#============================================================================== data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 12 _journal_issue 2 _journal_year 2021 _journal_page_first 147 _journal_page_last 153 #============================================================================== data_121227_6__18hdimer_1 # start Validation Reply Form _vrf_PLAT082_121227_6__18hdimer_1 ; PROBLEM: High R1 Value .................................. 0.17 Report RESPONSE: The diffraction was weak and thus agreement factors were high. The value was finally achieved by nallowing the theta. ; _vrf_PLAT084_121227_6__18hdimer_1 ; PROBLEM: High wR2 Value (i.e. > 0.25) ................... 0.45 Report RESPONSE: The diffraction is also due to weak diffraction. ; _vrf_PLAT097_121227_6__18hdimer_1 ; PROBLEM: Large Reported Max. (Positive) Residual Density 0.83 eA-3 RESPONSE: his is probably because, as a result of choosing the reflection data with strong diffraction intensity in order to achieve an appropriate R value, diffraction points that are not usually a problem are also included. ; _vrf_PLAT340_121227_6__18hdimer_1 ; PROBLEM: Low Bond Precision on C-C Bonds ............... 0.01226 Ang. RESPONSE: The diffraction is also due to weak diffraction. ; # end Validation Reply Form _audit_update_record ; 2021-03-01 # Formatted by publCIF ; _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C58 H38 O10' _chemical_formula_weight 894.88 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 7.798(4) _cell_length_b 14.957(7) _cell_length_c 19.498(9) _cell_angle_alpha 90 _cell_angle_beta 96.058(6) _cell_angle_gamma 90 _cell_volume 2261.5(18) _cell_formula_units_Z 2 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 6702 _cell_measurement_theta_min 1.72 _cell_measurement_theta_max 31.32 _exptl_crystal_description block _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.314 _exptl_crystal_F_000 932 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.200 _exptl_absorpt_coefficient_mu 0.090 _shelx_estimated_absorpt_T_min 0.982 _shelx_estimated_absorpt_T_max 0.982 _exptl_absorpt_correction_type numerical _exptl_absorpt_correction_T_min 0.9672 _exptl_absorpt_correction_T_max 0.9856 _exptl_absorpt_process_details ; NUMABS (Higashi, 1999) ; _exptl_absorpt_special_details ; ? ; _diffrn_ambient_temperature 173.1500 _diffrn_radiation_wavelength 0.7107 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Rigaku Saturn70' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 7.314 _diffrn_reflns_number 15616 _diffrn_reflns_av_unetI/netI 0.0550 _diffrn_reflns_av_R_equivalents 0.0614 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_theta_min 2.503 _diffrn_reflns_theta_max 25.998 _diffrn_reflns_theta_full 25.241 _diffrn_measured_fraction_theta_max 0.970 _diffrn_measured_fraction_theta_full 0.975 _diffrn_reflns_Laue_measured_fraction_max 0.970 _diffrn_reflns_Laue_measured_fraction_full 0.975 _diffrn_reflns_point_group_measured_fraction_max 0.970 _diffrn_reflns_point_group_measured_fraction_full 0.975 _reflns_number_total 4320 _reflns_number_gt 3615 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrystalClear (Rigaku/MSC Inc., 2006)' _computing_cell_refinement 'CrystalClear (Rigaku/MSC Inc., 2006)' _computing_data_reduction 'CrystalClear (Rigaku/MSC Inc., 2006)' _computing_structure_solution 'Il Milione (Burla, et al., 2007)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'CrystalStructure 4.0' _computing_publication_material 'CrystalStructure 4.0 (Rigaku, 2010)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1236P)^2^+39.9308P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4320 _refine_ls_number_parameters 307 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1798 _refine_ls_R_factor_gt 0.1673 _refine_ls_wR_factor_ref 0.4454 _refine_ls_wR_factor_gt 0.4394 _refine_ls_goodness_of_fit_ref 1.094 _refine_ls_restrained_S_all 1.094 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O4 O 0.4402(8) 0.2605(4) 0.4976(3) 0.0313(14) Uani 1 1 d . . . . . O2 O 0.3447(8) 0.0424(4) 0.2961(3) 0.0319(14) Uani 1 1 d . . . . . O1 O 0.0975(7) 0.2026(4) 0.3557(3) 0.0322(14) Uani 1 1 d . . . . . O5 O 0.0470(9) -0.1338(4) 0.3292(3) 0.0357(15) Uani 1 1 d . . . . . O3 O 0.1893(9) 0.3189(5) 0.5240(4) 0.0492(19) Uani 1 1 d . . . . . C9 C 0.2381(10) 0.0441(5) 0.4422(4) 0.0237(16) Uani 1 1 d . . . . . C10 C 0.2478(9) 0.0004(5) 0.5066(4) 0.0235(16) Uani 1 1 d . . . . . C1 C 0.2982(10) 0.1352(6) 0.4395(4) 0.0277(17) Uani 1 1 d . . . . . C8 C 0.1704(10) -0.0047(5) 0.3819(4) 0.0254(17) Uani 1 1 d . . . . . C3 C 0.3950(11) 0.1282(6) 0.5622(4) 0.0293(18) Uani 1 1 d . . . . . H3 H 0.453119 0.156277 0.601783 0.035 Uiso 1 1 calc R U . . . C6 C 0.0998(10) -0.1297(5) 0.4534(4) 0.0268(17) Uani 1 1 d . . . . . H6 H 0.048085 -0.186702 0.457330 0.032 Uiso 1 1 calc R U . . . C11 C 0.2526(10) 0.1957(5) 0.3778(4) 0.0240(16) Uani 1 1 d . . . . . C18 C 0.1972(10) 0.0272(5) 0.3102(4) 0.0245(16) Uani 1 1 d . . . . . C7 C 0.1020(10) -0.0899(5) 0.3886(4) 0.0256(17) Uani 1 1 d . . . . . C5 C 0.1730(10) -0.0859(6) 0.5121(4) 0.0291(18) Uani 1 1 d . . . . . H5 H 0.173303 -0.113502 0.555963 0.035 Uiso 1 1 calc R U . . . C26 C 0.3341(12) 0.3292(6) 0.5094(4) 0.0330(19) Uani 1 1 d . . . . . C4 C 0.3286(11) 0.0429(6) 0.5660(4) 0.0312(18) Uani 1 1 d . . . . . H4 H 0.337500 0.012615 0.609077 0.037 Uiso 1 1 calc R U . . . C12 C 0.3889(11) 0.2442(5) 0.3455(4) 0.0275(17) Uani 1 1 d . . . . . C2 C 0.3745(11) 0.1719(5) 0.4988(4) 0.0289(18) Uani 1 1 d . . . . . C13 C 0.5590(11) 0.2150(6) 0.3561(4) 0.0296(18) Uani 1 1 d . . . . . H13 H 0.588022 0.164945 0.385084 0.035 Uiso 1 1 calc R U . . . C27 C 0.4219(11) 0.4162(6) 0.5040(4) 0.0293(18) Uani 1 1 d . . . . . C24 C -0.1199(10) 0.0500(6) 0.2751(4) 0.0287(17) Uani 1 1 d . . . . . H24 H -0.139026 0.050327 0.322375 0.034 Uiso 1 1 calc R U . . . C19 C 0.0459(10) 0.0375(6) 0.2565(4) 0.0283(18) Uani 1 1 d . . . . . C17 C 0.3454(13) 0.3167(6) 0.3030(5) 0.040(2) Uani 1 1 d . . . . . H17 H 0.229372 0.336969 0.295894 0.048 Uiso 1 1 calc R U . . . C29 C 0.3466(12) 0.4924(6) 0.5295(5) 0.036(2) Uani 1 1 d . . . . . H29 H 0.240951 0.487365 0.549345 0.043 Uiso 1 1 calc R U . . . C28 C 0.5746(12) 0.4242(6) 0.4741(5) 0.035(2) Uani 1 1 d . . . . . H28 H 0.625707 0.372926 0.455943 0.042 Uiso 1 1 calc R U . . . C14 C 0.6869(13) 0.2589(6) 0.3244(5) 0.041(2) Uani 1 1 d . . . . . H14 H 0.803397 0.239603 0.332013 0.049 Uiso 1 1 calc R U . . . C25 C 0.0089(16) -0.2271(6) 0.3339(6) 