#============================================================================= data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 14 _journal_issue 2 _journal_year 2023 _journal_page_first 193 _journal_page_last 201 #============================================================================= #\#CIF_1.1 # CIF produced by WinGX routine CIF_UPDATE # Created on 2022-08-16 at 16:27:00 # Using CIFtbx version 3.0.4 1 Sep 2006 # Dictionary name : cif_core.dic # Dictionary vers : 2.4.5 # Request file : c:\wingx\files\archive.reqdat # CIF files read : cr11 project #------------------ AUDIT DETAILS -------------------------------------------# _audit_creation_date 2022-08-16 _audit_creation_method 'WinGX routine CIF_UPDATE' _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.3 _audit_conform_dict_location ftp://ftp.iucr.org/pub/cif_core.dic _audit_update_record ; ? 2022-12-23 # Formatted by publCIF ; #------------------ AUTHOR DETAILS -------------------------------------------# # Name and address of author for correspondence _publ_contact_author_name 'Correa, Rodrigo' _publ_contact_author_address ; ; _publ_contact_author_email ' rodrigocorrea@ufop.edu.br' _publ_contact_author_fax ' ' _publ_contact_author_phone ' ' # Insert blank lines between references _publ_section_references ; Blessing, R. H. (1995). Acta Cryst. A51, 33--38. Blessing, R. H. (1987). Cryst. Rev. 1, 3--58. Blessing, R. H. (1989). J. Appl. Cryst. 22, 396--397. Bruker (2012). APEX2 (Version 2012.10-0), SAINT (version 8.27B), SADABS (version 2012/1), BrukerAXS Inc, Madison, Wisconsin, USA. ABSCOR: Higashi, T. (1995). ABSCOR. Rigaku Corporation, Tokyo, Japan. CAD-4 Software: Enraf-Nonius (1989). CAD-4 Software (or CAD-4 EXPRESS). Enraf-Nonius, Delft, The Netherlands. Cambridge Structural Database: Allen, F. R. (2002). Acta Cryst. B58, 380--388. CAMERON: Watkin, D. J., Prout, C. K. & Pearce, L. J. (1996). CAMERON. Chemical Crystallography Laboratory, Oxford, England. CrysAlis CCD, CrysAlis RED and associated programs: Oxford Diffraction (2006). Program name(s). Oxford Diffraction Ltd, Abingdon, England. CRYSTALS: Betteridge, P. W., Carruthers, J. R., Cooper, R. I., Prout, K. & Watkin, D. J. (2003). J. Appl. Cryst. 36, 1487. COLLECT: Nonius (1998). COLLECT. Nonius BV, Delft, The Netherlands. DENZO/SCALEPACK: Otwinowski, Z. & Minor, W. (1997). Methods in Enzymology, Vol. 276, Macromolecular Crystallography, Part A, edited by C. W. Carter Jr & R. M. Sweet, pp. 307-326. New York: Academic Press. DIAMOND: Brandenburg, K. (2006). DIAMOND. Crystal Impact GbR, Bonn, Germany. DIF4 and REDU4: Stoe & Cie (1991). Program name(s). Stoe & Cie, Darmstadt, Germany. DIFABS: Walker, N. & Stuart, D. (1983). Acta Cryst. A39, 158--166. DIRAX: Duisenberg, A. J. M. (1992). J. Appl. Cryst. 25, 92--96. DIRDIF2008: Beurskens, P. T., Beurskens, G., de Gelder, R., Garci\'ia-Granda, S., Gould, R. O. & Smits, J. M. M. (2008). The DIRDIF2008 program system, Crystallography Laboratory, Radboud University Nijmegen, The Netherlands. EDMA: Palatinus, L., Prathapa, S. J. & van Smaalen, S. (2012). J. Appl. Cryst. 45, 575--580. enCIFer: Allen, F. H., Johnson, O., Shields, G. P., Smith, B. R. & Towler, M. (2004). J. Appl. Cryst. 37, 335--338. EVALCCD: Duisenberg, A. J. M., Kroon-Batenburg, L. M. J. & Schreurs, A. M. M. (2003). J. Appl. Cryst. 36, 220--229. JANA2000: Petricek, V. & Dusek, M. (2000). JANA2000. Institute of Physics, Czech Academy of Sciences, Prague, Czech Republic. Mercury: Macrae, C. F., Bruno, I. J., Chisholm, J. A., Edgington, P. R., McCabe, P., Pidcock, E., Rodriguez-Monge, L., Taylor, R., van de Streek, J. & Wood, P. A. (2008). J. Appl. Cryst. 41, 466--470. Mogul: Bruno, I. J., Cole, J. C., Kessler, M., Luo, J., Motherwell, W. D. S., Purkis, L. H., Smith, B. R., Taylor, R., Cooper, R. I., Harris, S. E. & Orpen, A. G. (2004). J. Chem. Inf. Comput. Sci. 44, 2133--2144. ORTEPII: Johnson, C. K. (1976). ORTEPII. Report ORNL-5138. Oak Ridge National Laboratory, Tennessee, USA. ORTEPIII: Burnett, M. N. & Johnson, C. K. (1996). ORTEPIII. Report ORNL-6895. Oak Ridge National Laboratory, Tennessee, USA. ORTEP-3: Farrugia, L. J. (2012). J. Appl. Cryst. 45, 849--854. PARST: Nardelli, M. (1995). J. Appl. Cryst. 28, 659. PLATON: Spek, A. L. (2009). Acta Cryst. D65, 148--155. PROCESS: Rigaku (1996). PROCESS. Rigaku Corporation, Tokyo, Japan. PROCESSAUTO: Rigaku (1998). PROCESS-AUTO. Rigaku Corporation, Tokyo, Japan. publCIF: Westrip, S. P. (2010). J. Appl. Cryst. 43, 920--925. SCHAKAL: Keller, E. (1999). University of Freiburg, Germany. SHELX: Sheldrick, G. M. (2015). Acta Cryst. C71, 3--8. SHELXD: Schneider, T. R. & Sheldrick, G. M. (2002). Acta Cryst. D58, 1772--1779. SHELXT: Sheldrick, G. M. (2015). Acta Cryst. A71, 3--8. SIR92: Altomare, A., Cascarano, G., Giacovazzo, C., Guagliardi, A., Burla, M. C., Polidori, G. & Camalli, M. (1994). J. Appl. Cryst. 27, 435. SIR97: Altomare, A., Burla, M. C., Camalli, M., Cascarano, G. L., Giacovazzo, C., Guagliardi, A., Moliterni, A. G. G., Polidori, G. & Spagna, R. (1999). J. Appl. Cryst. 32, 115--119. SIR2002: Burla, M. C., Camalli, M., Carrozzini, B., Cascarano, G. L., Giacovazzo, C., Polidori, G. & Spagna, R. (2003). J. Appl. Cryst. 36, 1103. SIR2004: Burla, M. C., Caliandro, R., Camalli, M., Carrozzini, B., Cascarano, G. L., De Caro, L., Giacovazzo, C., Polidori, G. & Spagna, R. (2005). J. Appl. Cryst. 38, 381--388. SIR2008 & IL MILIONE: Burla, M. C., Caliandro, R., Camalli, M., Carrozzini, B., Cascarano, G. L., De Caro, L., Giacovazzo, C., Polidori, G., Siliqi, D., & Spagna, R. (2007). J. Appl. Cryst. 40, 609--613. SIR2011: Burla, M. C., Caliandro, R., Camalli, M., Carrozzini, B., Cascarano, G. L., Giacovazzo, C., Mallamo, M., Mazzone, A., Polidori, G. & Spagna, R. (2012). J. Appl. Cryst. 45, 357--361. SUPERFLIP: Palatinus, L. & Chapuis, G. (2007). J. Appl. Cryst. 40, 786--790. TEXSAN: Molecular Structure Corporation & Rigaku (2000). TEXSAN. MSC, The Woodlands, Texas, USA, and Rigaku Corporation, Tokyo, Japan. WinGX: Farrugia, L. J. (2012). J. Appl. Cryst. 45, 849--854. X-AREA, X-RED, X-RED32, X-SHAPE: Stoe & Cie (2002). Program name(s). Stoe & Cie GmbH, Darmstadt, Germany. XCAD4: Harms, K. & Wocadlo, S. (1995). XCAD4. University of Marburg, Germany. XSCANS: Siemens (1994). XSCANS. Siemens Analytical X-ray Instruments Inc., Madison, Wisconsin, USA. ; #------------------ SECTION 2. COMPOUND(S) DETAILS -------------------------# data_shelx _audit_creation_date 2022-08-16T16:27:00-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.5 _audit_conform_dict_location ftp://ftp.iucr.org/pub/cif_core.dic _publ_requested_category FM #----------------------------------------------------------------------------# # CHEMICAL INFORMATION # #----------------------------------------------------------------------------# _chemical_formula_moiety 'C52 H48 Cl4 P4 Ru1' _chemical_formula_sum 'C26 H24 Cl2 P2 Ru0.50' _chemical_formula_weight 519.83 _chemical_compound_source 'synthesis as described' #----------------------------------------------------------------------------# # UNIT CELL INFORMATION # #----------------------------------------------------------------------------# _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.240(3) _cell_length_b 10.9290(18) _cell_length_c 11.993(3) _cell_angle_alpha 78.707(11) _cell_angle_beta 86.712(13) _cell_angle_gamma 82.598(13) _cell_volume 1177.1(5) _cell_formula_units_Z 2 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 9608 _cell_measurement_theta_min 3.467 _cell_measurement_theta_max 25.242 _cell_measurement_wavelength 0.71073 #----------------------------------------------------------------------------# # CRYSTAL INFORMATION # #----------------------------------------------------------------------------# _exptl_crystal_description prism _exptl_crystal_colour brown _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.03 _exptl_crystal_density_diffrn 1.467 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 532 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1 8 -4 0.024 1 -7 3 0.011 -1 0 0 0.179 1 0 0 0.18 0 1 2 0.072 -1 -2 -5 0.086 5 -3 -6 0.196 #----------------------------------------------------------------------------# # ABSORPTION CORRECTION # #----------------------------------------------------------------------------# _exptl_absorpt_coefficient_mu 0.732 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; P. Coppens, L. Leiserowitz, D Rabinovich, Acta Cryst. (1965), 18, 1035-1038 ; _exptl_absorpt_correction_T_min 0.822 _exptl_absorpt_correction_T_max 0.973 #----------------------------------------------------------------------------# # DATA COLLECTION # #----------------------------------------------------------------------------# _diffrn_source 'Enraf Nonius FR590' _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_monochromator 'horizonally mounted graphite crystal' _diffrn_radiation_probe x-ray _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 9 _diffrn_orient_matrix_ub_11 -0.011244 _diffrn_orient_matrix_ub_12 0.068606 _diffrn_orient_matrix_ub_13 0.045229 _diffrn_orient_matrix_ub_21 0.107181 _diffrn_orient_matrix_ub_22 -0.014576 _diffrn_orient_matrix_ub_23 0.013503 _diffrn_orient_matrix_ub_31 0.017597 _diffrn_orient_matrix_ub_32 0.06256 _diffrn_orient_matrix_ub_33 -0.070783 _diffrn_measurement_device '95mm CCD camera on \k-goniostat' _diffrn_measurement_device_type KappaCCD _diffrn_measurement_method 'CCD rotation images, thick slices' _diffrn_standards_number 0 _diffrn_standards_interval_time . _diffrn_standards_interval_count . _diffrn_standards_decay_% ? _diffrn_reflns_av_R_equivalents 0.0973 _diffrn_reflns_av_unetI/netI 0.1171 _diffrn_reflns_number 8434 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_theta_min 3.467 _diffrn_reflns_theta_max 25.993 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.995 _reflns_Friedel_coverage 0 _reflns_number_total 4607 _reflns_number_gt 3219 _reflns_threshold_expression 'I > 2\s(I)' _diffrn_reflns_reduction_process ; Scaled and merged with Sortav R.H. Blessing, (1987) Cryst. Rev. 1, 3-58 R.H. Blessing, (1989) J. Appl. Cryst. 