#============================================================================= data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 15 _journal_issue 3 _journal_year 2024 _journal_page_first 266 _journal_page_last 273 #============================================================================= data_pbbmor_2 _audit_creation_date 2024-04-01 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic PbBMOR_2 _chemical_formula_moiety 'C24 H26 N4 O4 Pb S2' _chemical_formula_sum 'C24 H26 N4 O4 Pb S2' _chemical_formula_weight 705.80 _chemical_melting_point ? _chemical_oxdiff_formula C24H20N3O5Cl loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -4.0753 8.5060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.3922(2) _cell_length_b 7.97550(10) _cell_length_c 23.3368(3) _cell_angle_alpha 90 _cell_angle_beta 92.5820(10) _cell_angle_gamma 90 _cell_volume 2490.06(6) _cell_formula_units_Z 4 _cell_measurement_reflns_used 24723 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 73.9840 _cell_measurement_theta_min 5.8440 _shelx_estimated_absorpt_T_max 0.197 _shelx_estimated_absorpt_T_min 0.136 _exptl_absorpt_coefficient_mu 15.072 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.53464 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.23a (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier . _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.883 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1376 _exptl_crystal_size_max 0.22 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.16 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0343 _diffrn_reflns_av_unetI/netI 0.0212 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.984 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 29875 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.401 _diffrn_reflns_theta_min 3.734 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_detector_type 'Pilatus 200K' _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 23.00 51.00 0.50 0.10 -- 47.48 74.00 15.00 56 2 \w -14.00 73.00 0.50 0.10 -- 47.48 -74.00-113.00 174 3 \w 58.00 116.00 0.50 0.10 -- 47.48 74.00 15.00 116 4 \w -90.00 -65.00 0.50 0.10 -- -90.25 74.00 15.00 50 5 \w 88.00 127.00 0.50 0.10 -- 101.53 -74.00-113.00 78 6 \w 76.00 172.00 0.50 0.10 -- 101.53 74.00 15.00 192 7 \w -123.00 -96.00 0.50 0.10 -- -47.48-125.00-180.00 54 8 \w -28.00 -2.00 0.50 0.10 -- -47.48 74.00 15.00 52 9 \w -61.00 -29.00 0.50 0.10 -- -47.48 -38.00-180.00 64 10 \w -124.00 -70.00 0.50 0.10 -- -47.48-125.00 -60.00 108 11 \w -127.00 -79.00 0.50 0.10 -- -47.48 -38.00-180.00 96 12 \w -109.00 -71.00 0.50 0.10 -- -47.48-125.00 150.00 76 13 \w 52.00 92.00 0.50 0.10 -- 47.48-125.00 60.00 80 14 \w -165.00-138.00 0.50 0.10 -- -90.25 -77.00 150.00 54 15 \w -128.00 -79.00 0.50 0.10 -- -90.25 -94.00 -30.00 98 16 \w -166.00-140.00 0.50 0.10 -- -90.25 -94.00 150.00 52 17 \w -136.00-106.00 0.50 0.10 -- -90.25 -61.00-150.00 60 18 \w -120.00 -80.00 0.50 0.10 -- -90.25 -94.00 150.00 80 19 \w -127.00 -63.00 0.50 0.10 -- -90.25 -77.00 150.00 128 20 \w -134.00 -75.00 0.50 0.10 -- -90.25 -30.00 150.00 118 21 \w 53.00 109.00 0.50 0.10 -- 101.53-111.00 -90.00 112 22 \w 85.00 111.00 0.50 0.10 -- 101.53 30.00 150.00 52 23 \w 135.00 165.00 0.50 0.10 -- 101.53 61.00-180.00 60 24 \w 82.00 107.00 0.50 0.10 -- 101.53-111.00 30.00 50 25 \w 30.00 109.00 0.50 0.10 -- 101.53 -61.00-120.00 158 26 \w 81.00 171.00 0.50 0.10 -- 101.53 30.00 120.00 180 27 \w 22.00 69.00 0.50 0.10 -- 101.53-111.00 30.00 94 28 \w 92.00 119.00 0.50 0.10 -- 101.53 -30.00-150.00 54 29 \w 21.00 83.00 0.50 0.10 -- 101.53 -30.00-150.00 124 30 \w 85.00 124.00 0.50 0.10 -- 101.53 61.00-180.00 78 31 \w 132.00 158.00 0.50 0.10 -- 101.53 45.00 -60.00 52 32 \w 22.00 110.00 0.50 0.10 -- 101.53 -94.00-180.00 176 33 \w 85.00 110.00 0.50 0.10 -- 101.53 45.00 -60.00 50 34 \w 127.00 177.00 0.50 0.10 -- 101.53 111.00-120.00 100 35 \w 58.00 102.00 0.50 0.10 -- 101.53-111.00 90.00 88 36 \w 145.00 177.00 0.50 0.10 -- 101.53 30.00 150.00 64 37 \w 81.00 175.00 0.50 0.10 -- 101.53 61.00 0.00 188 38 \w 62.00 125.00 0.50 0.10 -- 101.53 178.00-180.00 126 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 200K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0276565000 _diffrn_orient_matrix_UB_12 -0.1027354000 _diffrn_orient_matrix_UB_13 -0.0543143000 _diffrn_orient_matrix_UB_21 -0.0883356000 _diffrn_orient_matrix_UB_22 0.1191505000 _diffrn_orient_matrix_UB_23 -0.0139663000 _diffrn_orient_matrix_UB_31 0.0684686000 _diffrn_orient_matrix_UB_32 0.1120904000 _diffrn_orient_matrix_UB_33 -0.0349621000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4957 _reflns_number_total 5001 _reflns_odcompleteness_completeness 99.98 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 68.13 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.40.23a (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.40.23a (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.40.23a (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 1.330 _refine_diff_density_min -1.778 _refine_diff_density_rms 0.132 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.161 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 420 _refine_ls_number_reflns 5001 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0241 _refine_ls_R_factor_gt 0.0239 _refine_ls_restrained_S_all 1.161 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0079P)^2^+15.1813P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0584 _refine_ls_wR_factor_ref 0.0585 _refine_special_details ? _olex2_refinement_description ; ; _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.10700(2) 0.01764(2) 0.44411(2) 0.01022(6) Uani 1 1 d . . . . . S2 S 0.05338(7) 0.29738(12) 0.49831(4) 0.01152(18) Uani 1 1 d . . . . . S1 S 0.30469(7) 0.06758(12) 0.45674(4) 0.01252(18) Uani 1 1 d . . . . . O3 O 0.6224(2) 0.0312(4) 0.34874(13) 0.0226(7) Uani 1 1 d . . . . . O4 O 0.3933(2) 0.6160(4) 0.51186(13) 0.0180(6) Uani 1 1 d . . . . . O2 O 0.1430(2) -0.0454(4) 0.54577(11) 0.0146(6) Uani 1 1 d . . . . . O1 O 0.1336(2) 0.2016(4) 0.36263(12) 0.0140(6) Uani 1 1 d . . . . . N1 N 0.3033(2) 0.2443(4) 0.35687(14) 0.0142(7) Uani 1 1 d . . . . . N3 N 0.4156(2) 0.0294(4) 0.36588(14) 0.0137(7) Uani 1 1 d . . . . . N2 N 0.1700(2) 0.2086(4) 0.59197(14) 0.0127(6) Uani 1 1 d . . . . . N4 N 0.2190(2) 0.4407(4) 0.54369(14) 0.0121(6) Uani 1 1 d . . . . . C14 C 0.1509(3) 0.0456(5) 0.59010(17) 0.0117(7) Uani 1 1 d . . . . . C23 C 0.3998(3) 0.4830(5) 0.55280(19) 0.0176(8) Uani 1 1 d . . . . . H23A H 0.460(4) 0.516(6) 0.5800(19) 0.010(11) Uiso 1 1 d . . . . . H23B H 0.418(4) 0.376(7) 0.535(2) 0.024(13) Uiso 1 1 d . . . . . C15 C 0.1429(3) -0.0410(5) 0.64664(16) 0.0120(8) Uani 1 1 d . . . . . C9 C 0.4831(3) -0.0835(5) 0.39898(18) 0.0142(8) Uani 1 1 d . . . . . H9A H 0.486(4) -0.190(6) 0.378(2) 0.015(12) Uiso 1 1 d . . . . . H9B H 0.464(4) -0.108(6) 0.436(2) 0.013(11) Uiso 1 1 d . . . . . C10 C 0.5855(3) -0.0041(6) 0.40420(19) 0.0191(9) Uani 1 1 d . . . . . H10A H 0.577(4) 0.108(8) 0.426(2) 0.032(15) Uiso 1 1 d . . . . . H10B H 0.637(4) -0.077(7) 0.426(2) 0.022(13) Uiso 1 1 d . . . . . C22 C 0.3137(3) 0.5816(5) 0.47074(18) 0.0159(8) Uani 1 1 d . . . . . H22A H 0.328(3) 0.485(6) 0.447(2) 0.011(11) Uiso 1 1 d . . . . . H22B H 0.308(4) 0.681(7) 0.443(2) 0.018(12) Uiso 1 1 d . . . . . C17 C 0.1192(3) -0.2945(6) 0.7006(2) 0.0217(9) Uani 1 1 d . . . . . H17 H 0.109(4) -0.399(7) 0.700(2) 0.018(13) Uiso 1 1 d . . . . . C13 C 0.1563(3) 0.3122(5) 0.54684(16) 0.0110(7) Uani 1 1 d . . . . . C3 C 0.1899(3) 0.4722(5) 0.33839(17) 0.0128(8) Uani 1 1 d . . . . . C8 C 0.0973(3) 0.5432(5) 0.34867(17) 0.0155(8) Uani 1 1 d . . . . . H8 H 0.049(4) 0.474(6) 0.364(2) 0.019(13) Uiso 1 1 d . . . . . C12 C 0.4537(3) 0.0693(6) 0.30939(17) 0.0167(8) Uani 1 1 d . . . . . H12A H 0.415(4) 0.138(7) 0.291(2) 0.023(13) Uiso 1 1 d . . . . . H12B H 0.456(4) -0.042(7) 0.284(2) 0.025(14) Uiso 1 1 d . . . . . C20 C 0.1580(3) 0.0478(6) 0.69801(18) 0.0166(8) Uani 1 1 d . . . . . H20 H 0.177(4) 0.160(7) 0.699(2) 0.014(12) Uiso 1 1 d . . . . . C1 C 0.3396(3) 0.1157(5) 0.38742(16) 0.0118(7) Uani 1 1 d . . . . . C4 C 0.2633(3) 0.5711(6) 0.31440(18) 0.0166(8) Uani 1 1 d . . . . . H4 H 0.309(5) 0.524(8) 0.304(3) 0.04(2) Uiso 1 1 d . . . . . C11 C 0.5580(3) 0.1422(6) 0.31754(19) 0.0206(9) Uani 1 1 d . . . . . H11A H 0.586(3) 0.153(5) 0.2809(19) 0.005(10) Uiso 1 1 d . . . . . H11B H 0.558(4) 0.259(8) 0.337(2) 0.034(15) Uiso 1 1 d . . . . . C7 C 0.0785(4) 0.7101(6) 0.33579(18) 0.0209(9) Uani 1 1 d . . . . . H7 H 0.009(4) 0.759(7) 0.343(2) 0.021(13) Uiso 1 1 d . . . . . C5 