0.050(3) Uani 1 1 d . . . . . H25A H -0.029027 -0.250441 0.287868 0.060 Uiso 1 1 calc R U . . . H25B H 0.112542 -0.259133 0.353191 0.060 Uiso 1 1 calc R U . . . H25C H -0.082939 -0.235447 0.363980 0.060 Uiso 1 1 calc R U . . . C23 C -0.2570(11) 0.0618(7) 0.2247(5) 0.037(2) Uani 1 1 d . . . . . H23 H -0.369741 0.072578 0.237113 0.044 Uiso 1 1 calc R U . . . C15 C 0.6422(13) 0.3313(6) 0.2816(6) 0.043(2) Uani 1 1 d . . . . . H15 H 0.728782 0.361388 0.259599 0.052 Uiso 1 1 calc R U . . . C22 C -0.2272(14) 0.0578(7) 0.1558(5) 0.045(2) Uani 1 1 d . . . . . H22 H -0.321133 0.063553 0.120871 0.054 Uiso 1 1 calc R U . . . C20 C 0.0730(13) 0.0354(7) 0.1864(5) 0.042(2) Uani 1 1 d . . . . . H20 H 0.185873 0.026764 0.173343 0.050 Uiso 1 1 calc R U . . . C16 C 0.4742(14) 0.3597(7) 0.2706(5) 0.045(2) Uani 1 1 d . . . . . H16 H 0.445231 0.408921 0.240856 0.054 Uiso 1 1 calc R U . . . C21 C -0.0624(14) 0.0456(8) 0.1375(5) 0.048(3) Uani 1 1 d . . . . . H21 H -0.043837 0.044420 0.090108 0.058 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O4 0.035(3) 0.028(3) 0.031(3) -0.003(2) 0.004(2) -0.010(3) O2 0.031(3) 0.031(3) 0.034(3) -0.001(3) 0.006(2) 0.002(3) O1 0.028(3) 0.030(3) 0.038(3) 0.007(3) -0.001(2) 0.001(2) O5 0.054(4) 0.020(3) 0.033(3) -0.006(2) 0.004(3) -0.007(3) O3 0.043(4) 0.035(4) 0.073(5) -0.007(3) 0.022(4) -0.013(3) C9 0.023(4) 0.024(4) 0.026(4) 0.001(3) 0.007(3) 0.008(3) C10 0.021(4) 0.022(4) 0.028(4) 0.002(3) 0.002(3) 0.001(3) C1 0.030(4) 0.025(4) 0.029(4) -0.002(3) 0.007(3) -0.005(3) C8 0.030(4) 0.022(4) 0.026(4) 0.003(3) 0.006(3) 0.005(3) C3 0.035(4) 0.028(4) 0.024(4) -0.005(3) -0.002(3) -0.005(4) C6 0.034(4) 0.018(4) 0.029(4) 0.004(3) 0.002(3) -0.002(3) C11 0.026(4) 0.021(4) 0.025(4) -0.004(3) 0.001(3) -0.001(3) C18 0.026(4) 0.020(4) 0.029(4) 0.002(3) 0.010(3) 0.001(3) C7 0.028(4) 0.026(4) 0.023(4) -0.004(3) 0.003(3) 0.000(3) C5 0.026(4) 0.031(4) 0.031(4) 0.003(3) 0.001(3) 0.003(3) C26 0.041(5) 0.030(5) 0.028(4) -0.003(3) 0.004(4) -0.009(4) C4 0.030(4) 0.036(5) 0.027(4) 0.003(4) -0.001(3) -0.004(4) C12 0.033(4) 0.025(4) 0.024(4) 0.001(3) 0.006(3) 0.000(3) C2 0.031(4) 0.021(4) 0.035(4) 0.005(3) 0.008(3) 0.003(3) C13 0.029(4) 0.027(4) 0.034(4) 0.010(3) 0.007(3) -0.003(3) C27 0.038(5) 0.024(4) 0.025(4) -0.002(3) -0.001(3) -0.001(3) C24 0.028(4) 0.028(4) 0.031(4) -0.003(3) 0.005(3) -0.001(3) C19 0.030(4) 0.026(4) 0.030(4) 0.005(3) 0.007(3) 0.000(3) C17 0.046(5) 0.028(5) 0.049(6) 0.009(4) 0.017(4) 0.011(4) C29 0.040(5) 0.041(5) 0.030(4) -0.006(4) 0.013(4) -0.004(4) C28 0.042(5) 0.028(5) 0.037(5) -0.005(4) 0.011(4) -0.003(4) C14 0.037(5) 0.035(5) 0.053(6) -0.002(4) 0.020(4) -0.001(4) C25 0.079(8) 0.024(5) 0.048(6) -0.010(4) 0.012(5) -0.018(5) C23 0.027(4) 0.045(5) 0.038(5) 0.001(4) 0.005(4) -0.004(4) C15 0.043(5) 0.032(5) 0.058(6) 0.006(4) 0.028(5) -0.004(4) C22 0.049(6) 0.046(6) 0.037(5) 0.003(4) -0.005(4) -0.002(5) C20 0.042(5) 0.058(6) 0.026(4) -0.003(4) 0.006(4) 0.001(5) C16 0.053(6) 0.033(5) 0.051(6) 0.018(4) 0.010(5) 0.003(4) C21 0.054(6) 0.064(7) 0.026(5) 0.007(5) 0.000(4) 0.001(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O4 C26 1.355(11) . ? O4 C2 1.422(10) . ? O2 C18 1.231(9) . ? O1 C11 1.244(9) . ? O5 C7 1.360(10) . ? O5 C25 1.431(11) . ? O3 C26 1.203(11) . ? C9 C10 1.410(11) . ? C9 C8 1.437(11) . ? C9 C1 1.444(11) . ? C10 C4 1.411(11) . ? C10 C5 1.425(11) . ? C1 C2 1.360(12) . ? C1 C11 1.517(11) . ? C8 C7 1.393(11) . ? C8 C18 1.513(10) . ? C3 C4 1.382(12) . ? C3 C2 1.393(12) . ? C3 H3 0.9500 . ? C6 C5 1.387(12) . ? C6 C7 1.400(11) . ? C6 H6 0.9500 . ? C11 C12 1.481(11) . ? C18 C19 1.500(11) . ? C5 H5 0.9500 . ? C26 C27 1.479(12) . ? C4 H4 0.9500 . ? C12 C17 1.385(12) . ? C12 C13 1.392(12) . ? C13 C14 1.392(12) . ? C13 H13 0.9500 . ? C27 C28 1.386(12) . ? C27 C29 1.396(12) . ? C24 C23 1.385(12) . ? C24 C19 1.391(11) . ? C24 H24 0.9500 . ? C19 C20 1.405(12) . ? C17 C16 1.398(13) . ? C17 H17 0.9500 . ? C29 C28 1.395(13) 3_666 ? C29 H29 0.9500 . ? C28 H28 0.9500 . ? C14 C15 1.390(14) . ? C14 H14 0.9500 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C23 C22 1.389(14) . ? C23 H23 0.9500 . ? C15 C16 1.372(14) . ? C15 H15 0.9500 . ? C22 C21 1.382(15) . ? C22 H22 0.9500 . ? C20 C21 1.355(14) . ? C20 H20 0.9500 . ? C16 H16 0.9500 . ? C21 H21 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C26 O4 C2 118.4(6) . . ? C7 O5 C25 117.7(7) . . ? C10 C9 C8 118.3(7) . . ? C10 C9 C1 118.9(7) . . ? C8 C9 C1 122.8(7) . . ? C9 C10 C4 120.0(7) . . ? C9 C10 C5 120.2(7) . . ? C4 C10 C5 119.8(7) . . ? C2 C1 C9 117.7(7) . . ? C2 C1 C11 118.6(7) . . ? C9 C1 C11 122.8(7) . . ? C7 C8 C9 120.0(7) . . ? C7 C8 C18 117.8(7) . . ? C9 C8 C18 121.5(7) . . ? C4 C3 C2 118.2(8) . . ? C4 C3 H3 120.9 . . ? C2 C3 H3 120.9 . . ? C5 C6 C7 120.1(7) . . ? C5 C6 H6 120.0 . . ? C7 C6 H6 120.0 . . ? O1 C11 C12 121.8(7) . . ? O1 C11 C1 117.5(7) . . ? C12 C11 C1 120.7(7) . . ? O2 C18 C19 120.7(7) . . ? O2 C18 C8 119.2(7) . . ? C19 C18 C8 120.1(7) . . ? O5 C7 C8 116.9(7) . . ? O5 C7 C6 122.1(7) . . ? C8 C7 C6 121.0(7) . . ? C6 C5 C10 120.1(8) . . ? C6 C5 H5 119.9 . . ? C10 C5 H5 119.9 . . ? O3 C26 O4 123.3(8) . . ? O3 C26 C27 125.6(9) . . ? O4 C26 C27 111.1(7) . . ? C3 C4 C10 120.6(8) . . ? C3 C4 H4 119.7 . . ? C10 C4 H4 119.7 . . ? C17 C12 C13 120.3(8) . . ? C17 C12 C11 119.8(8) . . ? C13 C12 C11 119.9(7) . . ? C1 C2 C3 124.4(8) . . ? C1 C2 O4 119.2(7) . . ? C3 C2 O4 116.4(7) . . ? C12 C13 C14 120.1(8) . . ? C12 C13 H13 119.9 . . ? C14 C13 H13 119.9 . . ? C28 C27 C29 119.4(8) . . ? C28 C27 C26 122.1(8) . . ? C29 C27 C26 118.5(8) . . ? C23 C24 C19 120.1(8) . . ? C23 C24 H24 119.9 . . ? C19 C24 H24 119.9 . . ? C24 C19 C20 119.7(8) . . ? C24 C19 C18 121.1(7) . . ? C20 C19 C18 119.2(7) . . ? C12 C17 C16 119.2(9) . . ? C12 C17 H17 120.4 . . ? C16 C17 H17 120.4 . . ? C28 C29 C27 120.5(8) 3_666 . ? C28 C29 H29 119.7 3_666 . ? C27 C29 H29 119.7 . . ? C27 C28 C29 120.0(8) . 