22, 396-397 ; #----------------------------------------------------------------------------# # COMPUTER PROGRAMS USED # #----------------------------------------------------------------------------# _computing_data_collection 'Collect (Bruker AXS BV, 1997-2004)' _computing_cell_refinement ; HKL Scalepack (Otwinowski & Minor 1997) ; _computing_data_reduction ; HKL Denzo and Scalepack (Otwinowski & Minor 1997) ; _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'Ortep-3 for Windows (Farrugia, 1997)' _computing_publication_material ; WinGX publication routines (Farrugia, 1999) ; #----------------------------------------------------------------------------# # STRUCTURE SOLUTION # #----------------------------------------------------------------------------# _atom_sites_solution_hydrogens geom #----------------------------------------------------------------------------# # REFINEMENT INFORMATION # #----------------------------------------------------------------------------# _shelx_SHELXL_version_number 2018/3 _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; 'w=1/[\s^2^(Fo^2^)+(0.0392P)^2^] where P=(Fo^2^+2Fc^2^)/3' ; _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_number_reflns 4607 _refine_ls_number_parameters 277 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_R_factor_all 0.0795 _refine_ls_R_factor_gt 0.0537 _refine_ls_wR_factor_ref 0.1347 _refine_ls_wR_factor_gt 0.1222 _refine_ls_goodness_of_fit_ref 0.957 _refine_ls_restrained_S_all 0.957 _refine_ls_shift/su_max 0 _refine_ls_shift/su_mean 0 _refine_diff_density_max 0.729 _refine_diff_density_min -0.951 _refine_diff_density_rms 0.09 #----------------------------------------------------------------------------# # CONSTRAINTS AND RESTRAINTS # #----------------------------------------------------------------------------# #----------------------------------------------------------------------------# # ATOMIC TYPES, COORDINATES AND THERMAL PARAMETERS # #----------------------------------------------------------------------------# loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0 1 0 0.04623(16) Uani 1 2 d S . P . . P2 P 0.01062(11) 0.78800(10) -0.03826(9) 0.0501(3) Uani 1 1 d . . . . . P1 P 0.08924(11) 0.88052(10) 0.18374(9) 0.0502(3) Uani 1 1 d . . . . . Cl1 Cl 0.24991(10) 0.99131(10) -0.04304(9) 0.0565(3) Uani 1 1 d . . . . . C211 C 0.1255(4) 0.7478(4) -0.1578(4) 0.0540(10) Uani 1 1 d . . . . . C221 C -0.1596(4) 0.7277(4) -0.0568(4) 0.0556(10) Uani 1 1 d . . . . . C231 C 0.0902(4) 0.6770(4) 0.0865(4) 0.0587(11) Uani 1 1 d . . . . . H23A H 0.012505 0.649317 0.139558 0.07 Uiso 1 1 calc R U . . . H23B H 0.142875 0.603756 0.061857 0.07 Uiso 1 1 calc R U . . . C121 C -0.0268(4) 0.8060(4) 0.3007(3) 0.0543(10) Uani 1 1 d . . . . . C212 C 0.1708(4) 0.8393(4) -0.2444(4) 0.0596(11) Uani 1 1 d . . . . . H212 H 0.148243 0.923648 -0.239828 0.072 Uiso 1 1 calc R U . . . C111 C 0.2107(4) 0.9520(4) 0.2588(3) 0.0540(10) Uani 1 1 d . . . . . C131 C 0.1938(4) 0.7395(4) 0.1456(4) 0.0573(10) Uani 1 1 d . . . . . H13A H 0.27592 0.762074 0.095136 0.069 Uiso 1 1 calc R U . . . H13B H 0.230698 0.68269 0.213338 0.069 Uiso 1 1 calc R U . . . C126 C -0.1760(4) 0.8103(4) 0.2934(4) 0.0595(11) Uani 1 1 d . . . . . H126 H -0.223486 0.860891 0.231414 0.071 Uiso 1 1 calc R U . . . C124 C -0.1859(6) 0.6642(5) 0.4700(4) 0.0760(14) Uani 1 1 d . . . . . H124 H -0.238996 0.615397 0.525905 0.091 Uiso 1 1 calc R U . . . C122 C 0.0414(5) 0.7316(4) 0.3945(4) 0.0661(12) Uani 1 1 d . . . . . H122 H 0.141653 0.72881 0.400886 0.079 Uiso 1 1 calc R U . . . C226 C -0.2605(5) 0.7087(4) 0.0329(4) 0.0691(12) Uani 1 1 d . . . . . H226 H -0.239634 0.725585 0.102952 0.083 Uiso 1 1 calc R U . . . C116 C 0.1562(5) 1.0047(4) 0.3511(4) 0.0614(11) Uani 1 1 d . . . . . H116 H 0.058759 1.001118 0.374084 0.074 Uiso 1 1 calc R U . . . C125 C -0.2558(5) 0.7390(5) 0.3788(4) 0.0708(13) Uani 1 1 d . . . . . H125 H -0.356345 0.742296 0.373755 0.085 Uiso 1 1 calc R U . . . C123 C -0.0387(5) 0.6609(4) 0.4792(4) 0.0731(13) Uani 1 1 d . . . . . H123 H 0.007885 0.611433 0.542159 0.088 Uiso 1 1 calc R U . . . C213 C 0.2499(5) 0.8064(5) -0.3385(4) 0.0702(13) Uani 1 1 d . . . . . H213 H 0.27858 0.868911 -0.396843 0.084 Uiso 1 1 calc R U . . . C216 C 0.1637(5) 0.6218(4) -0.1668(4) 0.0677(12) Uani 1 1 d . . . . . H216 H 0.1346 0.55875 -0.109127 0.081 Uiso 1 1 calc R U . . . C112 C 0.3575(4) 0.9582(5) 0.2258(4) 0.0664(12) Uani 1 1 d . . . . . H112 H 0.396889 0.923113 0.164407 0.08 Uiso 1 1 calc R U . . . C215 C 0.2439(6) 0.5896(5) -0.2599(5) 0.0819(15) Uani 1 1 d . . . . . H215 H 0.269472 0.505558 -0.264651 0.098 Uiso 1 1 calc R U . . . C114 C 0.3876(5) 1.0690(5) 0.3753(4) 0.0754(14) Uani 1 1 d . . . . . H114 H 0.446544 1.108827 0.413504 0.09 Uiso 1 1 calc R U . . . C115 C 0.2433(5) 1.0624(4) 0.4097(4) 0.0696(13) Uani 1 1 d . . . . . H115 H 0.205025 1.096533 0.471879 0.084 Uiso 1 1 calc R U . . . C225 C -0.3915(5) 0.6652(5) 0.0205(5) 0.0810(15) Uani 1 1 d . . . . . H225 H -0.458111 0.652985 0.081639 0.097 Uiso 1 1 calc R U . . . C223 C -0.3251(6) 0.6588(5) -0.1733(5) 0.0840(16) Uani 1 1 d . . . . . H223 H -0.347429 0.641535 -0.242843 0.101 Uiso 1 1 calc R U . . . C224 C -0.4225(6) 0.6401(5) -0.0826(6) 0.0911(18) Uani 1 1 d . . . . . H224 H -0.510184 0.610219 -0.091139 0.109 Uiso 1 1 calc R U . . . C222 C -0.1945(5) 0.7029(4) -0.1622(4) 0.0674(12) Uani 1 1 d . . . . . H222 H -0.129511 0.716248 -0.224293 0.081 Uiso 1 1 calc R U . . . C214 C 0.2857(5) 0.6838(6) -0.3458(4) 0.0785(14) Uani 1 1 d . . . . . H214 H 0.338667 0.662938 -0.409181 0.094 Uiso 1 1 calc R U . . . C113 C 0.4442(5) 1.0166(5) 0.2842(5) 0.0770(14) Uani 1 1 d . . . . . H113 H 0.541802 1.020545 0.261756 0.092 Uiso 1 1 calc R U . . . Cl1S Cl 0.43047(14) 0.56909(15) 0.38552(12) 0.0890(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.0489(3) 0.0400(3) 0.0526(3) -0.0115(2) -0.00750(19) -0.00906(19) P2 0.0547(6) 0.0405(6) 0.0589(6) -0.0145(5) -0.0073(5) -0.0104(5) P1 0.0532(6) 0.0464(7) 0.0533(6) -0.0108(5) -0.0086(4) -0.0099(5) Cl1 0.0507(5) 0.0555(7) 0.0654(6) -0.0125(5) -0.0063(4) -0.0107(4) C211 0.055(2) 0.050(3) 0.061(3) -0.017(2) -0.0067(18) -0.0104(18) C221 0.059(2) 0.041(2) 0.067(3) -0.008(2) -0.010(2) -0.0095(18) C231 0.068(2) 0.044(3) 0.067(3) -0.012(2) -0.011(2) -0.0083(19) C121 0.059(2) 0.050(3) 0.057(2) -0.013(2) -0.0075(18) -0.0126(19) C212 0.065(2) 0.056(3) 0.061(3) -0.014(2) -0.010(2) -0.010(2) C111 0.059(2) 0.049(3) 0.055(2) -0.0086(19) -0.0100(18) -0.0087(19) C131 0.062(2) 0.050(3) 0.060(3) -0.011(2) -0.0102(19) -0.0031(19) C126 0.065(2) 0.057(3) 0.061(3) -0.016(2) -0.005(2) -0.018(2) C124 0.096(4) 0.061(3) 0.074(3) -0.009(3) 0.011(3) -0.031(3) C122 0.068(3) 0.059(3) 0.071(3) -0.007(2) -0.009(2) -0.008(2) C226 0.070(3) 0.059(3) 0.083(3) -0.016(2) -0.005(2) -0.016(2) C116 0.065(2) 0.056(3) 0.066(3) -0.016(2) -0.011(2) -0.010(2) C125 0.073(3) 0.075(4) 0.071(3) -0.021(3) 0.004(2) -0.027(3) C123 0.094(3) 0.056(3) 0.066(3) 0.002(2) -0.007(3) -0.012(3) C213 0.073(3) 0.075(4) 0.063(3) -0.011(3) -0.003(2) -0.012(3) C216 0.084(3) 0.051(3) 0.071(3) -0.019(2) 0.001(2) -0.008(2) C112 0.058(2) 0.077(4) 0.070(3) -0.022(3) -0.007(2) -0.012(2) C215 0.093(3) 0.071(4) 0.084(4) -0.032(3) 0.001(3) 0.005(3) C114 0.079(3) 0.073(4) 0.082(3) -0.018(3) -0.028(3) -0.022(3) C115 0.089(3) 0.063(3) 0.064(3) -0.022(2) -0.015(2) -0.016(2) C225 0.061(3) 0.070(4) 0.111(4) -0.008(3) 0.006(3) -0.021(2) C223 0.091(3) 0.080(4) 0.087(4) -0.008(3) -0.037(3) -0.030(3) C224 0.071(3) 0.073(4) 0.129(5) 0.001(3) -0.029(3) -0.027(3) C222 0.072(3) 0.062(3) 0.072(3) -0.012(2) -0.014(2) -0.019(2) C214 0.083(3) 0.091(4) 0.065(3) -0.029(3) 0.004(2) 0.001(3) C113 0.064(3) 0.081(4) 0.092(4) -0.021(3) -0.022(2) -0.016(3) Cl1S 0.0769(8) 0.0960(11) 0.0942(10) -0.0166(8) -0.0090(7) -0.0102(7) #----------------------------------------------------------------------------# # MOLECULAR GEOMETRY # #----------------------------------------------------------------------------# _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 Cl1 2.3310(12) . ? Ru1 Cl1 2.3310(12) 2_575 ? Ru1 P2 2.4374(11) . ? Ru1 P2 2.4374(11) 2_575 ? Ru1 P1 2.4587(11) . ? Ru1 P1 2.4587(11) 2_575 ? P2 C221 1.823(4) . ? P2 C211 1.825(4) . ? P2 C231 1.853(4) . ? P1 C111 1.816(4) . ? P1 C131 1.833(4) . ? P1 C121 1.840(4) . ? C211 C212 1.380(6) . ? C211 C216 1.400(6) . ? C221 C226 1.385(6) . ? C221 C222 1.406(6) . ? C231 C131 1.524(5) . ? C231 H23A 0.97 . ? C231 H23B 0.97 . ? C121 C126 1.381(5) . ? C121 C122 1.384(6) . ? C212 C213 1.390(6) . ? C212 H212 0.93 . ? C111 C116 1.386(6) . ? C111 C112 1.398(6) . ? C131 H13A 0.97 . ? C131 H13B 0.97 . ? C126 C125 1.396(6) . ? C126 H126 0.93 . ? C124 C123 1.367(6) . ? C124 C125 1.369(7) . ? C124 H124 0.93 . ? C122 C123 1.389(6) . ? C122 H122 0.93 . ? C226 C225 1.383(6) . ? C226 H226 0.93 . ? C116 C115 1.382(6) . ? C116 H116 0.93 . ? C125 H125 0.93 . ? C123 H123 0.93 . ? C213 C214 1.357(7) . ? C213 H213 0.93 . ? C216 C215 1.383(6) . ? C216 H216 0.93 . ? C112 C113 1.382(6) . ? C112 H112 0.93 . ? C215 C214 1.383(7) . ? C215 H215 0.93 . ? C114 C113 1.377(7) . ? C114 C115 1.379(7) . ? C114 H114 0.93 . ? C115 H115 0.93 . ? C225 C224 1.371(8) . ? C225 H225 0.93 . ? C223 C224 1.372(8) . ? C223 C222 1.379(6) . ? C223 H223 0.93 . ? C224 H224 0.93 . ? C222 H222 0.93 . ? C214 H214 0.93 . ? C113 H113 0.93 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Ru1 Cl1 180 . 