C 0.2435(4) 0.7372(6) 0.30085(18) 0.0215(9) Uani 1 1 d . . . . . H5 H 0.290(4) 0.803(8) 0.285(2) 0.035(16) Uiso 1 1 d . . . . . C24 C 0.3038(3) 0.4674(5) 0.58486(18) 0.0147(8) Uani 1 1 d . . . . . H24A H 0.305(3) 0.380(6) 0.610(2) 0.011(11) Uiso 1 1 d . . . . . H24B H 0.291(3) 0.570(6) 0.6046(18) 0.006(10) Uiso 1 1 d . . . . . C18 C 0.1348(3) -0.2067(6) 0.75147(18) 0.0210(9) Uani 1 1 d . . . . . H18 H 0.134(4) -0.269(7) 0.786(3) 0.035(16) Uiso 1 1 d . . . . . C2 C 0.2080(3) 0.2930(5) 0.35483(16) 0.0119(7) Uani 1 1 d . . . . . C16 C 0.1227(3) -0.2112(5) 0.64832(18) 0.0150(8) Uani 1 1 d . . . . . H16 H 0.111(4) -0.268(7) 0.615(2) 0.019(13) Uiso 1 1 d . . . . . C19 C 0.1538(3) -0.0369(6) 0.75024(18) 0.0202(9) Uani 1 1 d . . . . . H19 H 0.166(5) 0.025(7) 0.788(3) 0.037(16) Uiso 1 1 d . . . . . C6 C 0.1516(4) 0.8077(5) 0.31150(18) 0.0242(10) Uani 1 1 d . . . . . H6 H 0.137(4) 0.937(7) 0.307(2) 0.023(13) Uiso 1 1 d . . . . . C21 C 0.2137(3) 0.5716(5) 0.49899(17) 0.0133(8) Uani 1 1 d . . . . . H21A H 0.200(4) 0.675(7) 0.514(2) 0.017(12) Uiso 1 1 d . . . . . H21B H 0.160(3) 0.543(6) 0.470(2) 0.009(11) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.01146(8) 0.00988(8) 0.00953(8) -0.00052(5) 0.00278(5) -0.00126(5) S2 0.0090(4) 0.0118(4) 0.0137(4) -0.0005(3) 0.0002(3) 0.0019(3) S1 0.0119(4) 0.0162(5) 0.0096(4) 0.0026(3) 0.0020(3) 0.0020(3) O3 0.0119(14) 0.0361(19) 0.0201(15) -0.0022(13) 0.0044(12) -0.0012(13) O4 0.0164(14) 0.0159(14) 0.0217(15) 0.0031(12) 0.0022(12) -0.0039(11) O2 0.0223(14) 0.0123(13) 0.0094(13) 0.0004(11) 0.0035(11) -0.0005(11) O1 0.0124(13) 0.0151(14) 0.0146(13) 0.0032(11) 0.0014(10) -0.0010(11) N1 0.0129(16) 0.0149(17) 0.0152(16) 0.0056(13) 0.0048(13) 0.0022(13) N3 0.0099(15) 0.0206(18) 0.0107(16) 0.0024(13) 0.0014(12) 0.0041(13) N2 0.0152(16) 0.0135(16) 0.0096(15) 0.0011(13) 0.0011(12) -0.0020(13) N4 0.0157(16) 0.0095(15) 0.0112(15) 0.0021(12) 0.0009(13) -0.0005(13) C14 0.0064(16) 0.0137(19) 0.0151(19) 0.0011(15) 0.0019(14) 0.0023(14) C23 0.016(2) 0.016(2) 0.021(2) 0.0020(17) 0.0014(17) 0.0004(16) C15 0.0066(16) 0.019(2) 0.0108(18) 0.0031(15) 0.0036(14) 0.0025(15) C9 0.0142(19) 0.014(2) 0.0142(19) 0.0015(16) 0.0026(15) 0.0050(16) C10 0.0135(19) 0.027(2) 0.017(2) -0.0030(18) -0.0019(16) 0.0022(17) C22 0.017(2) 0.015(2) 0.0158(19) 0.0018(16) 0.0029(16) -0.0014(16) C17 0.022(2) 0.018(2) 0.025(2) 0.0082(18) -0.0018(17) -0.0038(18) C13 0.0093(17) 0.0126(19) 0.0115(17) -0.0028(14) 0.0045(14) 0.0026(14) C3 0.0159(19) 0.0104(19) 0.0116(18) 0.0009(14) -0.0046(15) 0.0012(15) C8 0.017(2) 0.020(2) 0.0096(18) 0.0010(16) -0.0030(15) 0.0033(17) C12 0.0138(19) 0.025(2) 0.0120(19) 0.0036(17) 0.0027(15) 0.0055(17) C20 0.017(2) 0.019(2) 0.0135(19) 0.0017(16) 0.0031(15) 0.0032(17) C1 0.0100(17) 0.0128(18) 0.0126(18) -0.0008(15) -0.0008(14) -0.0019(14) C4 0.018(2) 0.018(2) 0.0133(19) 0.0010(16) 0.0002(16) -0.0005(17) C11 0.023(2) 0.022(2) 0.018(2) 0.0006(17) 0.0096(17) -0.0025(18) C7 0.030(2) 0.018(2) 0.014(2) -0.0036(16) -0.0048(17) 0.0107(18) C5 0.034(3) 0.015(2) 0.014(2) 0.0029(16) -0.0049(18) -0.0089(19) C24 0.017(2) 0.013(2) 0.0142(19) -0.0003(16) -0.0011(16) -0.0024(16) C18 0.020(2) 0.029(2) 0.014(2) 0.0112(18) 0.0002(16) -0.0002(18) C2 0.0153(19) 0.0135(19) 0.0069(16) -0.0005(14) 0.0018(14) 0.0012(15) C16 0.0136(19) 0.018(2) 0.0134(19) 0.0024(16) -0.0005(15) -0.0019(16) C19 0.024(2) 0.026(2) 0.0107(19) 0.0007(17) 0.0026(16) 0.0039(18) C6 0.046(3) 0.011(2) 0.014(2) -0.0041(16) -0.0093(19) 0.0024(19) C21 0.0164(19) 0.0072(18) 0.0161(19) 0.0040(15) -0.0018(16) -0.0002(15) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 S2 2.6786(9) . ? Pb1 S1 2.6803(9) . ? Pb1 O2 2.452(3) . ? Pb1 O1 2.441(3) . ? S2 C13 1.748(4) . ? S1 C1 1.747(4) . ? O3 C10 1.434(5) . ? O3 C11 1.415(6) . ? O4 C23 1.427(5) . ? O4 C22 1.428(5) . ? O2 C14 1.264(5) . ? O1 C2 1.255(5) . ? N1 C1 1.329(5) . ? N1 C2 1.332(5) . ? N3 C9 1.470(5) . ? N3 C12 1.470(5) . ? N3 C1 1.345(5) . ? N2 C14 1.325(5) . ? N2 C13 1.344(5) . ? N4 C13 1.330(5) . ? N4 C24 1.470(5) . ? N4 C21 1.475(5) . ? C14 C15 1.498(5) . ? C23 H23A 1.04(5) . ? C23 H23B 0.99(6) . ? C23 C24 1.522(6) . ? C15 C20 1.399(6) . ? C15 C16 1.385(6) . ? C9 H9A 0.98(5) . ? C9 H9B 0.94(5) . ? C9 C10 1.511(6) . ? C10 H10A 1.04(6) . ? C10 H10B 1.01(5) . ? C22 H22A 0.97(5) . ? C22 H22B 1.03(5) . ? C22 C21 1.521(6) . ? C17 H17 0.84(6) . ? C17 C18 1.387(7) . ? C17 C16 1.391(6) . ? C3 C8 1.394(6) . ? C3 C4 1.396(6) . ? C3 C2 1.497(5) . ? C8 H8 0.93(5) . ? C8 C7 1.386(6) . ? C12 H12A 0.86(6) . ? C12 H12B 1.06(6) . ? C12 C11 1.517(6) . ? C20 H20 0.93(5) . ? C20 C19 1.397(6) . ? C4 H4 0.77(7) . ? C4 C5 1.385(6) . ? C11 H11A 0.95(4) . ? C11 H11B 1.04(6) . ? C7 H7 1.04(5) . ? C7 C6 1.392(7) . ? C5 H5 0.91(6) . ? C5 C6 1.386(7) . ? C24 H24A 0.92(5) . ? C24 H24B 0.96(5) . ? C18 H18 0.94(6) . ? C18 C19 1.378(7) . ? C16 H16 0.90(5) . ? C19 H19 1.01(6) . ? C6 H6 1.06(5) . ? C21 H21A 0.91(5) . ? C21 H21B 0.98(5) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S2 Pb1 S1 96.25(3) . . ? O2 Pb1 S2 76.06(7) . . ? O2 Pb1 S1 76.92(7) . . ? O1 Pb1 S2 85.34(7) . . ? O1 Pb1 S1 79.53(7) . . ? O1 Pb1 O2 147.98(9) . . ? C13 S2 Pb1 98.16(13) . . ? C1 S1 Pb1 103.62(13) . . ? C11 O3 C10 111.1(3) . . ? C23 O4 C22 109.2(3) . . ? C14 O2 Pb1 132.8(3) . . ? C2 O1 Pb1 127.4(2) . . ? C1 N1 C2 124.8(3) . . ? C12 N3 C9 112.0(3) . . ? C1 N3 C9 125.1(3) . . ? C1 N3 C12 121.6(3) . . ? C14 N2 C13 123.9(3) . . ? C13 N4 C24 123.2(3) . . ? C13 N4 C21 125.1(3) . . ? C24 N4 C21 111.8(3) . . ? O2 C14 N2 126.8(4) . . ? O2 C14 C15 116.7(4) . . ? N2 C14 C15 116.4(4) . . ? O4 C23 H23A 104(3) . . ? O4 C23 H23B 111(3) . . ? O4 C23 C24 111.2(3) . . ? H23A C23 H23B 106(4) . . ? C24 C23 H23A 112(3) . . ? C24 C23 H23B 112(3) . . ? C20 C15 C14 120.5(4) . . ? C16 C15 C14 119.9(4) . . ? C16 C15 C20 119.5(4) . . ? N3 C9 H9A 108(3) . . ? N3 C9 H9B 115(3) . . ? N3 C9 C10 108.7(3) . . ? H9A C9 H9B 107(4) . . ? C10 C9 H9A 111(3) . . ? C10 C9 H9B 107(3) . . ? O3 C10 C9 111.0(3) . . ? O3 C10 H10A 109(3) . . ? O3 C10 H10B 108(3) . . ? C9 C10 H10A 106(3) . . ? C9 C10 H10B 113(3) . . ? H10A C10 H10B 110(4) . . ? O4 C22 H22A 112(3) . . ? O4 C22 H22B 108(3) . . ? O4 C22 C21 111.3(3) . . ? H22A C22 H22B 105(4) . . ? C21 C22 H22A 114(3) . . ? C21 C22 H22B 106(3) . . ? C18 C17 H17 122(3) . . ? C18 C17 C16 120.0(4) . . ? C16 C17 H17 118(3) . . ? N2 C13 S2 122.9(3) . . ? N4 C13 S2 119.8(3) . . ? N4 C13 N2 116.9(3) . . ? C8 C3 C4 119.1(4) . . ? C8 C3 C2 118.6(4) . . ? C4 C3 C2 122.3(4) . . ? C3 C8 H8 118(3) . . ? C7 C8 C3 120.5(4) . . ? C7 C8 H8 122(3) . . ? N3 C12 H12A 111(3) . . ? N3 C12 H12B 109(3) . . ? N3 C12 C11 109.0(3) . . ? H12A C12 H12B 107(5) . . ? C11 C12 H12A 111(4) . . ? C11 C12 H12B 110(3) . . ? C15 C20 H20 122(3) . . ? C19 C20 C15 119.5(4) . . ? C19 C20 H20 118(3) . . ? N1 C1 S1 124.0(3) . . ? N1 C1 N3 117.4(3) . . ? N3 C1 S1 118.2(3) . . ? C3 C4 H4 116(5) . . ? C5 C4 C3 120.1(4) . . ? C5 C4 H4 123(5) . . ? O3 C11 C12 111.2(4) . . ? O3 C11 H11A 105(3) . . ? O3 C11 H11B 110(3) . . ? C12 C11 H11A 109(3) . . ? C12 C11 H11B 112(3) . . ? H11A C11 H11B 109(4) . . ? C8 C7 H7 119(3) . . ? C8 C7 C6 120.1(4) . . ? C6 C7 H7 121(3) . . ? C4 C5 H5 121(4) . . ? C6 C5 C4 120.6(4) . . ? C6 C5 H5 118(4) . . ? N4 C24 C23 109.6(3) . . ? N4 C24 H24A 108(3) . . ? N4 C24 H24B 107(3) . . ? C23 C24 H24A 113(3) . . ? C23 C24 H24B 110(3) . . ? H24A C24 H24B 110(4) . . ? C17 C18 H18 117(4) . . ? C19 C18 C17 119.9(4) . . ? C19 C18 H18 123(4) . . ? O1 C2 N1 126.3(4) . . ? O1 C2 C3 118.1(3) . . ? N1 C2 C3 115.5(3) . . ? C15 C16 C17 120.5(4) . . ? C15 C16 H16 120(3) . . ? C17 C16 H16 120(3) . . ? C20 C19 H19 120(3) . . ? C18 C19 C20 120.5(4) . . ? C18 C19 H19 119(3) . . ? C7 C6 H6 117(3) . . ? C5 C6 C7 119.6(4) . . ? C5 C6 H6 123(3) . . ? N4 C21 C22 109.2(3) . . ? N4 C21 H21A 112(3) . . ? N4 C21 H21B 109(3) . . ? C22 C21 H21A 108(3) . . ? C22 C21 H21B 111(3) . . ? H21A C21 H21B 108(4) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Pb1 S2 C13 N2 -72.6(3) . . . . ? Pb1 S2 C13 N4 114.9(3) . . . . ? Pb1 S1 C1 N1 59.2(4) . . . . ? Pb1 S1 C1 N3 -128.4(3) . . . . ? Pb1 O2 C14 N2 -21.4(6) . . . . ? Pb1 O2 C14 C15 161.9(2) . . . . ? Pb1 O1 C2 N1 52.6(5) . . . . ? Pb1 O1 C2 C3 -131.0(3) . . . . ? O4 C23 C24 N4 57.3(4) . . . . ? O4 C22 C21 N4 -57.8(4) . . . . ? O2 C14 C15 C20 175.3(4) . . . . ? O2 C14 C15 C16 -3.2(5) . . . . ? N3 C9 C10 O3 -57.1(4) . . . . ? N3 C12 C11 O3 56.5(5) . . . . ? N2 C14 C15 C20 -1.7(5) . . . . ? N2 C14 C15 C16 179.7(4) . . . . ? C14 N2 C13 S2 39.9(5) . . . . ? C14 N2 C13 N4 -147.4(4) . . . . ? C14 C15 C20 C19 -177.6(4) . . . . ? C14 