3_666 ? C27 C28 H28 120.0 . . ? C29 C28 H28 120.0 3_666 . ? C15 C14 C13 119.3(9) . . ? C15 C14 H14 120.4 . . ? C13 C14 H14 120.4 . . ? O5 C25 H25A 109.5 . . ? O5 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? O5 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C24 C23 C22 119.0(9) . . ? C24 C23 H23 120.5 . . ? C22 C23 H23 120.5 . . ? C16 C15 C14 120.6(9) . . ? C16 C15 H15 119.7 . . ? C14 C15 H15 119.7 . . ? C21 C22 C23 120.7(9) . . ? C21 C22 H22 119.6 . . ? C23 C22 H22 119.6 . . ? C21 C20 C19 119.7(9) . . ? C21 C20 H20 120.1 . . ? C19 C20 H20 120.1 . . ? C15 C16 C17 120.5(9) . . ? C15 C16 H16 119.8 . . ? C17 C16 H16 119.8 . . ? C20 C21 C22 120.7(9) . . ? C20 C21 H21 119.7 . . ? C22 C21 H21 119.7 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C8 C9 C10 C4 173.9(7) . . . . ? C1 C9 C10 C4 -5.4(11) . . . . ? C8 C9 C10 C5 -7.4(11) . . . . ? C1 C9 C10 C5 173.3(7) . . . . ? C10 C9 C1 C2 5.3(11) . . . . ? C8 C9 C1 C2 -174.0(7) . . . . ? C10 C9 C1 C11 -163.7(7) . . . . ? C8 C9 C1 C11 17.0(11) . . . . ? C10 C9 C8 C7 5.8(11) . . . . ? C1 C9 C8 C7 -174.9(7) . . . . ? C10 C9 C8 C18 -164.0(7) . . . . ? C1 C9 C8 C18 15.3(11) . . . . ? C2 C1 C11 O1 -117.7(9) . . . . ? C9 C1 C11 O1 51.2(11) . . . . ? C2 C1 C11 C12 62.4(10) . . . . ? C9 C1 C11 C12 -128.7(8) . . . . ? C7 C8 C18 O2 -116.0(9) . . . . ? C9 C8 C18 O2 54.0(10) . . . . ? C7 C8 C18 C19 62.3(10) . . . . ? C9 C8 C18 C19 -127.7(8) . . . . ? C25 O5 C7 C8 167.8(8) . . . . ? C25 O5 C7 C6 -8.6(12) . . . . ? C9 C8 C7 O5 -177.2(7) . . . . ? C18 C8 C7 O5 -7.1(11) . . . . ? C9 C8 C7 C6 -0.7(12) . . . . ? C18 C8 C7 C6 169.4(7) . . . . ? C5 C6 C7 O5 173.5(8) . . . . ? C5 C6 C7 C8 -2.8(12) . . . . ? C7 C6 C5 C10 1.2(12) . . . . ? C9 C10 C5 C6 4.0(11) . . . . ? C4 C10 C5 C6 -177.3(8) . . . . ? C2 O4 C26 O3 3.4(13) . . . . ? C2 O4 C26 C27 -178.2(7) . . . . ? C2 C3 C4 C10 2.2(13) . . . . ? C9 C10 C4 C3 1.6(12) . . . . ? C5 C10 C4 C3 -177.1(8) . . . . ? O1 C11 C12 C17 18.1(12) . . . . ? C1 C11 C12 C17 -162.0(8) . . . . ? O1 C11 C12 C13 -159.7(8) . . . . ? C1 C11 C12 C13 20.2(11) . . . . ? C9 C1 C2 C3 -1.5(13) . . . . ? C11 C1 C2 C3 168.0(8) . . . . ? C9 C1 C2 O4 178.0(7) . . . . ? C11 C1 C2 O4 -12.6(11) . . . . ? C4 C3 C2 C1 -2.3(13) . . . . ? C4 C3 C2 O4 178.3(7) . . . . ? C26 O4 C2 C1 90.0(9) . . . . ? C26 O4 C2 C3 -90.6(9) . . . . ? C17 C12 C13 C14 0.5(14) . . . . ? C11 C12 C13 C14 178.3(8) . . . . ? O3 C26 C27 C28 -167.0(9) . . . . ? O4 C26 C27 C28 14.7(11) . . . . ? O3 C26 C27 C29 12.4(14) . . . . ? O4 C26 C27 C29 -165.9(8) . . . . ? C23 C24 C19 C20 -1.2(13) . . . . ? C23 C24 C19 C18 178.2(8) . . . . ? O2 C18 C19 C24 -158.4(8) . . . . ? C8 C18 C19 C24 23.3(12) . . . . ? O2 C18 C19 C20 20.9(12) . . . . ? C8 C18 C19 C20 -157.4(8) . . . . ? C13 C12 C17 C16 0.4(14) . . . . ? C11 C12 C17 C16 -177.4(9) . . . . ? C28 C27 C29 C28 -1.0(15) . . . 3_666 ? C26 C27 C29 C28 179.5(8) . . . 3_666 ? C29 C27 C28 C29 1.0(15) . . . 3_666 ? C26 C27 C28 C29 -179.6(8) . . . 3_666 ? C12 C13 C14 C15 -0.8(14) . . . . ? C19 C24 C23 C22 2.3(14) . . . . ? C13 C14 C15 C16 0.3(16) . . . . ? C24 C23 C22 C21 -2.5(15) . . . . ? C24 C19 C20 C21 0.1(15) . . . . ? C18 C19 C20 C21 -179.3(9) . . . . ? C14 C15 C16 C17 0.6(17) . . . . ? C12 C17 C16 C15 -0.9(16) . . . . ? C19 C20 C21 C22 -0.3(17) . . . . ? C23 C22 C21 C20 1.4(17) . . . . ? _refine_diff_density_max 0.834 _refine_diff_density_min -0.607 _refine_diff_density_rms 0.157 _shelx_res_file ; TITL 121227_6__18Hdimer_1 121227_6__18hdimer_1.res created by SHELXL-2018/3 at 15:30:45 on 18-Feb-2021 REM Yadorkari-X generated REM SPGR P21/c monoclinic CELL 0.7107 7.7979 14.9575 19.498 90 96.058 90 ZERR 2 0.0036 0.0066 0.009 0 0.006 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H O UNIT 116 76 20 L.S. 10 PLAN 5 SIZE 0.2 0.2 0.2 TEMP -99.8 CONF HTAB WPDB -1 BOND $H LIST 4 MORE -1 fmap 2 acta SHEL 20.361088 0.810614 OMIT 0 1 1 OMIT 2 2 3 OMIT -2 3 2 OMIT -2 1 16 OMIT -6 7 7 OMIT 4 8 9 OMIT 0 12 2 OMIT -2 6 3 OMIT 0 0 2 REM REM REM WGHT 0.123600 39.930801 FVAR 2.75627 O4 3 0.440248 0.260498 0.497551 11.00000 0.03516 0.02798 = 0.03080 -0.00269 0.00373 -0.00979 O2 3 0.344693 0.042398 0.296128 11.00000 0.03120 0.03134 = 0.03373 -0.00091 0.00649 0.00208 O1 3 0.097526 0.202555 0.355665 11.00000 0.02781 0.03022 = 0.03762 0.00664 -0.00105 0.00094 O5 3 0.047028 -0.133801 0.329191 11.00000 0.05386 0.02031 = 0.03276 -0.00644 0.00381 -0.00661 O3 3 0.189273 0.318905 0.523994 11.00000 0.04302 0.03510 = 0.07296 -0.00714 0.02183 -0.01327 C9 1 0.238133 0.044092 0.442215 11.00000 0.02252 0.02409 = 0.02560 0.00082 0.00733 0.00751 C10 1 0.247780 0.000384 0.506589 11.00000 0.02096 0.02160 = 0.02792 0.00152 0.00190 0.00107 C1 1 0.298208 0.135203 0.439488 11.00000 0.02995 0.02510 = 0.02881 -0.00163 0.00728 -0.00468 C8 1 0.170364 -0.004671 0.381877 11.00000 0.02965 0.02164 = 0.02558 0.00339 0.00633 0.00540 C3 1 0.395033 0.128215 0.562226 11.00000 0.03495 0.02798 = 0.02388 -0.00530 -0.00209 -0.00528 AFIX 43 H3 2 0.453119 0.156277 0.601783 11.00000 -1.20000 AFIX 0 C6 1 0.099777 -0.129665 0.453447 11.00000 0.03353 0.01779 = 0.02894 0.00359 0.00241 -0.00155 AFIX 43 H6 2 0.048085 -0.186702 0.457330 11.00000 -1.20000 AFIX 0 C11 1 0.252565 0.195663 0.377800 11.00000 0.02571 0.02052 = 0.02536 -0.00444 0.00087 -0.00052 C18 1 0.197230 0.027182 0.310150 11.00000 0.02592 0.02014 = 0.02888 0.00200 0.00995 0.00115 C7 1 0.101955 -0.089881 0.388552 11.00000 0.02750 0.02612 = 0.02321 -0.00373 0.00287 -0.00012 C5 1 0.173000 -0.085901 0.512068 11.00000 0.02558 0.03052 = 0.03074 0.00258 0.00095 0.00305 AFIX 43 H5 2 0.173303 -0.113502 0.555963 11.00000 -1.20000 AFIX 0 C26 1 0.334139 0.329234 0.509434 11.00000 0.04150 0.03021 = 0.02753 -0.00258 0.00408 -0.00911 C4 1 0.328631 0.042916 0.566028 11.00000 0.02979 0.03609 = 0.02692 0.00259 -0.00091 -0.00379 AFIX 43 H4 2 0.337500 0.012615 0.609077 11.00000 -1.20000 AFIX 0 C12 1 0.388868 0.244220 0.345531 11.00000 0.03323 0.02542 = 0.02449 0.00083 0.00647 -0.00007 C2 1 0.374482 0.171918 0.498829 11.00000 0.03117 0.02109 = 0.03532 0.00476 0.00783 0.00287 C13 1 0.559048 0.214974 0.356144 11.00000 0.02857 0.02712 = 0.03375 0.01010 0.00690 -0.00271 AFIX 43 H13 2 0.588022 0.164945 0.385084 11.00000 -1.20000 AFIX 0 C27 1 0.421900 0.416234 0.504011 11.00000 0.03848 0.02400 = 0.02454 -0.00150 -0.00063 -0.00116 C24 1 -0.119866 0.049969 0.275061 11.00000 0.02813 0.02793 = 0.03055 -0.00330 0.00547 -0.00078 AFIX 43 H24 2 -0.139026 0.050327 0.322375 11.00000 -1.20000 AFIX 0 C19 1 0.045937 0.037508 0.256494 11.00000 0.02997 0.02601 = 0.02975 0.00457 0.00745 0.00034 C17 1 0.345353 0.316712 0.302989 11.00000 0.04626 0.02804 = 0.04861 0.00948 0.01693 0.01051 AFIX 43 H17 2 0.229372 0.336969 0.295894 11.00000 -1.20000 AFIX 0 C29 1 0.346635 0.492376 0.529463 11.00000 0.03998 0.04064 = 0.02965 -0.00574 0.01319 -0.00405 AFIX 43 H29 2 0.240951 0.487365 0.549345 11.00000 -1.20000 AFIX 0 C28 1 0.574609 0.424239 0.474072 11.00000 0.04188 0.02790 = 0.03670 -0.00542 0.01131 -0.00301 AFIX 43 H28 2 0.625707 0.372926 0.455943 11.00000 -1.20000 AFIX 0 C14 1 0.686873 0.258905 0.324426 11.00000 0.03702 