2_575 ? Cl1 Ru1 P2 88.26(4) . . ? Cl1 Ru1 P2 91.74(4) 2_575 . ? Cl1 Ru1 P2 91.74(4) . 2_575 ? Cl1 Ru1 P2 88.26(4) 2_575 2_575 ? P2 Ru1 P2 180 . 2_575 ? Cl1 Ru1 P1 81.47(4) . . ? Cl1 Ru1 P1 98.53(4) 2_575 . ? P2 Ru1 P1 80.97(4) . . ? P2 Ru1 P1 99.03(4) 2_575 . ? Cl1 Ru1 P1 98.53(4) . 2_575 ? Cl1 Ru1 P1 81.47(4) 2_575 2_575 ? P2 Ru1 P1 99.03(4) . 2_575 ? P2 Ru1 P1 80.97(4) 2_575 2_575 ? P1 Ru1 P1 180.00(4) . 2_575 ? C221 P2 C211 102.89(19) . . ? C221 P2 C231 103.56(18) . . ? C211 P2 C231 103.6(2) . . ? C221 P2 Ru1 118.74(15) . . ? C211 P2 Ru1 118.35(13) . . ? C231 P2 Ru1 107.79(13) . . ? C111 P1 C131 107.09(19) . . ? C111 P1 C121 102.02(18) . . ? C131 P1 C121 99.5(2) . . ? C111 P1 Ru1 117.70(14) . . ? C131 P1 Ru1 103.19(14) . . ? C121 P1 Ru1 124.86(13) . . ? C212 C211 C216 118.2(4) . . ? C212 C211 P2 121.6(3) . . ? C216 C211 P2 120.2(3) . . ? C226 C221 C222 118.2(4) . . ? C226 C221 P2 120.2(3) . . ? C222 C221 P2 121.6(3) . . ? C131 C231 P2 110.7(3) . . ? C131 C231 H23A 109.5 . . ? P2 C231 H23A 109.5 . . ? C131 C231 H23B 109.5 . . ? P2 C231 H23B 109.5 . . ? H23A C231 H23B 108.1 . . ? C126 C121 C122 119.0(4) . . ? C126 C121 P1 122.8(3) . . ? C122 C121 P1 117.9(3) . . ? C211 C212 C213 120.5(4) . . ? C211 C212 H212 119.8 . . ? C213 C212 H212 119.8 . . ? C116 C111 C112 118.3(4) . . ? C116 C111 P1 119.2(3) . . ? C112 C111 P1 122.4(3) . . ? C231 C131 P1 107.0(3) . . ? C231 C131 H13A 110.3 . . ? P1 C131 H13A 110.3 . . ? C231 C131 H13B 110.3 . . ? P1 C131 H13B 110.3 . . ? H13A C131 H13B 108.6 . . ? C121 C126 C125 120.2(4) . . ? C121 C126 H126 119.9 . . ? C125 C126 H126 119.9 . . ? C123 C124 C125 120.4(4) . . ? C123 C124 H124 119.8 . . ? C125 C124 H124 119.8 . . ? C121 C122 C123 120.5(4) . . ? C121 C122 H122 119.7 . . ? C123 C122 H122 119.7 . . ? C225 C226 C221 121.3(5) . . ? C225 C226 H226 119.3 . . ? C221 C226 H226 119.3 . . ? C115 C116 C111 121.5(4) . . ? C115 C116 H116 119.2 . . ? C111 C116 H116 119.2 . . ? C124 C125 C126 119.9(4) . . ? C124 C125 H125 120 . . ? C126 C125 H125 120 . . ? C124 C123 C122 119.9(5) . . ? C124 C123 H123 120 . . ? C122 C123 H123 120 . . ? C214 C213 C212 120.6(5) . . ? C214 C213 H213 119.7 . . ? C212 C213 H213 119.7 . . ? C215 C216 C211 121.1(5) . . ? C215 C216 H216 119.5 . . ? C211 C216 H216 119.5 . . ? C113 C112 C111 120.0(5) . . ? C113 C112 H112 120 . . ? C111 C112 H112 120 . . ? C214 C215 C216 119.2(5) . . ? C214 C215 H215 120.4 . . ? C216 C215 H215 120.4 . . ? C113 C114 C115 120.0(4) . . ? C113 C114 H114 120 . . ? C115 C114 H114 120 . . ? C114 C115 C116 119.5(5) . . ? C114 C115 H115 120.3 . . ? C116 C115 H115 120.3 . . ? C224 C225 C226 119.5(5) . . ? C224 C225 H225 120.3 . . ? C226 C225 H225 120.3 . . ? C224 C223 C222 120.5(5) . . ? C224 C223 H223 119.7 . . ? C222 C223 H223 119.7 . . ? C225 C224 C223 120.5(4) . . ? C225 C224 H224 119.7 . . ? C223 C224 H224 119.7 . . ? C223 C222 C221 119.9(5) . . ? C223 C222 H222 120 . . ? C221 C222 H222 120 . . ? C213 C214 C215 120.5(5) . . ? C213 C214 H214 119.7 . . ? C215 C214 H214 119.7 . . ? C114 C113 C112 120.7(5) . . ? C114 C113 H113 119.7 . . ? C112 C113 H113 119.7 . . ? _shelx_res_file ; TITL CR11 shelx.res created by SHELXL-2018/3 at 16:26:30 on 16-Aug-2022 CELL 0.71073 9.2400 10.9290 11.9930 78.707 86.712 82.598 ZERR 2.00 0.0029 0.0018 0.0027 0.011 0.013 0.013 LATT 1 SFAC RU P CL C H DISP Ru -1.25940 0.83630 DISP P 0.10230 0.09420 DISP Cl 0.14840 0.15850 DISP C 0.00330 0.00160 DISP H 0.00000 0.00000 UNIT 1 4 4 52 48 MERG 2 OMIT -3.00 52.00 OMIT -1 1 0 OMIT 2 0 3 OMIT 1 1 1 OMIT 1 0 2 FMAP 2 PLAN 20 ACTA BOND $H LIST 4 L.S. 8 WGHT 0.039200 FVAR 1.19360 RU1 1 10.000000 11.000000 10.000000 10.50000 0.04889 0.04002 = 0.05258 -0.01152 -0.00750 -0.00906 P2 2 0.010622 0.788004 -0.038265 11.00000 0.05469 0.04052 = 0.05890 -0.01449 -0.00725 -0.01044 P1 2 0.089239 0.880522 0.183744 11.00000 0.05317 0.04644 = 0.05334 -0.01084 -0.00863 -0.00991 CL1 3 0.249906 0.991313 -0.043041 11.00000 0.05066 0.05548 = 0.06540 -0.01247 -0.00625 -0.01069 C211 4 0.125542 0.747811 -0.157847 11.00000 0.05495 0.05013 = 0.06129 -0.01698 -0.00673 -0.01044 C221 4 -0.159584 0.727702 -0.056843 11.00000 0.05937 0.04115 = 0.06705 -0.00751 -0.00987 -0.00952 C231 4 0.090217 0.677035 0.086463 11.00000 0.06801 0.04379 = 0.06659 -0.01230 -0.01087 -0.00835 AFIX 23 H23A 5 0.012505 0.649317 0.139558 11.00000 -1.20000 H23B 5 0.142875 0.603756 0.061857 11.00000 -1.20000 AFIX 0 C121 4 -0.026780 0.805960 0.300729 11.00000 0.05922 0.04984 = 0.05733 -0.01298 -0.00753 -0.01263 C212 4 0.170819 0.839326 -0.244434 11.00000 0.06505 0.05562 = 0.06093 -0.01381 -0.00976 -0.00992 AFIX 43 H212 5 0.148243 0.923648 -0.239828 11.00000 -1.20000 AFIX 0 C111 4 0.210727 0.951991 0.258847 11.00000 0.05925 0.04871 = 0.05514 -0.00858 -0.00995 -0.00868 C131 4 0.193770 0.739504 0.145640 11.00000 0.06249 0.05010 = 0.05969 -0.01123 -0.01018 -0.00306 AFIX 23 H13A 5 0.275920 0.762074 0.095136 11.00000 -1.20000 H13B 5 0.230698 0.682690 0.213338 11.00000 -1.20000 AFIX 0 C126 4 -0.176007 0.810306 0.293413 11.00000 0.06510 0.05741 = 0.06121 -0.01646 -0.00498 -0.01756 AFIX 43 H126 5 -0.223486 0.860891 0.231414 11.00000 -1.20000 AFIX 0 C124 4 -0.185934 0.664228 0.469954 11.00000 0.09598 0.06095 = 0.07373 -0.00948 0.01093 -0.03053 AFIX 43 H124 5 -0.238996 0.615397 0.525905 11.00000 -1.20000 AFIX 0 C122 4 0.041401 0.731551 0.394514 11.00000 0.06778 0.05852 = 0.07108 -0.00743 -0.00919 -0.00830 AFIX 43 H122 5 0.141653 0.728810 0.400886 11.00000 -1.20000 AFIX 0 C226 4 -0.260464 0.708710 0.032917 11.00000 0.06978 0.05882 = 0.08261 -0.01635 -0.00456 -0.01648 AFIX 43 H226 5 -0.239634 0.725585 0.102952 11.00000 -1.20000 AFIX 0 C116 4 0.156220 1.004684 0.351090 11.00000 0.06529 0.05627 = 0.06623 -0.01574 -0.01114 -0.01004 AFIX 43 H116 5 0.058759 1.001118 0.374084 11.00000 -1.20000 AFIX 0 C125 4 -0.255807 0.739015 0.378781 11.00000 0.07256 0.07529 = 0.07128 -0.02092 0.00447 -0.02688 AFIX 43 H125 5 -0.356345 0.742296 0.373755 11.00000 -1.20000 AFIX 0 C123 4 -0.038656 0.660927 0.479206 11.00000 0.09441 0.05553 = 0.06553 0.00150 -0.00698 -0.01228 AFIX 43 H123 5 0.007885 0.611433 0.542159 11.00000 -1.20000 AFIX 0 C213 4 0.249923 0.806391 -0.338484 11.00000 0.07279 0.07462 = 0.06324 -0.01087 -0.00289 -0.01249 AFIX 43 H213 5 0.278580 0.868911 -0.396843 11.00000 -1.20000 AFIX 0 C216 4 0.163691 0.621804 -0.166771 11.00000 0.08363 0.05060 = 0.07146 -0.01923 0.00090 -0.00753 AFIX 43 H216 5 0.134600 0.558750 -0.109127 11.00000 -1.20000 AFIX 0 C112 4 0.357526 0.958240 0.225753 11.00000 0.05761 0.07662 = 0.06978 -0.02224 -0.00721 -0.01152 AFIX 43 H112 5 0.396889 0.923113 0.164407 11.00000 -1.20000 AFIX 0 C215 4 0.243919 0.589557 -0.259892 11.00000 0.09315 0.07111 = 0.08390 -0.03159 0.00087 0.00504 AFIX 43 H215 5 0.269472 0.505558 -0.264651 11.00000 -1.20000 AFIX 0 C114 4 0.387550 1.069010 0.375256 11.00000 0.07926 0.07258 = 0.08214 -0.01819 -0.02751 -0.02174 AFIX 43 H114 5 0.446544 1.108827 0.413504 11.00000 -1.20000 AFIX 0 C115 4 0.243340 1.062414 0.409709 11.00000 0.08892 0.06346 = 0.06425 -0.02241 -0.01543 -0.01648 AFIX 43 H115 5 0.205025 1.096533 0.471879 11.00000 -1.20000 AFIX 0 C225 4 -0.391504 0.665175 0.020522 11.00000 0.06096 0.06972 = 0.11096 -0.00753 0.00574 -0.02121 AFIX 43 H225 5 -0.458111 0.652985 0.081639 11.00000 -1.20000 AFIX 0 C223 4 -0.325122 0.658781 -0.173301 11.00000 0.09104 0.08038 = 0.08657 -0.00812 -0.03697 -0.02952 AFIX 43 H223 5 -0.347429 0.641535 -0.242843 11.00000 -1.20000 AFIX 0 C224 4 -0.422472 0.640114 -0.082605 11.00000 0.07085 0.07315 = 0.12900 0.00120 -0.02860 -0.02734 AFIX 43 H224 5 -0.510184 0.610219 -0.091139 11.00000 -1.20000 AFIX 0 C222 4 -0.194465 0.702907 -0.162193 11.00000 0.07226 0.06225 = 0.07160 -0.01203 -0.01381 -0.01896 AFIX 43 H222 5 -0.129511 0.716248 -0.224293 11.00000 -1.20000 AFIX 0 C214 4 0.285677 0.683774 -0.345847 11.00000 0.08255 0.09080 = 0.06456 -0.02932 0.00375 0.00050 AFIX 43 H214 5 0.338667 0.662938 -0.409181 11.00000 -1.20000 AFIX 0 C113 4 0.444212 1.016609 0.284174 11.00000 0.06374 0.08130 = 0.09207 -0.02117 -0.02226 -0.01580 AFIX 43 H113 5 0.541802 1.020545 0.261756 11.00000 -1.20000 AFIX 0 CL1S 3 0.430472 0.569087 0.385521 11.00000 0.07686 0.09597 = 0.09417 -0.01657 -0.00903 -0.01017 HKLF 4 REM CR11 REM wR2 = 0.1347, GooF = S = 0.957, Restrained GooF = 0.957 for all data REM R1 = 0.0537 for 3219 Fo > 4sig(Fo) and 0.0795 for all 4607 data REM 277 parameters refined using 0 restraints END WGHT 0.0392 0.0000 REM Highest difference peak 0.729, deepest hole -0.951, 1-sigma level 0.090 Q1 1 0.1504 0.9308 0.0061 11.00000 0.05 0.52 Q2 1 0.0527 0.8693 0.1977 11.00000 0.05 0.52 Q3 1 -0.0206 0.8927 0.1002 11.00000 0.05 0.51 Q4 1 0.1175 1.0642 -0.0551 11.00000 0.05 0.49 Q5 1 0.1000 1.0742 0.0360 11.00000 0.05 0.48 Q6 1 0.0656 1.0013 0.0957 11.00000 0.05 