C15 C16 C17 177.3(4) . . . . ? C23 O4 C22 C21 61.5(4) . . . . ? C15 C20 C19 C18 -0.2(6) . . . . ? C9 N3 C12 C11 -55.7(5) . . . . ? C9 N3 C1 S1 -10.7(5) . . . . ? C9 N3 C1 N1 162.2(4) . . . . ? C10 O3 C11 C12 -59.2(5) . . . . ? C22 O4 C23 C24 -61.1(4) . . . . ? C17 C18 C19 C20 -0.2(7) . . . . ? C13 N2 C14 O2 19.8(6) . . . . ? C13 N2 C14 C15 -163.5(3) . . . . ? C13 N4 C24 C23 125.4(4) . . . . ? C13 N4 C21 C22 -125.2(4) . . . . ? C3 C8 C7 C6 1.1(6) . . . . ? C3 C4 C5 C6 0.8(6) . . . . ? C8 C3 C4 C5 -0.3(6) . . . . ? C8 C3 C2 O1 18.7(5) . . . . ? C8 C3 C2 N1 -164.6(4) . . . . ? C8 C7 C6 C5 -0.6(6) . . . . ? C12 N3 C9 C10 56.2(4) . . . . ? C12 N3 C1 S1 -176.1(3) . . . . ? C12 N3 C1 N1 -3.2(6) . . . . ? C20 C15 C16 C17 -1.3(6) . . . . ? C1 N1 C2 O1 -27.0(6) . . . . ? C1 N1 C2 C3 156.5(4) . . . . ? C1 N3 C9 C10 -110.4(4) . . . . ? C1 N3 C12 C11 111.4(4) . . . . ? C4 C3 C8 C7 -0.6(6) . . . . ? C4 C3 C2 O1 -162.8(4) . . . . ? C4 C3 C2 N1 13.9(5) . . . . ? C4 C5 C6 C7 -0.3(6) . . . . ? C11 O3 C10 C9 59.8(5) . . . . ? C24 N4 C13 S2 176.4(3) . . . . ? C24 N4 C13 N2 3.5(5) . . . . ? C24 N4 C21 C22 54.0(4) . . . . ? C18 C17 C16 C15 0.9(7) . . . . ? C2 N1 C1 S1 -40.4(6) . . . . ? C2 N1 C1 N3 147.2(4) . . . . ? C2 C3 C8 C7 178.0(4) . . . . ? C2 C3 C4 C5 -178.8(4) . . . . ? C16 C15 C20 C19 0.9(6) . . . . ? C16 C17 C18 C19 -0.1(7) . . . . ? C21 N4 C13 S2 -4.5(5) . . . . ? C21 N4 C13 N2 -177.4(3) . . . . ? C21 N4 C24 C23 -53.9(4) . . . . ? loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 -2 3831.58 114.13 0 0 -2 4192.21 114.07 0 0 -3 0.99 0.47 0 0 -3 1.2 0.45 0 0 -4 9.24 1.11 0 0 -4 9.7 1.07 0 0 -5 2.04 0.81 0 0 -5 2.24 0.8 0 0 -5 0.76 0.52 0 0 -6 69.93 3.69 0 0 -6 61.91 3.67 0 0 -7 0.26 0.6 0 0 -7 1.82 0.7 0 0 -7 2.67 0.78 0 0 -8 3829.03 103.1 0 0 8 3554.11 103.97 0 0 -8 3688.6 103.54 0 0 -9 1.95 0.85 0 0 -9 1.86 0.92 0 0 -9 1.32 0.87 0 0 -10 4187.75 113.92 0 0 10 4046.26 115.29 0 0 -11 0.83 0.73 0 0 11 2 1.1 0 0 -11 1.71 1.02 0 0 -12 812.07 27.45 0 0 12 856.39 29.49 0 0 -12 780.49 28.87 0 0 -12 772.49 27.95 0 0 -13 1.41 1.67 0 0 -13 4.5 1.67 0 0 -13 0.78 0.91 0 0 13 2.17 1.14 0 0 -14 198.36 11.96 0 0 -14 180.94 11.34 0 0 -14 174.58 9.46 0 0 -14 174.38 10.75 0 0 -15 4.97 2.13 0 0 -15 3.44 1.73 0 0 -15 0.6 1.77 0 0 -15 1.24 1.25 0 0 -15 4.02 2.17 0 0 -15 0.43 1.59 0 0 -15 1.1 2.02 0 0 -16 1546.62 55.74 0 0 -16 1591.56 54.09 0 0 -16 1614.43 55.4 0 0 -16 1599.38 54.92 0 0 -16 1604.26 53.77 0 0 -16 1403.5 54.07 0 0 -16 1545.72 56.78 0 0 -17 -0.61 1.66 0 0 -17 -0.69 2.05 0 0 17 1.6 1.45 0 0 -17 3.54 1.97 0 0 -17 1.02 1.6 0 0 -17 1.8 1.77 0 0 -17 -0.63 1.72 0 0 18 1453.2 51.74 0 0 -18 1442.28 53.49 0 0 -18 1341.95 52.24 0 0 -18 1349.78 51.9 0 0 -18 1471.62 51.23 0 0 -18 1453.19 54.47 0 0 -19 4.21 2.59 0 0 -19 4.06 2.13 0 0 19 1.13 1.4 0 0 -19 -0.57 1.69 0 0 -19 1.53 2.4 0 0 19 2.48 1.69 0 0 -19 1.39 2.32 0 0 -20 4191.56 134.4 0 0 -20 4351.08 132.66 0 0 20 4204.6 133.26 0 0 20 4353.71 132.7 0 0 -20 4218.33 135.99 0 0 -20 4411.04 135.05 0 0 -20 3907.95 133.9 0 0 -21 1.51 2.51 0 0 -21 2.35 2.13 0 0 21 2.37 1.87 0 0 21 1.34 1.49 0 0 -21 0.6 1.75 0 0 -21 0.73 1.81 0 0 -21 4.93 2.83 0 0 22 600.83 28.8 0 0 -22 569.44 28.98 0 0 22 627.69 27.95 0 0 -22 670.85 31.05 0 0 -22 665.17 28.21 0 0 -22 564.66 29.23 0 0 -22 664.3 29.73 0 0 -23 6.59 2.94 0 0 -23 4.31 2.88 0 0 23 0.56 1.08 0 0 -24 102.73 9.86 0 0 24 106 8.99 0 0 24 96.2 9.2 0 0 25 4.13 1.98 0 0 25 1.63 1.35 0 0 -25 1.15 1.81 0 0 26 435.11 19.05 0 0 -26 412.54 20.06 0 0 26 443.73 20.55 0 0 27 2.93 1.34 0 0 27 5.1 1.8 0 0 -27 -0.37 1.31 0 0 -28 431.5 17.65 0 0 28 517.66 19.39 0 0 29 -0.42 0.97 0 1 0 2.39 0.48 0 -1 0 1.16 0.39 0 1 -1 4945.13 126.84 0 -1 1 4301.76 125.64 0 -1 1 4809.89 125.85 0 1 -1 4923.08 126.66 0 1 1 4499.68 125.65 0 -1 -1 4433.01 126.52 0 1 1 3906.24 125.74 0 -1 2 275.4 8.63 0 1 2 262.98 8.57 0 1 -2 285.5 9.55 0 -1 3 31.68 1.91 0 1 -3 28.23 2.24 0 1 3 31.11 1.89 0 1 -4 12.64 0.74 0 -1 4 14.73 1.41 0 1 4 12.69 1.33 0 -1 -4 10.61 1.48 0 1 5 1252.45 35.04 0 1 -5 1270.23 33.32 0 -1 -5 1345.33 35.62 0 -1 5 1388.09 35.27 0 -1 -5 1068.09 33.14 0 1 6 147.54 6.39 0 -1 6 156.62 6.54 0 1 -6 149.63 5.06 0 -1 -6 143 6.51 0 1 -7 3765.55 105.42 0 1 7 4005.62 104.85 0 -1 7 3990.42 104.84 0 -1 -7 3971.23 104.97 0 1 -8 584.02 17.82 0 -1 -8 548.11 19.85 0 -1 8 618.89 20.11 0 1 -8 582.79 20.38 0 1 8 595.47 19.89 0 1 -9 3978.47 114.27 0 1 9 4109.59 116.92 0 -1 -9 4077.38 116.74 0 -1 9 4235.4 117.06 0 -1 10 194.03 9.9 0 -1 -10 202.59 9.64 0 -1 -10 196.83 9.7 0 1 10 218.17 10.17 0 1 -10 231.7 10.72 0 1 -10 195.4 8.05 0 1 -11 3185.09 91.28 0 1 11 2904.21 90.27 0 -1 11 2995.26 90.54 0 -1 -11 2957.21 91.21 0 1 -11 2905.23 87.25 0 -1 -11 2993.84 89.39 0 -1 -11 3079.71 90.14 0 -1 -12 324.98 15.07 0 -1 12 400.99 16.42 0 -1 -12 348.99 16.44 0 1 -12 371.35 16.39 0 1 12 374.88 16.14 0 1 -13 527.3 21.86 0 -1 -13 527.66 22.19 0 -1 -13 536.58 22.19 0 -1 -13 513.12 20.85 0 1 -13 531.26 22.15 0 -1 -14 59.91 6.34 0 -1 -14 58.5 6.44 0 -1 -14 62.66 6.28 0 1 -14 58.95 6.01 0 1 -14 53.69 5.96 0 -1 -14 71.44 6.82 0 1 -14 62.33 6.19 0 -1 -14 64.39 6.29 0 -1 -14 57.7 6.1 0 1 -14 56.83 6.73 0 -1 -14 70.62 6.01 0 1 -14 59.06 7.08 0 1 -14 61.49 6.43 0 -1 -15 505.98 23.29 0 -1 -15 497.04 22.08 0 -1 -15 491.19 22.75 0 1 -15 497.72 23.98 0 1 -15 475.69 24.45 0 -1 -15 534.15 23.12 0 1 -15 494.16 22.91 0 -1 -15 514.25 22.85 0 1 -15 518.02 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-25 7 2.57 1 1 25 11.54 2.85 1 1 25 14.09 3.33 -1 -1 -26 279.91 14.84 1 1 26 279.64 14.54 1 -1 26 300.95 15.25 1 1 26 283.17 14.86 1 1 27 9.62 2.38 -1 -1 -27 6.77 1.98 1 1 27 4.91 1.93 1 -1 27 9.63 2.46 1 -1 28 709.84 25.06 1 1 28 670.92 24.03 1 1 28 711.06 24.96 -1 -2 28 69.82 4.79 1 -2 -28 71.68 5.5 -1 2 28 75.4 5.28 -1 2 27 646.85 23.93 1 -2 -27 631.77 24.63 -1 2 27 586.21 22.84 -1 -2 27 601.99 23.1 1 -2 -26 2.26 1.68 1 -2 -26 0.48 1.76 -1 2 26 4.55 1.85 -1 -2 26 4.68 1.68 -1 2 26 7.15 1.97 -1 2 25 1232.8 44.52 1 -2 -25 1230.71 46.57 1 -2 -25 1296.32 45.21 -1 -2 25 1246.4 44.98 -1 2 25 1311.74 45.6 1 -2 -24 37.25 5.39 -1 2 24 32.49 5.05 1 -2 -24 30.4 5.46 -1 2 24 35.79 5 1 2 -24 18.06 4.52 -1 -2 24 33.88 5.01 1 -2 -23 841.15 36.2 1 -2 -23 919.03 36.5 1 2 -23 903.67 37.13 1 -2 -23 886.34 37.97 1 2 -23 835.2 37.06 1 -2 -22 101.18 9.72 1 2 -22 95.31 9.67 1 -2 -22 102.37 10.12 1 2 -22 100.37 10.62 1 -2 -22 95.51 10.22 1 -2 -21 208.59 14.55 1 -2 -21 175.41 14.33 1 2 -21 166.17 14.27 1 -2 -21 189.42 14.05 -1 2 21 176.86 13.05 1 2 -21 174.84 14.54 1 2 -21 190.79 14.21 -1 -2 21 175.82 13.1 1 2 -20 148.49 13.63 1 2 -20 155.47 12.71 1 2 -20 154.47 11.51 1 -2 -20 160.86 12.83 1 -2 -20 158.43 12.7 1 -2 -20 172.09 13.93 -1 -2 20 151.24 11.9 1 2 -20 143.98 12.96 1 -2 -20 148.81 12.5 1 2 -20 132.93 11.51 -1 2 20 146.59 11.6 1 -2 -20 148.65 12.05 1 2 -19 127.17 10.9 1 2 -19 140.54 10.83 -1 -2 19 126.97 10.62 1 2 -19 130.92 11.27 1 -2 -19 123.3 10.78 1 -2 -19 122.68 11.01 -1 2 19 129.87 10.66 1 2 -19 137.25 10.81 1 -2 -19 137.23 11.61 1 -2 -19 113.64 9.8 1 -2 -19 122.04 11.15 1 2 -19 129.56 12.12 1 2 -19 131.84 12.61 1 -2 -19 135.42 11.67 1 -2 -19 122.02 11.12 1 2 -18 11.27 3.09 -1 -2 18 13.73 3.32 1 -2 -18 5.3 2.87 1 -2 -18 12.28 3.68 1 -2 -18 7.18 2.92 1 2 -18 11.68 4.06 1 -2 -18 8.74 2.87 1 2 -18 15.76 3.59 -1 2 18 9.6 2.68 1 2 -18 13.6 3.54 1 -2 -18 7.52 3.06 1 2 -18 11.55 3.11 1 -2 -18 9.34 3.41 1 -2 -18 7.31 2.46 1 2 -17 2051.7 67.69 1 -2 -17 2001.04 69.05 1 -2 -17 2083.1 68.56 1 2 -17 2004.9 68.05 1 2 -17 1943.44 72.1 1 -2 -17 1944.51 69.59 1 -2 -17 1971.92 69.32 1 2 -17 2021.17 67.8 1 -2 -17 2032.92 67.41 1 -2 -17 1968.98 69.05 1 -2 -17 1978.35 68.92 1 2 -17 2039.63 69.09 1 -2 -16 1.2 1.89 1 -2 -16 2.35 1.96 1 -2 -16 1.58 1.31 1 2 -16 2.1 1.31 1 2 -16 0.52 1.42 1 -2 -16 0.58 1.72 1 -2 -16 1.69 1.54 1 2 -16 0.99 1.24 1 2 -16 4.13 2.07 1 -2 -16 1.15 1.92 1 2 -16 1.68 1.65 1 2 -16 0.76 2.24 1 -2 -16 1.48 1.35 1 2 -15 2175.38 69.3 1 2 -15 2010.92 67.89 1 -2 -15 2039.41 69.56 1 2 -15 2089.09 67.92 1 -2 -15 2058.06 69.29 1 2 -15 2055.84 67.96 1 -2 -15 2011.33 67.6 1 2 -15 1865.14 71.38 1 -2 -15 2134.8 69.49 1 -2 -15 2056.2 69.51 1 -2 -15 2115.9 66.73 1 -2 -15 2112.98 69.14 1 -2 -15 2088.01 68.34 1 2 -15 2037.4 68.13 1 -2 -14 16.17 3.58 -1 -2 14 15.34 3.05 1 -2 -14 10.33 2.94 1 -2 -14 16.6 3.46 1 2 -14 12.6 2.97 1 2 -14 14.78 3.01 1 -2 -14 18.3 3.11 1 2 -14 15.24 3.21 1 2 -14 12.63 2.96 -1 2 14 16.04 3.23 1 2 -14 13.11 3.74 1 -2 -14 17.08 3.26 1 2 -14 14.88 3.34 1 -2 -14 13.31 3.27 1 -2 -14 18.11 3.7 1 -2 -14 15.43 3.05 -1 2 13 254.75 12.96 1 -2 -13 247.4 13.2 1 -2 -13 253.67 13.24 1 2 -13 246.42 13.06 1 -2 -13 