ; data_20zs_diiso4cl_0m _computing_structure_refinement 'SHELXL 2016/6 (Sheldrick, 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2ybc (x-z,y,z)' _symmetry_space_group_name_H-M 'P 1 21/n 1' _symmetry_space_group_name_Hall '-P 2ybc (x-z,y,z)' _symmetry_Int_Tables_number 14 _cell_length_a 7.28280(10) _cell_length_b 9.94270(10) _cell_length_c 24.0413(2) _cell_angle_alpha 90 _cell_angle_beta 97.0120(10) _cell_angle_gamma 90 _cell_volume 1727.83(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -9 0 1 252.125 275.907 7.748 3.604 o -9 0 3 38.430 44.251 3.725 30.238 o -9 0 5 5.104 13.707 2.533 107.624 o -9 0 7 0.990 0.298 1.937 279.173 o -9 1 0 116.001 122.613 3.753 11.309 o -9 1 1 9.667 16.091 3.278 67.096 o -9 1 2 1.874 -4.321 2.086 231.194 o -9 1 3 18.750 14.303 3.129 59.381 o -9 1 4 239.700 231.656 7.599 4.049 o -9 1 5 29.750 34.120 4.023 33.537 o -9 1 6 38.012 57.959 4.470 24.464 o -9 1 7 29.273 38.440 4.023 32.846 o -8 0 -6 54.384 49.913 4.321 22.324 o -8 0 -4 43.928 61.981 4.321 23.276 o -8 0 -2 48.187 55.426 3.725 25.487 o -8 0 0 135.372 124.693 4.768 9.305 o -8 0 2 462.237 511.749 9.387 1.524 o -8 0 4 92.563 90.573 3.725 14.822 o -8 0 6 262.575 273.970 6.258 3.736 o -8 0 8 256.459 275.907 6.556 3.752 o -8 0 10 9.618 8.046 2.086 124.088 o -8 0 12 173.026 176.543 6.109 6.254 o -8 0 14 47.792 54.830 4.321 23.212 o -8 0 16 20.083 22.647 3.576 46.883 o -8 1 -7 62.451 65.902 3.458 21.791 o -8 1 -6 19.180 15.508 2.682 66.856 o -8 1 -5 116.519 118.917 3.966 11.223 o -8 1 -4 0.682 -1.054 1.464 486.594 o -8 1 -3 32.949 35.607 4.172 30.916 o -8 1 -2 39.226 49.225 2.577 35.545 o -8 1 -1 84.378 81.383 2.828 17.813 o -8 1 0 145.331 138.400 5.811 7.876 o -8 1 1 195.522 203.213 6.556 5.271 o -8 1 2 1.872 -0.447 2.086 231.226 o -8 1 3 217.236 235.380 7.003 4.480 o -8 1 4 114.243 115.306 5.066 10.480 o -8 1 5 68.887 74.929 4.321 17.676 o -8 1 6 2.632 -1.639 1.937 247.296 o -8 1 7 176.903 183.397 6.109 6.067 o -8 1 8 5.991 5.364 2.235 142.582 o -8 1 9 14.481 13.409 2.682 76.907 o -8 1 10 18.354 16.389 2.831 64.380 o -8 1 11 18.989 19.352 1.896 80.282 o -8 1 12 1.063 0.287 1.357 510.653 o -8 1 13 63.582 70.599 3.075 22.088 o -8 1 14 1.439 2.673 2.235 193.830 o -8 1 15 181.155 198.697 5.111 6.120 o -8 1 16 0.025 -0.023 1.676 412.028 o -8 1 17 25.073 35.959 3.107 43.854 o -8 2 -7 14.222 15.048 2.183 90.105 o -8 2 -6 6.835 8.047 1.823 159.369 o -8 2 -5 2.260 0.519 1.461 382.446 o -8 2 -4 94.240 97.977 3.418 14.646 o -8 2 -3 17.676 21.229 2.980 59.246 o -8 2 -2 185.207 169.540 7.152 5.628 o -8 2 -1 2.631 1.639 2.384 167.731 o -8 2 0 0.510 5.662 2.533 152.470 o -8 2 1 60.852 70.772 4.917 17.610 o -8 2 2 294.072 278.291 8.493 3.068 o -8 2 3 3.679 -0.745 2.384 165.759 o -8 2 4 39.993 43.357 4.023 28.171 o -8 2 5 32.737 35.014 3.725 34.348 o -8 2 6 50.564 51.105 4.321 23.012 o -8 2 7 5.541 5.215 2.533 123.903 o -8 2 8 0.118 -1.341 2.086 264.228 o -8 2 9 8.836 6.109 2.533 107.875 o -8 2 10 4.896 3.278 2.533 132.281 o -8 2 11 90.696 100.556 5.662 11.807 o -8 2 12 13.618 13.409 3.129 66.886 o -8 2 13 0.530 -6.854 2.086 255.679 o -8 2 14 26.067 30.310 5.513 24.999 o -8 2 15 0.009 -0.775 2.905 137.459 o -8 2 16 86.301 84.427 4.991 13.816 o -8 3 -7 0.020 0.754 1.713 377.187 o -8 3 -6 20.155 23.843 2.425 64.044 o -8 3 -5 95.787 95.444 3.471 14.548 o -8 3 -4 7.617 5.513 3.129 85.555 o -8 3 -3 82.115 97.576 6.258 11.653 o -8 3 -2 2.400 3.278 2.682 134.306 o -8 3 -1 18.136 15.048 3.427 54.227 o -8 3 0 46.276 43.953 4.619 23.503 o -8 3 1 1.450 6.556 2.831 119.491 o -8 3 2 60.280 65.557 5.215 17.243 o -8 3 3 181.010 176.394 7.450 5.528 o -8 3 4 0.594 -2.980 2.235 222.942 o -8 3 5 51.553 56.916 4.917 20.073 o -8 3 6 0.172 0.000 2.384 202.077 o -8 3 7 36.472 35.907 4.321 28.709 o -8 3 8 0.134 1.192 2.533 173.877 o -8 3 9 0.106 -1.043 2.384 202.903 o -8 3 10 