0.43 Q7 1 0.5034 0.5251 0.4617 11.00000 0.05 0.40 Q8 1 0.0539 1.1227 -0.0399 11.00000 0.05 0.36 Q9 1 0.0490 0.9128 -0.0835 11.00000 0.05 0.35 Q10 1 0.0733 1.1022 0.2233 11.00000 0.05 0.31 Q11 1 -0.1791 0.8976 0.2174 11.00000 0.05 0.30 Q12 1 0.2532 0.7987 -0.1006 11.00000 0.05 0.29 Q13 1 -0.1118 0.7361 -0.0862 11.00000 0.05 0.29 Q14 1 0.3444 0.6811 0.2029 11.00000 0.05 0.28 Q15 1 0.1796 0.5661 0.4347 11.00000 0.05 0.28 Q16 1 0.1218 0.7440 -0.1242 11.00000 0.05 0.27 Q17 1 -0.1984 0.7392 -0.1110 11.00000 0.05 0.26 Q18 1 -0.4427 0.6505 -0.3585 11.00000 0.05 0.26 Q19 1 0.2930 1.0529 0.4016 11.00000 0.05 0.26 Q20 1 0.2100 0.8888 -0.0737 11.00000 0.05 0.26 ; _shelx_res_checksum 53531 _shelx_hkl_file ; -11 -1 -3 42.2182 41.1484 1 -11 -1 -2 60.3656 40.0562 1 -11 -1 -1 89.3875 33.7825 1 -11 -1 0 54.8165 33.8312 1 -11 -1 1 69.5875 27.6431 1 -11 -1 2 29.248 29.4585 1 -11 -1 3 36.1771 36.3911 1 -11 0 -2-15.9839 38.3434 1 -11 0 -1 81.7573 39.8582 1 -11 0 0 71.6885 43.8618 1 -11 0 1-26.5898 36.3925 1 -11 0 2-0.69597 34.379 1 -11 0 3 44.9043 31.0329 1 -11 1 -1-0.09317 33.8502 1 -11 1 0 8.42036 33.9616 1 -11 1 1 28.2482 46.5755 1 -11 1 2 34.1656 40.4311 1 -11 1 3-13.2921 37.5269 1 -11 2 0 38.3177 44.3536 1 -11 2 1 78.0866 48.4488 1 -11 2 2 31.4612 55.666 1 -10 -3 6-5.41941 34.3128 1 -10 -2 -1 15.5073 30.0767 1 -10 -2 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2 3 -1 4.25874 4.81556 1 2 3 0 234.303 33.5382 1 2 3 1 1355.14 80.8199 1 2 3 2 443.639 26.7947 1 2 3 3 670.337 43.3544 1 2 3 4 11.1348 11.7744 1 2 3 5 47.0144 12.3082 1 2 3 6 1817.48 226.969 1 2 3 7 2283.19 329.66 1 2 3 8 1404.33 144.558 1 2 3 9 1128.58 87.9534 1 2 3 10 615.087 39.4477 1 2 3 11 1783.06 131.38 1 2 3 12 661.864 52.8466 1 2 3 13 164.734 34.8961 1 2 3 14 63.0199 21.60 1 2 4 -12 23.7642 23.3991 1 2 4 -11 81.1621 22.1866 1 2 4 -10 279.864 83.8168 1 2 4 -9 301.718 40.0955 1 2 4 -8 114.67 20.1227 1 2 4 -7 3.27321 18.0911 1 2 4 -6 8.52016 14.1228 1 2 4 -5 371.389 26.5138 1 2 4 -4 550.979 32.3114 1 2 4 -3 1631.16 84.5631 1 2 4 -2 889.675 51.5482 1 2 4 -1 435.709 33.5552 1 2 4 0 765.934 40.7206 1 2 4 1 201.946 26.8031 1 2 4 2 3413.51 365.662 1 2 4 3 4562.43 289.176 1 2 4 4 145.144 14.4537 1 2 4 5 1178.82 79.2392 1 2 4 6 932.849 65.6481 1 2 4 7 6105.55 650.683 1 2 4 8 2208.82 185.152 1 2 4 9-17.0172 18.7515 1 2 4 10 1181.97 106.552 1 2 4 11 536.434 61.3751 1 2 4 12 325.494 52.0704 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42.9656 1 3 -9 2 287.262 70.4976 1 3 -9 3 92.3339 15.4506 1 3 -9 4 136.544 21.3848 1 3 -9 5 31.0762 10.6201 1 3 -9 6 13.4772 11.1441 1 3 -9 7-46.2116 35.854 1 3 -9 8 21.7714 50.7687 1 3 -8 -12 27.8721 41.2535 1 3 -8 -11 39.8655 44.0224 1 3 -8 -10 81.3663 23.9734 1 3 -8 -9 48.8347 19.6565 1 3 -8 -8 295.207 35.5308 1 3 -8 -6 422.45 37.4505 1 3 -8 -5 696.43 90.7069 1 3 -8 -4 623.843 79.2343 1 3 -8 -3 230.467 29.843 1 3 -8 -2 640.666 100.992 1 3 -8 -1 971.595 109.045 1 3 -8 0 67.4767 16.4644 1 3 -8 1-1.64306 12.5372 1 3 -8 2 7.13218 11.6824 1 3 -8 3 71.2139 12.6312 1 3 -8 4 164.488 42.2282 1 3 -8 5-0.98393 30.4379 1 3 -8 6 71.6839 18.0151 1 3 -8 7 23.9228 15.2912 1 3 -8 8 0.17905 15.0449 1 3 -8 9 31.4195 38.0578 1 3 -7 -12-49.8088 45.9358 1 3 -7 -11 164.937 63.5042 1 3 -7 -10 179.685 37.8214 1 3 -7 -9 122.093 19.9856 1 3 -7 -8 250.615 43.1973 1 3 -7 -7 228.929 26.0423 1 3 -7 -5 1057.99 132.273 1 3 -7 -4 211.657 30.0816 1 3 -7 -3 173.685 49.4896 1 3 -7 -2 31.2686 25.5082 1 3 -7 -1 426.578 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3393.11 206.047 1 3 2 4 694.209 119.251 1 3 2 5 408.619 38.154 1 3 2 6 286.944 28.0088 1 3 2 7 8.82356 8.4627 1 3 2 8 657.35 54.6315 1 3 2 9 73.3251 20.7389 1 3 2 10 341.318 45.0163 1 3 2 11 112.582 24.2607 1 3 2 12 349.736 41.4006 1 3 2 13 116.427 19.9614 1 3 2 14 49.6593 37.9991 1 3 3 -13 13.6478 33.1241 1 3 3 -12 41.8182 29.5634 1 3 3 -11 126.258 79.3093 1 3 3 -10 420.218 49.603 1 3 3 -9 294.207 72.448 1 3 3 -8 212.727 24.9651 1 3 3 -7 54.5509 20.7981 1 3 3 -6 1155.55 150.445 1 3 3 -5 3653.48 271.945 1 3 3 -4 2423.01 165.097 1 3 3 -3 1133.24 81.5356 1 3 3 -2 0.1086 4.75146 1 3 3 -1 28.9437 6.13084 1 3 3 0 799.521 43.2422 1 3 3 1 16.1046 7.21779 1 3 3 2 103.71 16.625 1 3 3 3 1040.14 100.91 1 3 3 4 701.028 59.1578 1 3 3 5 1127.69 119.155 1 3 3 6 423.672 36.3718 1 3 3 7 512.164 76.6014 1 3 3 8 239.985 31.9329 1 3 3 9 445.87 51.9085 1 3 3 10 1267.86 108.538 1 3 3 11 224.155 57.4687 1 3 3 12 352.869 45.9325 1 3 3 13 196.374 21.4415 1 3 3 14 18.6623 29.8113 1 3 4 -12-2.21924 27.277 1 3 4 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755.466 1 3 5 3 1104.91 75.1069 1 3 5 4 13.2919 20.2433 1 3 5 5 437.081 34.1148 1 3 5 6 204.521 18.4364 1 3 5 7 841.042 71.2792 1 3 5 8 50.4962 17.8999 1 3 5 9 48.6024 42.2934 1 3 5 10 29.1519 14.3132 1 3 5 11 3.81031 9.70024 1 3 5 12 102.973 23.4248 1 3 5 13 162.784 20.2293 1 3 5 14 32.3753 31.2321 1 3 6 -11-9.43303 32.5429 1 3 6 -10 118.465 48.6834 1 3 6 -9 357.393 45.1237 1 3 6 -8 425.702 48.3401 1 3 6 -7 1073.89 149.095 1 3 6 -6 408.75 31.9997 1 3 6 -5 1248.27 87.8327 1 3 6 -4 2792.92 249.341 1 3 6 -3 1000.55 67.4649 1 3 6 -2 3818.25 260.46 1 3 6 -1 745.425 39.4836 1 3 6 0 141.801 11.3653 1 3 6 1 650.58 38.8057 1 3 6 2 23.9801 8.09501 1 3 6 3 45.9578 16.3777 1 3 6 4 163.362 23.6127 1 3 6 5 320.569 28.0197 1 3 6 6 176.267 46.8533 1 3 6 7 15.7144 13.6533 1 3 6 8 22.3994 15.932 1 3 6 9 95.6407 26.206 1 3 6 10 6.73816 16.8302 1 3 6 11 41.9793 15.2381 1 3 6 12 109.492 25.7045 1 3 6 13 136.132 26.2728 1 3 6 14 270.78 61.2042 1 3 7 -10 41.6571 24.1719 1 3 7 -9 263.513 72.3072 1 3 7 -8 687.876 208.988 1 3 7 -7 488.537 49.9094 1 3 7 -6 238.435 43.058 1 3 7 -5 119.18 13.8148 1 3 7 -4 284.937 25.7413 1 3 7 -3 772.709 97.4617 1 3 7 -2 276.71 35.2271 1 3 7 -1 650.749 34.4997 1 3 7 0 928.094 70.0978 1 3 7 1 338.491 38.5548 1 3 7 2 777.594 129.805 1 3 7 3 123.551 17.0063 1 3 7 4 124.182 15.3165 1 3 7 5 148.295 37.0558 1 3 7 6 667.57 108.121 1 3 7 7 153.988 19.8414 1 3 7 8 7.31634 11.2002 1 3 7 9 764.271 71.2839 1 3 7 10 756.762 61.2035 1 3 7 11 42.705 17.0582 1 3 7 12 121.378 20.4053 1 3 7 13 139.331 103.211 1 3 8 -9-7.77856 27.2097 1 3 8 -8 196.861 39.5509 1 3 8 -7 167.968 31.8303 1 3 8 -6 3.98983 12.0678 1 3 8 -5 131.171 19.4368 1 3 8 -4 16.4278 10.5118 1 3 8 -3 93.7759 11.9802 1 3 8 -2 608.005 38.3831 1 3 8 -1-0.37568 11.9094 1 3 8 0 37.1449 8.71532 1 3 8 1 21.7425 16.9813 1 3 8 2 320.323 22.5353 1 3 8 3 990.735 164.02 1 3 8 4 514.699 39.77 1 3 8 5 411.724 66.5536 1 3 8 6 208.255 24.2429 1 3 8 7 132.304 19.4378 1 3 8 8 487.621 57.4303 1 3 8 9 911.694 92.7874 1 3 8 10 645.865 124.251 1 3 8 11 65.962 16.7002 1 3 8 12 21.654 19.1103 1 3 8 13 23.3752 37.4296 1 3 9 -8 8.1006 41.8168 1 3 9 -7 154.692 41.4773 1 3 9 -6 201.757 46.098 1 3 9 -5 70.9421 13.7287 1 3 9 -4 69.6279 12.5985 1 3 9 -3 66.531 11.3091 1 3 9 -2 230.637 36.4425 1 3 9 -1 1275.14 172.761 1 3 9 0 657.748 63.6208 1 3 9 1 317.626 28.9251 1 3 9 2 2.142 10.2393 1 3 9 3 150.401 16.1508 1 3 9 4 1210.72 99.2886 1 3 9 5 814.082 98.6867 1 3 9 6 667.458 56.949 1 3 9 7 119.069 16.952 1 3 9 8 24.7743 17.2598 1 3 9 9 276.745 31.8787 1 3 9 10 89.215 21.6825 1 3 9 11 135.748 36.37 1 3 9 12 42.2622 49.443 1 3 10 -7 93.0944 70.3828 1 3 10 -6 215.721 62.545 1 3 10 -5 312.874 68.5749 1 3 10 -4 139.567 22.5997 1 3 10 -3 192.677 28.3492 1 3 10 -2 416.953 39.1427 1 3 10 -1 1108.12 132.934 1 3 10 0 732.862 81.7448 1 3 10 1 103.327 19.2984 1 3 10 2 0.4329 13.3228 1 3 10 3 7.79823 12.8287 1 3 10 4 65.8597 23.1547 1 3 10 5 44.2832 22.1685 1 3 10 6 1.16708 29.3202 1 3 10 7 44.25 33.3277 1 3 10 8 24.5656 34.9145 1 3 10 9 7.96097 42.376 1 3 10 10 74.637 51.3084 1 3 10 11 173.728 53.4746 1 3 11 -5 267.798 49.9306 1 3 11 -4 323.647 160.116 1 3 11 -3 47.2984 21.4737 1 3 11 -2 12.099 20.7236 1 3 11 -1 76.4378 42.5849 1 3 11 0 72.9424 42.1926 1 3 11 1 171.862 21.3932 1 3 11 2 10.9672 16.7902 1 3 11 3 78.2138 24.4883 1 3 11 4-16.1327 23.8632 1 3 11 5 2.81766 17.3935 1 3 11 6 26.3283 22.5975 1 3 11 7 45.0868 25.7237 1 3 11 8 44.0257 30.0197 1 3 11 9-0.55136 35.0479 1 3 11 10-1.08129 33.1935 1 3 12 -3 10.4564 26.2072 1 3 12 -2 17.4948 19.5679 1 3 12 -1 10.3245 21.1404 1 3 12 0-2.68784 27.0304 1 3 12 1 24.906 26.5259 1 3 12 2-2.39705 28.3718 1 3 12 3-6.87106 29.0811 1 3 12 4 4.09539 24.3597 1 3 12 5 150.801 29.7015 1 3 12 6 163.347 49.5496 1 3 12 7 183.669 64.546 1 3 12 8 28.1742 45.4069 1 3 12 9-18.4835 41.6907 1 3 13 -1 14.7065 23.2962 1 3 13 0-2.77277 32.9555 1 3 13 1 100.904 46.766 1 3 13 2 61.3685 37.561 1 3 13 3 98.5738 61.5399 1 3 13 4-43.9332 37.2771 1 3 13 5 5.72275 22.8024 1 3 13 6 97.4514 88.5989 1 4 -12 -4 34.1162 45.806 1 4 -12 -3-8.87331 35.5909 1 4 -12 -2 11.761 29.6118 1 4 -12 -1 -20.76 29.9663 1 4 -11 -7-5.31939 60.3107 1 4 -11 -6 15.7373 21.299 1 4 -11 -5 5.94936 15.4724 1 4 -11 -4 7.3398 16.578 1 4 -11 -3 21.8019 11.9076 1 4 -11 -2-0.37169 25.4066 1 4 -11 -1 17.8211 16.3528 1 4 -11 0-43.2773 86.7512 1 4 -11 1 67.2453 24.865 1 4 -10 -9 13.1316 19.8511 1 4 -10 -8 13.5945 31.6713 1 4 -10 -7 -11.921 25.8202 1 4 -10 -6 35.0163 27.8288 1 4 -10 -5 -9.696 22.4546 1 4 -10 -4 12.1563 20.0905 1 4 -10 -3 169.948 39.9426 1 4 -10 -2 147.737 27.5563 1 4 -10 -1 55.6901 21.0862 1 4 -10 0 147.434 44.6863 1 4 -10 1 223.669 133.666 1 4 -10 2 313.046 122.189 1 4 -10 3 378.841 52.9947 1 4 -10 4 86.0033 45.7536 1 4 -9 -10 14.4097 21.0625 1 4 -9 -9 31.3802 19.9786 1 4 -9 -8 16.6844 22.4822 1 4 -9 -7 58.2222 27.6243 1 4 -9 -6 59.6359 17.5112 1 4 -9 -5 32.0368 32.3064 