232.52 13.48 1 -2 -13 241.44 13.82 1 -2 -13 269.18 13.54 1 -2 -13 225.6 13.61 1 2 -13 225.93 15.04 -1 -2 13 259.91 13.12 1 -2 -13 250.31 13.9 1 -2 -13 243.13 12.51 1 2 -13 235.18 13.11 1 2 -12 581.49 23.13 -1 -2 12 601.78 23.08 -1 2 12 563.33 22.67 1 -2 -12 547.79 23.13 1 -2 -12 617.44 23.53 1 -2 -12 621.71 23.13 -1 2 11 464.09 18.55 1 -2 -11 462.63 18.74 1 -2 -11 451.72 18.88 1 -2 -11 443.3 18.44 1 2 -11 466.76 19.89 -1 -2 11 465.45 18.49 1 2 -11 451.78 18.66 1 -2 -10 52.74 4.71 1 -2 -10 55.73 5 1 2 -10 52.1 5.05 1 -2 -10 61.47 4.98 1 2 -10 59.89 4.9 -1 2 10 54.28 4.56 -1 -2 10 56.21 4.67 -1 2 9 2691.44 78.51 1 -2 -9 2517.74 79.18 1 2 -9 2573.96 78.67 1 -2 -9 2566.27 78.58 -1 -2 9 2649.55 78.47 1 -2 -8 5.52 1.55 -1 -2 8 10.68 1.82 1 -2 -8 7.59 1.19 1 2 -8 7.8 1.71 1 -2 -8 10.15 1.75 -1 2 8 10.6 1.77 -1 2 7 5085.05 144.39 1 -2 -7 5397.11 145.9 1 2 -7 5211.52 144.67 -1 -2 7 4996.96 144.38 1 -2 -7 5234.45 144.71 1 2 -7 4843.78 146.21 -1 -2 6 0.29 0.46 1 -2 -6 1.64 0.97 1 2 -6 2.12 1.17 -1 2 6 2.04 0.79 1 2 -6 0.9 0.94 1 -2 -6 2.9 0.95 -1 -2 5 3543.91 102.26 1 -2 -5 3361.24 102.2 1 2 -5 3691.54 104.46 1 2 -5 3450.33 103.86 -1 2 5 3569.52 102.24 1 2 -5 3648.17 102.45 1 -2 -4 615.79 19.63 1 2 -4 628.32 21.17 -1 2 4 620.45 19.53 -1 -2 4 584.8 19.45 1 2 -4 655.93 21.61 1 2 -4 646.51 19.72 1 2 -3 18.95 1.51 -1 2 3 16.47 1.14 -1 -2 3 16.32 0.87 1 -2 -3 15.93 1.93 1 2 -3 15.41 1.95 -1 2 2 351.12 11.68 1 -2 -2 370.34 12.93 1 2 -2 379.3 13.33 1 2 -2 393.45 13.42 -1 -2 2 351.1 11.3 1 2 -2 369.3 11.48 1 -2 -2 361.7 11.42 1 -2 -1 374.58 11.94 1 2 -1 363.61 11.94 1 -2 -1 350.39 13.28 1 2 0 559.65 16.7 1 -2 0 557.92 16.67 -1 -2 0 592.31 18.06 1 2 1 458.08 13.86 -1 -2 -1 471.82 15.34 -1 2 -1 496.9 14.98 -1 2 -1 485.03 15.87 1 -2 1 442.79 13.86 1 -2 2 239.5 8.07 1 2 2 233.18 8.04 -1 2 -2 255.43 8.9 -1 -2 -2 246.41 9.39 -1 2 -2 263.34 9.97 1 -2 3 3038.49 87.06 -1 2 -3 3031.17 87.8 -1 -2 -3 3042.68 88.53 1 2 3 2962.68 87.03 -1 2 -3 3125.31 89.25 1 2 4 300.86 10.79 1 -2 4 324.25 10.95 -1 -2 -4 308.54 11.98 -1 2 -4 318.47 11.55 -1 2 -4 308.51 12.45 -1 2 -5 1203.04 37.28 1 -2 5 1144.23 35.12 -1 2 -5 1194.51 33.8 1 -2 6 2.86 0.99 1 2 6 5.48 1.16 -1 2 -6 5.35 1.51 -1 2 -6 5.36 0.7 -1 2 -7 300.71 13.85 1 -2 7 285.02 11.38 1 2 7 297.06 11.48 -1 -2 -7 264.29 12.55 1 -2 8 275.91 11.37 1 2 8 269.4 11.26 -1 -2 -8 258.89 11.98 1 2 9 2586.7 80.98 1 -2 9 2775.77 81.34 -1 -2 -9 2766.55 82.48 1 -2 10 27.38 3.28 -1 -2 -10 24.02 3.35 1 2 10 29.67 3.27 -1 2 -10 29.85 3.9 1 2 11 3172.61 94.16 -1 -2 -11 3101.14 95.14 1 -2 11 3036.95 94.08 -1 2 -11 3137.52 96.24 1 -2 12 41.2 4.45 -1 -2 -12 42.13 4.76 1 2 12 48.24 4.73 -1 2 -12 50.54 5.51 -1 -2 -12 32.63 4.56 -1 -2 -13 1230.55 44.2 -1 -2 -13 1149.63 43.58 -1 2 -13 1296.76 44.5 1 2 13 1324.16 42.68 -1 2 -13 1192.76 45.15 -1 -2 -13 1169.84 43.79 1 -2 13 1187.74 42.2 -1 -2 -13 1228.48 43.15 -1 -2 -13 1220.86 44.31 -1 2 -13 1253.17 43.89 -1 -2 -13 1341.58 44.81 1 -2 14 7.52 2.18 -1 2 -14 4.28 1.91 -1 -2 -14 4.08 2.13 -1 -2 -14 1.96 1.55 -1 -2 -14 1.35 1.23 1 2 14 4.16 1.54 -1 -2 -14 3.16 1.94 -1 -2 -14 4.13 2.23 -1 -2 -14 2.47 1.59 -1 2 -14 2.31 2.13 -1 2 -14 1.76 1.6 -1 2 -14 4.41 2.18 -1 -2 -14 7.96 2.66 -1 2 -14 3.67 2.19 1 -2 15 381.62 18.06 -1 2 -15 354.12 18.63 -1 -2 -15 351.99 18.32 -1 2 -15 364.53 17.77 -1 -2 -15 376.19 19.41 1 2 15 380.89 18.58 -1 -2 -15 386.46 19.62 -1 2 -15 318.69 19.05 -1 -2 -15 356.39 18.83 1 2 15 343.32 17.5 -1 2 -15 327.17 19.19 -1 -2 -15 372.25 17.62 -1 2 -15 342.89 18.32 -1 -2 -15 354.82 19.11 -1 -2 -15 351.61 18.43 -1 -2 -15 365.93 18.13 -1 2 -15 395.18 19.86 -1 2 -16 82.54 8.78 -1 -2 -16 79 7.62 -1 -2 -16 74.17 7.97 -1 -2 -16 69.05 7.63 -1 2 -16 64.61 7.94 -1 -2 -16 67.11 7.69 -1 2 -16 69.67 7.73 -1 -2 -16 78.23 7.71 -1 2 -16 69.45 6.97 1 2 16 77.46 7.45 -1 2 -16 68.43 7.35 -1 -2 -16 81.31 7.25 -1 -2 -16 73.93 7.62 -1 2 -16 71.16 7.87 1 2 16 67.38 7.24 1 -2 16 72.77 7.27 -1 2 -17 225.51 14.77 1 -2 17 224.15 14.19 -1 -2 -17 238.95 14.96 -1 -2 -17 246.03 15.89 1 2 17 254.35 14.86 -1 -2 -17 241.34 14.69 -1 2 -17 264.31 16.8 -1 -2 -17 248.29 16.04 -1 -2 -17 234.14 15.89 -1 -2 -17 252.9 14.16 -1 -2 -17 247.96 15.3 1 2 17 234.2 14.83 -1 2 -17 236.42 15.43 -1 2 -17 237.05 14.16 -1 2 -17 241.34 16.27 -1 2 -17 221.44 15.04 -1 -2 -17 241.87 15.7 -1 -2 -18 32.29 5.6 -1 -2 -18 44.07 6.61 -1 2 -18 42.86 6.45 1 2 18 38.11 5.69 -1 -2 -18 38.15 6.21 -1 -2 -18 34.24 5.47 -1 2 -18 36.22 6.38 -1 -2 -18 26.99 4.81 -1 2 -18 36.94 5.63 -1 2 -18 31.9 5.94 -1 -2 -18 39.26 5.85 1 -2 18 34.06 5.47 1 2 18 45.33 6.04 1 -2 19 1478.28 54.32 1 2 19 1570.48 54.73 -1 -2 -19 1544.42 56.3 -1 2 -19 1423.51 54.95 -1 2 -19 1512.34 56.6 -1 -2 -19 1443.38 53.77 -1 2 -19 1561.74 56.84 -1 -2 -19 1437.09 54.85 -1 -2 -19 1499.44 56.15 -1 -2 -19 1497.77 56.59 -1 -2 -19 1546.64 54.48 -1 2 -19 1563.01 56.61 -1 -2 -20 46.58 6.89 -1 2 -20 43.62 6.82 -1 -2 -20 48.86 6.94 -1 2 -20 40.97 6.35 1 -2 20 48.11 6.42 -1 -2 -20 39.91 5.94 -1 -2 -20 37.37 6.18 1 2 20 52.54 6.61 -1 2 -20 46.71 7.08 -1 -2 -21 619.87 28.83 1 -2 21 547.92 25.86 -1 -2 -21 531.9 26.68 1 2 21 565.96 25.66 -1 2 -21 546.87 26.82 1 2 21 554.41 26 -1 -2 -21 540.5 26.9 -1 -2 -21 563.41 27.54 -1 2 -21 484.25 25.93 -1 2 -21 547.9 26.92 1 -2 21 540.3 25.96 -1 2 -22 31.21 5.35 -1 2 -22 29.3 5.32 1 2 22 15.12 3.83 -1 -2 -22 22.97 4.8 -1 -2 -22 26.2 5.33 1 -2 22 25.47 4.76 -1 -2 -22 24.97 5.16 -1 2 -23 34.42 5.44 -1 -2 -23 40.86 6.22 1 2 23 42.6 5.74 -1 2 -23 32.57 5.59 -1 -2 -23 42.7 6.39 1 -2 23 44.13 5.8 -1 -2 -24 67.17 7.5 -1 2 -24 63.05 6.93 1 -2 24 67.03 7.03 1 2 24 65.71 6.87 1 2 24 64.18 6.98 -1 -2 -24 65.37 7.53 -1 -2 -25 89.44 8.2 1 2 25 94.66 7.69 1 -2 25 86.18 7.56 1 2 25 92.82 7.97 -1 -2 -25 92.32 8.23 1 2 26 14.95 2.85 1 -2 26 13.29 2.72 1 2 26 12.19 2.86 -1 -2 -26 11.48 2.84 1 -2 27 586.67 22.3 1 2 27 580.5 21.92 1 2 27 610.79 22.84 -1 -2 -27 594.73 22.56 1 2 28 1.33 1.07 -1 3 27 197.54 10.18 1 -3 -27 214.26 10.91 1 -3 -26 591.93 21.85 1 -3 -26 597.27 23.31 -1 -3 26 500.4 19.83 -1 3 26 579.3 22.12 1 3 -26 471.35 20.38 1 -3 -25 85.81 7.29 -1 -3 25 73.65 6.2 -1 3 25 81.26 7.1 1 -3 -25 88.5 7.96 1 3 -25 75.08 6.4 -1 3 25 73.91 6.01 1 3 -24 743.38 29.73 -1 3 24 748.64 30.38 1 -3 -24 804.31 31.12 -1 3 24 731.1 28.65 -1 -3 24 721.67 28.99 1 -3 -24 779.38 32.15 1 -3 -23 80.18 8.04 -1 -3 23 64.31 6.71 1 3 -23 77.57 7.7 -1 3 23 66.48 7.32 -1 3 23 64.07 6.52 1 -3 -23 61.7 7.66 -1 3 22 138.41 10.26 -1 -3 22 161 11.19 -1 3 22 130.45 10.9 1 -3 -22 137.71 11.36 1 3 -21 99.68 9.49 1 3 -21 104.54 9.23 -1 3 21 97.68 9.11 1 -3 -21 81.8 8.7 1 -3 -21 95.25 9.59 1 -3 -20 130.54 11.75 1 -3 -20 128.55 11.04 -1 3 20 134.81 11.24 1 3 -20 120.54 12.05 1 3 -20 134.06 11.26 1 -3 -20 146.84 12.09 1 3 -20 113.18 11.85 1 3 -20 137.2 11.01 -1 3 19 252.75 16.13 1 -3 -19 272.22 16.59 1 -3 -19 256.19 17.16 1 -3 -19 266.59 15.03 1 3 -19 240.67 15.76 1 3 -19 247.03 18.14 1 -3 -19 261.22 17.29 -1 -3 19 248.86 15.34 1 3 -19 275.72 16.72 1 3 -19 219.65 16.94 1 -3 -18 1467.21 54.21 1 -3 -18 1525.18 56.1 1 3 -18 1490.93 58.68 1 3 -18 1588.74 54.92 1 -3 -18 1435.22 54.09 1 -3 -18 1491.47 52.66 1 3 -18 1436.79 57.06 -1 -3 18 1468.63 53.13 1 -3 -18 1526.29 56.42 1 3 -18 1532.63 54.73 1 3 -17 8.4 3.62 1 3 -17 2.33 2.12 1 3 -17 4.74 2.29 1 -3 -17 5.69 2.45 1 3 -17 6 2.02 1 -3 -17 7.02 3.1 -1 3 17 4.59 1.97 1 -3 -17 9.48 3.37 1 -3 -17 4.78 2.85 -1 -3 17 7.84 2.47 1 3 -17 5.4 2.41 1 -3 -17 1.81 1.78 1 -3 -17 4.74 2.29 1 -3 -17 7.71 2.38 1 3 -16 2630.82 85.26 -1 3 16 2474.06 82.58 1 3 -16 2426.77 88.45 -1 3 16 2528.27 81.86 1 -3 -16 2666.32 84.76 1 -3 -16 2525.03 83.41 1 3 -16 2521.25 87.53 1 3 -16 2562.76 84.78 1 3 -16 2647.75 84.68 1 -3 -16 2607 83.58 -1 -3 16 2601.45 83.1 1 -3 -16 2766.56 85.51 1 3 -16 2428.31 82.93 1 -3 -16 2741.53 87.1 1 -3 -16 2682.54 85.89 1 3 -15 167.33 13.02 1 3 -15 160.44 11.74 1 -3 -15 156.71 11.31 1 3 -15 164.77 11.1 -1 3 15 180.67 11.16 -1 -3 15 165.36 10.9 1 -3 -15 147.07 11.96 1 3 -15 158.62 11.33 -1 3 15 174.48 10.95 1 -3 -15 185.55 11.66 1 -3 -15 188.45 12.82 1 -3 -15 177.54 12.39 1 -3 -15 188.87 11.88 1 -3 -15 166.59 11.82 1 3 -15 162.27 13.66 1 3 -15 161.29 11.79 1 -3 -14 1160.48 43.76 -1 3 14 1261.45 43.37 1 -3 -14 1349.55 46.55 1 -3 -14 1242.84 44.11 1 -3 -14 1218.09 45.02 1 3 -14 1196.66 43.29 1 -3 -14 1298.72 45.4 1 3 -14 1138.73 47.55 1 -3 -14 1301.32 44.06 1 3 -14 1228.4 45.08 1 3 -14 1224.17 45.11 1 3 -14 1218.31 46.9 1 3 -13 631.43 30.2 1 3 -13 698.04 26.83 1 -3 -13 693.31 28.62 1 -3 -13 688.85 28.22 1 -3 -13 667.64 26.6 1 -3 -13 719.5 28.54 1 3 -13 706.07 28.61 1 -3 -13 704.49 27.74 1 3 -13 668.58 28.18 1 3 -13 668.46 29.52 