0.03474 = 0.05306 -0.00192 0.01965 -0.00087 AFIX 43 H14 2 0.803397 0.239603 0.332013 11.00000 -1.20000 AFIX 0 C25 1 0.008896 -0.227055 0.333931 11.00000 0.07881 0.02382 = 0.04773 -0.00989 0.01174 -0.01768 AFIX 33 H25A 2 -0.029027 -0.250441 0.287868 11.00000 -1.20000 H25B 2 0.112542 -0.259133 0.353191 11.00000 -1.20000 H25C 2 -0.082939 -0.235447 0.363980 11.00000 -1.20000 AFIX 0 C23 1 -0.256966 0.061846 0.224709 11.00000 0.02708 0.04472 = 0.03823 0.00136 0.00525 -0.00419 AFIX 43 H23 2 -0.369741 0.072578 0.237113 11.00000 -1.20000 AFIX 0 C15 1 0.642219 0.331288 0.281550 11.00000 0.04318 0.03231 = 0.05813 0.00580 0.02763 -0.00388 AFIX 43 H15 2 0.728782 0.361388 0.259599 11.00000 -1.20000 AFIX 0 C22 1 -0.227179 0.057839 0.155797 11.00000 0.04916 0.04558 = 0.03749 0.00290 -0.00455 -0.00227 AFIX 43 H22 2 -0.321133 0.063553 0.120871 11.00000 -1.20000 AFIX 0 C20 1 0.073048 0.035370 0.186385 11.00000 0.04169 0.05813 = 0.02594 -0.00313 0.00607 0.00118 AFIX 43 H20 2 0.185873 0.026764 0.173343 11.00000 -1.20000 AFIX 0 C16 1 0.474199 0.359692 0.270627 11.00000 0.05290 0.03256 = 0.05093 0.01800 0.01037 0.00258 AFIX 43 H16 2 0.445231 0.408921 0.240856 11.00000 -1.20000 AFIX 0 C21 1 -0.062373 0.045631 0.137479 11.00000 0.05434 0.06406 = 0.02566 0.00664 -0.00049 0.00099 AFIX 43 H21 2 -0.043837 0.044420 0.090108 11.00000 -1.20000 AFIX 0 HKLF 4 REM 121227_6__18Hdimer_1 REM wR2 = 0.4454, GooF = S = 1.094, Restrained GooF = 1.094 for all data REM R1 = 0.1673 for 3615 Fo > 4sig(Fo) and 0.1798 for all 4320 data REM 307 parameters refined using 0 restraints END WGHT 0.1247 39.5639 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.834, deepest hole -0.607, 1-sigma level 0.157 Q1 1 0.0475 -0.2633 0.4993 11.00000 0.05 0.83 Q2 1 0.1572 0.3308 0.2922 11.00000 0.05 0.75 Q3 1 0.6912 0.3173 0.5200 11.00000 0.05 0.72 Q4 1 0.2252 -0.0044 0.6144 11.00000 0.05 0.70 Q5 1 0.4958 0.2597 0.3753 11.00000 0.05 0.68 ; _shelx_res_checksum 98042 _shelx_hkl_file ; 0 -1 1 80.45 28.86 0 1 -1 -35.67 10.25 0 -1 1 -55.18 18.68 0 1 1 -26.05 10.05 0 1 1 -46.77 15.52 0 0 -2 -18.01 23.59 0 0 -2 82.91 81.72 0 1 -2 8975.84 485.70 1 0 0 1605.15 114.06 -1 0 0 1758.95 114.79 1 0 0 1805.75 144.99 -1 0 0 1815.43 115.80 0 -2 0 7343.43 403.96 -1 0 1 205.44 74.27 -1 0 1 157.71 60.87 1 0 -1 127.96 53.45 1 0 -1 139.07 74.33 1 0 1 363.08 79.86 -1 0 -1 413.43 87.32 1 0 1 437.67 85.98 -1 0 -1 382.40 74.71 1 1 034829.94 781.58 1 -1 -1 2816.17 199.15 1 1 -1 2156.28 143.67 -1 -1 1 2147.46 148.52 -1 -1 1 2165.66 147.39 1 -1 -1 2835.74 191.69 -1 1 1 3137.45 244.04 -1 -1 1 2296.77 209.63 -1 1 1 2952.12 195.99 0 0 -3 218.41 87.98 0 0 -3 163.43 88.19 0 0 3 164.64 54.33 0 0 3 92.14 72.14 0 -1 3 4898.75 286.79 0 -1 -3 4693.96 275.47 0 1 -3 4569.09 313.78 0 1 3 4995.90 292.41 0 -1 3 4919.03 313.95 0 1 -3 5236.60 330.22 0 1 3 4915.33 296.13 0 -1 -3 5071.34 338.87 0 2 2 1167.19 96.35 0 2 -2 1212.56 212.53 0 2 2 1217.32 126.22 0 2 2 1158.59 122.39 0 -2 2 1281.42 126.74 0 2 2 1093.99 105.44 0 -2 2 928.94 144.18 0 2 -2 1072.32 115.30 -1 1 2 3080.98 225.16 -1 1 2 3598.65 347.57 -1 -1 2 2879.62 255.04 1 -1 -2 3610.78 252.97 1 1 -2 2573.02 221.06 1 1 -2 2095.15 146.57 -1 -1 2 2468.26 185.18 1 -1 -2 3263.19 218.48 -1 0 -2 902.92 193.82 -1 0 -2 976.87 157.18 1 0 2 1071.91 137.55 1 0 2 1475.62 209.07 -1 -2 014082.03 322.67 -1 2 111614.36 264.92 -1 2 112845.01 284.98 1 -2 -111971.76 281.74 -1 -2 114471.91 328.49 1 2 -114244.58 329.21 1 2 -113817.05 331.59 1 -2 -112948.13 291.43 -1 -2 114371.06 320.28 1 0 -3 227.54 84.69 -1 0 3 107.67 76.62 1 0 -3 154.21 67.78 -1 0 3 209.74 99.52 0 -3 0 34.45 26.33 0 -3 0 225.26 87.77 0 3 0 28.77 28.12 0 3 0 21.15 16.85 -1 1 3 1051.33 179.16 -1 -1 3 1675.10 262.93 -1 -1 3 1591.43 196.32 -1 1 3 1299.47 204.66 1 1 -3 1593.35 263.30 1 -1 -3 1531.02 204.88 -1 1 3 1006.10 189.11 1 1 -3 1500.69 167.89 0 2 3 306.57 166.54 0 -2 3 600.73 212.57 0 2 -3 427.66 135.29 0 2 -3 376.70 117.25 0 2 3 555.44 109.50 0 -2 -3 699.11 182.66 0 -2 3 601.77 129.76 0 2 3 515.83 140.00 1 -2 -225492.21 571.53 -1 2 224387.20 546.58 -1 -2 225737.11 560.42 1 -2 -223737.42 560.18 -1 2 226847.12 582.58 -1 -2 226113.40 587.38 1 2 -226763.03 578.24 1 2 -224998.35 539.83 -1 0 -3 22.04 34.68 1 0 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0 6 1265.81 239.29 8 -3 -2 255.32 89.46 8 3 -2 280.88 124.24 -8 -3 2 296.21 95.91 8 -3 -2 295.86 138.76 -1 3 20 93.61 365.12 -1 -3 20 1255.59 195.42 -1 3 20 764.83 226.82 0 12 13 4352.90 294.65 0 -12 13 4295.88 281.81 2 11 13 3066.73 319.54 2 -11 13 2740.11 311.63 7 -8 -1 106.54 69.80 -7 -8 1 173.64 55.82 7 -8 -1 219.99 54.00 7 8 -1 164.64 74.71 -7 -5 10 1844.54 355.35 7 -5 -10 1788.75 418.46 7 5 -10 1995.43 503.81 -7 5 10 2110.67 442.79 5 -11 6 412.87 165.25 5 11 6 667.41 196.11 8 -3 -3 861.31 180.74 8 -3 -3 652.16 240.26 -8 -3 3 928.68 170.59 8 3 -3 898.89 193.79 6 10 3 303.62 111.62 6 -10 3 292.85 103.64 1 8 17 452.10 157.19 1 8 17 138.34 62.29 1 -8 17 293.20 123.78 1 -8 17 120.98 73.86 7 8 -3 338.40 136.50 7 -8 -3 1278.62 109.20 -7 -8 3 342.89 80.51 7 -8 -3 294.12 124.87 7 -7 -7 517.17 241.26 7 -7 -7 3466.50 468.53 -7 -7 7 3396.12 295.44 7 7 -7 2004.87 300.20 -1 14 9 949.50 272.88 -1 -14 9 869.78 237.10 1 15 5 68.17 68.63 1 -15 5 188.24 81.82 8 -3 -1 253.55 92.62 8 3 -1 580.26 136.89 8 -3 -1 384.65 82.81 8 2 1 248.17 58.63 8 -2 1 252.44 101.57 8 -2 1 69.67 77.51 8 2 1 200.98 94.80 5 5 -16 8209.04 725.31 5 -5 -16 8107.79 506.89 -5 5 16 7553.70 818.36 -5 -5 16 7225.12 913.94 -3 -14 6 -22.93 40.77 3 -14 -6 37.67 32.53 3 14 -6 -0.64 25.62 -3 6 18 -53.24 91.12 -3 -6 18 -29.60 109.29 3 6 -18 87.37 80.89 3 -6 -18 -20.36 89.27 4 -10 11 25.64 63.02 4 10 11 8.77 68.29 2 7 -18 341.34 111.42 -2 -7 18 393.25 144.49 -2 7 18 313.91 126.79 -8 -1 6 1032.49 336.03 -8 1 6 1217.15 231.29 8 -1 -6 1072.90 214.49 8 1 -6 1318.89 185.85 3 8 15 116.98 118.95 3 -8 15 -8.82 104.05 3 -8 15 2.92 20.04 8 0 2 1330.17 268.36 8 0 2 1364.77 236.78 -7 -2 12 822.03 179.29 7 -2 -12 756.53 164.91 -7 2 12 428.82 178.59 7 2 -12 355.01 97.98 2 -2 19 1071.22 264.61 2 -2 19 1285.20 318.77 2 2 19 1172.65 322.77 2 2 19 1291.03 141.66 -4 -4 18 5775.49 648.07 -4 4 18 6556.01 412.34 4 -4 -18 5116.74 509.00 4 4 -18 6007.24 620.54 1 11 14 509.38 160.54 1 -11 14 565.40 136.27 -6 6 13 3894.38 423.08 -6 -6 13 3887.91 378.73 6 -6 -13 4256.37 277.43 6 6 -13 3648.09 601.00 6 7 -12 1054.61 387.38 -6 7 12 624.64 167.78 -6 -7 12 886.51 243.59 6 -7 -12 869.17 201.15 7 -4 -11 570.93 114.19 -7 -4 11 248.77 121.84 7 4 -11 44.30 65.00 -7 4 