1 4 -9 -4 145.546 31.2498 1 4 -9 -3 203.941 32.5933 1 4 -9 -2 801.417 202.184 1 4 -9 -1 710.094 71.2502 1 4 -9 0 184.028 81.3012 1 4 -9 1 229.735 136.847 1 4 -9 2 97.9751 32.0542 1 4 -9 3 168.816 60.4547 1 4 -9 4 235.968 24.7051 1 4 -9 5 14.9203 19.1177 1 4 -9 6 46.9415 15.7406 1 4 -9 7 31.638 19.6269 1 4 -8 -11 40.4783 38.8367 1 4 -8 -10 11.8801 19.5114 1 4 -8 -9 38.6157 14.3489 1 4 -8 -8 300.024 28.7132 1 4 -8 -7 162.577 35.104 1 4 -8 -6 183.295 45.094 1 4 -8 -5 39.6148 22.5699 1 4 -8 -4 71.3322 34.4349 1 4 -8 -3 504.185 66.5636 1 4 -8 -2 509.481 85.4281 1 4 -8 -1 888.124 106.84 1 4 -8 0 211.425 55.2761 1 4 -8 1 60.1008 19.4969 1 4 -8 2 283.027 82.9676 1 4 -8 3 164.985 38.0467 1 4 -8 4 252.018 46.9587 1 4 -8 5 79.3691 15.869 1 4 -8 6 67.6384 24.7166 1 4 -8 7-2.14961 43.0822 1 4 -8 8 11.5803 17.9844 1 4 -7 -12 7.40603 41.9782 1 4 -7 -11 12.1685 24.4539 1 4 -7 -10 56.3209 29.7174 1 4 -7 -9 7.35773 14.9275 1 4 -7 -8 48.9376 17.0557 1 4 -7 -7 56.3773 18.5407 1 4 -7 -6 41.4137 27.0875 1 4 -7 -5 611.946 83.149 1 4 -7 -4 79.0912 27.6652 1 4 -7 -3 1.4609 20.1572 1 4 -7 -2 252.048 28.0702 1 4 -7 -1 164.349 20.4336 1 4 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72.1331 27.7459 1 4 -5 -5 108.867 28.6634 1 4 -5 -4 485.904 63.3772 1 4 -5 -3 721.58 92.1975 1 4 -5 -2 1093.63 123.24 1 4 -5 -1 1688.52 211.507 1 4 -5 0 4258.46 482.159 1 4 -5 1 2409.71 283.893 1 4 -5 2 724.333 45.7046 1 4 -5 3 1075.77 85.2497 1 4 -5 4 405.492 46.7991 1 4 -5 5 935.486 81.1641 1 4 -5 6 582.013 84.5576 1 4 -5 7 102.348 19.9273 1 4 -5 8 17.8518 13.648 1 4 -5 9 23.1889 14.9264 1 4 -5 10-6.54892 28.6529 1 4 -5 11 68.2198 23.9556 1 4 -4 -12 9.63565 29.195 1 4 -4 -11 14.5411 25.9562 1 4 -4 -10 44.8297 27.2475 1 4 -4 -9 82.2825 31.358 1 4 -4 -8 1.62469 20.6113 1 4 -4 -7 97.539 25.1069 1 4 -4 -6 798.806 114.813 1 4 -4 -5 1270.10 186.461 1 4 -4 -3 1844.74 238.239 1 4 -4 -2 285.80 34.4889 1 4 -4 -1 1572.85 137.448 1 4 -4 0 994.965 88.8325 1 4 -4 1 6144.56 551.073 1 4 -4 2 3646.01 290.043 1 4 -4 3 130.301 15.1456 1 4 -4 4 573.203 52.5629 1 4 -4 5 166.116 31.415 1 4 -4 6 257.627 47.462 1 4 -4 7 521.136 73.6408 1 4 -4 8 9.37648 19.2083 1 4 -4 9 20.8255 22.149 1 4 -4 10-1.36004 31.1617 1 4 -4 11-8.93065 60.2912 1 4 -4 12 3.61193 22.7688 1 4 -3 -12-22.7819 27.8932 1 4 -3 -11 23.3592 34.0514 1 4 -3 -10 185.268 34.7664 1 4 -3 -9 17.1274 19.209 1 4 -3 -8 288.778 57.434 1 4 -3 -7 179.28 35.7801 1 4 -3 -6 62.5568 36.5279 1 4 -3 -5 1333.08 216.135 1 4 -3 -4 1119.04 146.037 1 4 -3 -3 2392.16 296.696 1 4 -3 -2 1154.95 174.854 1 4 -3 -1 185.657 20.1957 1 4 -3 0 1945.10 237.759 1 4 -3 1 2756.58 174.575 1 4 -3 2 1620.55 115.47 1 4 -3 3 426.034 40.0127 1 4 -3 4 58.4659 8.92484 1 4 -3 5 492.093 53.6649 1 4 -3 6 23.426 12.5192 1 4 -3 7 174.318 30.2894 1 4 -3 8 293.391 41.1737 1 4 -3 9 32.1029 19.3426 1 4 -3 10-10.1844 33.2036 1 4 -3 11-1.52219 33.2127 1 4 -3 12 8.86323 19.8701 1 4 -2 -13 24.0127 47.6481 1 4 -2 -12 62.9658 28.1769 1 4 -2 -11 27.0436 32.6914 1 4 -2 -10 12.8636 27.8753 1 4 -2 -9 439.628 76.1317 1 4 -2 -8 73.9209 17.282 1 4 -2 -7 333.62 53.3475 1 4 -2 -6 121.077 29.5107 1 4 -2 -5 31.5369 13.7663 1 4 -2 -4 2648.71 368.969 1 4 -2 -3 315.108 41.1906 1 4 -2 -2 2840.98 229.986 1 4 -2 -1 1193.68 85.9036 1 4 -2 0 8.28054 10.8578 1 4 -2 1 5477.29 347.441 1 4 -2 2 1060.15 61.695 1 4 -2 3 966.50 65.801 1 4 -2 4 1047.17 62.5129 1 4 -2 5 19.1536 11.6779 1 4 -2 6 52.8361 15.6287 1 4 -2 7 684.696 69.7895 1 4 -2 8 380.336 50.4718 1 4 -2 9 161.499 23.7601 1 4 -2 10-14.3531 30.9342 1 4 -2 11 49.0168 19.9259 1 4 -2 12 128.201 24.7258 1 4 -2 13 80.7446 23.3975 1 4 -1 -13 5.70255 36.3936 1 4 -1 -12 -13.444 33.4189 1 4 -1 -11 7.73342 28.635 1 4 -1 -10 25.5091 21.7026 1 4 -1 -9 18.8151 20.2709 1 4 -1 -8 393.417 37.7366 1 4 -1 -7 117.282 15.0653 1 4 -1 -6 118.831 22.9471 1 4 -1 -5 37.488 17.9468 1 4 -1 -4 38.112 15.3595 1 4 -1 -3 2499.58 201.845 1 4 -1 -2 2262.42 162.637 1 4 -1 -1 2959.14 222.762 1 4 -1 0 664.463 47.8898 1 4 -1 1 1127.39 57.4707 1 4 -1 2 2883.97 161.692 1 4 -1 3 1729.84 97.1002 1 4 -1 4 3406.64 304.893 1 4 -1 5 1364.57 103.956 1 4 -1 6 104.177 14.0577 1 4 -1 7 1797.21 149.969 1 4 -1 8 602.577 68.252 1 4 -1 9 131.909 22.9804 1 4 -1 10 143.239 22.6635 1 4 -1 11 4.80174 23.2214 1 4 -1 12 111.349 20.8088 1 4 -1 13 2.40024 22.3806 1 4 0 -13-6.67634 51.7109 1 4 0 -12 33.4527 31.88 1 4 0 -11-36.8306 38.7993 1 4 0 -10 4.89882 26.533 1 4 0 -9 8.34205 21.431 1 4 0 -8 57.7006 19.4048 1 4 0 -7 739.369 63.2591 1 4 0 -6 76.9368 25.8236 1 4 0 -5 450.371 55.3594 1 4 0 -4 533.779 76.1255 1 4 0 -3 2480.68 152.976 1 4 0 -2 9843.93 579.293 1 4 0 -1 863.779 46.6988 1 4 0 0 4252.56 273.364 1 4 0 1 2031.52 104.398 1 4 0 2 1615.34 82.7173 1 4 0 311485.50 450.486 1 4 0 4 5830.52 460.403 1 4 0 5 149.938 14.3647 1 4 0 6 259.078 29.5341 1 4 0 7 120.535 15.6517 1 4 0 8 420.398 56.3844 1 4 0 9 378.759 82.8301 1 4 0 10 0.02258 16.751 1 4 0 11 25.5707 22.3334 1 4 0 12 24.1093 17.558 1 4 0 13 2.60725 19.6966 1 4 1 -13 8.66464 36.5127 1 4 1 -12 22.6207 37.5931 1 4 1 -11 45.4096 40.0408 1 4 1 -10 48.8863 20.5605 1 4 1 -9 9.32158 24.7912 1 4 1 -8-7.72653 12.9392 1 4 1 -7 655.257 45.7015 1 4 1 -6 1731.42 134.099 1 4 1 -5 601.204 40.5754 1 4 1 -4 787.668 64.7507 1 4 1 -3 4797.63 433.557 1 4 1 -2 6832.48 617.739 1 4 1 -1 7305.63 488.677 1 4 1 0 5807.30 343.146 1 4 1 1 4421.21 259.525 1 4 1 2 6749.91 396.638 1 4 1 3 2025.86 154.947 1 4 1 4 1062.80 61.7957 1 4 1 5 298.285 28.362 1 4 1 6 241.217 30.1953 1 4 1 7 39.0891 13.0917 1 4 1 8 19.4606 11.8262 1 4 1 9 66.603 13.2245 1 4 1 10 54.3911 13.9903 1 4 1 11 5.45634 18.1261 1 4 1 12 18.332 17.028 1 4 1 13 5.78212 18.8542 1 4 1 14 29.9133 24.4287 1 4 2 -13 15.5828 41.8425 1 4 2 -12 40.7104 35.0736 1 4 2 -11 35.6794 30.6977 1 4 2 -10 187.083 25.7329 1 4 2 -9 7.13577 13.5406 1 4 2 -8 79.59 28.5373 1 4 2 -7 2877.07 297.158 1 4 2 -6 1147.60 90.9924 1 4 2 -5 1196.32 86.9667 1 4 2 -4 234.731 14.1367 1 4 2 -3 172.732 11.1054 1 4 2 -2 5044.00 355.748 1 4 2 -1 1737.69 118.398 1 4 2 0 1951.41 108.63 1 4 2 1 1926.58 99.4171 1 4 2 2 829.364 58.6814 1 4 2 3 85.9672 13.2389 1 4 2 4 1726.00 122.655 1 4 2 5 2291.97 187.96 1 4 2 6 175.125 20.3412 1 4 2 7 59.1021 13.9396 1 4 2 8 16.9602 15.9475 1 4 2 9 6.6953 12.1696 1 4 2 10 84.9755 28.6101 1 4 2 11 221.103 27.3656 1 4 2 12 80.7146 20.7005 1 4 2 13 2.33602 17.9137 1 4 2 14 75.87 27.4575 1 4 3 -12 0.42802 20.7937 1 4 3 -11 98.494 34.0918 1 4 3 -10 30.8049 28.7157 1 4 3 -9 26.1573 14.3584 1 4 3 -8 28.125 14.5993 1 4 3 -7 138.872 24.3071 1 4 3 -6 841.012 61.8764 1 4 3 -5 410.554 31.1625 1 4 3 -4 231.635 16.6573 1 4 3 -3 232.88 26.1367 1 4 3 -2 667.403 39.2721 1 4 3 -1 1623.64 82.1249 1 4 3 0 356.899 20.4691 1 4 3 1 1546.93 85.8877 1 4 3 2 543.116 34.3156 1 4 3 3 273.795 28.0896 1 4 3 4 4271.56 307.319 1 4 3 5 682.416 51.192 1 4 3 6 781.21 62.4906 1 4 3 7 987.196 77.8919 1 4 3 8 6.25444 13.8176 1 4 3 9 546.531 49.5482 1 4 3 10 216.779 27.9126 1 4 3 11 123.438 24.8937 1 4 3 12 208.618 44.2643 1 4 3 13-26.6959 35.6046 1 4 3 14 2.83822 27.9374 1 4 4 -12 2.14533 27.7828 1 4 4 -11 13.8888 29.1894 1 4 4 -10 89.9756 68.9618 1 4 4 -9 70.5139 20.1302 1 4 4 -8 7.49692 14.773 1 4 4 -7 70.6445 27.3756 1 4 4 -6 36.723 14.9925 1 4 4 -5 1687.09 156.843 1 4 4 -4 149.335 10.3892 1 4 4 -3 2021.17 115.63 1 4 4 -2 841.701 54.5001 1 4 4 -1 186.425 11.3288 1 4 4 0 9781.21 548.822 1 4 4 2 5143.18 341.255 1 4 4 3 2367.22 188.342 1 4 4 4 255.847 23.6615 1 4 4 5 2518.43 226.919 1 4 4 6 1270.22 102.436 1 4 4 7 1145.28 121.563 1 4 4 8 780.027 67.4869 1 4 4 9 95.4534 22.4991 1 4 4 10 19.3889 14.239 1 4 4 11 80.916 21.5316 1 4 4 12 92.9957 26.2591 1 4 4 13 35.9581 14.3014 1 4 4 14-80.6549 151.557 1 4 5 -11 28.1444 23.2632 1 4 5 -10 26.4072 38.3978 1 4 5 -9 48.5114 18.0587 1 4 5 -8-9.54566 19.9931 1 4 5 -7 58.2613 18.093 1 4 5 -6 136.282 27.899 1 4 5 -5 1078.54 75.8991 1 4 5 -4 2365.00 153.757 1 4 5 -3 844.041 46.6854 1 4 5 -2 1616.94 116.958 1 4 5 -1 2038.95 135.928 1 4 5 0 2484.80 153.242 1 4 5 1 6506.83 428.143 1 4 5 2 1205.53 85.9079 1 4 5 3 2445.65 189.173 1 4 5 4 2561.07 208.003 1 4 5 5 35.6422 11.0845 1 4 5 6 1145.55 88.7345 1 4 5 7 273.86 21.9283 1 4 5 8-2.88347 19.5392 1 4 5 9 10.851 14.5253 1 4 5 10 165.862 21.6496 1 4 5 11 13.9351 14.2958 1 4 5 12 67.3236 15.583 1 4 5 13 24.872 15.6061 1 4 5 14-22.6286 33.6063 1 4 6 -11 13.059 24.5099 1 4 6 -10 32.8966 22.2629 1 4 6 -9 208.958 48.2111 1 4 6 -8 194.151 47.401 1 4 6 -7 102.542 19.9003 1 4 6 -6 575.817 120.37 1 4 6 -5 947.09 72.5917 1 4 6 -4 1401.70 111.422 1 4 6 -3 3649.70 269.164 1 4 6 -2 1826.35 142.258 1 4 6 -1 1145.53 92.1204 1 4 6 0 624.151 37.3203 1 4 6 1 453.19 34.0329 1 4 6 2 1790.73 148.956 1 4 6 3 349.443 66.6522 1 4 6 4 52.5561 18.4871 1 4 6 5 214.831 20.5529 1 4 6 6 3.6931 11.7336 1 4 6 7 137.889 18.5724 1 4 6 8 27.4487 18.4435 1 4 6 9 26.8527 13.6011 1 4 6 10 45.0741 17.7756 1 4 6 11 28.6746 16.3806 1 4 6 12 6.07098 15.0407 1 4 6 13 105.313 31.2112 1 4 7 -10 22.8677 48.9495 1 4 7 -9 81.1723 52.2825 1 4 7 -8 135.213 61.314 1 4 7 -7 147.379 22.6033 1 4 7 -6 167.976 23.9854 1 4 7 -5 188.391 23.4509 1 4 7 -4 471.61 38.2828 1 4 7 -3 987.418 70.5784 1 4 7 -2 1171.22 88.7385 1 4 7 -1 523.349 29.4758 1 4 7 0 257.662 33.794 1 4 7 1 892.001 77.9031 1 4 7 2 484.671 34.3363 1 4 7 3 448.554 41.3373 1 4 7 4 29.2083 20.8201 1 4 7 5 6.0515 13.6281 1 4 7 6 58.8862 26.2148 1 4 7 7 402.138 36.5532 1 4 7 8 625.524 62.0897 1 4 7 9 212.461 29.4569 1 4 7 10-6.52423 25.9786 1 4 7 11 119.62 32.042 1 4 7 12 45.6435 