0.067 -5.811 2.086 265.311 o -8 3 11 0.009 -2.682 2.384 204.129 o -8 3 12 46.484 46.486 4.917 21.934 o -8 3 13 109.378 94.298 6.258 10.120 o -8 3 14 37.268 43.655 5.066 23.442 o -8 3 15 51.354 61.869 3.576 24.413 o -8 4 -7 58.161 59.273 3.418 23.612 o -8 4 -6 220.172 245.302 9.983 3.663 o -8 4 -5 15.073 16.259 2.205 85.649 o -8 4 -4 1.395 1.788 2.831 131.420 o -8 4 -3 0.749 -0.149 2.682 155.606 o -8 4 -2 3.203 5.662 2.980 104.991 o -8 4 -1 84.382 89.679 5.960 12.216 o -8 4 0 0.379 0.447 2.682 156.705 o -8 4 1 15.908 18.773 3.874 47.332 o -8 4 2 1.621 1.490 2.682 144.393 o -8 4 3 14.941 4.768 3.129 71.668 o -8 4 4 8.649 4.172 2.980 90.740 o -8 4 5 1.046 0.000 2.831 138.400 o -8 4 6 269.349 269.351 9.685 3.139 o -8 4 7 43.776 42.165 5.215 21.625 o -8 4 8 43.920 44.549 4.917 22.638 o -8 4 9 1.305 0.298 2.831 136.032 o -8 4 10 19.279 11.621 3.427 54.807 o -8 4 11 0.027 -1.043 2.533 180.659 o -8 4 12 73.407 81.932 6.109 13.101 o -8 4 13 21.567 20.859 4.023 40.879 o -8 5 -4 29.761 34.567 5.215 25.387 o -8 5 -3 33.415 30.097 4.768 27.719 o -8 5 -2 16.973 13.409 3.874 48.600 o -8 5 -1 21.979 16.240 3.874 43.888 o -8 5 0 6.663 1.043 2.980 101.134 o -8 5 1 6.109 3.278 3.129 92.160 o -8 5 2 18.449 12.963 3.725 49.932 o -8 5 3 12.938 12.963 3.725 55.043 o -8 5 4 52.416 51.850 5.364 18.840 o -8 5 5 68.791 75.376 6.109 13.756 o -8 5 6 34.932 44.996 5.364 22.377 o -8 5 7 0.015 2.980 3.129 112.399 o -8 5 8 1.712 -1.937 2.831 134.575 o -8 5 9 22.563 17.879 4.172 39.461 o -8 5 10 263.028 271.139 10.728 3.010 o -7 0 -5 364.736 344.891 8.344 2.347 o -7 0 -3 367.630 324.777 7.450 2.461 o -7 0 -1 696.361 712.861 11.025 0.833 o -7 0 1 506.277 499.830 8.046 1.456 o -7 0 3 39.515 35.014 2.086 42.564 o -7 0 5 132.911 129.014 3.278 10.313 o -7 0 7 518.213 508.918 7.897 1.414 o -7 0 9 29.363 30.097 2.533 48.745 o -7 0 11 83.031 83.124 4.023 15.882 o -7 0 13 87.067 92.063 4.619 13.979 o -7 0 15 6.508 7.748 2.533 113.840 o -7 0 17 1.149 1.937 2.384 180.241 o -7 0 19 132.361 150.320 7.301 7.164 o -7 0 21 55.722 64.812 5.811 16.255 o -7 1 -6 65.662 70.542 3.075 21.650 o -7 1 -5 128.350 112.700 3.500 10.992 o -7 1 -4 21.350 30.346 2.112 62.628 o -7 1 -3 0.519 -2.146 1.038 919.924 o -7 1 -2 74.801 69.446 2.831 20.473 o -7 1 -1 148.869 140.635 5.364 7.968 o -7 1 0 516.696 481.503 9.536 1.406 o -7 1 1 119.114 122.011 4.768 10.263 o -7 1 2 27.798 35.312 2.980 43.436 o -7 1 3 13.134 21.455 2.682 71.907 o -7 1 4 111.728 97.725 4.023 12.321 o -7 1 5 43.098 47.678 3.129 31.175 o -7 1 6 100.709 111.135 4.321 12.341 o -7 1 7 14.807 17.283 2.384 80.218 o -7 1 8 24.027 32.332 2.980 47.403 o -7 1 9 93.299 102.493 4.619 12.943 o -7 1 10 238.423 242.681 7.003 4.118 o -7 1 11 23.984 27.084 3.203 46.895 o -7 1 12 63.057 72.216 3.494 20.932 o -7 1 13 82.774 86.367 3.114 17.233 o -7 1 14 117.980 117.715 3.753 11.342 o -7 1 15 7.762 10.802 2.533 103.282 o -7 1 16 0.263 -1.372 1.525 479.826 o -7 1 17 40.671 40.416 2.990 34.545 o -7 1 18 143.626 141.166 4.772 8.525 o -7 1 19 44.000 39.308 3.212 32.026 o -7 1 20 31.787 39.676 3.366 36.436 o -7 1 21 15.777 20.703 2.896 63.660 o -7 2 -6 10.179 10.479 1.788 130.800 o -7 2 -5 3.500 5.610 1.461 263.288 o -7 2 -4 1.146 0.544 1.128 652.718 o -7 2 -3 24.569 33.524 3.725 38.741 o -7 2 -2 124.788 118.882 5.662 9.279 o -7 2 -1 379.554 374.675 9.238 2.120 o -7 2 0 242.533 240.893 7.599 3.953 o -7 2 1 13.615 17.730 2.831 70.690 o -7 2 2 251.834 239.403 7.152 3.932 o -7 2 3 285.405 253.111 7.450 3.418 o -7 2 4 87.180 95.192 4.917 13.367 o -7 2 5 251.292 237.317 7.152 3.953 o -7 2 6 146.373 137.655 5.662 7.943 o -7 2 7 170.127 165.517 5.960 6.547 o -7 2 8 22.396 22.051 3.278 49.312 o -7 2 9 16.611 16.687 2.831 66.726 o -7 2 10 19.370 14.899 2.831 63.997 o -7 2 11 61.217 70.623 4.768 17.962 o -7 2 12 0.723 -0.596 2.086 251.861 o -7 2 13 85.676 98.550 