1 3 -12 189.2 11.73 1 3 -12 184.57 12.19 1 -3 -12 186.81 11.39 1 -3 -12 175.71 11.38 1 3 -12 182.8 10.37 1 -3 -12 206.7 11.69 1 3 -12 172.3 11.37 1 -3 -12 168.43 10.07 1 3 -12 162.73 12.48 1 -3 -12 160.67 11.35 1 -3 -12 182.95 11.42 1 3 -12 174.9 11.66 1 3 -11 671.19 26.69 1 -3 -11 677.2 26.16 1 3 -11 682.48 27.15 1 -3 -11 701.2 26.73 1 -3 -11 641.26 24.68 1 3 -11 598.04 27.67 1 -3 -11 607.08 26.32 1 3 -11 623.5 24.52 1 -3 -11 743.47 27.41 1 3 -11 693.69 27.67 -1 3 10 228.69 11.05 1 -3 -10 250.23 13.05 1 -3 -10 249.63 12.83 1 -3 -10 236.44 11.46 1 -3 -10 242.91 11.97 -1 -3 10 237.79 11.21 1 3 -10 254.8 13.61 1 -3 -10 248.49 12.98 1 3 -10 263.11 13.81 1 3 -10 238.39 11.47 1 -3 -9 541.96 21.75 -1 -3 9 545.18 19.81 1 3 -9 533.44 22.31 1 3 -9 522.65 19.88 1 -3 -9 565.53 22.09 1 3 -9 563.94 22.78 1 -3 -9 551.71 21.15 -1 3 9 569.81 19.99 1 -3 -9 514.23 19.83 1 3 -8 2662.21 81.09 1 3 -8 2476.35 79.95 1 -3 -8 2520.42 77.07 1 -3 -8 2663.56 79.85 1 -3 -8 2633.41 78.97 -1 -3 8 2451.04 76.99 1 -3 -8 2826.33 80 -1 3 8 2544.46 77.06 1 3 -8 2586.04 77.2 1 3 -7 705.16 25.36 1 3 -7 699.09 25.63 -1 3 7 642.35 22.29 -1 -3 7 677.29 22.5 1 -3 -7 652.84 24.62 1 -3 -7 685.33 22.65 1 3 -7 673.83 22.62 1 -3 -7 686.95 24.99 1 -3 -6 2769.46 81.27 1 3 -6 2785.11 82.1 -1 3 6 2602.11 78.12 1 3 -6 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1491.3 45.51 1 3 8 1391.45 45.25 -1 3 -8 1439.46 47.51 -1 3 -8 1532.15 49.16 1 -3 9 198.88 9.65 1 3 9 204.14 9.65 -1 3 -9 206.9 12.22 -1 3 -9 199.06 11.1 -1 -3 -10 1807.17 57.36 -1 3 -10 1758.41 57.46 1 3 10 1660.35 54.48 -1 3 -10 1674.54 58.03 1 -3 10 1792.44 54.88 -1 -3 -11 3.33 1.8 -1 -3 -11 4.17 1.86 -1 -3 -11 5.31 2.03 -1 -3 -11 2.58 1.73 -1 3 -11 1.73 1.68 -1 -3 -11 3.68 1.59 1 3 11 6.35 1.82 1 -3 11 6.73 1.87 -1 3 -11 3.99 1.53 -1 3 -11 6.45 2.29 -1 3 -11 2.56 1.71 -1 -3 -11 4.69 2.07 1 3 11 4.02 1.73 1 3 12 1864.5 61.53 -1 -3 -12 1928.95 62.36 1 3 12 1868.61 61 -1 -3 -12 1993.06 61.06 -1 3 -12 1867.04 60.54 -1 3 -12 1849.94 64.13 -1 -3 -12 1962.18 62.48 -1 -3 -12 1955.39 63.36 -1 3 -12 1693.7 62.46 -1 -3 -12 1809.55 63.07 1 3 12 1797.56 59.6 -1 3 -12 1847.95 62.33 -1 -3 -12 1851.18 62.54 1 -3 12 1923.84 60.11 -1 3 -13 73.51 7.84 -1 -3 -13 81.87 7.68 -1 -3 -13 88.1 8.12 -1 -3 -13 90.66 7.81 -1 -3 -13 82.88 7.92 -1 3 -13 84.44 7.11 -1 3 -13 81.62 8.21 -1 3 -13 66.6 7.4 -1 -3 -13 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7.26 2.92 8 2 20 1.72 1.36 8 -2 20 2.15 1.52 -8 -2 -21 68.99 6.95 8 2 21 76.05 6.52 8 -2 21 81.78 6.68 -8 2 -21 75.92 7.38 -8 -2 -22 473.54 20.57 8 2 22 508.05 19.95 8 -2 22 486.69 19.75 8 2 22 510.43 20.56 -8 2 -22 494.52 21.39 -8 -2 -22 491.45 21.46 8 2 23 4.22 1.57 8 2 23 6.07 1.8 8 -2 23 3.43 1.47 8 2 24 658.56 22.78 -8 3 24 47.29 4.41 8 3 -24 66.42 5.34 8 -3 -23 274.75 12.69 8 3 -23 282.29 14.17 8 -3 -22 54.64 5.28 8 3 -22 64.15 5.61 8 -3 -22 59.85 5.7 8 -3 -22 52.33 5.71 8 3 -22 53.65 6.06 8 -3 -21 767.79 29.41 8 3 -21 761.95 29.61 8 -3 -21 738.06 28.51 8 -3 -21 846.91 30.9 8 -3 -21 808.04 31.11 8 3 -21 740.27 31.32 8 -3 -20 1.8 1.51 8 3 -20 6.48 2.53 8 3 -20 4.87 2.02 8 -3 -20 6.14 1.94 8 -3 -20 8.59 2.81 8 -3 -20 7.41 2.57 8 3 -20 3.54 2.18 8 -3 -19 429.22 21.21 8 3 -19 492.64 22.41 8 3 -19 448.43 20.95 8 -3 -19 484.7 21.53 8 -3 -19 491.29 22.99 8 -3 -19 509.88 23.64 8 -3 -18 55.27 6.54 8 3 -18 47.46 6.07 8 3 -18 51.86 6.11 8 -3 -18 49.32 5.91 8 -3 -18 60.78 7.25 8 -3 -17 64.69 7.56 8 3 -17 61.2 7.2 8 3 -17 65.42 7.08 8 -3 -17 76.54 7.67 8 -3 -17 53.51 6.47 8 -3 -17 66.03 7.99 8 3 -16 56.95 6.6 8 3 -16 54.2 6.25 8 3 -16 57.59 6.52 8 -3 -16 51.89 6.23 8 -3 -16 54.13 6.47 8 -3 -16 56.6 7.23 8 3 -15 350.52 18.82 8 3 -15 338.53 18.4 8 3 -15 347.73 18.47 8 -3 -15 377.46 19.08 8 -3 -15 400.15 22.01 8 -3 -15 368.9 21.15 8 -3 -15 370.08 19.13 8 3 -15 331.33 19.91 8 -3 -15 375.98 20.61 8 3 -14 9.98 3.57 8 3 -14 16.74 3.85 -8 -3 14 13.87 3.57 8 3 -14 16.6 3.72 8 -3 -14 16.49 4.35 8 -3 -14 15.11 4.55 8 3 -14 14.56 3.47 8 -3 -14 13.97 3.3 -8 3 14 15.97 3.75 8 -3 -14 12.18 3.34 8 3 -14 16.3 4.02 8 -3 -14 17.42 4.1 8 3 -13 1143.17 46.56 8 3 -13 1219.24 44.94 -8 3 13 1251.01 45.27 8 3 -13 1231.47 44.83 8 -3 -13 1299.35 48.67 8 3 -13 1129.64 43.54 8 -3 -13 1101.77 43.33 8 -3 -13 1265.49 47.93 8 -3 -13 1244.29 44.68 8 3 -13 1143.86 45.85 8 -3 -13 1175.06 46.09 -8 -3 13 1128.08 44.68 8 3 -12 19.39 4.25 -8 3 12 25.85 4.79 8 3 -12 24.14 4.74 8 -3 -12 24.64 5.22 8 3 -12 18.7 4.15 8 -3 -12 17.82 4.66 8 3 -12 18.41 3.79 8 -3 -12 20.38 3.9 8 -3 -12 16.96 3.89 8 3 -12 15.32 4.35 8 3 -12 25.05 4.9 8 -3 -12 22.16 4.62 8 3 -11 1513.37 55.86 8 3 -11 1476.89 53.48 8 -3 -11 1377.15 52.63 8 3 -11 1462.91 53.41 -8 3 11 1560.85 54.66 8 -3 -11 1497.37 54.9 8 3 -11 1505.42 53.72 8 -3 -11 1583.84 57.38 8 3 -11 1495.89 52.53 8 -3 -11 1462.1 52.25 8 -3 -11 1512.74 55.97 8 -3 -11 1558.24 53.34 8 3 -11 1471.49 54.58 8 -3 -11 1512.53 54.86 8 3 -10 116.77 10.77 8 3 -10 118.85 9.99 8 -3 -10 102.86 9.15 -8 3 10 112.31 9.94 8 3 -10 109.09 9.46 8 -3 -10 111.22 10.24 8 3 -10 126.97 10.3 8 -3 -10 146.14 11.49 8 3 -10 120.36 9.45 8 -3 -10 115.09 9.25 8 -3 -10 114.74 10.64 8 -3 -10 127.74 9.96 8 -3 -10 114.3 10.13 8 3 -10 113.19 10.3 8 3 -9 914.54 38.65 8 3 -9 967.06 37.77 -8 3 9 1022.55 38.93 8 -3 -9 971.25 38.91 8 3 -9 969.34 37.98 8 -3 -9 940.87 36.9 8 3 -9 880.05 36.61 8 -3 -9 938.19 39.71 8 -3 -9 1028.73 39.9 8 3 -9 911.07 36.13 8 -3 -9 985 36.68 8 -3 -9 990.5 39.64 8 -3 -9 989.07 37.3 8 -3 -9 956.91 38.27 8 3 -9 986.13 38.91 8 -3 -9 943.53 37.34 8 3 -8 163.33 12.62 8 3 -8 169.41 12.11 -8 3 8 184.43 12.93 8 -3 -8 175.22 12.85 8 3 -8 167.06 12.13 8 -3 -8 151.48 11.09 8 3 -8 166.93 11.57 8 -3 -8 179.44 13.33 8 -3 -8 175.56 12.93 8 3 -8 165.87 11.1 8 -3 -8 163.38 11.14 8 -3 -8 185 13.38 8 -3 -8 163.13 11.4 8 -3 -8 175.08 12.35 8 -3 -8 172.19 12.13 8 3 -8 171.23 12.46 8 3 -7 12.82 3.6 8 3 -7 6.05 2.54 8 -3 -7 4.8 2.33 8 3 -7 25.18 4.44 8 -3 -7 9.37 3.35 8 -3 -7 12.27 3.53 8 -3 -7 10.93 3.37 8 3 -7 8.43 2.71 8 -3 -7 10.22 2.77 8 3 -7 10.01 2.69 8 -3 -7 6.96 2.32 8 -3 -7 11.9 3.13 8 -3 -7 7.83 2.73 8 3 -7 6.14 2.26 8 -3 -7 25.05 4.44 8 3 -6 46.31 6.4 8 3 -6 54.49 6.44 8 -3 -6 55.37 6.78 8 3 -6 48.16 6.13 8 -3 -6 42.87 6.28 8 -3 -6 45.5 6.36 8 3 -6 50.16 5.93 8 -3 -6 48.41 5.65 8 3 -6 56.06 5.83 8 -3 -6 59.12 6.12 8 -3 -6 57.04 6.26 8 -3 -6 54.81 6.53 8 -3 -6 61.89 6.96 8 3 -6 43.31 5.86 8 3 -5 746.86 31.75 8 3 -5 765.73 31.36 8 -3 -5 704.37 31.5 8 3 -5 769.16 31.21 8 -3 -5 749.57 31.97 8 -3 -5 782.17 32.5 8 3 -5 750.88 29.9 8 -3 -5 733.7 29.71 8 3 -5 731.43 29.17 8 -3 -5 764.88 29.86 8 -3 -5 803.94 30.8 8 -3 -5 747.08 30.89 8 -3 -5 768.33 31.88 8 3 -5 743.29 30.77 8 3 -4 10.23 3.13 8 3 -4 13.66 3.54 8 3 -4 11.72 2.72 8 -3 -4 8.02 2.34 8 -3 -4 9.5 2.76 8 -3 -4 12.09 3.12 8 -3 -4 7.74 2.77 8 3 -4 7.42 2.77 8 -3 -4 13.71 3.38 -8 -3 3 1195.04 46.29 8 -3 -3 1364.7 49.11 8 -3 -3 1331.21 47.01 8 -3 -3 1410.57 50.16 8 3 -3 1405.65 47.13 8 -3 -3 1311.98 46.57 8 -3 -3 1395.84 47.81 8 -3 -3 1289.2 47.73 8 -3 -3 1467.1 49.96 -8 -3 2 100 8.8 8 -3 -2 151.29 10.94 8 3 -2 124.71 9.67 8 -3 -2 140.32 10.84 8 -3 -2 131.93 9.55 8 -3 -2 144.27 11.08 -8 3 2 122.41 10.77 8 3 -2 126.05 9.12 8 -3 -2 134.34 9.35 8 -3 -2 126.59 9.5 8 -3 -2 135.94 10.48 -8 -3 1 1413.18 54.34 8 -3 -1 1695.7 56.66 8 3 -1 1524.21 53.71 8 3 -1 1645.28 55.25 8 -3 -1 1742.2 57.23 8 -3 -1 1716.31 57.8 8 -3 -1 1634.76 54.35 -8 3 1 1502.91 56.93 8 -3 -1 1625.34 55.01 8 3 -1 1631.45 54.03 8 -3 -1 1551.33 53.64 8 3 0 325.71 16.18 -8 -3 0 284.03 16.51 8 -3 0 312.16 17.06 8 3 0 300.19 16.33 8 -3 0 339.38 17.87 8 -3 0 322.8 18 8 -3 0 329.96 16.24 -8 3 0 301.73 18.06 8 -3 0 317.59 16.6 8 3 0 319.05 15.88 8 -3 0 310.87 15.75 8 3 1 24.1 4 -8 -3 -1 24.66 4.58 8 -3 1 35.8 5.07 8 3 1 27.57 4.34 8 -3 1 28.11 4.74 8 -3 1 41.85 5.82 -8 3 -1 29.11 5.03 8 -3 1 30.12 4.66 8 3 1 31.31 4.24 8 -3 1 43.63 5.66 8 -3 1 28.81 4.12 8 -3 1 26.63 4.23 -8 -3 -2 130.07 10.78 8 -3 2 140.63 10.31 8 3 2 130.52 9.84 8 -3 2 144.03 10.73 8 3 2 136.25 10.04 8 -3 2 141.49 11.25 8 -3 2 148.45 10.36 -8 3 -2 139.22 11.14 8 -3 2 153.39 11.06 8 3 2 130.85 9.54 8 -3 2 143.23 10.04 8 3 3 508.25 22.33 8 -3 3 475.08 21.93 -8 -3 -3 529.85 25.04 8 3 3 549.34 23.34 8 3 3 519.96 22.91 8 -3 3 540.22 24.04 8 -3 3 498.21 22.31 -8 3 -3 533.77 24.72 8 -3 3 582.98 24.83 8 3 4 133.82 9.5 8 -3 4 135.54 9.62 8 3 4 132.98 9.73 8 3 4 149.19 10.07 8 -3 4 148.05 10.51 8 -3 4 123.59 9.31 -8 3 -4 105.64 9.68 8 -3 4 149.35 10.82 -8 3 -5 1594.33 61.84 8 3 5 1711.44 56.56 8 -3 5 1631.08 56.21 8 3 5 1707.7 57.38 8 3 5 1711.68 56.64 8 -3 5 1745.76 57.5 -8 -3 -5 1633.69 57.43 8 -3 5 1649.95 56.49 -8 3 -5 1596.21 58.04 8 -3 5 1761.67 58.69 8 -3 6 6.46 2.47 8 3 6 6.85 2.45 8 3 6 8.99 2.89 -8 3 -6 4.84 3.11 8 3 6 3.52 2.03 8 -3 6 8.65 2.69 -8 -3 -6 8.1 3.01 -8 3 -6 5.95 2.49 8 -3 6 8.64 2.89 8 3 6 6.42 2.56 8 -3 6 5.08 2.25 -8 3 -7 2662.64 92.3 8 3 7 2725.9 87 8 3 7 2710.72 85.89 8 -3 7 2641.29 85.73 -8 3 -7 2635.42 86.7 8 3 7 2692.65 85.03 -8 -3 -7 2528.98 87.01 8 3 7 2737.35 85.93 8 -3 7 2775.55 86.13 8 -3 7 2774.21 87.42 -8 3 -8 62.05 8.47 8 3 8 61.25 6.78 8 3 8 43.87 5.63 8 -3 8 52.31 6.06 8 3 8 47.08 5.39 -8 -3 -8 47.86 6.44 8 3 8 55.88 6.16 8 -3 8 52.12 5.99 8 -3 8 48.41 6.07 -8 3 -9 761.03 36.42 8 3 9 819.69 32.56 8 3 9 793.67 31.51 8 -3 9 719.5 30.98 -8 -3 -9 800.26 33.64 8 3 9 855.73 31.96 8 -3 9 786.59 31.51 8 -3 9 819.45 32.34 -8 3 -9 727.06 32.08 8 3 10 114.22 9.63 8 3 10 122.1 9.51 8 -3 10 104.04 8.97 -8 3 -10 105.44 11.45 -8 -3 -10 111.75 10.17 8 3 10 111.98 9.03 8 -3 10 130.41 9.77 -8 3 -10 100.25 9.55 8 3 11 10.27 3.19 8 -3 11 13.13 3.33 -8 -3 -11 18.93 4.31 -8 3 -11 15.67 4.06 8 3 11 8.61 2.73 8 -3 11 16.9 3.71 8 3 12 170.73 12.38 8 -3 12 152.93 11.5 -8 -3 -12 191.19 13.84 -8 3 -12 217.77 14.35 8 3 12 166.73 11.64 8 -3 12 145.75 11.23 -8 3 -12 213.83 14.61 -8 3 -13 452.21 22.81 -8 3 -13 389.36 24.42 8 3 13 497.37 23.3 8 -3 13 468.29 22.11 -8 -3 -13 494.6 24.5 8 3 13 503.87 22.36 8 -3 13 484 22.15 -8 3 -13 412.2 23.2 -8 -3 -13 407 23.66 -8 -3 -14 2.97 2.19 -8 3 -14 3.48 2.24 8 3 14 5.26 2.76 -8 3 -14 2.5 2.46 -8 -3 -14 3.36 2.36 -8 3 -14 2.12 2.09 8 3 14 4.07 2.12 8 -3 14 3.59 2.06 8 3 15 841.78 34.17 -8 -3 -15 837.96 35.3 -8 3 -15 763.15 32.67 8 3 15 852.46 32.98 8 -3 15 837.79 32.87 -8 3 -15 837.52 36.08 8 3 16 199.51 13.49 -8 -3 -16 221.22 14.78 8 3 16 216.29 13.04 8 -3 16 215.93 13.08 -8 3 -16 205.4 14.84 8 3 17 490.82 22.3 -8 -3 -17 454.7 22.66 8 3 17 458.09 20.58 8 -3 17 424.77 20.12 -8 3 -17 408.76 22.4 8 3 18 216.63 13.27 -8 -3 -18 218.58 14.65 -8 -3 -18 210.97 13.76 8 3 18 218.79 12.35 8 -3 18 209.49 12.16 -8 3 -18 190.99 13.64 -8 -3 -19 97.88 8.46 8 3 19 99.65 8.29 -8 -3 -19 98.92 9.04 8 3 19 106.78 7.69 8 -3 19 100.18 7.55 8 3 20 197.59 11.37 -8 -3 -20 176.64 10.95 -8 -3 -20 173.04 11.7 8 3 20 173.25 9.75 8 -3 20 168.95 9.7 8 3 21 265.55 12.96 -8 -3 -21 207.77 11.55 -8 -3 -21 230.73 13.11 8 -3 21 266.78 11.58 8 3 22 58.51 4.99 -8 -3 -22 58.66 5.42 8 3 23 791.89 26.92 8 4 -23 187.47 9.77 8 -4 -22 499.92 19.06 8 4 -22 467.4 19.59 8 -4 -21 70.71 6.38 -8 4 21 73.07 6.7 8 -4 -21 70.43 5.92 8 4 -21 75.77 6.96 -8 4 20 749.86 30.73 8 -4 -20 777.85 29.86 8 -4 -20 709.01 28.22 8 4 -20 749.21 30.63 8 4 -19 14.43 3.59 8 -4 -19 6.69 3.2 -8 4 19 3.08 2.39 8 -4 -19 5.69 2.44 8 -4 -19 13.45 3.39 8 4 -19 7.46 3.33 8 4 -18 165.93 10.78 8 -4 -18 172.88 12.23 8 -4 -18 163.15 11.02 8 -4 -18 150.99 10.94 8 4 -18 171.56 12.74 8 4 -17 115.54 10.59 8 4 -17 140.89 10.2 8 -4 -17 134.31 10.12 8 -4 -17 127.11 10.16 8 4 -17 129.17 11.28 8 4 -16 3.99 2.56 8 4 -16 2.66 1.88 8 -4 -16 1.07 1.69 8 -4 -16 4.53 2.36 8 4 -16 2.83 2.36 8 4 -15 262.94 16.84 8 4 -15 243.04 15.21 8 4 -15 247.74 14.16 8 -4 -15 272.62 15.78 8 -4 -15 244.09 15.4 8 4 -15 246.36 17.03 8 4 -14 664.25 30.53 8 4 -14 669.16 29.01 8 4 -14 644.64 27.49 8 -4 -14 665.54 31.03 8 -4 -14 646.98 28.69 8 -4 -14 630.52 28.71 8 4 -14 645.43 30.83 8 4 -13 187.74 14.61 8 4 -13 217.1 14.63 8 4 -13 232.07 14.15 8 -4 -13 233.21 16.51 8 -4 -13 221.28 16.04 8 -4 -13 238.8 14.92 8 -4 -13 217 14.45 8 4 -13 220.16 15.82 8 4 -12 1900.24 68.9 8 4 -12 1923.58 67.38 -8 4 12 2026.5 68.27 8 -4 -12 2054.32 68.99 8 4 -12 1928.36 66.26 8 -4 -12 2080.29 71.38 8 -4 -12 1814.3 69.03 8 -4 -12 1981.6 67.2 8 -4 -12 1830.1 66.59 8 4 -12 1957.42 69.66 8 4 -11 9.41 3.2 -8 4 11 2.6 2.98 8 -4 -11 10.81 3.69 8 4 -11 2.31 2.04 8 -4 -11 6.77 3.02 8 -4 -11 6.28 3.5 8 4 -11 4.25 3.05 8 -4 -11 10.84 3.29 8 -4 -11 6.08 2.79 8 4 -11 1.45 2.15 8 4 -10 1963.35 67.55 8 4 -10 1845.45 65.67 -8 4 10 2018.62 67.12 8 -4 -10 1930.52 67.22 8 4 -10 1792.57 64.7 8 -4 -10 1970.09 67.76 8 -4 -10 1891.35 65.28 8 -4 -10 1767.62 64.62 8 4 -10 1838.85 67.31 8 4 -9 88.7 9.37 8 4 -9 89.08 9 -8 4 9 88.18 9.15 8 -4 -9 100.7 9.76 8 4 -9 105.81 9.41 8 -4 -9 97.49 10.28 8 -4 -9 83.03 9.14 8 -4 -9 75.04 8.16 8 -4 -9 86.37 8.6 8 4 -9 92.19 9.56 8 -4 -9 89.14 8.63 8 4 -8 352.89 20.43 8 4 -8 362.45 20.16 -8 4 8 397.02 21.34 8 -4 -8 387.79 21.02 8 4 -8 339.88 19.24 8 -4 -8 364.53 21.42 8 -4 -8 400 21.62 8 -4 -8 395.42 22.03 8 -4 -8 374.56 19.85 8 -4 -8 360.47 19.42 8 4 -8 371.84 20.76 8 -4 -8 350.04 19.41 8 4 -7 242.02 15.86 8 4 -7 248.93 15.65 8 -4 -7 235.11 15.72 8 4 -7 224.25 14.79 8 -4 -7 231.05 15.81 8 -4 -7 228.55 15.96 8 -4 -7 228.8 14.75 8 -4 -7 227.97 14.39 8 4 -7 235.41 15.59 8 -4 -7 243.23 15.4 8 4 -6 249.38 16.62 8 4 -6 289.49 17.06 8 -4 -6 283.36 17.2 8 4 -6 285.86 16.57 8 -4 -6 252.81 16.89 8 -4 -6 263.55 17.33 -8 4 6 259.28 18.88 8 -4 -6 269.83 16.25 8 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-4 4.19 2.21 10 1 -4 5.52 2.73 10 1 -4 4.65 2.67 10 -1 -4 6.34 2.65 10 -1 -4 4.76 2.73 10 1 -4 4.79 2.58 10 1 -3 83.3 8.5 10 -1 -3 90.65 8.22 10 1 -3 101.5 8.72 10 1 -3 104.72 9.59 10 -1 -3 89.71 8.8 10 -1 -3 94.48 8.91 10 1 -3 109.85 9.68 10 1 -3 97.39 8.85 10 -1 -3 97.19 8.88 10 1 -3 69.94 7.94 10 1 -2 77.66 8.21 -10 -1 2 91.72 9.1 10 -1 -2 91.78 8.11 10 1 -2 99.25 8.55 10 1 -2 89.57 8.84 10 -1 -2 101.3 9.21 10 1 -2 96.18 8.36 10 1 -2 78.04 8.11 10 -1 -2 93.02 8.83 10 -1 -2 101.58 9.16 10 1 -2 81.8 8.1 10 -1 -2 88.43 8.44 -10 -1 1 477.59 23.67 10 -1 -1 451.11 20.73 10 1 -1 459.4 21.29 10 1 -1 444.56 22.38 10 -1 -1 433.69 22.42 10 1 -1 465.75 22.45 10 -1 -1 462.21 22.46 10 -1 -1 447.38 21.91 10 1 -1 416.97 21.86 10 1 -1 449.24 21.92 10 -1 -1 455.23 22.07 10 -1 -1 458.97 22.51 10 -1 -1 457.9 21.85 10 -1 0 0.57 1.68 10 1 0 5.1 2.44 -10 -1 0 -0.66 1.46 10 1 0 -0.47 1.38 10 1 0 1.71 2.11 10 -1 0 0.54 1.6 10 1 0 2.29 1.56 10 -1 0 3.41 2 10 1 0 1.68 1.4 10 -1 0 1.67 1.24 10 -1 0 -0.53 1.45 10 1 1 1986.97 68.48 -10 -1 -1 2023.72 70.35 10 1 1 2079.33 66.6 10 1 1 1998.56 68.34 10 1 1 2058.74 68.83 10 -1 1 2023.9 68.72 10 -1 1 2022.14 67.84 10 -1 1 2044.36 68.69 10 1 1 1998.51 68.4 10 -1 1 1965.19 68.06 10 -1 1 2023.77 67.79 10 -1 2 27.01 4.78 10 1 2 22.71 4.52 -10 -1 -2 28.86 5.38 10 1 2 22.48 3.82 10 1 2 25.11 4.58 10 1 2 33.67 5.28 10 -1 2 17.6 3.97 10 -1 2 22.62 4.41 10 -1 2 24.73 4.34 10 1 2 20.88 4.22 10 -1 2 24.61 4.45 10 1 3 1949.58 66.36 10 -1 3 1945.24 66.22 10 -1 3 1866.52 66.24 -10 -1 -3 1923.74 68.26 10 1 3 2038.23 65.85 10 1 3 1921.94 66.6 10 -1 3 1895 66.61 10 -1 3 1972.19 65.29 10 1 3 1919.9 66.56 10 -1 3 1988 65.43 10 1 4 114.46 9.63 10 1 4 99.65 9.29 -10 1 -4 105.83 10.13 -10 -1 -4 102.38 10.02 10 -1 4 103.49 9.25 10 1 4 106.3 8.77 10 1 4 115.9 9.84 10 -1 4 115.02 9.77 10 -1 4 109.2 8.85 10 -1 4 102.35 9.31 10 -1 4 107.72 8.8 10 1 5 35.82 5.65 10 -1 5 34.92 5.33 -10 1 -5 42.63 6.32 10 -1 5 38.94 5.57 10 -1 5 52.24 5.77 10 1 5 37 4.97 10 1 5 46.44 6 10 1 5 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250 16.08 10 3 5 20.12 4.14 -10 3 -5 29.11 6.19 -10 3 -5 15.96 4.1 10 3 5 25.13 4.41 10 -3 5 16.76 4.44 10 -3 5 20.51 3.84 10 -3 5 29.04 4.84 10 3 5 20.49 4.07 10 -3 5 22.79 4.31 10 -3 5 28.28 4.91 10 -3 5 20.58 4.09 -10 3 -6 445.34 26.55 10 3 6 440.94 22.59 -10 3 -6 466.89 23.79 10 3 6 498.23 21.74 10 -3 6 513.15 25.12 10 3 6 466.54 22.38 10 -3 6 481.34 22.57 10 -3 6 498.94 23.5 10 -3 6 426.06 21.78 10 -3 7 183.92 12.81 -10 3 -7 213.7 16.88 10 3 7 212.6 13.86 10 3 7 206.13 13.38 10 -3 7 219.7 13.57 10 -3 7 193.82 13.28 10 -3 8 105.23 9.28 -10 3 -8 127.65 12.84 10 3 8 133.25 10.67 -10 -3 -8 120.57 9.65 10 3 8 110.72 9.45 10 -3 8 134.7 10.24 -10 3 -9 756.12 36.53 10 3 9 734.37 31.89 -10 -3 -9 750.97 31.31 10 3 9 794.36 31.71 10 -3 9 788.92 31.59 10 3 10 2.3 1.92 -10 3 -10 1.77 2.61 -10 -3 -10 6.56 2.72 10 3 10 1.54 1.62 10 -3 10 2.59 2.31 10 3 11 1582.92 54.67 -10 -3 -11 1479.38 53.67 10 3 11 1509.83 53.16 10 -3 11 1538.9 53.32 10 3 12 26.59 4.75 10 3 12 32.64 4.82 10 -3 12 25.47 4.3 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26.83 10 4 -15 241.17 14.76 10 4 -15 216.66 12.61 -10 4 15 232.19 16.01 10 -4 -15 250.9 13.52 10 -4 -15 227.27 13.6 10 4 -15 228.55 13.98 10 4 -14 431.73 22.1 10 4 -14 410.08 19.81 10 -4 -14 448.11 22.49 -10 4 14 428.83 23.78 10 -4 -14 437.33 20.65 10 -4 -14 439.42 21.01 10 4 -14 418.59 20.96 10 4 -13 276.66 17.43 10 4 -13 288.74 16.08 10 -4 -13 311.95 18.39 10 -4 -13 306.74 16.86 10 -4 -13 285.09 16.44 10 4 -13 293.35 16.83 10 4 -12 7.25 2.94 -10 4 12 3.55 2.47 10 4 -12 5.96 2.49 10 -4 -12 4.85 2.89 10 -4 -12 10.27 3.24 10 4 -12 5.81 