15.1894 1 4 7 13 94.8058 43.2066 1 4 8 -9 25.6469 26.47 1 4 8 -8 83.0736 28.6189 1 4 8 -7 38.3876 25.7897 1 4 8 -6 11.1611 11.722 1 4 8 -5 0.33507 11.7236 1 4 8 -4 12.8228 10.2536 1 4 8 -3 231.376 40.5456 1 4 8 -2 373.821 21.6526 1 4 8 -1 494.658 29.8181 1 4 8 0 19.2936 10.2111 1 4 8 1 104.032 12.7452 1 4 8 2 1301.87 97.2278 1 4 8 3 1294.51 106.502 1 4 8 4 2041.82 303.235 1 4 8 5 843.164 72.0006 1 4 8 6 67.286 24.444 1 4 8 7 283.29 30.5176 1 4 8 8 345.404 35.1548 1 4 8 9 323.468 35.7241 1 4 8 10 473.201 68.9509 1 4 8 11-39.0916 74.118 1 4 8 12-10.4047 29.9337 1 4 8 13 47.1795 30.1754 1 4 9 -8 19.5022 34.8995 1 4 9 -7 79.1268 63.9883 1 4 9 -6 31.6763 13.5814 1 4 9 -5 101.331 18.1552 1 4 9 -4 123.839 15.7967 1 4 9 -3 285.461 23.0149 1 4 9 -2 1630.72 150.809 1 4 9 -1 564.032 60.1622 1 4 9 0 510.887 30.8096 1 4 9 1 737.111 43.2165 1 4 9 2 269.483 23.8897 1 4 9 3 1502.26 119.059 1 4 9 4 1089.13 89.3851 1 4 9 5 250.667 35.977 1 4 9 6 142.473 36.4734 1 4 9 7 11.4758 30.6553 1 4 9 8 106.62 20.4205 1 4 9 9 234.423 65.3038 1 4 9 10 51.2699 27.7704 1 4 9 11 7.10088 17.5976 1 4 9 12 3.81876 25.8832 1 4 10 -7 70.9133 67.7537 1 4 10 -6 366.142 80.4222 1 4 10 -5 125.427 21.5853 1 4 10 -4 349.329 43.6566 1 4 10 -3 315.629 53.0832 1 4 10 -2 572.068 80.1374 1 4 10 -1 2230.60 271.019 1 4 10 0 1103.34 65.1908 1 4 10 1 632.716 40.2747 1 4 10 2 81.5826 20.2353 1 4 10 3 36.0289 16.5296 1 4 10 4 483.023 56.5457 1 4 10 5 63.0242 16.148 1 4 10 6 28.2746 29.8238 1 4 10 7 15.0282 20.6936 1 4 10 8 36.4756 21.1729 1 4 10 9 43.0727 34.5659 1 4 10 10 2.38688 16.8245 1 4 10 11 3.08328 21.4618 1 4 11 -5 119.08 36.5771 1 4 11 -4 37.2159 27.8952 1 4 11 -3 29.5489 31.1675 1 4 11 -2 48.3682 35.2368 1 4 11 -1 332.475 61.6905 1 4 11 0 577.925 93.16 1 4 11 1 75.3351 15.4155 1 4 11 2 13.966 18.2836 1 4 11 3 27.1635 19.6418 1 4 11 4 41.3919 16.0826 1 4 11 5 176.737 62.0239 1 4 11 6 9.38016 41.4618 1 4 11 7 11.5119 14.2045 1 4 11 8 5.16225 15.7375 1 4 11 9 15.4449 26.5852 1 4 11 10 89.1914 23.6782 1 4 12 -3 2.01183 31.311 1 4 12 -2-2.27431 38.2245 1 4 12 -1 38.0512 28.3911 1 4 12 0 67.8897 30.2076 1 4 12 1 92.8631 27.9435 1 4 12 2-3.29118 26.7486 1 4 12 3-4.73082 32.6717 1 4 12 4 10.664 20.4882 1 4 12 5-7.59157 23.7757 1 4 12 6 47.9073 25.4782 1 4 12 7 55.9114 32.2226 1 4 12 8 20.3733 29.8013 1 4 13 0 97.1715 66.5708 1 4 13 1 136.771 59.3953 1 4 13 2 82.8724 42.0279 1 4 13 3 72.7778 55.0552 1 4 13 4 7.83966 39.5541 1 4 13 5 28.7906 38.7872 1 4 13 6 34.2378 38.162 1 5 -11 -5-1.65272 23.371 1 5 -11 -4 30.5807 24.0926 1 5 -11 -3 -6.6386 56.7446 1 5 -11 -2-0.09154 28.3837 1 5 -11 -1 3.70032 43.6895 1 5 -11 0 27.7412 38.8102 1 5 -11 1-22.5914 36.7566 1 5 -10 -8 24.7166 30.8491 1 5 -10 -7-23.2423 36.9288 1 5 -10 -6 6.99697 26.5917 1 5 -10 -5-14.9863 45.7482 1 5 -10 -4 39.8246 25.0152 1 5 -10 -3 35.5055 19.1689 1 5 -10 -2 23.0406 25.5952 1 5 -10 -1 3.9472 16.255 1 5 -10 0-9.20039 29.6068 1 5 -10 1 102.27 81.6987 1 5 -10 2 124.296 94.9537 1 5 -10 3 63.4702 70.5683 1 5 -9 -9 8.22694 19.136 1 5 -9 -8 68.5434 22.457 1 5 -9 -7-2.60102 24.194 1 5 -9 -6 56.9645 43.7686 1 5 -9 -5 47.6147 26.1249 1 5 -9 -4 1.25403 32.2677 1 5 -9 -3 120.045 42.3718 1 5 -9 -2 286.638 90.0544 1 5 -9 -1-6.13329 21.0785 1 5 -9 0 69.6281 53.3506 1 5 -9 1 48.6531 40.9126 1 5 -9 2 102.663 36.8119 1 5 -9 3 154.295 64.2085 1 5 -9 4 71.9642 24.5705 1 5 -9 5 38.8831 17.5474 1 5 -9 6 12.3641 19.4232 1 5 -8 -10 21.8401 18.5862 1 5 -8 -9 66.5683 55.5201 1 5 -8 -8 89.4181 22.9033 1 5 -8 -7 27.8402 79.6556 1 5 -8 -6 63.8227 34.7583 1 5 -8 -5-5.40603 32.9857 1 5 -8 -4 39.4664 34.8722 1 5 -8 -3 97.1414 30.3722 1 5 -8 -2 353.676 61.1086 1 5 -8 -1 269.85 40.74 1 5 -8 0 0.85675 12.626 1 5 -8 1 62.51 18.4023 1 5 -8 2 21.4064 36.3298 1 5 -8 3 146.08 51.1087 1 5 -8 4 106.325 18.6225 1 5 -8 5 13.2387 13.0942 1 5 -8 6 23.6196 13.2396 1 5 -8 7 7.26816 20.4376 1 5 -7 -11 -20.638 37.6478 1 5 -7 -10-0.42556 21.3374 1 5 -7 -9 18.832 17.8672 1 5 -7 -8 32.575 30.9494 1 5 -7 -7 91.989 39.2938 1 5 -7 -6 25.186 21.8635 1 5 -7 -5-11.5507 31.744 1 5 -7 -4-0.37128 26.9997 1 5 -7 -3 1.14807 22.9183 1 5 -7 -2 31.218 33.1601 1 5 -7 -1 81.5318 16.3014 1 5 -7 0 4.63761 18.6017 1 5 -7 1 49.1954 17.494 1 5 -7 2 134.211 76.0138 1 5 -7 3 192.694 33.6721 1 5 -7 4 280.618 50.3317 1 5 -7 5 171.514 28.3298 1 5 -7 6 -2.1566 28.018 1 5 -7 7 61.0644 15.7015 1 5 -7 8 55.3952 21.3004 1 5 -6 -11 45.7754 31.2052 1 5 -6 -10 20.5538 15.5143 1 5 -6 -9 6.00442 16.7777 1 5 -6 -8-16.9892 40.6402 1 5 -6 -7 64.9895 33.0695 1 5 -6 -6-40.3804 51.6006 1 5 -6 -5 144.522 49.9884 1 5 -6 -4 2.74528 19.4086 1 5 -6 -3 513.186 72.8911 1 5 -6 -2 147.531 25.2522 1 5 -6 -1 125.741 24.3104 1 5 -6 0 261.406 24.5616 1 5 -6 1 69.1464 11.5035 1 5 -6 2-18.1904 37.0249 1 5 -6 3 660.026 88.5142 1 5 -6 4 559.315 50.9254 1 5 -6 5 220.746 42.6927 1 5 -6 6 578.473 75.2318 1 5 -6 7 176.867 28.9845 1 5 -6 8 72.1926 24.3571 1 5 -6 9 122.289 33.0588 1 5 -5 -11 27.0897 23.5597 1 5 -5 -10-17.0183 29.2269 1 5 -5 -9 13.9784 14.9539 1 5 -5 -8 5.77751 22.4933 1 5 -5 -7 13.0461 24.7122 1 5 -5 -6 79.2616 36.1559 1 5 -5 -5-10.5724 24.2262 1 5 -5 -4-5.05168 27.6247 1 5 -5 -3 45.828 22.4558 1 5 -5 -2 65.2434 21.2405 1 5 -5 -1 1157.59 159.477 1 5 -5 0 1162.03 119.188 1 5 -5 1 405.801 30.9376 1 5 -5 2 33.4138 10.6123 1 5 -5 3 399.395 35.1753 1 5 -5 4 1097.30 88.0518 1 5 -5 5 905.598 74.8953 1 5 -5 6 720.371 75.2005 1 5 -5 7 516.729 73.2586 1 5 -5 8 3.53443 11.2367 1 5 -5 9 94.1868 19.1506 1 5 -5 10 126.785 31.1255 1 5 -4 -12 27.3241 34.804 1 5 -4 -11-1.96501 27.7388 1 5 -4 -10 95.0039 33.886 1 5 -4 -9 74.3802 32.8298 1 5 -4 -8 12.2964 23.644 1 5 -4 -7 26.9005 37.5431 1 5 -4 -6 95.4204 34.177 1 5 -4 -5 1070.45 172.778 1 5 -4 -4 59.7396 26.3872 1 5 -4 -3 16.4591 21.7726 1 5 -4 -2 70.0617 29.5447 1 5 -4 -1 67.6501 15.9276 1 5 -4 0 2056.85 175.079 1 5 -4 1 1174.08 120.421 1 5 -4 2 366.653 27.1492 1 5 -4 3 1250.69 84.9954 1 5 -4 4 378.615 32.8729 1 5 -4 5 589.936 50.7484 1 5 -4 6 1019.42 125.678 1 5 -4 7 192.087 50.2485 1 5 -4 8 50.5232 15.139 1 5 -4 9 1.84298 12.6771 1 5 -4 10 2.78087 14.6577 1 5 -4 11 45.3597 19.4137 1 5 -3 -12 37.7133 35.6328 1 5 -3 -11 35.1932 30.9335 1 5 -3 -10 94.5001 33.7492 1 5 -3 -9 225.962 62.7401 1 5 -3 -8 26.7466 25.0345 1 5 -3 -7-23.5887 39.0906 1 5 -3 -6 181.727 32.5995 1 5 -3 -5 454.792 74.5251 1 5 -3 -4 1122.95 147.674 1 5 -3 -3-13.4444 13.9756 1 5 -3 -2 53.6244 25.4708 1 5 -3 -1 65.8716 17.279 1 5 -3 0 257.055 71.9763 1 5 -3 1 1766.74 117.791 1 5 -3 2 1247.56 80.0685 1 5 -3 3 1.70411 8.77634 1 5 -3 4 123.561 14.3803 1 5 -3 5 81.8803 11.9914 1 5 -3 6 598.135 76.4867 1 5 -3 7 651.045 50.2143 1 5 -3 8 32.3374 15.5168 1 5 -3 9 120.717 37.6786 1 5 -3 10 28.2556 20.2201 1 5 -3 11 12.6553 19.6394 1 5 -3 12 53.2525 33.7415 1 5 -2 -12 55.0317 32.917 1 5 -2 -11 27.0626 36.8061 1 5 -2 -10 118.836 40.0047 1 5 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473.017 62.2715 1 5 2 11 132.046 22.2423 1 5 2 12 72.3058 24.138 1 5 2 13 16.1368 19.6052 1 5 3 -12-30.7635 45.3615 1 5 3 -11 55.2774 24.7699 1 5 3 -10 33.8507 14.0626 1 5 3 -9 48.6931 21.3847 1 5 3 -8 76.8803 21.6369 1 5 3 -7 130.832 17.8871 1 5 3 -6 13.7473 21.50 1 5 3 -5 25.4072 10.1951 1 5 3 -4 52.911 8.81326 1 5 3 -3 216.97 16.6937 1 5 3 -2 185.26 13.0975 1 5 3 -1 207.773 16.0744 1 5 3 0 1274.98 104.008 1 5 3 1 286.141 19.8604 1 5 3 2 423.256 26.4099 1 5 3 3 399.369 32.1296 1 5 3 4 1235.49 91.0905 1 5 3 5 4440.98 338.405 1 5 3 6 4368.59 332.712 1 5 3 7 670.236 54.3738 1 5 3 8 944.928 95.8732 1 5 3 9 584.042 80.6767 1 5 3 10 485.828 91.9173 1 5 3 11 607.443 72.3874 1 5 3 12 48.1986 24.6842 1 5 3 13 32.9889 25.9758 1 5 4 -11 31.545 20.1863 1 5 4 -10 19.9894 19.8328 1 5 4 -9 45.2924 17.0978 1 5 4 -8 22.6856 18.8834 1 5 4 -7 59.6615 13.0425 1 5 4 -6 8.49786 13.7191 1 5 4 -5 2.60731 10.3858 1 5 4 -4 25.1604 7.67722 1 5 4 -3 22.8792 6.46338 1 5 4 -2 78.882 9.59736 1 5 4 -1 1452.35 76.7764 1 5 4 0 708.285 35.5258 1 5 4 1 3834.72 228.445 1 5 4 2 1224.59 90.7991 1 5 4 3 469.485 48.2782 1 5 4 4 1939.36 154.863 1 5 4 5 3092.84 247.663 1 5 4 6 4358.06 375.694 1 5 4 7 2082.69 185.153 1 5 4 8 17.8592 17.5857 1 5 4 9 743.871 78.173 1 5 4 10 389.44 34.0266 1 5 4 11 174.94 25.6718 1 5 4 12 137.878 45.4768 1 5 4 13-30.8411 33.7427 1 5 5 -11 24.3447 26.9506 1 5 5 -10 21.3742 25.4953 1 5 5 -9 12.0648 16.6966 1 5 5 -8 11.732 14.2556 1 5 5 -7 7.57319 20.5759 1 5 5 -6 12.5114 10.4075 1 5 5 -5 320.862 24.9936 1 5 5 -4 442.741 27.5287 1 5 5 -3 1228.11 87.3118 1 5 5 -2 160.357 12.1641 1 5 5 -1 242.577 18.4653 1 5 5 0 3535.87 189.156 1 5 5 1 3066.35 167.362 1 5 5 2 2470.90 164.959 1 5 5 3 2020.15 137.607 1 5 5 4 784.491 44.7022 1 5 5 5 852.344 58.3066 1 5 5 6 692.122 65.8636 1 5 5 7 175.76 23.3063 1 5 5 8 133.186 23.2736 1 5 5 9 1.81466 13.0351 1 5 5 10 140.184 22.4601 1 5 5 11 9.9396 12.5633 1 5 5 12 37.1733 18.6917 1 5 5 13 35.7866 18.4655 1 5 6 -10 54.7437 33.0479 1 5 6 -9 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24.2158 1 5 7 10 40.0834 17.566 1 5 7 11 79.7525 20.8172 1 5 7 12 293.107 45.1421 1 5 7 13 89.5645 31.4416 1 5 8 -8 43.4581 28.9762 1 5 8 -7 10.1354 20.5691 1 5 8 -6 52.3218 34.6272 1 5 8 -5 40.1127 11.3313 1 5 8 -4 26.079 34.2797 1 5 8 -3 7.44027 11.6903 1 5 8 -2 725.076 45.337 1 5 8 -1 121.921 16.7545 1 5 8 0 10.1794 10.1631 1 5 8 1 266.357 19.0232 1 5 8 2 808.903 56.6162 1 5 8 3 2018.84 294.799 1 5 8 4 821.745 73.8002 1 5 8 5 231.657 25.1934 1 5 8 6 527.614 68.5589 1 5 8 7 83.258 22.646 1 5 8 8 602.405 63.1687 1 5 8 9 