3.427 15.579 o -7 2 14 1.333 0.182 1.639 363.385 o -7 2 15 141.095 142.676 4.150 8.973 o -7 2 16 122.604 119.172 4.116 10.683 o -7 2 17 369.456 361.389 7.147 2.359 o -7 2 18 70.652 69.967 3.712 19.217 o -7 2 19 19.239 17.059 2.541 68.438 o -7 2 20 22.864 23.386 2.821 54.700 o -7 2 21 14.351 25.199 3.650 49.392 o -7 3 -6 20.601 24.840 2.176 66.835 o -7 3 -5 0.470 -0.130 1.150 779.347 o -7 3 -4 150.869 153.449 7.003 6.749 o -7 3 -3 3.465 2.980 2.384 155.480 o -7 3 -2 22.681 16.389 3.278 51.588 o -7 3 -1 42.258 38.589 4.172 27.395 o -7 3 0 406.826 405.070 10.430 1.853 o -7 3 1 19.430 18.773 3.278 53.568 o -7 3 2 35.537 42.910 4.321 27.919 o -7 3 3 244.058 244.320 8.046 3.822 o -7 3 4 5.609 3.278 2.533 128.450 o -7 3 5 57.216 49.168 4.321 21.822 o -7 3 6 14.191 18.326 3.278 59.543 o -7 3 7 35.322 39.185 4.321 28.556 o -7 3 8 441.607 433.974 11.025 1.641 o -7 3 9 108.266 117.839 6.109 9.718 o -7 3 10 259.339 265.328 8.642 3.428 o -7 3 11 135.753 120.968 6.258 8.281 o -7 3 12 22.656 18.773 3.427 48.417 o -7 3 13 92.045 74.050 5.513 12.925 o -7 3 14 150.784 142.602 4.991 8.067 o -7 3 15 95.266 101.897 6.407 10.515 o -7 3 16 2.319 2.095 1.647 296.265 o -7 3 17 54.726 55.075 3.293 25.459 o -7 3 18 344.159 362.450 7.482 2.488 o -7 3 19 148.232 142.124 7.897 6.472 o -7 3 20 75.494 81.828 4.768 15.451 o -7 4 -6 22.391 21.569 3.082 52.301 o -7 4 -5 59.318 72.606 2.498 24.351 o -7 4 -4 115.032 111.752 7.077 8.627 o -7 4 -3 32.063 43.008 3.686 33.196 o -7 4 -2 12.096 14.286 3.650 56.707 o -7 4 -1 134.697 137.655 6.854 7.590 o -7 4 0 44.830 47.053 3.579 28.372 o -7 4 1 44.740 41.420 4.321 25.554 o -7 4 2 44.884 43.804 4.470 24.513 o -7 4 3 19.720 20.412 3.576 48.047 o -7 4 4 52.367 54.085 4.917 20.175 o -7 4 5 5.237 5.513 2.682 115.062 o -7 4 6 27.875 29.054 4.023 35.471 o -7 4 7 216.711 241.191 8.791 4.010 o -7 4 8 133.695 134.080 6.854 7.685 o -7 4 9 117.617 124.991 6.705 8.578 o -7 4 10 35.295 31.587 4.619 27.887 o -7 4 11 135.148 145.850 7.152 7.243 o -7 4 12 25.579 24.584 4.172 36.230 o -7 4 13 9.861 8.940 3.129 77.104 o -7 4 14 9.626 10.281 3.427 67.592 o -7 4 15 144.226 137.747 4.128 8.953 o -7 4 16 4.202 2.555 1.754 229.829 o -7 4 17 198.924 205.001 9.238 4.361 o -7 4 18 118.961 137.159 4.832 9.790 o -7 4 19 14.466 16.736 2.541 77.370 o -7 5 -6 34.554 36.966 2.302 43.892 o -7 5 -5 49.838 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585.656 552.262 5.359 1.239 o 4 2 7 261.452 243.952 3.922 4.285 o 4 2 8 103.229 103.333 2.730 14.156 o 4 2 9 20.782 18.349 1.665 81.994 o 4 2 10 94.427 93.062 4.309 13.686 o 4 2 11 752.830 755.853 8.641 0.767 o 4 2 12 506.177 488.345 6.021 1.528 o 4 2 13 14.880 13.008 1.598 110.211 o 4 2 14 22.813 23.515 1.998 67.266 o 4 2 15 0.014 -1.688 1.215 783.009 o 4 2 16 4.195 4.401 1.527 250.150 o 4 2 17 437.581 439.113 6.625 1.850 o 4 2 18 79.378 76.561 2.833 18.998 o 4 2 19 5.439 6.313 1.644 199.392 o 4 2 20 0.036 0.739 1.454 513.919 o 4 2 21 5.960 3.536 1.840 187.736 o 4 2 22 0.757 0.194 1.801 327.061 o 4 2 23 11.183 13.726 2.430 92.203 o 4 2 24 75.635 90.112 4.469 15.537 o 4 3 4 3.776 2.629 1.230 347.011 o 4 3 5 858.001 824.795 6.811 0.643 o 4 3 6 250.136 235.690 3.402 4.602 o 4 3 7 11.030 6.597 1.127 177.649 o 4 3 8 441.899 406.854 5.050 1.959 o 4 3 9 820.143 804.553 8.732 0.674 o 4 3 10 389.138 378.501 6.505 2.236 o 4 3 11 231.887 241.915 4.829 4.648 o 4 3 12 248.096 220.875 4.961 4.529 o 4 3 13 13.245 5.066 1.366 151.135 o 4 3 14 167.907 160.309 3.682 7.653 o 4 3 15 97.199 97.055 3.269 14.558 o 4 3 16 120.906 118.603 3.541 11.274 o 4 3 17 193.441 188.529 4.284 6.182 o 4 3 18 16.795 17.329 2.054 84.114 o 4 3 19 109.715 102.974 4.753 11.494 o 4 3 20 0.405 -0.938 1.693 385.656 o 4 3 21 25.239 31.554 3.143 44.938 o 4 3 22 28.039 26.879 2.968 46.505 o 4 3 23 0.233 -3.398 1.901 313.832 o 4 3 24 30.847 36.687 