11 213.42 89.62 -4 6 17 173.88 113.74 -4 -6 17 173.73 103.47 4 -6 -17 296.17 201.63 4 6 -17 272.44 112.40 -6 9 9 38.45 86.90 -6 -9 9 36.31 49.12 6 9 -9 77.63 53.04 6 -9 -9 48.40 30.37 6 -2 12 1763.08 287.57 6 2 12 1519.99 298.76 6 2 12 1727.69 365.20 6 -2 12 1447.24 313.63 5 8 11 110.87 86.10 5 -8 11 189.76 59.78 3 10 13 1222.15 300.00 3 -10 13 907.21 221.17 -7 -8 0 1099.04 205.26 7 -8 0 1024.64 196.04 7 -8 0 1557.76 275.31 7 8 0 1118.88 325.74 -3 -4 19 6556.68 402.67 3 4 -19 5986.99 433.56 3 -4 -19 6392.39 372.92 -3 4 19 6961.96 385.72 3 -12 10 765.07 169.70 3 12 10 837.20 137.77 0 -15 6 261.64 73.38 0 15 6 0.19 29.04 3 -5 17 246.77 142.23 3 5 17 133.88 85.30 3 -5 17 136.87 68.03 3 5 17 66.06 92.15 8 -1 2 263.31 143.10 8 1 2 551.85 121.55 8 -1 2 187.69 98.90 8 1 2 445.63 109.58 2 -7 17 199.14 107.72 2 7 17 178.63 111.22 2 7 17 125.64 46.37 2 -7 17 206.61 111.33 5 7 12 537.55 193.78 5 -7 12 194.78 76.93 5 -7 12 178.16 90.08 8 3 -4 798.30 158.04 -8 -3 4 800.88 161.46 8 -3 -4 542.39 156.12 8 -3 -4 790.35 185.28 -7 6 9 140.99 111.11 7 -6 -9 138.35 66.39 7 6 -9 381.37 109.41 2 15 -4 129.63 55.50 2 -15 -4 74.19 36.83 7 3 8 437.76 163.10 7 3 8 183.19 60.62 7 -3 8 280.56 140.87 7 -3 8 307.92 133.47 7 -8 -4 562.15 155.04 -7 -8 4 641.03 252.73 7 8 -4 752.16 211.64 7 -8 -4 1068.90 229.23 0 -3 20 -22.62 89.12 0 3 20 -54.02 78.64 0 3 20 44.54 56.33 0 -3 20 47.72 50.99 5 12 3 93.49 52.71 5 -12 3 58.54 52.52 2 -15 3 157.02 57.65 2 15 3 67.45 24.56 8 3 0 178.64 93.79 8 -3 0 312.85 122.86 8 3 0 124.04 84.78 8 -3 0 440.71 145.26 3 2 18 357.52 151.14 3 -2 18 870.19 201.22 3 -2 18 603.65 191.17 3 2 18 789.87 191.17 -5 -3 17 150.54 85.06 -5 3 17 162.16 136.09 5 -3 -17 47.17 88.92 5 3 -17 -39.96 111.40 5 4 14 387.21 135.84 5 -4 14 98.94 89.59 5 4 14 267.96 86.17 5 -4 14 125.93 57.41 6 9 6 -13.59 69.53 6 -9 6 179.33 97.70 5 10 -11 338.51 125.16 5 -10 -11 176.94 69.22 -5 10 11 248.35 142.04 -5 -10 11 199.13 141.22 4 -4 16 4615.07 522.35 4 -4 16 5995.90 387.70 4 4 16 5196.31 407.24 4 4 16 5335.83 496.63 1 0 20 1201.32 187.22 1 0 20 1233.75 286.75 -5 -11 9 304.37 123.49 5 -11 -9 197.44 79.31 -5 11 9 103.69 82.19 5 11 -9 208.88 63.46 6 -7 9 281.79 118.53 6 -7 9 207.56 80.30 6 7 9 535.00 143.96 3 -13 8 638.47 328.69 3 13 8 62.81 61.58 1 13 11 391.91 139.86 1 -13 11 247.69 109.56 -1 15 6 28.58 40.66 -1 -15 6 -12.09 32.50 4 6 15 306.29 132.88 4 -6 15 450.98 108.49 4 6 15 369.81 99.92 4 -6 15 108.58 69.87 6 6 10 1642.88 188.94 6 -6 10 726.20 271.01 6 -6 10 1830.97 271.78 -8 2 6 431.97 157.26 8 2 -6 480.53 160.47 8 -2 -6 259.07 134.05 -8 -2 6 185.02 66.44 -6 3 15 4327.09 556.60 -6 -3 15 4555.10 449.96 6 3 -15 4980.03 579.88 6 -3 -15 4490.04 318.47 -1 -6 19 39.67 56.56 -1 6 19 151.20 104.84 -1 6 19 33.07 59.10 1 6 -19 105.69 51.02 4 13 -7 957.38 215.29 -4 -13 7 662.52 157.42 4 -13 -7 785.78 144.60 -2 13 11 823.06 85.12 -2 13 11 692.49 221.94 2 13 -11 828.76 194.71 -2 -13 11 887.42 198.27 5 12 -6 95.66 55.91 -5 -12 6 4.02 18.55 5 -12 -6 -20.16 40.15 5 -12 -6 182.61 105.38 1 1 20 874.58 182.01 1 1 20 964.77 198.75 1 -1 20 983.92 170.97 1 -1 20 792.79 145.97 3 14 5 86.20 109.33 3 -14 5 -0.04 58.05 -7 -8 -1 436.03 97.97 7 -8 1 784.04 179.93 7 8 1 412.53 136.18 7 -8 1 317.59 85.55 -6 5 14 38.99 83.96 -6 -5 14 171.19 63.09 6 5 -14 292.74 130.77 6 -5 -14 179.36 71.80 -6 8 11 768.63 135.18 6 -8 -11 703.19 169.93 6 8 -11 619.15 156.28 -6 -8 11 601.48 211.31 5 9 10 130.37 81.27 5 -9 10 23.15 47.57 -2 3 20 331.88 116.04 2 3 -20 181.69 55.36 2 -3 -20 213.79 130.96 -2 -3 20 546.86 218.23 -8 -3 5 115.27 75.60 8 -3 -5 72.15 226.74 8 3 -5 83.86 100.98 8 -3 -5 39.89 46.73 1 -5 19 55.67 66.98 1 -5 19 100.64 88.76 1 5 19 85.94 62.04 1 5 19 -28.31 46.87 8 -2 2 406.79 129.91 8 2 2 643.57 128.33 8 -2 2 545.38 199.58 8 2 2 254.15 125.44 -7 -7 -4 143.88 65.74 7 -7 4 152.25 61.47 7 7 4 204.68 61.40 7 -7 4 407.78 184.12 2 -13 10 584.59 185.03 2 13 10 514.59 188.39 4 -13 5 1326.56 328.36 4 13 5 1540.48 189.71 -8 0 7 69.47 73.22 8 0 -7 154.36 77.13 3 -7 16 810.74 163.02 3 -7 16 829.88 343.73 3 7 16 784.09 397.58 6 -10 -7 578.36 164.04 -6 -10 7 678.91 169.34 6 10 -7 758.04 170.61 6 -10 -7 257.50 211.82 5 -6 13 131.54 64.04 5 6 13 -106.56 104.78 5 -6 13 60.58 39.38 -7 -8 5 403.33 105.66 7 -8 -5 295.31 166.14 7 -8 -5 487.38 129.11 7 8 -5 708.13 154.33 8 -3 1 158.55 84.90 8 3 1 84.21 62.58 8 3 1 210.69 83.55 8 -3 1 302.79 101.15 7 0 9 134.85 117.85 7 0 9 61.13 70.95 -4 -12 10 628.16 170.09 4 12 -10 612.55 147.35 -4 12 10 481.70 212.13 -4 0 19 -35.54 113.02 4 0 -19 -16.93 116.17 -7 3 12 437.41 136.34 7 3 -12 628.57 120.32 -7 -3 12 330.03 137.90 7 -3 -12 216.24 96.28 2 3 19 246.15 193.01 2 -3 19 605.96 143.21 2 -3 19 506.92 159.08 2 3 19 445.88 172.59 -8 1 7 2832.11 613.85 8 1 -7 2262.62 534.02 8 -1 -7 2489.93 488.64 -8 -1 7 2555.81 349.67 1 14 9 34.99 47.56 1 -14 9 73.10 55.45 0 -6 19 903.30 196.42 0 6 19 710.02 194.49 0 6 19 926.89 152.39 6 -10 4 823.39 194.80 6 10 4 1278.11 290.36 8 0 3 -38.60 83.91 8 0 3 100.59 72.14 -1 10 16 828.63 144.81 -1 -10 16 841.06 208.83 1 10 -16 1308.00 238.17 6 -8 8 1506.07 219.81 6 8 8 1678.75 323.63 -4 -11 12 108.47 50.83 -4 11 12 161.86 72.75 4 -11 -12 136.75 112.50 4 11 -12 218.29 109.65 1 7 18 415.25 106.56 1 7 18 481.35 150.85 1 -7 18 540.27 175.03 1 -7 18 513.18 137.15 6 3 12 1979.21 340.75 6 3 12 1756.60 299.90 6 -3 12 2243.42 364.73 6 -3 12 1717.28 345.61 -2 12 13 478.76 119.57 2 12 -13 390.54 139.70 -2 12 13 397.91 100.57 -2 -12 13 452.29 139.00 7 1 9 49.77 84.98 7 -1 9 131.25 93.46 7 1 9 171.19 70.33 7 -1 9 60.00 65.64 -1 -9 17 1588.35 502.83 -1 9 17 1440.29 347.03 1 9 -17 1373.73 209.11 -1 9 17 1579.50 176.30 5 1 15 241.20 115.19 5 -1 15 165.95 94.70 5 1 15 209.42 113.14 5 -1 15 319.74 100.33 8 -4 -2 131.48 102.09 8 4 -2 701.65 108.21 8 -4 -2 41.64 52.85 -8 -4 2 1.52 62.72 -1 4 20 392.51 149.15 -1 -4 20 558.44 210.17 1 4 -20 512.39 177.72 -1 4 20 519.93 165.27 3 -11 12 251.09 99.80 3 11 12 337.24 90.76 -4 1 19 227.83 141.33 4 1 -19 89.93 74.64 -4 -1 19 258.30 128.32 4 -1 -19 103.93 52.48 2 -15 -5 1373.60 292.00 4 -12 8 1348.92 253.28 4 12 8 1310.76 321.66 -5 -8 14 599.14 178.99 5 -8 -14 824.17 215.64 5 8 -14 534.25 171.09 -5 8 14 625.74 180.42 6 -5 11 40.09 81.15 6 5 11 52.29 40.91 6 5 11 143.73 106.90 6 -5 11 -7.10 97.79 3 -9 -16 87.62 55.73 3 9 -16 145.75 90.44 -3 9 16 72.55 64.71 -3 -9 16 182.41 149.92 -7 -7 8 -17.62 73.66 7 -7 -8 95.25 95.24 7 7 -8 -49.11 100.56 7 -5 7 1330.34 281.76 7 5 7 1261.39 449.75 7 5 7 1398.05 224.08 7 -5 7 1759.36 254.71 -3 -12 12 224.46 78.76 3 12 -12 28.00 52.88 -3 12 12 37.97 54.45 -3 12 12 -5.60 49.89 2 15 4 740.94 227.53 2 -15 4 780.53 176.79 8 -4 -3 -83.07 104.88 -8 -4 3 227.95 95.15 8 -4 -3 164.21 82.09 8 4 -3 152.00 103.36 8 1 3 880.65 251.07 8 -1 3 1406.87 192.22 8 -1 3 1305.48 244.74 8 1 3 1070.47 204.63 1 15 6 311.83 116.34 1 -15 6 127.45 69.34 1 2 20 542.52 152.91 1 -2 20 204.56 58.54 1 2 20 238.52 143.76 1 -2 20 234.79 127.81 -3 -14 7 1531.28 119.08 3 14 -7 1604.56 203.98 3 -14 -7 1489.40 357.09 2 12 12 858.55 171.06 2 -12 12 1004.97 187.91 -8 -4 1 92.32 62.49 8 -4 -1 240.73 113.61 8 4 -1 381.47 154.45 8 -4 -1 219.66 89.75 3 -3 18 529.61 173.38 3 -3 18 328.42 161.14 3 3 18 357.38 104.57 3 3 18 151.79 153.69 0 -10 16 104.13 57.46 0 10 -16 -3.17 51.03 0 10 16 -31.01 82.75 -5 -7 15 88.50 92.79 5 7 -15 91.52 64.81 -5 7 15 112.48 69.76 5 -7 -15 165.37 124.85 1 -12 13 144.26 122.90 1 12 13 42.70 95.48 3 13 -10 13.87 69.91 -3 13 10 46.63 52.89 -3 -13 10 34.31 57.03 -3 13 10 97.93 64.23 4 11 10 515.88 120.51 4 -11 10 582.32 131.38 -3 0 20 355.45 151.74 3 0 -20 260.83 134.40 5 12 4 408.65 93.72 5 -12 4 524.48 179.71 4 0 17 2.60 85.55 4 0 17 81.58 71.80 7 -6 6 2295.02 354.31 7 6 6 2234.63 516.53 7 -6 6 2595.71 486.46 0 9 17 35.70 32.96 0 -9 17 51.28 51.27 0 9 17 51.82 78.81 0 9 -17 38.53 41.65 7 -8 2 1680.66 301.95 7 -8 2 1147.25 247.51 7 8 2 1495.91 273.70 -3 10 15 448.63 113.88 -3 -10 15 546.69 188.59 3 10 -15 637.22 135.28 -2 -14 9 213.80 109.73 -2 14 9 365.85 145.89 -2 14 9 213.83 74.69 -3 8 17 599.47 191.34 3 -8 -17 740.55 199.57 3 8 -17 622.94 207.06 -3 -8 17 756.49 164.49 -8 -3 6 106.38 67.98 8 3 -6 -15.72 101.95 8 -3 -6 49.95 69.41 6 11 -2 151.31 90.27 6 -11 -2 272.23 91.88 8 -4 -4 249.82 104.40 8 4 -4 116.52 76.87 -8 -4 4 205.74 71.67 8 -4 -4 145.01 71.03 6 -11 -1 383.91 127.83 6 11 -1 437.27 149.43 3 1 -20 1250.71 428.79 -3 -1 20 1374.27 249.20 -3 1 20 1138.15 181.55 3 -1 -20 1374.65 383.10 8 -2 -7 1294.51 339.68 -8 -2 7 1243.92 280.32 -8 2 7 1608.34 385.01 8 2 -7 1577.61 268.60 -2 6 19 165.06 83.23 2 6 -19 -9.52 73.52 -2 -6 19 28.60 110.27 2 -6 -19 -22.27 103.24 4 1 17 238.66 118.00 4 1 17 122.25 88.17 4 -1 17 -46.37 91.12 4 -1 17 49.13 47.71 -1 11 15 2377.61 227.29 1 11 -15 860.87 231.67 -1 -11 15 1227.13 322.12 7 -4 8 488.58 118.25 7 4 8 397.08 135.89 7 -4 8 310.87 97.45 7 4 8 385.91 153.53 2 14 8 263.07 85.16 2 -14 8 244.36 78.87 0 4 20 140.37 140.07 0 4 20 211.58 150.13 0 -4 20 273.21 149.65 0 -4 20 168.53 83.83 8 4 0 -30.31 109.83 8 -4 0 66.78 33.79 8 -4 0 210.19 120.68 0 -15 7 1912.35 167.22 0 15 7 2013.74 229.89 5 11 7 483.09 131.46 5 -11 7 617.18 181.48 5 -9 -13 131.17 43.88 5 9 -13 184.41 71.79 -5 -9 13 80.48 55.56 -5 9 13 115.09 76.00 -7 0 13 150.74 96.88 7 0 -13 -72.08 107.06 -5 4 17 511.95 136.35 -5 -4 17 343.79 130.72 5 4 -17 356.98 80.94 5 -4 -17 369.35 162.26 7 -2 9 1179.13 135.76 7 -2 9 895.93 164.08 7 2 9 1014.72 209.28 7 2 9 900.70 125.32 5 -2 15 -44.59 69.95 5 2 15 140.14 68.72 5 2 15 -8.41 61.06 5 -2 15 -32.13 81.87 4 2 -19 -25.35 102.52 -4 -2 19 173.90 107.87 4 -2 -19 234.68 129.23 -4 2 19 200.42 89.83 8 3 2 200.52 78.87 8 -3 2 187.32 93.52 8 3 2 143.90 116.48 8 -3 2 107.33 148.21 7 -8 -6 909.41 224.29 -7 -8 6 318.91 205.41 7 -8 -6 350.81 135.97 7 8 -6 1124.43 154.47 6 11 -3 546.93 150.62 6 -11 -3 77.26 97.08 -1 -13 12 496.59 125.92 -1 13 12 838.30 156.92 0 13 12 85.90 74.69 0 -13 12 39.35 68.04 -4 5 18 195.81 153.92 -4 -5 18 255.91 176.17 4 5 -18 525.86 129.72 4 -5 -18 360.64 152.46 4 14 -1 136.16 98.37 4 -14 -1 109.10 69.00 -1 8 18 48.84 50.74 1 8 -18 -45.22 64.44 -1 8 18 1.59 95.97 -1 -8 18 86.99 52.59 0 -11 15 3.27 64.08 0 11 15 53.51 88.17 6 -11 0 251.12 112.39 6 11 0 174.53 81.20 2 -6 18 87.95 61.91 2 6 18 72.48 110.22 2 6 18 116.03 51.05 2 -6 18 141.49 95.57 8 2 3 936.20 204.79 8 -2 3 1131.39 198.52 8 2 3 1071.44 208.39 8 -2 3 906.42 186.36 -7 5 11 4034.00 486.63 7 -5 -11 4252.25 482.82 7 5 -11 3715.83 421.50 -7 -5 11 3764.27 340.62 5 12 -7 1309.00 249.06 5 -12 -7 830.78 206.75 -5 -12 7 1067.93 219.17 5 -12 -7 1041.76 226.15 -7 1 13 465.52 106.43 7 -1 -13 209.05 95.02 -7 -1 13 308.92 145.68 7 1 -13 335.97 98.06 5 -10 9 884.88 115.90 4 -14 -2 2437.33 512.65 4 14 -2 2829.45 380.94 -3 -5 19 524.11 152.25 3 5 -19 585.94 118.91 3 -5 -19 756.31 236.11 -3 5 19 622.16 171.43 0 -14 10 1676.95 370.13 0 14 10 2164.09 184.63 4 -14 0 1820.67 259.05 4 14 0 2303.26 278.63 6 4 -15 1340.74 236.60 -6 4 15 1549.56 464.90 -6 -4 15 1843.48 454.99 6 -4 -15 1604.45 277.12 4 9 -15 649.10 128.95 4 -9 -15 453.09 185.26 -4 9 15 601.91 163.55 -4 -9 15 310.67 161.58 6 9 -10 125.03 40.56 -6 -9 10 181.52 85.17 -6 9 10 262.30 117.15 6 -9 -10 324.56 122.90 -1 -15 7 525.99 128.29 -1 15 7 439.06 135.75 4 8 -16 1558.08 355.14 4 -8 -16 1565.25 424.11 -4 -8 16 1598.93 452.14 -4 8 16 1782.25 369.60 7 -6 -10 1142.99 254.32 7 6 -10 937.81 267.24 -7 6 10 671.58 187.04 -1 14 10 508.56 117.68 -1 -14 10 362.53 98.07 8 0 -8 80.10 72.09 -8 0 8 -0.07 100.55 6 0 -16 193.63 131.54 -6 0 16 126.85 111.16 5 6 -16 109.79 100.14 -5 6 16 403.52 136.03 -5 -6 16 234.95 128.29 5 -6 -16 65.17 75.07 2 -4 -20 1954.79 218.93 2 4 -20 2280.84 491.42 -2 -4 20 2072.06 454.55 -2 4 20 2426.26 250.03 8 -4 -5 337.67 191.32 -8 -4 5 565.61 112.65 8 4 -5 197.48 89.20 8 -4 -5 518.32 157.94 3 -14 6 56.02 57.81 3 14 6 161.85 93.66 4 13 -8 28.23 28.35 -4 -13 8 43.77 44.71 -4 13 8 55.04 42.46 -3 -2 20 112.93 87.42 3 2 -20 -121.83 101.21 3 -2 -20 126.10 97.92 -3 2 20 -20.92 100.45 0 8 -18 2018.15 341.20 0 8 18 2054.85 270.52 0 8 18 2003.07 555.10 0 -8 18 2032.38 504.86 4 2 17 191.29 127.53 4 2 17 119.75 56.35 4 -2 17 105.32 58.16 4 -2 17 180.97 114.53 6 -11 -4 1780.63 355.27 6 11 -4 2661.68 213.09 -6 -10 8 71.15 104.49 6 -10 -8 168.18 94.35 6 -10 -8 32.47 52.12 6 10 -8 135.37 45.64 4 5 16 497.99 169.70 4 -5 16 633.55 124.56 4 -5 16 437.63 135.67 4 5 16 433.04 141.42 1 3 20 164.77 58.91 1 3 20 154.55 94.75 1 -3 20 280.40 112.84 1 -3 20 122.02 68.93 -8 -1 8 210.32 131.46 8 1 -8 201.32 86.77 -8 1 8 108.49 135.20 8 -1 -8 125.17 109.10 4 -14 -3 212.68 82.24 4 14 -3 201.35 81.58 -6 1 16 602.99 148.87 6 -1 -16 463.71 178.11 -6 -1 16 561.71 146.30 6 1 -16 631.99 153.36 -2 -10 16 819.10 304.68 2 10 -16 763.66 194.85 -2 10 16 740.13 201.57 -2 10 16 916.34 281.48 7 7 5 234.93 110.04 7 -7 5 143.13 53.58 7 -7 5 221.76 138.04 2 9 -17 672.49 138.74 -2 9 17 538.82 151.38 -2 9 17 618.55 169.18 -2 -9 17 464.47 152.63 8 -4 1 707.24 138.63 8 4 1 673.22 187.00 8 4 1 542.04 138.95 8 -4 1 728.33 145.68 6 -9 7 170.87 