689.102 66.5028 1 5 8 10 127.355 22.4803 1 5 8 11 54.6995 22.7206 1 5 8 12 81.8076 24.0239 1 5 9 -7 28.3777 45.2403 1 5 9 -6 41.024 31.2239 1 5 9 -5 2.97691 9.64404 1 5 9 -4 115.436 21.3461 1 5 9 -3 297.416 60.506 1 5 9 -2 691.73 46.8804 1 5 9 -1 309.004 19.5957 1 5 9 0 41.3899 11.2336 1 5 9 1 375.922 24.326 1 5 9 2 2418.29 182.617 1 5 9 3 1784.66 167.314 1 5 9 4 1111.95 93.0501 1 5 9 5 547.064 112.369 1 5 9 6 342.091 31.0965 1 5 9 7 461.262 44.1883 1 5 9 8 367.605 92.639 1 5 9 9 710.634 111.734 1 5 9 10 165.466 26.3913 1 5 9 11 59.6062 34.5984 1 5 10 -6 34.2511 34.2747 1 5 10 -5 11.5831 36.8406 1 5 10 -4-3.27679 22.3592 1 5 10 -3 54.0555 11.9327 1 5 10 -2 481.588 43.2634 1 5 10 -1 370.899 27.1312 1 5 10 0 531.615 43.5634 1 5 10 1 557.636 38.8041 1 5 10 2 70.7081 12.3211 1 5 10 3 805.855 106.825 1 5 10 4 444.692 31.3005 1 5 10 5 663.799 157.579 1 5 10 6 439.996 64.803 1 5 10 7 67.4586 25.8895 1 5 10 8 47.701 24.1555 1 5 10 9 126.635 51.5061 1 5 10 10 45.1542 38.3523 1 5 10 11 -34.136 61.8991 1 5 11 -4 34.9481 32.3858 1 5 11 -3 18.8918 17.0804 1 5 11 -2 220.128 51.4934 1 5 11 -1 242.189 50.8627 1 5 11 0 262.839 24.8443 1 5 11 1 53.3617 12.4545 1 5 11 2 13.0867 13.4882 1 5 11 3 37.937 16.4224 1 5 11 4 297.843 28.1745 1 5 11 5 132.988 21.6892 1 5 11 6 82.4723 24.5589 1 5 11 7 3.36639 23.3751 1 5 11 8 1.3978 21.4492 1 5 11 9 4.18074 37.2075 1 5 12 -2-3.60881 30.1071 1 5 12 -1 27.4245 36.6109 1 5 12 0 59.6409 30.2267 1 5 12 1 18.3513 33.0995 1 5 12 2 40.3897 44.0497 1 5 12 3 76.0073 24.8291 1 5 12 4 54.0354 20.1402 1 5 12 5 179.718 44.308 1 5 12 6 142.669 38.3771 1 5 12 7 48.9526 28.3243 1 6 -10 -6 31.3982 58.124 1 6 -10 -5 -1.0091 33.4146 1 6 -10 -4-3.67728 30.0682 1 6 -10 -3 32.5048 27.239 1 6 -10 -2 44.5398 23.7498 1 6 -10 -1-14.1698 29.2639 1 6 -10 0 37.1239 17.6693 1 6 -10 1 52.5556 54.4492 1 6 -10 2 46.1016 18.9225 1 6 -9 -8-23.0953 27.0624 1 6 -9 -7-14.9156 62.9933 1 6 -9 -6 28.4835 40.9301 1 6 -9 -5 22.5199 44.3848 1 6 -9 -4 89.5687 57.1256 1 6 -9 -3 56.8378 45.2479 1 6 -9 -2 148.858 62.3515 1 6 -9 -1 1.60639 16.4506 1 6 -9 0 6.62046 14.8861 1 6 -9 1 86.8455 41.1772 1 6 -9 2 70.0795 39.0275 1 6 -9 3 16.2844 29.4989 1 6 -9 4 16.5697 30.3538 1 6 -8 -9 37.1034 23.4523 1 6 -8 -8 135.966 54.4796 1 6 -8 -7 98.4544 30.0875 1 6 -8 -6 66.2529 45.0164 1 6 -8 -5 38.3077 36.9577 1 6 -8 -4 -78.971 40.6206 1 6 -8 -3 123.759 35.0232 1 6 -8 -2 236.011 43.4351 1 6 -8 -1 47.9988 21.1479 1 6 -8 0-9.74349 16.5064 1 6 -8 1 4.22251 31.4124 1 6 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33.0402 1 6 -6 7 64.508 19.7034 1 6 -6 8 101.665 33.9311 1 6 -6 9 78.4648 32.7982 1 6 -5 -10 44.2682 13.272 1 6 -5 -9 10.4058 40.095 1 6 -5 -8 35.5789 34.5823 1 6 -5 -7 92.0021 54.7486 1 6 -5 -6 169.519 44.1136 1 6 -5 -5 246.976 52.2128 1 6 -5 -4 33.9406 32.0103 1 6 -5 -3 11.0965 18.8771 1 6 -5 -2 500.964 65.828 1 6 -5 -1 173.434 40.0591 1 6 -5 0 143.658 18.2168 1 6 -5 1 312.895 28.795 1 6 -5 2 32.4678 19.2927 1 6 -5 3 353.813 39.6494 1 6 -5 4 335.90 37.5204 1 6 -5 5 264.416 23.7723 1 6 -5 6 272.153 26.0437 1 6 -5 7 28.8328 15.0359 1 6 -5 8 38.6783 23.1749 1 6 -5 9 64.4416 28.791 1 6 -4 -11 6.41393 28.0134 1 6 -4 -10 36.5922 37.9508 1 6 -4 -9 150.48 36.2564 1 6 -4 -8 74.1037 31.6643 1 6 -4 -7 15.6513 23.8895 1 6 -4 -6 934.136 152.595 1 6 -4 -5 304.326 53.5838 1 6 -4 -4-5.09792 18.4818 1 6 -4 -3 273.981 42.5166 1 6 -4 -2 215.288 25.8508 1 6 -4 -1 790.226 74.6398 1 6 -4 0 490.761 105.364 1 6 -4 1 183.245 21.0762 1 6 -4 2 296.33 31.6096 1 6 -4 3 34.6277 14.1945 1 6 -4 4 325.214 36.0519 1 6 -4 5 220.512 22.6938 1 6 -4 6 120.286 16.2569 1 6 -4 7 74.4767 17.0421 1 6 -4 8 10.4997 13.779 1 6 -4 9 5.18078 13.9054 1 6 -4 10 50.6291 25.104 1 6 -3 -11 30.6248 33.6786 1 6 -3 -10 229.676 47.9301 1 6 -3 -9 154.502 40.3589 1 6 -3 -8 197.657 49.6596 1 6 -3 -7 32.23 24.5609 1 6 -3 -6 557.31 83.9117 1 6 -3 -4 100.046 23.8533 1 6 -3 -3 25.6195 19.4139 1 6 -3 -2 132.43 20.5411 1 6 -3 -1 -14.089 24.0111 1 6 -3 0 133.239 21.9395 1 6 -3 1 9.54304 19.9543 1 6 -3 2 4.48948 9.90681 1 6 -3 3 57.4525 10.1714 1 6 -3 4 500.496 50.5575 1 6 -3 5 138.351 30.7867 1 6 -3 6 218.793 42.0362 1 6 -3 7 32.0889 17.4922 1 6 -3 8 29.632 13.7655 1 6 -3 9-5.16857 30.0295 1 6 -3 10 7.82677 14.5047 1 6 -3 11 87.5363 51.62 1 6 -2 -11 19.6206 35.1322 1 6 -2 -10 168.615 37.376 1 6 -2 -9 395.252 62.9096 1 6 -2 -8 107.176 51.191 1 6 -2 -7 20.0143 38.2848 1 6 -2 -6 190.697 39.1961 1 6 -2 -5 289.396 58.3651 1 6 -2 -4 280.297 60.4473 1 6 -2 -3 98.4098 17.7472 1 6 -2 -2 155.188 22.0876 1 6 -2 -1 7.04791 11.8917 1 6 -2 0 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37.5721 1 7 -4 -8 28.998 74.767 1 7 -4 -7 194.793 58.4648 1 7 -4 -6 420.323 72.8621 1 7 -4 -5 251.188 49.0905 1 7 -4 -4 298.219 47.6003 1 7 -4 -3 162.953 34.1799 1 7 -4 -2 1154.27 165.626 1 7 -4 -1 778.527 81.4756 1 7 -4 0 482.27 47.0913 1 7 -4 1 373.724 37.0813 1 7 -4 2 28.5031 18.0572 1 7 -4 3-1.43176 19.6425 1 7 -4 4 184.311 21.611 1 7 -4 5 85.7666 16.7914 1 7 -4 6 51.542 14.4177 1 7 -4 7 66.6384 20.3474 1 7 -4 8 29.8509 14.0726 1 7 -4 9-6.89343 27.2507 1 7 -3 -10 52.3495 46.6863 1 7 -3 -9 79.7349 34.8938 1 7 -3 -8 188.35 72.9423 1 7 -3 -7 71.5903 38.8004 1 7 -3 -6 658.622 101.225 1 7 -3 -5 602.452 92.3215 1 7 -3 -4 689.867 110.532 1 7 -3 -3 546.816 62.8934 1 7 -3 -2 180.778 25.1274 1 7 -3 -1 848.431 95.4717 1 7 -3 0 292.501 28.1638 1 7 -3 1 42.2499 13.2619 1 7 -3 2 73.566 11.71 1 7 -3 3 49.8769 12.5573 1 7 -3 4 10.1618 12.3273 1 7 -3 5 37.4632 12.6959 1 7 -3 6 11.579 13.2525 1 7 -3 7 13.2523 13.6511 1 7 -3 8 106.475 17.3653 1 7 -3 9 1.10366 15.8643 1 7 -3 10 12.5101 16.2079 1 7 -2 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35.2863 1 7 -1 8-0.26175 30.7581 1 7 -1 9 53.7009 19.42 1 7 -1 10 26.5844 20.9628 1 7 -1 11 58.7648 25.7085 1 7 0 -10 39.7243 27.4786 1 7 0 -9 105.38 47.2118 1 7 0 -8 210.387 103.293 1 7 0 -7 102.816 32.6623 1 7 0 -6 322.79 53.1586 1 7 0 -5 182.293 35.7715 1 7 0 -4 393.553 41.4041 1 7 0 -3 2820.39 351.861 1 7 0 -2 997.451 95.7047 1 7 0 -1 277.122 28.7262 1 7 0 0 1015.72 105.428 1 7 0 1 315.509 27.4236 1 7 0 2 1070.69 66.6334 1 7 0 3 931.772 60.4238 1 7 0 4 -0.7415 18.0276 1 7 0 5 152.417 17.5403 1 7 0 6 9.45728 12.5607 1 7 0 7 41.6358 16.2085 1 7 0 8 56.6087 17.9918 1 7 0 9 30.8447 20.5691 1 7 0 10 18.6293 19.717 1 7 0 11 22.6832 23.5991 1 7 1 -10 19.5167 21.6684 1 7 1 -9 203.676 136.173 1 7 1 -8 268.276 124.84 1 7 1 -7 783.515 209.639 1 7 1 -6 295.228 100.725 1 7 1 -5 562.623 55.4192 1 7 1 -4 1025.82 101.796 1 7 1 -3 1748.29 131.699 1 7 1 -2 2378.86 247.685 1 7 1 -1 845.125 54.5566 1 7 1 0 3.65595 9.14011 1 7 1 1 339.511 43.1072 1 7 1 2 220.57 17.9945 1 7 1 3 427.659 26.4021 1 7 1 4 11.6709 10.0315 1 7 1 5 23.3687 12.6356 1 7 1 6-6.28221 24.2889 1 7 1 7 10.9305 12.9249 1 7 1 8 264.991 49.1262 1 7 1 9 53.429 33.182 1 7 1 10 15.7174 19.7679 1 7 1 11 1.65852 33.2885 1 7 1 12 9.32969 17.7857 1 7 2 -9 63.6146 30.3731 1 7 2 -8 491.48 120.246 1 7 2 -7 258.094 50.718 1 7 2 -6 227.319 71.3003 1 7 2 -5 531.408 50.7952 1 7 2 -4 183.438 22.8661 1 7 2 -3 76.1702 10.6872 1 7 2 -2 497.291 33.2219 1 7 2 -1 105.584 12.639 1 7 2 0 23.4497 9.82296 1 7 2 1 232.841 25.607 1 7 2 2 165.742 18.8792 1 7 2 3 259.989 24.6204 1 7 2 4 17.8726 12.1198 1 7 2 5 71.6208 11.8409 1 7 2 6 49.1537 13.6264 1 7 2 7 12.0415 30.2876 1 7 2 8 201.268 20.8993 1 7 2 9 42.5892 15.6066 1 7 2 10 86.2491 20.586 1 7 2 11-7.49652 32.9617 1 7 2 12 19.8144 21.5754 1 7 3 -10 44.0215 26.2347 1 7 3 -9 40.4534 14.7867 1 7 3 -8 137.676 54.6988 1 7 3 -7 398.556 82.6362 1 7 3 -6 351.616 51.5424 1 7 3 -5 141.953 15.7212 1 7 3 -4 72.481 15.9263 1 7 3 -3 1.67925 10.6404 1 7 3 -2 654.883 49.2791 1 7 3 -1 567.285 39.8521 1 7 3 0 48.9768 11.1814 1 7 3 1 75.5507 9.7829 1 7 3 2 101.758 22.966 1 7 3 3 1079.83 114.446 1 7 3 4 7.43243 10.8884 1 7 3 5-1.42628 20.3531 1 7 3 6 139.013 23.2839 1 7 3 7-0.02482 18.4288 1 7 3 8 6.86936 11.522 1 7 3 9 328.862 32.0117 1 7 3 10 171.221 33.9755 1 7 3 11 141.125 30.1768 1 7 3 12 38.6764 23.2917 1 7 4 -10 12.7427 23.0878 1 7 4 -9 20.7719 33.0334 1 7 4 -8 25.5927 14.913 1 7 4 -7 89.402 44.6112 1 7 4 -6 476.706 81.5942 1 7 4 -5 116.941 21.5901 1 7 4 -4 68.7136 13.7269 1 7 4 -3 1049.36 82.2384 1 7 4 -2 87.6068 11.0119 1 7 4 -1 2031.83 126.186 1 7 4 0 782.307 46.3889 1 7 4 1 176.095 19.6848 1 7 4 2 117.44 13.6872 1 7 4 3 425.147 41.0964 1 7 4 4 349.276 39.2053 1 7 4 5 523.476 93.8723 1 7 4 6 143.835 29.244 1 7 4 7 326.291 54.9644 1 7 4 8 20.5637 42.2929 1 7 4 9 76.6475 26.05 1 7 4 10 565.70 69.5913 1 7 4 11 92.9251 23.5591 1 7 4 12 40.3942 23.548 1 7 5 -9-10.7816 26.5473 1 7 5 -8-5.04711 23.8898 1 7 5 -7 102.396 24.7197 1 7 5 -6 272.434 32.3636 1 7 5 -5 553.868 38.8812 1 7 5 -4 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456.214 33.0362 1 7 7 -3 396.051 27.3109 1 7 7 -2-6.66767 23.0423 1 7 7 -1 69.0388 14.9581 1 7 7 0 13.9427 8.62558 1 7 7 1-1.49988 20.1842 1 7 7 2 161.049 14.0703 1 7 7 3-3.28587 24.4825 1 7 7 4 124.725 27.2534 1 7 7 5-4.93916 25.4137 1 7 7 6-14.8844 24.204 1 7 7 7 118.319 16.4816 1 7 7 8 161.59 22.4133 1 7 7 9 17.8372 17.2292 1 7 7 10 30.995 18.4736 1 7 7 11 66.2462 23.5844 1 7 8 -6-7.16895 45.1108 1 7 8 -5 21.6476 25.0633 1 7 8 -4 147.292 18.3099 1 7 8 -3 2.74156 10.9388 1 7 8 -2 11.1526 9.67765 1 7 8 -1 40.1074 10.1929 1 7 8 0 78.3971 11.6407 1 7 8 1 13.1708 12.0098 1 7 8 2 192.816 15.2422 1 7 8 3 8.85636 9.51198 1 7 8 4 6.98416 14.7842 1 7 8 5 3.41878 20.4277 1 7 8 6 149.207 19.9396 1 7 8 7 400.486 34.3618 1 7 8 