6.681 18.111 o 4 4 4 323.272 337.269 4.108 2.992 o 4 4 5 241.085 234.102 3.502 4.765 o 4 4 6 374.989 392.876 4.803 2.364 o 4 4 7 85.361 81.207 2.453 18.226 o 4 4 8 65.101 55.850 2.240 25.724 o 4 4 9 0.518 1.523 1.312 533.055 o 4 4 10 231.045 220.949 5.259 4.764 o 4 4 11 8.402 3.044 2.092 145.333 o 4 4 12 241.444 228.644 4.977 4.572 o 4 4 13 0.116 -1.043 1.826 343.812 o 4 4 14 12.805 16.740 2.019 96.947 o 4 4 15 14.961 12.475 2.008 97.227 o 4 4 16 1.664 -2.489 1.471 420.688 o 4 4 17 12.743 10.482 2.068 106.153 o 4 4 18 50.546 56.231 9.387 9.585 o 4 4 19 7.372 3.348 2.342 132.329 o 4 4 20 6.406 7.246 2.701 106.054 o 4 4 21 45.111 46.463 4.296 24.936 o 4 4 22 0.061 -0.321 4.768 51.013 o 4 4 23 16.775 21.374 3.901 45.351 o 4 5 4 306.785 290.238 3.049 3.459 o 4 5 5 0.687 0.266 0.795 1256.090 o 4 5 6 340.539 328.478 3.628 2.908 o 4 5 7 0.351 -0.179 0.885 1277.290 o 4 5 8 22.138 21.957 1.468 78.304 o 4 5 9 5.604 4.285 1.105 288.394 o 4 5 10 33.085 39.539 1.849 47.405 o 4 5 11 108.768 81.547 2.450 15.012 o 4 5 12 1.716 2.326 1.259 443.775 o 4 5 13 101.109 87.431 2.667 15.348 o 4 5 14 61.542 58.125 2.406 25.985 o 4 5 15 17.965 24.966 2.184 70.978 o 4 5 16 4.407 6.036 1.737 203.524 o 4 5 17 22.466 17.199 2.422 65.575 o 4 5 18 0.389 0.101 1.802 340.879 o 4 5 19 0.082 2.138 1.930 280.773 o 4 5 20 13.298 13.671 2.568 82.420 o 4 5 21 72.993 77.076 4.186 17.253 o 4 5 22 67.183 72.576 4.258 18.246 o 4 6 4 257.916 261.192 4.514 4.132 o 4 6 5 580.946 551.020 5.051 1.255 o 4 6 6 114.776 109.600 2.425 12.969 o 4 6 7 135.552 142.723 2.771 10.008 o 4 6 8 6.801 10.102 1.310 191.976 o 4 6 9 12.434 8.286 1.331 147.086 o 4 6 10 341.778 359.306 4.419 2.729 o 4 6 11 4.601 2.383 1.269 313.910 o 4 6 12 309.810 283.436 4.802 3.327 o 4 6 13 79.414 81.919 3.718 16.973 o 4 6 14 10.712 15.611 2.301 95.455 o 4 6 15 54.866 54.692 2.951 26.724 o 4 6 16 4.318 3.260 1.737 224.823 o 4 6 17 59.714 52.656 3.058 25.257 o 4 6 18 11.055 10.009 1.999 117.024 o 4 6 19 7.904 4.076 2.095 144.965 o 4 6 20 7.413 6.334 2.229 131.544 o 4 7 4 0.029 0.265 1.029 1039.890 o 4 7 5 349.933 345.475 4.289 2.727 o 4 7 6 95.043 103.259 2.598 15.201 o 4 7 7 39.198 40.850 2.208 40.072 o 4 7 8 98.325 107.548 2.996 14.185 o 4 7 9 2.925 3.747 1.443 304.719 o 4 7 10 51.768 55.476 2.549 29.090 o 4 7 11 80.893 94.930 3.147 16.843 o 4 7 12 18.547 13.120 2.086 84.150 o 4 7 13 83.173 91.721 3.413 16.339 o 4 7 14 41.414 42.248 2.704 35.468 o 4 7 15 57.113 59.552 5.032 18.616 o 4 7 16 16.851 17.155 2.366 76.537 o 4 7 17 7.636 6.054 1.997 147.396 o 4 7 18 0.218 1.649 1.839 309.180 o 4 7 19 16.033 13.311 2.327 83.489 o 4 8 4 70.235 73.679 4.296 17.632 o 4 8 5 97.663 105.714 3.079 14.262 o 4 8 6 3.903 5.414 1.515 247.885 o 4 8 7 132.283 133.826 3.433 10.111 o 4 8 8 35.821 36.515 2.365 42.675 o 4 8 9 222.339 216.947 4.346 5.153 o 4 8 10 129.469 124.025 3.532 10.523 o 4 8 11 10.350 13.240 1.859 119.358 o 4 8 12 9.801 4.539 1.788 152.545 o 4 8 13 109.406 107.228 3.805 12.347 o 4 8 14 200.888 205.563 5.333 5.496 o 4 8 15 119.547 129.225 4.516 10.237 o 4 8 16 1.675 0.832 1.871 273.251 o 4 8 17 52.298 51.066 3.341 26.525 o 4 9 4 44.460 47.795 2.768 32.454 o 4 9 5 39.586 41.720 2.531 37.603 o 4 9 6 69.372 67.377 2.908 21.605 o 4 9 7 11.915 12.648 1.865 113.378 o 4 9 8 13.391 15.561 1.924 100.103 o 4 9 9 8.808 8.120 1.792 146.478 o 4 9 10 85.320 85.576 3.311 16.622 o 4 9 11 59.169 56.932 3.035 24.904 o 4 9 12 63.422 61.789 4.473 19.102 o 4 9 13 0.044 2.505 2.839 136.224 o 4 9 14 58.795 67.700 3.566 22.056 o 4 10 4 5.884 7.141 1.820 172.031 o 4 10 5 33.542 32.953 2.486 44.640 o 4 10 6 18.099 17.825 2.134 78.669 o 4 10 7 233.384 239.933 5.306 4.551 o 4 10 8 2.940 3.967 2.538 141.294 o 4 10 9 10.529 5.844 1.851 138.874 o 4 10 10 2.788 2.696 1.836 239.001 o 5 0 5 963.823 958.090 13.409 0.488 o 5 0 7 135.597 124.097 4.768 