109.88 6 9 7 325.96 151.55 4 14 1 72.20 76.64 4 -14 1 16.55 51.64 6 -11 1 2816.48 480.80 6 11 1 3306.35 321.07 4 9 13 561.60 200.44 4 -9 13 305.82 103.67 4 -13 6 33.53 101.59 4 13 6 -28.34 88.47 3 6 17 1142.04 172.91 3 -6 17 887.10 179.95 3 -6 17 789.17 176.22 3 6 17 715.20 157.07 2 -15 -6 18.90 30.74 -2 -15 6 19.83 29.57 -5 0 18 2462.49 423.90 5 0 -18 2614.65 468.52 -7 -4 12 1460.61 378.99 7 4 -12 1283.25 252.04 7 -4 -12 1210.86 303.77 -7 4 12 942.69 345.10 2 -4 19 871.67 277.86 2 4 19 873.54 273.57 2 4 19 1308.23 230.31 2 -4 19 802.69 260.54 8 0 4 119.67 71.28 8 0 4 173.58 75.60 4 8 14 879.17 217.46 4 -8 14 883.44 189.04 -5 -11 10 964.26 314.33 5 -11 -10 1095.21 229.00 -5 11 10 946.42 272.86 5 11 -10 1188.46 253.23 2 15 5 148.87 75.86 2 -15 5 249.68 114.52 -3 11 14 83.31 79.89 -3 11 14 101.79 59.23 3 11 -14 80.67 49.05 -3 -11 14 78.30 97.30 3 15 -1 -17.76 61.56 3 -15 -1 155.08 46.30 2 10 15 1863.90 200.77 2 -10 15 1726.08 203.46 6 -10 5 159.35 92.27 6 10 5 -29.31 102.98 6 4 12 3696.36 632.98 6 -4 12 4172.80 268.09 6 4 12 3303.84 355.31 6 -4 12 4184.51 338.27 7 8 3 718.93 200.88 7 -8 3 179.08 66.70 2 9 16 1462.81 213.51 2 -9 16 1166.28 139.04 -7 -2 13 3225.48 347.26 -7 2 13 3218.37 447.34 7 -2 -13 3592.97 698.60 7 2 -13 2907.39 539.43 3 -7 -18 1674.00 472.91 -3 7 18 1607.32 335.56 3 7 -18 1810.53 173.00 -3 -7 18 1770.27 393.04 3 15 0 361.59 86.69 3 -15 0 181.98 72.72 -5 -1 18 144.71 79.91 5 -1 -18 93.31 51.28 -5 1 18 143.33 49.16 5 1 -18 102.28 76.69 4 10 -14 -1.71 76.20 4 -10 -14 -18.76 75.47 -4 -10 14 8.93 47.91 -4 10 14 96.98 72.88 8 -3 -7 6.85 59.76 -8 -3 7 178.65 89.11 -8 3 7 93.55 108.35 8 3 -7 369.57 152.87 8 1 4 -132.40 72.93 8 1 4 -23.18 97.72 8 -1 4 81.53 62.86 8 -1 4 132.10 70.08 3 -15 -2 140.43 66.09 3 15 -2 37.88 38.47 6 0 13 156.54 68.24 6 0 13 51.24 56.42 6 -7 -13 6168.68 470.97 6 7 -13 6255.60 373.00 -6 -7 13 6027.80 618.68 -6 7 13 6895.96 265.66 4 7 -17 243.91 101.63 -4 -7 17 130.51 122.32 -4 7 17 210.49 56.06 4 -7 -17 145.50 93.18 3 -13 9 284.16 128.64 3 13 9 -2.11 64.93 3 4 18 7.06 107.64 3 -4 18 15.06 59.10 3 -4 18 92.36 70.29 3 4 18 -34.21 61.15 7 3 9 861.03 224.11 7 3 9 1095.47 195.96 7 -3 9 742.38 136.42 7 -3 9 717.93 204.08 5 -3 15 144.16 78.18 5 3 15 173.30 43.72 5 -3 15 248.91 113.70 5 3 15 130.73 94.05 -4 3 19 2357.68 250.35 4 -3 -19 2030.38 510.46 4 3 -19 1883.81 419.67 -4 -3 19 2198.30 459.05 -1 0 21 15.72 72.41 1 0 -21 251.82 142.35 1 -16 0 353.70 78.03 7 -7 -9 71.99 60.79 7 7 -9 107.60 118.40 -7 -7 9 94.64 84.84 -7 7 9 148.16 141.81 5 -12 5 555.62 129.79 5 12 5 393.18 123.28 -5 -10 12 2009.42 458.43 5 -10 -12 2034.52 326.05 -5 10 12 2152.26 346.50 5 10 -12 2149.40 215.62 -1 12 14 162.35 79.90 -1 -12 14 166.89 118.46 1 -16 -1 365.19 88.22 8 -3 3 84.36 62.95 8 -3 3 147.20 74.48 8 3 3 210.08 91.68 8 3 3 202.45 90.92 6 -1 13 443.70 94.00 6 -1 13 477.78 118.49 6 1 13 372.85 178.93 6 1 13 602.00 147.63 3 15 1 152.87 80.42 3 -15 1 14.16 37.66 4 14 -4 620.47 128.24 4 -14 -4 601.02 163.67 -3 14 8 30.00 46.59 3 14 -8 53.42 53.30 -3 -14 8 31.05 36.03 -3 14 8 58.38 61.82 1 -15 7 47.17 36.26 1 15 7 -3.82 59.12 7 -8 -7 59.53 78.16 7 8 -7 154.89 106.96 -7 -8 7 99.16 52.98 7 -8 -7 180.57 50.06 -8 2 8 457.94 128.56 8 2 -8 460.55 181.68 8 -2 -8 628.71 144.70 -8 -2 8 347.80 144.05 6 2 -16 103.15 63.76 6 -2 -16 164.30 54.01 -6 2 16 165.33 101.62 -6 -2 16 43.72 102.00 6 -6 -14 1005.31 320.11 6 6 -14 1216.20 194.95 -6 6 14 1238.58 254.01 -6 -6 14 1081.83 356.49 4 10 12 125.43 78.64 4 -10 12 -6.18 101.62 -2 11 15 2258.15 309.23 2 11 -15 1742.60 216.05 -2 -11 15 2117.20 425.76 -2 11 15 2002.15 235.69 2 8 -18 403.04 127.92 -2 8 18 416.31 165.30 -2 -8 18 252.60 109.33 -2 8 18 467.06 90.81 6 -11 -5 2016.03 444.03 6 11 -5 2244.52 321.20 4 14 2 131.60 75.22 4 -14 2 246.25 105.29 8 -4 -6 396.53 160.83 -8 -4 6 473.07 149.91 8 4 -6 387.39 177.78 8 -4 -6 340.65 140.79 -8 -5 2 603.00 112.72 8 5 -2 650.99 133.78 8 -5 -2 617.07 166.31 8 -5 -2 561.01 131.55 1 5 -20 467.36 69.86 -1 -5 20 428.10 142.24 -1 5 20 523.28 143.47 -1 5 20 552.94 118.78 1 -6 19 137.58 49.17 1 -6 19 134.81 72.01 1 6 19 163.72 65.55 1 6 19 179.06 76.37 -1 -1 21 341.88 189.93 1 1 -21 212.13 139.91 -1 1 21 190.65 165.75 1 -1 -21 127.84 89.01 1 -16 1 4.18 31.15 0 -12 14 119.92 52.93 0 12 14 -79.47 96.33 8 -5 -3 288.37 115.01 8 -5 -3 385.57 136.84 8 5 -3 398.73 154.46 -8 -5 3 209.56 82.47 3 15 -3 140.83 75.96 3 -15 -3 124.56 81.01 6 8 -12 2802.70 345.41 -6 -8 12 2915.31 328.37 -6 8 12 2542.51 536.23 6 -8 -12 2625.94 502.96 5 -13 -1 1813.50 392.99 5 13 -1 2245.79 253.04 6 11 2 1078.85 273.58 6 -11 2 1153.98 238.10 1 -10 16 102.60 82.84 1 10 16 164.60 104.84 -8 -5 1 740.29 137.70 8 -5 -1 610.14 186.00 8 -5 -1 666.00 161.68 8 5 -1 1152.70 209.83 5 -13 -2 190.06 104.40 5 13 -2 35.73 39.52 4 7 15 138.58 61.83 4 -7 15 155.93 77.74 4 -7 15 54.66 38.66 7 -9 -2 154.23 110.71 7 9 -2 22.54 52.06 7 -9 -2 63.21 35.02 6 7 10 5295.86 331.97 6 -7 10 4067.41 457.44 2 11 14 1268.63 310.72 2 -11 14 1407.05 324.94 0 -16 3 173.96 55.35 8 -4 2 1231.89 204.66 8 -4 2 1053.96 198.78 8 4 2 1107.33 231.29 8 4 2 1063.69 215.26 2 8 17 238.53 121.05 2 -8 17 168.34 82.35 2 -8 17 161.11 108.92 5 -8 12 819.89 187.42 5 8 12 751.47 235.37 -5 2 18 106.83 79.35 -5 -2 18 182.34 119.06 5 2 -18 59.28 90.75 5 -2 -18 175.42 91.10 -1 -7 19 832.94 231.38 1 7 -19 400.22 137.42 -1 7 19 532.76 188.77 -1 7 19 622.49 188.37 3 -3 -20 60.92 83.02 3 3 -20 9.30 95.74 -3 -3 20 -9.30 105.54 -3 3 20 -27.17 100.31 8 2 4 1256.47 297.21 8 2 4 1424.39 326.02 8 -2 4 1481.63 315.82 8 -2 4 1240.81 140.48 7 -9 -1 824.16 252.11 7 9 -1 393.95 190.30 -4 -12 11 94.35 86.52 4 12 -11 138.39 60.86 -4 12 11 116.17 59.71 4 3 17 815.40 242.61 4 -3 17 887.60 223.38 4 -3 17 1071.25 193.31 4 3 17 790.22 176.07 5 -13 0 424.21 114.87 5 13 0 599.78 132.54 -2 13 12 369.70 151.94 -2 13 12 226.63 88.79 -2 -13 12 261.38 146.47 1 9 17 128.77 109.07 1 -9 17 247.72 117.20 1 -9 17 236.08 86.06 7 -9 -3 272.16 181.49 -7 -9 3 285.42 75.66 7 9 -3 330.45 118.84 7 -9 -3 451.84 127.11 1 -13 12 111.24 86.04 1 13 12 83.61 88.37 1 14 10 478.15 137.57 1 -14 10 386.22 101.49 0 0 21 38.19 106.15 0 0 21 -24.98 59.25 3 9 15 138.52 84.82 3 -9 15 195.83 91.31 5 12 -8 620.39 177.68 5 -12 -8 530.82 160.07 5 -12 -8 640.91 159.59 8 5 -4 727.15 208.24 8 -5 -4 291.46 84.92 -8 -5 4 571.64 113.63 8 -5 -4 525.90 145.27 5 13 -3 30.39 67.35 5 -13 -3 144.27 84.51 6 -6 11 1098.53 325.82 6 -6 11 1937.12 289.51 6 6 11 1392.38 349.16 1 -16 2 398.47 121.33 3 -15 2 1194.21 287.82 3 15 2 