8 137.875 22.0119 1 7 8 9 110.02 20.2509 1 7 8 10 42.2144 27.523 1 7 9 -5-9.80816 44.7997 1 7 9 -4 7.99762 16.1301 1 7 9 -3 153.666 15.5378 1 7 9 -2 33.0442 16.4238 1 7 9 -1 73.6566 14.6267 1 7 9 0 115.272 13.6671 1 7 9 1 13.657 10.5872 1 7 9 2 110.767 13.496 1 7 9 3 523.44 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20.4184 44.5906 1 9 -2 -1 48.6102 22.1598 1 9 -2 0 159.012 19.3613 1 9 -2 1 26.384 19.6449 1 9 -2 2 23.7026 16.0363 1 9 -2 3 55.3452 25.9442 1 9 -2 4 237.592 38.5175 1 9 -2 5 194.309 23.8127 1 9 -2 6 117.816 18.1681 1 9 -2 7 78.504 23.2773 1 9 -2 8 34.7407 28.6007 1 9 -1 -8 -2.6375 34.4875 1 9 -1 -7-12.9919 34.8931 1 9 -1 -6 4.43996 39.3448 1 9 -1 -5 19.6756 25.7493 1 9 -1 -4-0.23149 30.1879 1 9 -1 -3-22.5627 62.489 1 9 -1 -2 8.07019 21.1499 1 9 -1 -1 115.143 21.2102 1 9 -1 0 180.636 30.2682 1 9 -1 1 136.248 23.3691 1 9 -1 2 240.433 31.1564 1 9 -1 3 77.6714 17.5545 1 9 -1 4 352.842 31.9697 1 9 -1 5 290.797 26.9899 1 9 -1 6 212.24 22.5554 1 9 -1 7 497.599 42.5603 1 9 -1 8 99.3744 20.3852 1 9 -1 9 12.4002 43.9637 1 9 0 -8 13.2292 33.5692 1 9 0 -7 21.2164 21.3108 1 9 0 -6 21.1847 38.1642 1 9 0 -5 16.5263 40.05 1 9 0 -4 27.0532 44.1612 1 9 0 -3-6.84114 29.0892 1 9 0 -2 1.31125 16.8085 1 9 0 -1 8.02999 15.8522 1 9 0 0 207.398 30.2815 1 9 0 1 886.305 79.2765 1 9 0 2 470.352 45.4762 1 9 0 3 355.331 33.142 1 9 0 4 211.127 23.3013 1 9 0 5 209.274 31.46 1 9 0 6 333.729 29.4328 1 9 0 7 431.598 39.9632 1 9 0 8 158.865 22.4717 1 9 0 9 20.4818 21.5258 1 9 1 -8 5.29589 26.9658 1 9 1 -7 0.3266 29.5187 1 9 1 -6 37.7645 19.4054 1 9 1 -5 24.8421 22.2383 1 9 1 -4 189.031 63.2087 1 9 1 -3 104.343 22.3315 1 9 1 -2 39.8975 24.1779 1 9 1 -1 213.242 31.3086 1 9 1 0 94.2864 16.458 1 9 1 1 437.069 35.9861 1 9 1 2 435.827 30.9173 1 9 1 3 63.9694 17.9357 1 9 1 4 410.984 36.8602 1 9 1 5 54.1733 16.7944 1 9 1 6 162.196 18.3493 1 9 1 7 309.672 29.8266 1 9 1 8 12.1755 17.4739 1 9 1 9 43.3367 20.3027 1 9 2 -8 48.0862 30.5794 1 9 2 -7 56.0042 26.5799 1 9 2 -6 10.488 20.3399 1 9 2 -5 4.46632 17.5531 1 9 2 -4 38.0765 20.0355 1 9 2 -3 355.915 42.3285 1 9 2 -2 118.762 28.1019 1 9 2 -1 12.0781 18.2026 1 9 2 0 121.965 20.134 1 9 2 1-3.74125 25.6902 1 9 2 2 228.382 18.0646 1 9 2 3 401.508 29.2286 1 9 2 4 96.7867 14.8817 1 9 2 5 168.97 19.9823 1 9 2 6 6.62898 15.557 1 9 2 7 28.9056 13.387 1 9 2 8 224.763 31.6483 1 9 2 9 41.5155 15.463 1 9 2 10 33.2059 54.0421 1 9 3 -8 21.7394 22.3279 1 9 3 -7 20.6935 14.0592 1 9 3 -6 18.9809 16.5525 1 9 3 -5 38.4558 12.5962 1 9 3 -4 48.427 12.0607 1 9 3 -3-2.33509 21.4271 1 9 3 -2 3.87438 11.5348 1 9 3 -1 9.43453 17.4597 1 9 3 0 0.49355 12.78 1 9 3 1 208.275 20.5292 1 9 3 2 117.821 15.8377 1 9 3 3 374.023 33.0052 1 9 3 4 532.289 37.6514 1 9 3 5 11.2121 17.173 1 9 3 6 55.1036 16.6719 1 9 3 7 155.402 28.1886 1 9 3 8 354.757 34.6022 1 9 3 9 289.334 62.3518 1 9 3 10 24.7073 22.3771 1 9 4 -7-9.97762 26.9291 1 9 4 -6 25.8323 25.6384 1 9 4 -5 1.12024 11.2747 1 9 4 -4-2.10139 26.2257 1 9 4 -3 22.6404 16.2359 1 9 4 -2 24.842 12.7146 1 9 4 -1 135.291 16.0847 1 9 4 0 119.353 14.4497 1 9 4 1 55.7027 15.4153 1 9 4 2 195.016 20.7746 1 9 4 3 295.158 32.5664 1 9 4 4 1036.34 81.1381 1 9 4 5 494.689 41.2784 1 9 4 6 165.43 30.2562 1 9 4 7 336.439 30.5433 1 9 4 8 389.286 38.999 1 9 4 9 232.367 47.9973 1 9 4 10 91.9607 20.3627 1 9 5 -6 22.8629 24.2618 1 9 5 -5 8.03982 15.6245 1 9 5 -4-1.77177 28.0628 1 9 5 -3 14.8404 22.8627 1 9 5 -2 420.054 31.8859 1 9 5 -1 383.469 29.4366 1 9 5 0 335.224 33.9441 1 9 5 1 354.386 23.449 1 9 5 2 100.73 17.9607 1 9 5 3 652.847 44.6539 1 9 5 4 1140.85 128.391 1 9 5 5 613.713 49.6297 1 9 5 6 300.677 31.245 1 9 5 7 38.4022 30.9512 1 9 5 8 71.9596 16.1565 1 9 5 9 88.4139 23.551 1 9 6 -6 37.5862 16.1443 1 9 6 -5 22.1245 15.6557 1 9 6 -4 6.00791 16.7558 1 9 6 -3 35.8131 14.0193 1 9 6 -2 59.5436 12.7554 1 9 6 -1 515.255 36.4442 1 9 6 0 361.972 23.6276 1 9 6 1 194.266 19.545 1 9 6 2 171.507 16.3329 1 9 6 3 100.18 15.8471 1 9 6 4 165.652 20.5838 1 9 6 5 383.372 31.219 1 9 6 6 82.539 17.4476 1 9 6 7 9.30465 19.8141 1 9 6 8 5.11696 31.9751 1 9 6 9-21.8467 77.4548 1 9 7 -5 55.371 53.519 1 9 7 -4 24.9755 34.9614 1 9 7 -3 3.93779 11.776 1 9 7 -2 6.98895 12.1112 1 9 7 -1 10.7701 12.6232 1 9 7 0 112.223 13.9681 1 9 7 1 78.4363 13.7573 1 9 7 2 12.2135 14.3913 1 9 7 3 43.6417 12.7695 1 9 7 4 1.79607 13.4536 1 9 7 5 177.524 21.107 1 9 7 6 333.325 31.3322 1 9 7 7 16.0446 20.493 1 9 7 8 39.1425 26.1649 1 9 8 -3 17.5925 15.1982 1 9 8 -2 39.5836 16.9089 1 9 8 -1-3.52509 39.8586 1 9 8 0 29.831 14.1555 1 9 8 1 194.04 20.4686 1 9 8 2 145.794 18.2549 1 9 8 3 15.5301 13.6524 1 9 8 4 72.1664 15.6863 1 9 8 5 181.286 24.0921 1 9 8 6 371.654 38.9964 1 9 8 7 331.586 36.8573 1 9 9 -1 2.54153 36.3631 1 9 9 0 142.239 20.1386 1 9 9 1 203.421 38.4832 1 9 9 2 330.079 55.6678 1 9 9 3 181.016 39.4602 1 9 9 4 79.5242 18.1708 1 9 9 5 283.794 30.2049 1 9 9 6 125.477 29.2428 1 10 -5 -2 44.6175 36.7863 1 10 -5 -1 41.7775 48.7562 1 10 -5 0 123.882 96.7474 1 10 -5 1 38.3584 31.0803 1 10 -4 -2 23.2359 40.0529 1 10 -4 -1 19.3522 26.3879 1 10 -4 0 9.00657 17.8838 1 10 -4 1 36.766 27.282 1 10 -4 2 18.1382 21.4951 1 10 -4 3-1.38194 40.6571 1 10 -3 -3-15.4396 32.8214 1 10 -3 -2 36.2582 21.9956 1 10 -3 -1 80.1013 23.0337 1 10 -3 0 2.20691 21.5255 1 10 -3 1-8.53789 39.8126 1 10 -3 2 18.6347 27.8173 1 10 -3 3-25.1126 41.2991 1 10 -3 4 40.61 41.5662 1 10 -3 5 0.28777 26.1422 1 10 -2 -4 27.352 34.6024 1 10 -2 -3-1.56186 38.8023 1 10 -2 -2 5.12512 26.2266 1 10 -2 -1 19.5553 20.5296 1 10 -2 0 8.54366 20.9343 1 10 -2 1 21.9182 33.0431 1 10 -2 2 6.96607 20.7668 1 10 -2 3 20.6728 16.5156 1 10 -2 4 3.59619 17.1712 1 10 -2 5 86.9989 39.22 1 10 -2 6 15.4265 20.6289 1 10 -1 -5 19.4979 31.5617 1 10 -1 -4 24.2765 18.9279 1 10 -1 -3 23.1165 21.0967 1 10 -1 -2 0.79748 23.224 1 10 -1 -1-13.1948 34.5726 1 10 -1 0 2.9429 19.1919 1 10 -1 1 19.6639 18.1866 1 10 -1 2 13.1543 17.0396 1 10 -1 3 4.52177 21.9758 1 10 -1 4 7.95391 25.9784 1 10 -1 5 35.9702 25.9621 1 10 -1 6 226.724 51.181 1 10 -1 7 43.39 27.8935 1 10 0 -5 3.14969 50.741 1 10 0 -4-7.63745 98.1344 1 10 0 -3-4.98171 27.7217 1 10 0 -2 30.6706 22.9278 1 10 0 -1 86.9282 22.2382 1 10 0 0 42.3427 20.861 1 10 0 1 98.4986 22.7391 1 10 0 2 124.104 23.1474 1 10 0 3 23.2408 16.1553 1 10 0 4 15.6452 16.4273 1 10 0 5 43.1164 26.5501 1 10 0 6 152.522 25.4893 1 10 0 7 164.138 35.5993 1 10 1 -6 0.47339 23.7714 1 10 1 -5 55.1185 21.2645 1 10 1 -4 54.008 32.1418 1 10 1 -3 15.9094 30.0677 1 10 1 -2 24.8353 29.8539 1 10 1 -1 3.26613 14.373 1 10 1 0 53.3826 22.6024 1 10 1 1 114.724 21.5014 1 10 1 2 113.115 31.0713 1 10 1 3 71.9182 19.7711 1 10 1 4 9.86274 18.2528 1 10 1 5 36.2546 27.8456 1 10 1 6 100.768 27.74 1 10 1 7 104.483 86.3452 1 10 2 -6 0.23927 23.5756 1 10 2 -5 4.9547 18.3505 1 10 2 -4 57.9795 29.7977 1 10 2 -3 92.0897 21.9719 1 10 2 -2 37.3112 24.2474 1 10 2 -1 10.5653 17.1189 1 10 2 0 29.1496 15.3646 1 10 2 1 4.40257 17.1533 1 10 2 2 9.18539 16.9597 1 10 2 3-4.05974 36.3652 1 10 2 4 7.67685 12.9054 1 10 2 5 11.3789 18.3943 1 10 2 6 26.3356 15.4933 1 10 2 7 35.0482 32.2299 1 10 2 8-37.6605 69.3961 1 10 3 -6 19.7772 19.6733 1 10 3 -5 19.7463 20.0074 1 10 3 -4 0.14452 19.4108 1 10 3 -3 42.078 37.1491 1 10 3 -2 11.0207 18.3081 1 10 3 -1 56.1279 13.2247 1 10 3 0 35.8506 13.3751 1 10 3 1 10.7539 16.4228 1 10 3 2 2.81361 11.885 1 10 3 3 53.606 18.5152 1 10 3 4 13.6429 17.4352 1 10 3 5 9.40224 14.7424 1 10 3 6 13.6043 15.0184 1 10 3 7 48.2874 25.4057 1 10 3 8 193.937 31.3793 1 10 4 -5-0.20309 20.7899 1 10 4 -4 14.7749 31.2469 1 10 4 -3 9.05381 13.1748 1 10 4 -2-6.19579 28.5643 1 10 4 -1 7.59298 14.9718 1 10 4 0 36.1618 15.7463 1 10 4 1 40.4008 15.1704 1 10 4 2 67.0417 15.6882 1 10 4 3 131.485 18.2164 1 10 4 4 288.879 37.594 1 10 4 5 55.7452 17.9545 1 10 4 6 80.7913 19.9523 1 10 4 7 199.188 30.7008 1 10 4 8 256.462 34.3427 1 10 5 -4 26.3701 21.4947 1 10 5 -3 51.888 19.8014 1 10 5 -2 72.9103 13.5382 1 10 5 -1 128.408 20.7596 1 10 5 0 62.4644 15.423 1 10 5 1-7.83753 25.9584 1 10 5 2 98.1561 16.6941 1 10 5 3 61.3928 17.6821 1 10 5 4 211.772 24.0752 1 10 5 5 257.157 52.8692 1 10 5 6-20.1796 36.7789 1 10 5 7 80.9543 21.8403 1 10 6 -3 1.42384 17.7186 1 10 6 -2 149.947 19.288 1 10 6 -1 51.2037 17.0102 1 10 6 0 30.2768 14.2628 1 10 6 1 6.56455 13.5096 1 10 6 2-7.75846 25.9713 1 10 6 3 40.4792 16.5229 1 10 6 4 84.9727 16.035 1 10 6 5 58.1343 18.3165 1 10 6 6 29.128 23.3114 1 10 6 7 12.0233 20.882 1 10 7 -2-9.32796 29.0772 1 10 7 -1 2.80798 15.3533 1 10 7 0 4.9863 14.5584 1 10 7 1-0.74661 33.7681 1 10 7 2-27.9625 27.5642 1 10 7 3 8.82946 14.7718 1 10 7 4 35.9746 16.7399 1 10 7 5 12.8921 18.8195 1 10 7 6 10.8378 17.5454 1 10 8 0 14.788 16.2717 1 10 8 1 40.1323 13.6425 1 10 8 2-8.74771 27.271 1 10 8 3-5.81948 38.4986 1 10 8 4 10.0311 14.1316 1 11 -2 -2 50.6252 37.2285 1 11 -2 -1 4.82055 40.5485 1 11 -2 0 15.4645 29.8184 1 11 -2 1-55.8084 38.1137 1 11 -2 2-15.3952 30.4002 1 11 -1 -3 68.8238 63.7739 1 11 -1 -2 9.04552 25.9238 1 11 -1 -1 28.3133 28.1928 1 11 -1 0 38.8951 26.2363 1 11 -1 1-17.7498 36.3217 1 11 -1 2-27.3169 42.9371 1 11 -1 3-4.26965 61.5793 1 11 0 -3 48.0107 50.0731 1 11 0 -2 2.23593 26.8546 1 11 0 -1 39.1054 21.7252 1 11 0 0 116.56 31.1399 1 11 0 1 115.848 58.9475 1 11 0 2-6.02088 50.6508 1 11 0 3 -10.489 31.3594 1 11 0 4 36.7538 62.5467 1 11 1 -3 58.4557 38.2255 1 11 1 -2 11.9145 14.8911 1 11 1 -1 68.1456 23.3115 1 11 1 0 98.3505 31.7739 1 11 1 1 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_publcif_info_cif.paper_type ?