2.75 10 4 -11 186.98 14.05 -10 4 11 222.09 14.53 10 4 -11 187.66 12.98 10 -4 -11 214.54 15.16 10 -4 -11 176.34 12.85 10 4 -11 195.75 13.5 10 4 -10 745.23 32.94 -10 4 10 785.34 33.01 10 4 -10 736 31.46 10 -4 -10 729.23 33.51 -10 4 10 734.88 35.59 10 -4 -10 733.51 30.15 10 -4 -10 701.74 31.11 10 4 -10 722.22 31.31 10 4 -9 16.06 4.2 -10 4 9 6.87 3.17 10 4 -9 13.91 3.7 -10 4 9 9.76 4.08 10 -4 -9 12.52 3.35 10 -4 -9 10.3 3.39 10 4 -9 5.96 2.75 10 4 -8 1358.65 52.59 -10 4 8 1478.14 53.65 10 4 -8 1296.36 50.85 10 -4 -8 1418.76 52.71 -10 4 8 1397.2 55.95 10 -4 -8 1399.41 49.96 10 -4 -8 1352.26 50.96 10 4 -8 1414.43 51.13 10 -4 -8 1419.37 51.29 10 4 -7 160.73 12.89 10 4 -7 153.38 12.09 10 -4 -7 177.29 13.31 -10 4 7 167.44 14.65 10 -4 -7 152.15 11.28 10 -4 -7 164.9 12.34 10 -4 -7 148.24 11.91 10 4 -6 845.14 36.33 10 4 -6 838 34.95 10 -4 -6 811.35 35.34 10 -4 -6 910.59 37.09 10 -4 -6 830.69 36.93 -10 4 6 896.21 39.53 10 -4 -6 834.36 33.79 10 -4 -6 798.99 34.31 10 -4 -6 811.74 35.15 10 4 -5 270.23 17.53 -10 4 5 288.19 18.62 10 4 -5 257.57 16.4 10 -4 -5 250.83 16.63 10 -4 -5 300.68 18.99 -10 4 5 290.63 19.76 10 -4 -5 270.8 15.99 10 -4 -5 269.57 16.4 10 -4 -5 288.3 17.5 10 4 -4 352.15 20.21 -10 4 4 339.05 20.73 10 -4 -4 409.56 20.65 10 -4 -4 316.24 20.24 -10 4 4 330.09 21.51 10 -4 -4 360.45 18.85 10 -4 -4 334.94 18.79 10 -4 -4 339.47 19.86 10 4 -3 506.92 25.93 -10 4 3 523.83 27.41 10 -4 -3 545.79 25.28 10 -4 -3 528.13 26.06 10 -4 -3 535.12 27.02 -10 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8.14 -10 -4 -14 102.39 8.23 -10 4 -15 64.86 6.08 10 4 15 72.77 6.41 -10 -4 -15 74.76 7.43 -10 -4 -15 83.93 7 10 4 16 123.38 8.24 -10 -4 -16 133.97 9.57 -10 -4 -16 113.47 9.16 10 4 17 110.17 7.23 -10 -4 -17 114.22 8.17 -10 -4 -17 112.55 8.37 10 -4 17 107.85 7.39 10 -4 18 516.36 20.26 10 4 18 574.81 20.45 10 -4 19 70.72 4.84 10 -5 -18 21.93 3.18 10 -5 -17 923.65 33.65 -10 5 17 982.78 35.33 10 -5 -16 32.24 4.48 -10 5 16 44.58 5.73 10 5 -15 619.91 25.75 -10 5 15 621.18 27.57 10 -5 -15 603.67 23.56 10 5 -14 343.91 17.9 10 5 -14 335.03 15.94 -10 5 14 397.41 20.82 10 -5 -14 369.61 16.49 10 -5 -14 399.17 17.68 10 5 -13 154.18 11.35 10 5 -13 154.56 10.02 -10 5 13 155.73 12.87 10 -5 -13 155.52 9.97 10 -5 -13 171.36 11.11 10 5 -12 330.41 17.98 10 5 -12 326.24 16.53 -10 5 12 339.74 20.32 10 -5 -12 326.04 16.37 10 5 -11 26.18 4.81 10 5 -11 21.23 3.93 10 -5 -11 30.72 5.51 10 -5 -11 21.59 4.02 10 5 -10 275.82 16.75 -10 5 10 295.2 17.14 10 5 -10 275.91 15.61 10 -5 -10 275.22 17.4 10 -5 -10 267.2 15.17 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5 1 557.56 28.12 10 5 -1 586.68 26.27 10 -5 -1 528.41 26.23 10 -5 -1 546.02 27.19 -10 5 1 550.45 28.56 10 -5 -1 572.03 26.2 10 5 0 108.6 9.79 -10 5 0 93.64 10.12 10 5 0 97.52 9.06 10 -5 0 100.55 9.61 10 -5 0 78.73 9.07 -10 5 0 90.55 10.15 10 -5 0 91.45 8.9 10 5 1 1362.7 50.43 -10 5 -1 1437.94 53.4 10 5 1 1461.64 50.61 10 -5 1 1409.96 51.03 10 -5 1 1250.9 50.9 -10 5 -1 1240.69 52.1 10 -5 1 1416.1 50.87 -10 5 -2 72.22 8.84 10 5 2 72.64 7.66 10 -5 2 86.99 8.58 10 -5 2 72.54 8.46 -10 5 -2 64.47 8.35 10 -5 2 88.82 8.67 -10 5 -3 1218.09 47.73 10 5 3 1309.47 45.89 10 -5 3 1246.49 45.96 10 -5 3 1180.07 46.69 -10 5 -3 1120.86 47.05 10 -5 3 1291.25 47.04 -10 5 -4 294.32 17.68 10 5 4 294.76 16.08 10 -5 4 255.01 16.33 -10 5 -4 242.29 16.56 10 -5 4 286.95 16.86 10 5 5 132.02 9.95 10 -5 5 118.59 10.23 -10 5 -5 110.76 10.23 10 -5 5 127.51 10.57 10 5 6 409.6 19.79 -10 -5 -6 383.83 19.29 10 -5 6 402.98 20.71 10 5 7 27.34 4.26 -10 -5 -7 30.48 4.72 10 -5 7 21.77 4.24 10 -5 7 23.04 4.59 10 5 8 186.78 11.43 -10 -5 -8 220.68 12.94 10 -5 8 179.46 12.66 -10 5 -8 211.27 15.02 -10 5 -9 230.33 15.37 10 5 9 234.4 12.6 -10 -5 -9 229.33 13.6 10 -5 9 263.36 15.06 -10 5 -10 28.12 4.94 -10 -5 -10 24.98 4.24 10 -5 10 28.7 4.66 -10 -5 -11 290.91 16.57 -10 -5 -11 281.19 14.95 -10 5 -11 260.12 15.67 10 -5 11 323.24 16.28 -10 5 -12 79.52 7.46 -10 -5 -12 70.28 7.27 -10 -5 -12 68.41 6.44 10 -5 12 53.34 5.96 -10 5 -13 71.49 6.69 -10 -5 -13 76.31 7.21 -10 -5 -13 62.41 6.55 -10 -5 -13 59.1 5.79 10 -5 13 65.18 6.38 -10 -5 -14 262.24 14.38 -10 -5 -14 262.49 14.29 -10 -5 -14 286.49 13.56 10 -5 14 293.49 14.15 -10 5 -14 274.88 13.81 -10 5 -15 126.85 7.95 -10 -5 -15 136.98 9.12 -10 -5 -15 137.92 8.14 -10 -5 -15 133.84 8.9 10 -5 15 142.27 8.54 10 -5 16 173.44 9.26 10 -5 17 489.45 18.06 10 -6 -16 500.13 18.77 -10 6 15 21.87 2.75 10 -6 -15 24.96 3.4 10 -6 -14 270.65 13.28 -10 6 14 269.28 14.38 10 -6 -14 273.71 11.96 10 -6 -13 215.13 12.07 -10 6 13 245.13 14.13 10 -6 -13 224.14 11.13 10 -6 -13 217.08 11.42 10 6 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302.75 12.74 11 -1 20 299.68 12.75 11 2 -21 416.04 16.2 11 -2 -21 436.9 17.09 11 -2 -20 140 8.54 11 2 -20 146.19 8.77 11 -2 -20 140.46 9.07 11 -2 -19 30.79 4.07 11 2 -19 40.1 4.63 11 2 -19 36.04 4.18 11 -2 -19 35.98 4.29 11 -2 -19 37.47 4.7 11 2 -18 228.56 13.12 11 -2 -18 206.66 12.34 11 2 -18 228.53 12.91 11 2 -18 211.3 12.09 11 -2 -18 212.19 12.14 11 -2 -18 240.43 12.16 11 -2 -18 231.63 13.53 11 2 -17 780.69 31.59 11 2 -17 776.77 30.48 11 -2 -17 802.88 30.84 11 -2 -17 795.07 32.18 11 2 -16 130.68 10.51 11 2 -16 116.19 9.19 11 -2 -16 133.18 9.84 11 2 -16 121.19 9.19 11 -2 -16 124.25 10.51 11 2 -15 2197.55 74.27 11 -2 -15 2226.91 73.54 11 2 -15 2184.25 72.34 11 -2 -15 2294.64 72.27 11 -2 -15 2269.32 73.13 11 -2 -15 2149.13 71.22 11 2 -15 2177.63 72.2 11 -2 -15 2139.84 74.45 11 2 -14 3.1 2.49 11 2 -14 2.21 2.13 11 -2 -14 0.58 2.35 11 -2 -14 6.78 2.85 11 2 -14 9.68 3.05 11 -2 -14 2.7 2.33 11 -2 -14 4.95 2.34 11 2 -14 2.08 2.09 11 -2 -14 5.76 2.85 11 2 -13 1251.58 47.3 -11 2 13 1267.08 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180.52 13.26 -11 -2 2 192.11 13.78 11 2 -2 191.79 12.87 11 -2 -2 179.34 13.11 11 2 -2 188.64 13.4 11 -2 -2 173.78 13.63 -11 2 2 179.5 13.12 11 2 -2 176.31 13.09 11 -2 -2 187.31 13.26 11 -2 -2 209.59 13.89 11 -2 -2 198.9 13.57 11 2 -1 7.42 2.76 -11 -2 1 2.68 1.98 11 2 -1 1.09 1.5 11 -2 -1 2.1 2.34 11 -2 -1 9.16 3.12 11 2 -1 5.52 2.56 11 -2 -1 3.05 1.92 11 -2 -1 9.92 3.01 11 2 -1 8.74 2.87 11 -2 -1 1.83 1.8 11 2 0 145.24 11.57 -11 -2 0 118.66 10.98 11 2 0 140.39 10.6 11 -2 0 142.62 11.98 11 -2 0 142.41 11.4 11 2 0 136.51 11.21 11 -2 0 137.07 11.04 11 2 0 134.58 11.11 11 -2 0 134.9 10.99 11 -2 0 148.11 11.42 11 2 1 806.7 34.22 -11 -2 -1 694.48 34.15 11 2 1 835.5 32.95 11 -2 1 843.41 35.89 11 2 1 810.82 34.08 11 -2 1 896.16 34.98 11 -2 1 826.8 33.76 11 2 1 800.63 33.85 11 -2 1 772.47 33.57 11 -2 1 882.02 34.5 11 2 2 198.29 13.79 -11 -2 -2 186.99 14.29 11 2 2 195.38 12.35 11 -2 2 180.86 13.98 11 2 2 187.6 13.37 11 -2 2 193.3 13.52 11 -2 2 213.29 13.58 11 2 2 198.29 13.6 11 -2 2 193.17 13.42 11 -2 2 190.79 13.14 11 -2 3 920.47 37.9 11 2 3 962.21 38.66 -11 2 -3 922.52 39.97 -11 -2 -3 874.5 39.39 11 2 3 964.25 36.07 11 2 3 971.93 38.36 11 -2 3 965.11 38.41 11 -2 3 990.37 37.41 11 2 3 960.36 38.24 11 -2 3 955.69 38.13 11 -2 3 968.74 37.75 11 -2 4 326.7 18.19 11 2 4 324.82 18.54 -11 2 -4 321.46 19.53 -11 -2 -4 286.64 18.96 11 2 4 325.61 16.42 11 2 4 358.91 18.9 11 -2 4 344.34 18.64 11 -2 4 299.94 16.71 11 2 4 313.73 18.01 11 -2 4 318.84 18.09 11 -2 4 321.16 17.7 11 -2 5 1921.74 65.45 11 2 5 1845.24 65.68 -11 2 -5 1838.75 67.29 -11 -2 -5 1862.56 68.17 11 -2 5 1887.75 63.14 11 2 5 2009.08 66.13 11 -2 5 1995.13 66.21 11 -2 5 1843.44 63.13 11 -2 5 1968.13 64.72 11 2 5 1874.09 65.28 11 -2 5 1768.96 65.12 11 -2 6 3 2.31 11 -2 6 2.26 2.09 11 2 6 5.53 2.65 -11 2 -6 3.48 2.19 -11 -2 -6 4.63 2.85 11 2 6 1.78 1.75 11 -2 6 2.97 1.87 11 2 6 2.39 2 11 2 7 484.11 23.65 11 -2 7 492.82 23.97 11 -2 7 489.44 23.3 11 2 7 481.26 23.9 -11 2 -7 479.37 24.77 11 2 7 515.65 24.09 11 -2 7 519.1 24.19 11 2 8 14.63 3.58 11 -2 8 10.64 3.24 11 -2 8 6.46 2.5 11 2 8 14.59 3.78 -11 2 -8 18.53 4.31 11 2 8 13.95 3.73 11 -2 8 14.04 3.76 11 -2 9 249.95 14.74 11 2 9 252.24 15.68 11 2 9 238.06 14.85 11 -2 9 255 15.39 11 -2 10 8.48 2.62 11 2 10 7.08 2.95 11 2 10 10.07 2.73 11 -2 10 10.7 2.81 11 -2 11 538.01 24.4 11 2 11 537.77 25.71 11 2 11 617.01 26.34 11 -2 11 632.41 26.75 11 2 12 43.83 5.95 11 -2 12 38.4 5 11 -2 12 39.06 5.42 11 2 12 28.76 4.77 11 2 13 401.84 20.32 11 -2 13 426.45 18.98 11 2 13 413.38 20.12 11 -2 13 424.79 20.36 11 2 14 5.51 2.5 11 2 14 10.76 2.71 11 -2 14 8.94 2.78 11 2 15 113.5 9.08 11 2 15 122.54 9 11 -2 15 137.26 9.5 11 2 16 63.46 6.3 11 2 16 67.01 6.14 11 -2 16 65.89 6.05 -11 -2 -16 62.47 6.06 11 2 17 33.64 4.19 11 -2 17 33.57 4.18 -11 -2 -17 35.79 4.32 -11 -2 -18 2.22 1.43 11 2 18 6.4 1.75 11 -2 18 5.51 1.77 -11 -2 -18 5.14 1.75 11 -2 19 358.01 14.3 