9.309 o 5 0 9 97.311 86.550 4.470 13.496 o 5 0 11 98.653 89.666 5.364 12.029 o 5 0 13 14.115 7.719 2.067 106.218 o 5 0 15 47.847 50.741 6.332 16.467 o 5 0 17 74.154 73.491 8.783 9.171 o 5 0 19 41.526 49.257 4.332 25.320 o 5 0 21 173.750 164.859 7.822 5.648 o 5 1 5 124.424 125.993 2.577 11.405 o 5 1 6 64.368 52.446 2.012 27.041 o 5 1 7 1.802 2.243 1.092 518.523 o 5 1 8 291.773 296.757 5.129 3.415 o 5 1 9 26.482 22.618 1.925 63.406 o 5 1 10 0.225 1.345 1.254 612.950 o 5 1 11 0.078 -0.266 1.238 743.345 o 5 1 12 429.543 406.835 6.459 1.962 o 5 1 13 58.833 68.700 3.123 23.242 o 5 1 14 10.880 17.696 2.095 99.007 o 5 1 15 189.262 184.570 6.782 5.517 o 5 1 16 44.336 41.041 3.003 32.699 o 5 1 17 201.932 200.177 5.378 5.520 o 5 1 18 409.664 423.307 7.817 1.951 o 5 1 19 96.341 90.889 5.658 11.755 o 5 1 20 4.346 1.082 1.934 211.192 o 5 1 21 91.838 93.273 4.631 13.458 o 5 1 22 4.602 3.717 2.186 163.235 o 5 2 5 1202.420 1180.670 8.938 0.349 o 5 2 6 8.274 7.754 1.125 203.318 o 5 2 7 10.187 4.875 1.198 191.730 o 5 2 8 141.745 146.262 3.446 9.232 o 5 2 9 227.100 229.885 4.425 4.917 o 5 2 10 270.244 249.328 4.757 4.010 o 5 2 11 55.638 60.817 2.819 26.050 o 5 2 12 107.512 111.196 4.018 12.126 o 5 2 13 0.192 0.082 1.488 505.528 o 5 2 14 18.966 14.285 2.093 81.623 o 5 2 15 1205.190 1200.430 13.269 0.336 o 5 2 16 310.185 320.576 6.634 2.971 o 5 2 17 26.567 28.956 2.899 47.634 o 5 2 18 122.469 125.390 4.940 9.832 o 5 2 19 11.983 8.815 2.207 106.314 o 5 2 20 32.962 32.642 3.107 39.816 o 5 2 21 0.284 1.106 1.989 272.745 o 5 2 22 20.814 20.974 2.939 56.441 o 5 3 5 368.737 349.823 4.088 2.582 o 5 3 6 312.497 303.711 4.136 3.251 o 5 3 7 7.157 4.586 1.120 247.534 o 5 3 8 186.774 188.212 3.984 6.459 o 5 3 9 58.071 67.126 4.227 20.268 o 5 3 10 149.850 136.418 4.555 8.482 o 5 3 11 64.825 62.993 3.835 20.547 o 5 3 12 918.939 923.635 10.697 0.540 o 5 3 13 208.384 220.743 8.343 4.375 o 5 3 14 44.661 46.322 2.975 31.622 o 5 3 15 115.542 111.553 4.115 11.417 o 5 3 16 8.613 6.481 1.877 147.807 o 5 3 17 0.552 -0.734 2.391 196.343 o 5 3 18 17.983 18.706 2.509 69.828 o 5 3 19 19.108 18.415 2.540 67.579 o 5 3 20 89.307 97.832 6.050 11.463 o 5 3 21 31.792 30.164 6.556 18.895 o 5 4 5 1956.530 1835.610 13.147 0.147 o 5 4 6 281.899 266.472 4.091 3.817 o 5 4 7 559.146 559.134 6.419 1.276 o 5 4 8 13.259 12.084 2.323 92.398 o 5 4 9 3.327 -0.238 1.335 390.088 o 5 4 10 266.157 277.098 5.415 3.793 o 5 4 11 395.036 353.158 6.689 2.263 o 5 4 12 63.733 73.325 3.794 19.918 o 5 4 13 65.236 78.027 3.470 20.036 o 5 4 14 3.437 0.592 1.548 310.648 o 5 4 15 156.317 160.078 4.842 7.597 o 5 4 16 0.612 -1.636 1.575 429.885 o 5 4 17 10.213 10.813 3.035 77.558 o 5 4 18 7.980 8.879 2.265 119.989 o 5 4 19 4.514 3.593 2.831 112.792 o 5 4 20 77.566 77.951 11.465 6.311 o 5 5 5 45.059 42.590 2.046 37.014 o 5 5 6 553.561 568.602 6.629 1.274 o 5 5 7 607.365 582.846 6.932 1.135 o 5 5 8 31.204 25.296 4.098 34.188 o 5 5 9 60.448 55.074 2.644 26.048 o 5 5 10 49.864 45.804 3.211 28.672 o 5 5 11 16.715 12.376 3.826 50.014 o 5 5 12 9.907 7.476 3.014 82.385 o 5 5 13 8.120 7.196 1.901 147.016 o 5 5 14 171.045 180.637 5.157 6.636 o 5 5 15 12.664 13.483 1.962 104.973 o 5 5 16 83.944 79.718 3.783 16.401 o 5 5 17 38.700 42.759 3.395 32.405 o 5 5 18 0.047 -1.247 1.875 328.661 o 5 5 19 83.847 90.085 7.279 10.336 o 5 6 5 181.260 179.181 3.779 6.825 o 5 6 6 103.682 103.089 3.136 13.724 o 5 6 7 224.468 241.774 4.639 4.816 o 5 6 8 281.939 275.172 5.093 3.652 o 5 6 9 306.297 297.326 4.765 3.295 o 5 6 10 714.931 723.423 8.829 0.829 o 5 6 11 194.812 187.682 4.387 6.127 o 5 6 12 2.650 1.587 1.541 321.750 o 5 6 13 85.932 94.322 3.524 15.661 o 5 6 14 31.876 34.676 3.041 40.417 o 5 6 15 6.115 6.732 2.166 142.663 o 5 6 16 6.954 8.417 2.148 133.614 o 5 6 17 5.133 4.474 2.193 155.281 o 5 6 18 87.938 95.983 4.468 13.936 o 5 7 5 32.347 