938.50 329.62 2 -13 11 179.03 91.91 2 13 11 130.28 66.75 7 6 7 254.21 96.35 7 -6 7 203.52 95.47 7 -6 7 116.76 90.63 7 5 8 59.63 26.62 7 -5 8 40.11 60.18 7 5 8 75.70 74.26 7 -5 8 -0.03 65.16 5 -7 13 -76.43 103.16 5 -7 13 56.49 33.25 5 7 13 87.78 87.38 6 2 13 262.33 82.91 6 2 13 71.41 72.84 6 -2 13 61.00 84.49 6 -2 13 311.80 58.49 4 12 9 -1.12 92.93 4 -12 9 164.79 96.17 0 5 20 206.34 92.42 0 5 20 183.14 147.57 0 -5 20 66.17 86.15 0 15 8 1489.64 195.69 0 -15 8 1472.73 222.46 6 -8 9 1108.85 177.93 6 8 9 945.45 259.83 8 5 0 772.27 171.26 8 -5 0 351.64 124.64 8 -5 0 518.69 127.88 -8 -5 0 512.97 130.58 5 9 11 -3.38 107.66 5 -9 11 121.47 83.23 -7 3 13 -46.16 111.76 -7 -3 13 249.53 135.22 7 3 -13 64.41 50.96 7 -3 -13 191.99 103.86 -5 -5 17 1539.48 332.90 5 -5 -17 1445.75 364.11 -5 5 17 1327.08 275.74 5 5 -17 1508.76 312.22 7 -9 0 640.88 145.04 7 9 0 331.69 152.21 3 10 14 -11.52 112.55 3 -10 14 299.23 136.52 1 -11 15 5390.58 707.34 1 11 15 5711.80 454.65 0 -1 21 -52.97 102.66 0 1 21 152.46 75.25 0 -1 21 47.92 98.51 0 1 21 187.27 124.40 1 2 -21 555.82 158.26 -1 -2 21 385.61 157.96 -1 2 21 595.27 190.42 8 0 -9 -48.99 109.16 -8 0 9 143.34 72.64 7 0 10 495.58 160.55 7 0 10 264.66 158.53 0 -7 19 702.58 213.44 0 7 19 702.58 206.45 0 7 19 759.12 193.51 7 -9 -4 702.81 165.02 7 -9 -4 915.43 237.44 -7 -9 4 763.23 168.85 7 9 -4 1154.73 220.89 1 4 20 -122.70 109.29 1 4 20 23.90 67.30 1 -4 20 90.96 71.88 1 -4 20 123.79 76.95 -2 -14 10 520.61 171.52 -2 14 10 925.41 100.56 4 -14 -5 994.99 227.63 4 14 -5 939.80 287.11 -3 13 11 506.80 117.94 3 13 -11 441.09 149.58 -3 13 11 399.23 65.11 -3 -13 11 550.80 185.54 -2 0 21 147.82 97.90 2 0 -21 20.68 67.28 5 13 1 491.59 237.50 5 -13 1 655.67 248.94 3 15 -4 2311.97 251.67 3 -15 -4 2104.77 386.59 -1 -15 8 100.37 71.56 -1 15 8 114.17 49.23 -6 5 15 865.38 206.32 6 -5 -15 700.26 158.12 6 5 -15 718.52 189.11 -6 -5 15 811.92 231.25 7 -8 4 129.55 65.05 7 8 4 219.74 84.65 -2 -15 7 194.29 97.45 4 14 3 2605.59 227.15 4 -14 3 2217.80 380.90 5 11 8 891.04 185.23 5 -11 8 474.04 92.80 8 -1 -9 68.67 64.01 -8 -1 9 114.52 51.60 8 1 -9 143.97 100.15 -8 1 9 80.27 97.08 2 -14 9 642.51 154.56 2 14 9 573.54 172.78 -4 11 13 743.02 136.98 -4 -11 13 656.54 205.73 4 -11 -13 591.65 168.22 4 11 -13 855.45 189.41 7 -1 10 481.79 179.76 7 1 10 398.87 136.83 7 1 10 442.76 124.10 7 -1 10 418.08 131.76 3 8 16 4837.54 362.29 3 -8 16 3507.26 372.84 -6 -11 6 1077.42 260.72 6 -11 -6 930.16 203.80 6 11 -6 1628.99 239.71 6 -11 -6 967.98 359.62 2 15 6 429.19 129.81 2 -15 6 36.37 61.17 -8 -3 8 520.46 124.64 8 -3 -8 353.81 104.10 -8 3 8 221.51 115.47 8 3 -8 398.08 156.21 -2 1 21 402.45 174.01 2 -1 -21 257.10 219.44 -2 -1 21 604.12 186.86 2 1 -21 248.78 125.51 -6 3 16 1449.97 402.16 6 -3 -16 1487.98 401.57 6 3 -16 1693.25 421.52 -6 -3 16 2036.04 473.17 -6 10 9 742.28 143.91 6 -10 -9 777.65 156.96 -6 -10 9 641.56 149.74 6 10 -9 762.89 258.10 3 14 7 184.97 70.23 3 -14 7 196.13 87.10 5 13 -4 1071.54 149.05 5 -13 -4 1135.44 254.11 -2 5 20 277.82 129.62 2 5 -20 315.20 138.68 2 -5 -20 379.63 109.91 -2 -5 20 299.57 114.96 4 13 -9 291.50 107.18 -4 13 9 27.48 44.84 -4 -13 9 179.49 80.03 -4 13 9 190.75 77.02 8 -5 -5 650.13 176.86 8 5 -5 818.88 186.61 8 -5 -5 381.85 124.34 -8 -5 5 877.09 216.60 2 0 20 53.48 49.44 2 0 20 53.30 90.85 0 -16 4 -33.86 45.10 8 0 5 62.43 54.19 8 0 5 -64.77 76.43 8 -4 -7 749.31 141.43 -8 -4 7 783.25 157.82 -8 4 7 863.05 188.96 8 4 -7 747.30 217.57 4 -6 -18 428.55 179.32 4 6 -18 511.28 162.12 -4 6 18 617.13 195.30 -4 -6 18 283.33 118.33 -3 -12 13 5629.79 414.32 3 12 -13 5092.76 382.32 -3 12 13 4739.37 445.97 -3 12 13 5303.99 295.91 7 -7 6 1157.84 201.13 7 7 6 883.10 283.64 7 -7 6 817.37 176.70 6 11 3 2606.39 225.39 6 -11 3 2731.74 498.30 1 16 3 62.80 51.46 1 -16 3 -3.08 57.97 7 9 1 -31.51 110.08 7 -9 1 69.74 82.40 -7 -6 11 617.39 210.97 7 -6 -11 608.84 194.80 7 6 -11 652.62 211.10 -7 6 11 413.34 124.15 1 -8 18 310.68 106.25 1 -8 18 230.98 174.75 1 8 18 168.97 52.14 1 8 18 239.88 91.52 -6 -9 11 719.21 223.86 -6 9 11 963.39 158.81 6 -9 -11 839.98 157.89 6 9 -11 890.14 247.19 3 0 19 51.03 105.50 3 0 19 47.05 45.37 8 -5 1 927.50 162.77 8 5 1 539.83 185.95 -8 -5 -1 590.40 102.39 8 -5 1 552.69 115.06 7 4 9 458.10 173.36 7 -4 9 349.20 113.33 7 -4 9 325.58 128.14 7 4 9 522.87 159.76 4 -11 11 818.40 221.90 4 11 11 609.67 163.96 -3 6 19 228.23 69.73 -3 -6 19 489.29 165.97 3 -6 -19 310.31 190.35 3 6 -19 233.39 91.25 0 2 21 857.30 186.63 0 -2 21 1049.37 226.13 0 -2 21 907.29 258.18 0 2 21 754.82 271.03 5 4 15 1081.75 300.99 5 4 15 1022.13 239.91 5 -4 15 981.29 224.45 5 -4 15 975.53 264.15 4 13 7 295.53 92.14 4 -13 7 281.77 116.26 2 1 20 162.55 93.81 2 -1 20 476.46 118.22 2 -1 20 477.93 170.02 2 1 20 491.65 138.11 4 4 -19 666.96 145.71 4 -4 -19 832.32 221.13 -4 4 19 1035.00 258.72 -4 -4 19 948.33 312.01 5 -3 -18 164.54 96.09 5 3 -18 130.47 90.81 -5 3 18 178.59 94.20 -5 -3 18 258.79 105.00 8 -1 5 -4.39 39.77 8 1 5 74.56 43.69 8 -1 5 77.73 63.69 8 1 5 247.60 100.59 7 5 -12 117.94 74.59 -7 5 12 -31.09 114.20 7 -5 -12 137.95 77.00 -7 -5 12 30.60 62.80 2 -5 19 174.35 80.06 2 5 19 236.57 113.48 2 5 19 272.39 96.62 2 -5 19 87.04 106.35 3 15 3 158.58 92.97 3 -15 3 4.64 40.43 6 10 6 369.86 146.51 6 -10 6 105.82 119.46 8 -3 4 131.48 86.37 8 3 4 -35.24 102.06 8 -3 4 109.13 92.94 8 3 4 77.27 37.33 -2 12 14 390.76 95.77 -2 -12 14 179.59 112.25 -2 12 14 316.03 123.01 2 12 -14 315.41 111.37 -2 7 19 832.27 252.37 2 7 -19 905.30 313.14 -2 -7 19 1309.82 359.21 -2 7 19 860.08 342.04 7 -8 -8 83.80 86.12 -7 -8 8 -49.68 61.96 7 8 -8 115.07 52.38 7 -8 -8 174.18 85.98 8 -4 3 473.64 98.70 8 4 3 320.52 190.12 8 4 3 313.25 81.78 8 -4 3 468.65 119.54 7 -9 -5 68.65 127.72 7 -9 -5 -12.97 53.17 -7 -9 5 72.27 66.77 7 9 -5 36.16 46.63 3 -1 19 99.02 68.47 3 1 19 103.18 82.27 3 1 19 168.52 66.66 3 -1 19 43.94 64.12 6 -5 12 1898.81 311.42 6 5 12 1695.14 526.50 6 -5 12 2254.35 307.33 3 -11 13 468.74 251.27 3 11 13 1048.68 208.39 -5 -8 15 117.78 102.26 5 8 -15 121.38 82.46 -5 8 15 194.01 80.84 5 13 2 2944.27 234.27 5 -13 2 2110.34 552.53 2 12 13 216.72 85.05 2 -12 13 398.04 133.64 -8 2 9 0.35 84.29 8 2 -9 35.23 82.52 8 -2 -9 91.48 37.85 -8 -2 9 100.48 128.16 7 -2 10 1014.37 173.67 7 -2 10 919.47 225.96 7 2 10 1449.14 230.67 7 2 10 891.63 199.98 5 -12 6 1365.22 351.20 5 12 6 1309.20 172.42 4 -6 16 267.55 106.68 4 6 16 238.44 163.25 4 -6 16 204.26 102.36 2 -7 18 378.25 113.91 2 7 18 327.98 144.72 2 -7 18 627.11 202.03 2 7 18 238.64 104.34 0 -14 11 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