36.070 2.107 47.536 o 5 7 6 24.169 23.195 1.926 66.439 o 5 7 7 7.732 7.922 1.550 173.923 o 5 7 8 12.032 11.312 1.723 121.988 o 5 7 9 15.193 17.949 2.126 85.418 o 5 7 10 188.176 185.092 4.646 6.264 o 5 7 11 383.467 409.979 6.864 2.161 o 5 7 12 67.911 64.327 3.618 20.433 o 5 7 13 15.010 6.565 2.111 103.308 o 5 7 14 36.097 39.910 3.173 35.657 o 5 7 15 23.701 18.963 2.608 59.527 o 5 7 16 127.207 124.310 5.182 9.416 o 5 8 5 1.474 1.569 1.529 369.006 o 5 8 6 205.374 231.654 4.949 5.220 o 5 8 7 31.593 29.414 2.456 47.886 o 5 8 8 0.071 0.601 1.633 414.742 o 5 8 9 39.970 37.222 2.706 37.516 o 5 8 10 6.338 5.627 1.845 172.503 o 5 8 11 18.477 19.267 2.645 65.812 o 5 8 12 38.678 35.099 4.445 27.426 o 5 8 13 88.630 85.001 4.075 15.038 o 5 9 5 12.280 13.404 2.038 103.667 o 5 9 6 8.036 4.323 1.884 159.843 o 5 9 7 25.425 26.147 2.838 50.571 o 5 9 8 68.028 79.166 5.009 15.955 o 5 9 9 25.629 27.906 2.713 51.116 o 5 9 10 0.812 1.244 1.785 313.885 o 6 0 6 5.232 4.470 1.937 179.879 o 6 0 8 115.660 129.014 5.513 9.610 o 6 0 10 21.406 23.839 3.427 47.380 o 6 0 12 18.870 13.707 3.129 59.596 o 6 0 14 13.663 13.111 3.129 67.043 o 6 0 16 46.115 56.022 5.215 20.008 o 6 0 18 42.545 46.039 5.513 20.294 o 6 0 20 70.675 78.207 6.705 12.379 o 6 1 6 76.894 65.587 2.648 20.809 o 6 1 7 368.625 357.403 6.024 2.450 o 6 1 8 21.367 31.552 2.461 56.938 o 6 1 9 234.864 240.339 5.345 4.516 o 6 1 10 50.594 48.031 3.001 28.976 o 6 1 11 12.751 10.298 2.002 109.151 o 6 1 12 2.973 0.624 2.756 132.281 o 6 1 13 18.921 27.027 2.821 57.039 o 6 1 14 4.345 2.669 1.841 213.468 o 6 1 15 24.563 17.925 2.522 60.464 o 6 1 16 0.022 0.089 1.841 339.913 o 6 1 17 55.150 55.927 3.941 22.895 o 6 1 18 12.691 15.965 2.845 73.501 o 6 1 19 2.427 5.206 3.799 71.453 o 6 2 6 0.734 2.123 1.212 549.817 o 6 2 7 194.141 195.044 3.976 6.158 o 6 2 8 590.686 581.752 7.426 1.162 o 6 2 9 0.438 0.040 2.257 220.788 o 6 2 10 85.728 103.287 3.440 15.275 o 6 2 11 17.082 21.076 2.512 69.273 o 6 2 12 43.294 40.824 2.804 34.327 o 6 2 13 76.697 80.852 3.522 17.807 o 6 2 14 92.368 90.743 3.814 14.708 o 6 2 15 79.273 76.919 3.627 17.515 o 6 2 16 97.199 116.609 4.399 12.313 o 6 2 17 47.225 52.005 3.545 27.018 o 6 2 18 3.140 -0.124 1.829 259.706 o 6 2 19 43.069 48.239 3.647 28.407 o 6 3 6 0.053 -0.761 1.157 855.713 o 6 3 7 2.549 3.831 1.286 356.193 o 6 3 8 68.662 77.927 2.948 20.595 o 6 3 9 117.691 118.674 3.954 11.160 o 6 3 10 309.209 295.206 5.657 3.192 o 6 3 11 53.830 54.614 2.903 27.232 o 6 3 12 117.621 125.941 4.263 10.665 o 6 3 13 1.425 2.275 2.273 190.774 o 6 3 14 243.093 257.330 6.006 4.141 o 6 3 15 26.512 21.946 2.555 55.272 o 6 3 16 8.463 7.254 2.130 129.587 o 6 3 17 353.276 351.076 7.403 2.472 o 6 3 18 3.953 4.376 2.172 167.462 o 6 4 6 0.290 -0.324 1.050 962.196 o 6 4 7 209.994 203.267 4.925 5.429 o 6 4 8 353.372 340.375 5.348 2.656 o 6 4 9 0.606 -0.985 1.672 385.463 o 6 4 10 83.567 104.743 4.175 14.371 o 6 4 11 13.618 10.470 1.934 108.120 o 6 4 12 66.603 76.132 3.605 19.638 o 6 4 13 198.630 192.829 5.272 5.710 o 6 4 14 1.313 3.320 2.097 212.491 o 6 4 15 223.601 258.059 6.292 4.367 o 6 4 16 6.666 7.378 2.093 142.405 o 6 4 17 257.507 271.191 6.825 3.725 o 6 5 6 229.608 230.152 4.296 4.891 o 6 5 7 3.914 6.335 1.612 224.999 o 6 5 8 22.951 23.882 2.169 64.124 o 6 5 9 236.832 240.305 4.855 4.573 o 6 5 10 103.888 110.728 3.989 12.466 o 6 5 11 68.992 72.278 5.795 14.521 o 6 5 12 56.608 54.828 3.255 25.122 o 6 5 13 0.339 0.175 1.890 311.607 o 6 5 14 76.198 74.198 3.763 17.895 o 6 5 15 0.517 -0.592 1.931 296.777 o 6 5 16 97.860 94.970 4.416 13.142 o 6 6 6 59.606 66.774 3.632 21.785 o 6 6 7 83.853 101.645 3.377 15.683 o 6 6 8 29.405 34.951 2.449 47.465 o 6 6 9 1.915 3.297 1.625 296.297 o 6 6 10 1.202 1.684 1.673 328.979 o 6 6 11 10.845 7.818 2.510 99.001 o 6 6 12 94.911 100.908 4.763 12.682 o 6 6 13 85.687 91.064 4.169 14.878 o 6 6 14 0.013 -0.163 1.819 350.508 o 6 7 6 5.556 4.939 1.770 192.191 o 6 7 7 65.782 82.615 3.241 20.050 o 6 7 8 1.538 -1.228 1.527 402.938 o 6 7 9 137.576 148.922 4.331 8.887 o 6 7 10 22.191 17.169 2.308 68.110 o 6 7 11 0.071 2.371 2.256 209.611 o 6 7 12 42.253 48.501 5.066 21.941 o 6 8 6 277.670 295.433 11.692 2.670 o 6 8 7 79.639 90.625 4.231 15.476 o 6 8 8 0.061 0.532 2.061 265.850 o 6 8 9 84.207 85.330 3.933 15.761 o 7 0 7 313.948 291.700 8.344 2.870 o 7 0 9 86.216 80.889 5.215 13.616 o 7 0 11 165.134 179.523 7.599 5.773 o 7 0 13 1.969 -2.086 2.235 203.694 o 7 0 15 9.856 5.364 3.278 75.708 o 7 1 7 135.236 131.197 4.105 9.595 o 7 1 8 38.883 37.768 3.501 32.685 o 7 1 9 111.621 100.606 3.987 12.251 o 7 1 10 146.754 137.752 7.375 6.877 o 7 1 11 27.183 23.230 5.215 27.496 o 7 1 12 13.557 13.702 2.369 87.879 o 7 1 13 5.373 3.968 1.993 174.945 o 7 1 14 23.022 31.915 3.212 45.672 o 7 1 15 3.532 3.906 2.183 172.249 o 7 1 16 2.174 -0.478 2.052 232.639 o 7 2 7 3.137 3.989 1.610 261.459 o 7 2 8 15.045 11.978 1.896 101.495 o 7 2 9 3.921 1.117 1.647 268.644 o 7 2 10 10.050 5.049 1.862 143.899 o 7 2 11 72.909 72.437 3.818 18.410 o 7 2 12 30.810 31.247 3.181 40.894 o 7 2 13 366.279 367.005 8.411 2.270 o 7 2 14 60.368 62.555 6.183 14.950 o 7 2 15 1.874 3.150 2.205 190.337 o 7 3 7 67.639 68.230 3.110 21.393 o 7 3 8 11.913 11.802 2.607 86.670 o 7 3 9 2.041 1.276 1.647 316.286 o 7 3 10 43.523 46.794 3.220 30.703 o 7 3 11 19.312 23.543 2.884 57.577 o 7 3 12 19.338 27.683 4.023 40.194 o 7 3 13 35.803 42.451 3.501 32.992 o 7 3 14 103.958 107.148 8.791 7.566 o 7 4 7 0.299 -1.664 1.762 361.542 o 7 4 8 74.039 83.159 3.281 18.505 o 7 4 9 116.656 129.105 4.050 10.800 o 7 4 10 2.757 1.157 1.923 237.174 o 7 4 11 14.963 19.242 2.313 79.590 o 7 4 12 4.453 0.974 1.772 236.119 o 7 4 13 5.198 7.261 2.355 132.682 o 7 5 7 50.827 55.233 2.772 28.607 o 7 5 8 70.133 78.114 3.395 19.337 o 7 5 9 0.003 -0.261 1.646 428.147 o 7 5 10 1.640 1.976 2.238 195.047 o 7 5 11 89.168 91.866 4.835 13.461 o 7 6 7 98.774 115.950 3.713 12.976 o 7 6 8 104.624 116.945 5.312 10.768 o 7 6 9 7.237 9.582 3.488 70.094 o 8 0 8 27.973 18.624 3.576 42.711 o 8 0 10 6.037 6.556 3.129 88.111 o 8 1 8 1.850 1.463 1.937 248.260 o 8 1 9 22.466 18.199 4.544 35.511 o 8 1 10 2.400 3.254 1.993 214.185 o 8 2 8 3.064 5.103 2.011 191.262 o 8 2 9 28.827 31.497 2.968 44.174 o 8 2 10 0.025 -1.043 1.791 360.851 o 8 3 8 4.314 3.895 1.788 212.750 o 8 3 9 1.913 2.868 4.693 49.974 o ; _iucr_refine_instructions_details ; TITL 20zs_diiso4cl_0m_a.res in P2(1)/n REM Old TITL 20zs_Diiso4Cl_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.140, Rweak 0.006, Alpha 0.020, Orientation as input REM Formula found by SHELXT: C19 N Cl CELL 0.71073 7.2828 9.9427 24.0413 90 97.012 90 ZERR 4 0.0001 0.0001 0.0002 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl N UNIT 76 88 4 4 EQIV $1 -1+X,+Y,+Z L.S. 4 PLAN 5 0 0 SIZE 0.14 0.19 0.31 TEMP -123.15 HTAB C4 N1_$1 CONF BOND $H list 4 fmap 2 acta MORE -1 WGHT 0.0427 0.5336 FVAR 0.819249 REM REM REM Cl1 3 0.15484 0.97803 0.44796 11.00000 0.04260 0.04426 0.04366 = -0.00576 0.00958 0.01646 N1 4 0.80833 0.57958 0.35726 11.00000 0.02707 0.02603 0.02591 = -0.00195 0.00252 0.00130 C8 1 0.91106 0.48143 0.33087 11.00000 0.02270 0.02285 0.02890 = -0.00411 0.00149 -0.00174 C1 1 0.59772 0.78046 0.40866 11.00000 0.02578 0.03259 0.02338 = -0.00011 0.00110 0.00071 AFIX 43 H1 2 0.72846 0.78793 0.41612 11.00000 -1.20000 AFIX 0 C6 1 0.51918 0.67445 0.37577 11.00000 0.02672 0.02524 0.02354 = 0.00342 0.00470 0.00042 C9 1 1.03406 0.39964 0.36577 11.00000 0.02979 0.02439 0.02866 = -0.00240 0.00066 -0.00139 C7 1 0.63360 0.57270 0.35208 11.00000 0.02810 0.02445 0.02619 = -0.00101 0.00333 -0.00273 AFIX 43 H7 2 0.57422 0.49904 0.33214 11.00000 -1.20000 AFIX 0 C5 1 0.32765 0.66604 0.36458 11.00000 0.02757 0.02900 0.03132 = -0.00025 0.00437 -0.00329 AFIX 43 H5 2 0.27367 0.59525 0.34159 11.00000 -1.20000 AFIX 0 C13 1 0.90169 0.47548 0.27210 11.00000 0.02459 0.02725 0.02824 = -0.00338 -0.00008 -0.00024 C10 1 1.14421 0.30916 0.34089 11.00000 0.03264 0.02921 0.03723 = -0.00109 -0.00239 0.00630 AFIX 43 H10 2 1.22564 0.25160 0.36378 11.00000 -1.20000 AFIX 0 C3 1 0.29561 0.86193 0.41926 11.00000 0.03411 0.03096 0.02560 = 0.00344 0.00773 0.00873 C2 1 0.48633 0.87440 0.43037 11.00000 0.03466 0.03148 0.02430 = -0.00324 0.00202 0.00107 AFIX 43 H2 2 0.53959 0.94666 0.45264 11.00000 -1.20000 AFIX 0 C4 1 0.21411 0.75912 0.38638 11.00000 0.02388 0.03590 0.03481 = 0.00320 0.00419 0.00131 AFIX 43 H4 2 0.08331 0.75237 0.37889 11.00000 -1.20000 AFIX 0 C12 1 1.01888 0.38454 0.24947 11.00000 0.03377 0.03627 0.02842 = -0.00670 0.00248 0.00285 AFIX 43 H12 2 1.01714 0.37968 0.20995 11.00000 -1.20000 AFIX 0 C18 1 0.77012 0.56108 0.23281 11.00000 0.03074 0.03256 0.02704 = -0.00371 -0.00078 0.00408 AFIX 13 H18 2 0.71254 0.62907 0.25598 11.00000 -1.20000 AFIX 0 C11 1 1.13700 0.30168 0.28314 11.00000 0.03311 0.03451 0.03899 = -0.00871 0.00389 0.00905 AFIX 43 H11 2 1.21342 0.23946 0.26670 11.00000 -1.20000 AFIX 0 C15 1 1.03895 0.41001 0.42906 11.00000 0.04475 0.02888 0.02780 = -0.00057 -0.00088 0.00350 AFIX 13 H15 2 1.00692 0.50485 0.43781 11.00000 -1.20000 AFIX 0 C17 1 0.61475 0.47342 0.20313 11.00000 0.03699 0.04708 0.04090 = -0.00379 -0.00989 0.00135 AFIX 137 H17a 2 0.66833 0.40308 0.18153 11.00000 -1.50000 H17b 2 0.54549 0.43176 0.23108 11.00000 -1.50000 H17c 2 0.53118 0.52939 0.17780 11.00000 -1.50000 AFIX 0 C19 1 0.86848 0.63671 0.18983 11.00000 0.04698 0.04527 0.04173 = 0.00917 0.00518 0.00477 AFIX 137 H19a 2 0.96729 0.69236 0.20928 11.00000 -1.50000 H19b 2 0.92180 0.57206 0.16554 11.00000 -1.50000 H19c 2 0.77955 0.69430 0.16707 11.00000 -1.50000 AFIX 0 C16 1 1.22961 0.38041 0.46089 11.00000 0.05824 0.04630 0.03378 = 0.00171 -0.01036 0.00744 AFIX 137 H16a 2 1.25937 0.28510 0.45673 11.00000 -1.50000 H16b 2 1.32293 0.43583 0.44566 11.00000 -1.50000 H16c 2 1.22865 0.40136 0.50069 11.00000 -1.50000 AFIX 0 C14 1 0.89109 0.31941 0.44936 11.00000 0.06272 0.03904 0.03398 = 0.00086 0.01141 -0.00064 AFIX 137 H14a 2 0.76898 0.34572 0.43087 11.00000 -1.50000 H14b 2 0.91578 0.22560 0.44021 11.00000 -1.50000 H14c 2 0.89373 0.32883 0.49003 11.00000 -1.50000 AFIX 0 HKLF 4 END Q1 1 0.416667 0.65625 0.38 11 0.05 0.24 Q2 1 1.041667 0.40625 0.4 11 0.05 0.24 Q3 1 0.833333 0.53125 0.253333 11 0.05 0.22 Q4 1 0.375 0.84375 0.433333 11 0.05 0.22 Q5 1 1.125 0.40625 0.446667 11 0.05 0.21 Q6 1 1.125 0.375 0.353333 11 0.05 0.21 Q7 1 0.541667 0.84375 0.406667 11 0.05 0.21 Q8 1 0.541667 0.71875 0.393333 11 0.05 0.2 Q9 1 0.583333 0.625 0.366667 11 0.05 0.2 Q10 1 0.916667 0.40625 0.26 11 0.05 0.2 Q11 1 0.708333 0.53125 0.22 11 0.05 0.2 Q12 1 0.875 0.46875 0.3 11 0.05 0.19 Q13 1 0.25 0.8125 0.4 11 0.05 0.18 Q14 1 0.958333 0.4375 0.346667 11 0.05 0.18 Q15 1 0.25 1.03125 0.433333 11 0.05 0.18 Q16 1 0.25 0.90625 0.426667 11 0.05 0.17 Q17 1 1.041667 0.3125 0.273333 11 0.05 0.17 Q18 1 0.875 0.625 0.38 11 0.05 0.16 Q19 1 0.708333 0.59375 0.34 11 0.05 0.15 Q20 1 0.958333 0.375 0.433333 11 0.05 0.15 REM The information below was added by Olex2. REM REM R1 = 0.0337 for 2966 Fo > 4sig(Fo) and 0.0411 for all 3448 data REM 194 parameters refined using 0 restraints REM Highest difference peak 0.2397, deepest hole -0.2428 REM Mean Shift 0.0000, Max Shift 0.0002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0411 REM R1_gt = 0.0337 REM wR_ref = 0.0927 REM GOOF = 1.0495 REM Shift_max = 0.0002 REM Shift_mean = 0.0000 REM Reflections_all = 3448 REM Reflections_gt = 2966 REM Parameters = 194 REM Hole = -0.2428 REM Peak = 0.2397 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received'