11 2 19 345.35 14.15 11 2 20 3.38 1.29 11 -3 -20 111.32 7.01 -11 3 19 115.97 8.73 11 -3 -19 121.83 7.47 11 -3 -19 126.77 8.16 11 3 -18 205.83 11.9 11 -3 -18 192.7 10.15 -11 3 18 208.17 12.8 11 -3 -18 202.64 11.01 11 -3 -18 186.92 11.24 11 3 -17 164.49 11.03 11 -3 -17 152.35 9.49 11 3 -17 157.49 9.69 11 -3 -17 164.63 10.68 11 -3 -16 963.16 35.41 11 3 -16 1031.86 36.08 11 -3 -16 1041.84 37.72 11 3 -15 0.89 1.65 11 -3 -15 5.77 2.15 11 -3 -15 4.92 2.19 11 -3 -15 4.77 2.58 11 3 -14 1106.85 42.59 11 -3 -14 1221.92 45.1 11 -3 -14 1231.62 43.2 11 -3 -14 1178.5 42.62 11 -3 -14 1182.79 44.53 -11 3 13 64.14 6.81 11 3 -13 47.84 6.1 11 -3 -13 51.06 6.73 11 -3 -13 60.76 6.87 11 -3 -13 55.47 6.44 11 -3 -13 62.22 7.35 -11 3 12 308.38 17.3 11 3 -12 303.1 17.3 11 -3 -12 346.03 19.2 11 -3 -12 315.73 17.52 11 -3 -12 302.65 17.91 11 3 -11 280.49 17.6 -11 3 11 286.86 17.08 11 3 -11 294.84 16.95 11 -3 -11 293.86 18.04 11 -3 -11 303.41 17.2 11 -3 -11 273.95 17.12 11 3 -10 73.32 8.45 -11 3 10 90.48 9.05 11 3 -10 82.33 8.36 11 -3 -10 84.18 9.08 11 -3 -10 82.99 8.52 11 -3 -10 70.54 8.12 11 3 -9 415.46 22.26 -11 3 9 396.28 21.56 11 3 -9 377.03 20.55 11 -3 -9 402.95 22.34 11 -3 -9 406.84 21.44 11 -3 -9 354.97 20.65 11 3 -8 786.29 35.61 -11 3 8 871.73 36.18 11 3 -8 783.78 34.45 11 -3 -8 825.12 35.02 11 -3 -8 862.76 36.88 11 -3 -8 870.41 35.55 11 -3 -8 826.04 35.35 11 3 -7 159.89 13.22 -11 3 7 202.24 14.68 11 -3 -7 187.55 13.43 11 -3 -7 165.28 13.64 -11 3 7 179.04 14.57 11 -3 -7 169.57 12.99 11 -3 -7 182.05 13.55 11 3 -6 1882.02 67.55 11 -3 -6 1927.48 66.01 11 -3 -6 1903.75 68.21 -11 3 6 1968.04 69.42 11 -3 -6 1808.51 66.39 11 -3 -6 1887.27 66.68 11 3 -5 11.95 4.01 11 3 -5 17.66 4.19 11 -3 -5 12.38 3.55 11 -3 -5 14.1 4.38 -11 3 5 7.7 3.45 11 -3 -5 9.22 3.46 11 -3 -5 17.32 4.12 11 3 -4 1515.37 57.15 11 3 -4 1639.27 56.3 11 -3 -4 1523.66 58.03 -11 3 4 1569.59 58.53 11 -3 -4 1509.47 56.5 11 -3 -4 1547.51 56.54 11 -3 -4 1533.71 56.41 11 3 -3 365.9 20.64 11 3 -3 363.21 19.63 11 -3 -3 360.64 19.37 11 3 -3 337.17 18.93 11 -3 -3 330.76 18.62 -11 3 3 360.19 20.96 11 -3 -3 373.55 20.2 11 -3 -3 394.79 20.66 11 -3 -3 317.97 19.06 11 3 -2 310.72 18.79 11 3 -2 313.7 17.75 11 -3 -2 311.61 17.56 11 3 -2 287.58 17.14 -11 3 2 301.82 18.64 11 -3 -2 303.52 17.27 11 -3 -2 297.38 17.78 11 -3 -2 293.57 17.82 11 3 -1 297.9 17.25 11 3 -1 330.98 17.94 11 -3 -1 303.36 17.43 11 3 -1 301.75 17.48 -11 3 1 303.79 18.63 11 -3 -1 296.53 17.39 11 -3 -1 328.01 18.49 11 -3 -1 326.66 18.79 11 -3 -1 323.11 18.58 11 3 0 76.72 8.09 -11 -3 0 70.34 8.21 11 3 0 86.5 8.3 11 -3 0 83.05 8.16 11 3 0 74.82 7.78 -11 3 0 80 8.66 11 -3 0 63.23 7.55 11 -3 0 88.48 8.57 11 -3 0 82.23 8.56 -11 -3 -1 47.13 6.86 11 3 1 74.82 7.87 11 3 1 69.65 7.33 11 -3 1 70.95 7.5 11 3 1 66.18 7.29 11 -3 1 57.53 7.8 11 -3 1 66.18 7.35 11 -3 1 53.33 6.76 11 -3 1 61.19 7.54 11 3 2 910.15 36.5 11 3 2 942.26 35.66 11 -3 2 937.33 39.27 11 -3 2 911.31 36.17 11 3 2 911.19 36.18 11 -3 2 883.18 36.07 11 -3 2 819.66 35.18 11 -3 2 921.19 37.3 -11 3 -3 82.4 10.25 11 3 3 65.02 7.49 11 3 3 61.9 6.8 11 -3 3 78.08 8.95 11 -3 3 68.3 7.44 11 3 3 64.1 7.28 11 -3 3 74.67 7.46 11 -3 3 69.62 7.79 -11 3 -4 1394.13 58.67 11 3 4 1569.7 54.73 -11 3 -4 1502.88 56.27 11 3 4 1559.28 52.85 11 -3 4 1562.53 56.89 11 3 4 1494.09 53.8 11 -3 4 1560.35 54.16 11 -3 4 1512.03 52.92 11 -3 4 1463.79 54.36 11 3 5 7.58 2.98 -11 3 -5 7.29 3.52 -11 3 -5 5.42 2.51 11 3 5 7.84 2.47 11 -3 5 5.58 3.39 11 -3 5 4.16 2.07 11 -3 5 7.05 2.69 11 3 5 9.24 2.84 11 -3 5 7.11 2.52 11 -3 5 6.93 2.74 -11 3 -6 310.57 21.37 11 3 6 345.17 18.62 11 -3 6 355.51 20.08 11 3 6 332.1 17.89 11 -3 6 322.18 17.72 11 -3 6 348.64 17.81 11 -3 6 338.85 18.3 11 3 7 181.31 12.96 11 -3 7 196.56 14.27 11 3 7 200.66 12.94 11 -3 7 199.1 12.91 11 -3 7 191.38 12.43 11 3 8 57.78 6.78 11 -3 8 55.8 7.15 11 3 8 49.8 6.08 11 -3 8 69.85 7.14 11 -3 8 57.72 6.5 11 3 9 238.9 14.73 11 -3 9 253.05 15.84 11 3 9 223.27 13.77 11 -3 9 229.39 13.92 11 -3 9 250.37 14.3 11 3 10 832.64 33.83 11 -3 10 840.54 34.77 11 3 10 871.82 33.25 11 -3 10 831.08 32.94 -11 3 -11 66.69 7.14 11 3 11 54.96 6.49 11 -3 11 54.48 6.76 11 3 11 56.2 6.14 11 -3 11 62.82 6.55 -11 3 -12 1203.85 45.25 11 3 12 1249.66 45.87 -11 -3 -12 1238.05 44.27 11 -3 12 1350.36 47.03 11 3 12 1323 45.11 11 -3 12 1333.72 45.29 11 3 13 19.8 3.79 11 -3 13 19.07 3.76 11 3 13 17.99 3.49 11 -3 13 23.94 3.86 11 3 14 866.55 33.36 11 -3 14 893.47 33.3 11 3 14 912.67 32.31 11 -3 14 865.14 31.96 11 3 15 6.45 2.34 11 -3 15 5.86 2.17 11 3 15 7.41 1.94 11 -3 15 6.71 1.89 11 3 16 91.65 7.03 11 -3 16 91.17 6.56 11 -3 16 90.2 6.19 11 -3 16 85.33 6.34 11 3 17 85.67 6.33 -11 -3 -17 77.19 6.48 -11 -3 -17 79.44 6.8 11 -3 17 72.68 5.41 -11 -3 -17 82.87 6.04 11 3 18 28.75 3.37 11 3 19 35.8 3.35 11 -4 -18 195.46 10.19 11 4 -17 331.32 15.43 11 -4 -17 313.12 14.74 -11 4 17 332.3 16.48 11 -4 -17 281.11 13.41 11 4 -16 45.46 5.49 -11 4 16 56.17 6.46 11 -4 -16 45.88 4.93 11 4 -15 507.92 22.99 11 4 -15 524.28 21.24 11 -4 -15 531.17 21.22 11 -4 -15 513.04 21.67 11 4 -14 11.37 3.29 11 4 -14 20.52 3.56 11 -4 -14 19.93 3.47 11 -4 -14 18.26 3.35 11 -4 -14 14.15 3.09 11 4 -13 564.3 25.56 11 4 -13 552.41 23.82 11 -4 -13 564.03 25.89 -11 4 13 557.78 27.19 11 -4 -13 603.31 24.67 11 -4 -13 533.94 23.91 11 4 -12 218.25 14.38 -11 4 12 220.47 13.63 11 4 -12 212.7 13.02 11 -4 -12 203.23 14.1 -11 4 12 221.35 15.63 11 -4 -12 211.83 13.24 11 -4 -12 189.76 12.65 11 4 -11 63.5 7.44 -11 4 11 59.81 7.05 11 4 -11 70.42 7.19 11 -4 -11 61.94 7.71 -11 4 11 61.38 8.11 11 -4 -11 71.93 7.45 11 -4 -11 58.22 6.79 11 4 -10 853.23 35.87 -11 4 10 853.07 35.35 11 4 -10 851.03 34.42 11 -4 -10 907.01 37.11 -11 4 10 895.74 38.73 11 -4 -10 871.8 35.22 11 -4 -10 840.59 34.4 11 4 -9 317.7 18.62 -11 4 9 325.56 18.74 11 4 -9 322.69 17.73 11 -4 -9 312.57 19.07 -11 4 9 310.03 19.99 11 -4 -9 315.72 18.05 11 -4 -9 300.17 17.19 11 4 -8 279.23 17.37 -11 4 8 300.98 18.18 11 4 -8 268.54 16.45 -11 4 8 271.84 18.57 11 -4 -8 279.08 16.34 11 4 -7 705.18 32.15 -11 4 7 744.82 32.82 11 4 -7 742.56 31.43 -11 4 7 788.12 35.1 11 -4 -7 679.26 30.52 11 4 -6 99.37 9.82 11 4 -6 99.05 9.38 -11 4 6 100.17 10.79 11 -4 -6 107.65 9.57 11 4 -5 915.91 38.51 -11 4 5 936.59 39.47 11 -4 -5 871.2 38.99 -11 4 5 934.33 40.47 11 -4 -5 970.85 37.54 11 4 -4 23.78 4.94 -11 4 4 22.21 5.05 11 -4 -4 21.47 5.11 -11 4 4 22.01 5.28 11 -4 -4 16.87 4.03 11 4 -3 361.53 20.41 -11 4 3 357.07 21.39 11 4 -3 375.12 19.85 11 -4 -3 367.98 21.33 -11 4 3 367.72 21.63 11 -4 -3 373.63 18.61 11 -4 -3 329.55 18.66 11 4 -2 268.04 17.06 -11 4 2 275.34 18.04 11 4 -2 270.61 16.25 11 -4 -2 275.81 17.84 -11 4 2 250.89 17.42 11 -4 -2 279.26 15.54 11 -4 -2 262.17 15.83 11 4 -1 4 2.46 11 4 -1 4.01 2.3 11 -4 -1 1.46 1.82 -11 4 1 5.09 3.13 11 -4 -1 3.12 2.24 11 -4 -1 7.38 2.76 11 4 0 118.55 10.92 11 4 0 140.52 10.82 11 -4 0 137.58 12.04 -11 4 0 129.31 11.51 11 -4 0 139.8 10.98 11 -4 0 137.41 10.45 11 -4 0 140.76 10.85 11 4 1 420.52 22.1 11 4 1 414.16 20.9 11 -4 1 427.37 23.1 -11 4 -1 395.58 21.92 11 -4 1 441 21.53 11 -4 1 402.21 20.26 11 -4 1 417.81 20.8 11 4 2 58.83 7.31 11 4 2 63.63 6.79 11 4 2 69.26 7.27 11 -4 2 70.73 8.33 -11 4 -2 62.49 7.49 11 -4 2 70.88 7.37 11 -4 2 65.81 7.05 11 -4 2 53.71 6.61 11 4 3 1136.04 43.4 11 4 3 1257.32 44.53 11 -4 3 1134.25 46.41 11 -4 3 1313.29 44.58 11 -4 3 1243.94 44.76 11 -4 3 1134.58 43.8 11 4 4 7.05 2.57 11 4 4 7.4 2.64 11 -4 4 8.02 3.16 11 -4 4 4.61 2.19 11 -4 4 9.04 2.78 11 4 5 638.99 27.65 11 4 5 639.39 27.1 11 -4 5 684.7 30.34 11 -4 5 701.61 28.74 11 4 6 55.52 6.28 11 4 6 48.47 5.53 11 -4 6 49.93 6.74 11 -4 6 47.73 6.06 11 4 7 15.59 3.46 11 4 7 18.85 3.37 11 -4 7 11.92 3.47 11 -4 7 17.54 3.7 11 -4 8 57.02 6.71 11 -4 8 52.81 6.22 11 4 8 53.26 6.02 11 4 9 176.65 11.46 11 -4 9 188.24 12.45 11 -4 9 171.43 11.56 -11 4 -10 226.42 14.69 11 4 10 260.34 14.04 11 -4 10 257.07 14.54 11 -4 10 232.07 13.69 -11 4 -11 794.65 30.64 11 4 11 691.38 28.25 11 -4 11 697.83 28.56 11 -4 11 743.92 29.03 -11 4 -12 14.02 3.39 11 4 12 10.32 2.67 -11 -4 -12 8.85 2.51 11 -4 12 9.33 2.58 11 -4 12 12.74 2.87 -11 4 -13 537.73 22.95 11 4 13 585.76 23.11 -11 -4 -13 555.21 22.11 11 -4 13 590.82 23.28 -11 4 -14 14.02 2.68 11 4 14 15.59 2.93 11 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5 7 101.44 7.77 13 5 -6 11.23 2.53 -13 5 6 12.05 2.79 13 -5 -6 10.5 2.6 -13 5 6 9.79 2.52 13 -5 -6 13.97 2.73 13 5 -5 149.31 9.43 -13 5 5 176.21 10.67 13 -5 -5 151.75 10.13 13 -5 -5 165.33 9.72 13 5 -4 264.29 13.56 -13 5 4 277.77 14.58 13 5 -4 294.01 13.9 13 -5 -4 294.41 15 -13 5 4 268.52 14.06 13 -5 -4 289.73 13.87 13 5 -3 8.48 2.33 -13 5 3 5.95 2.28 13 5 -3 7.24 2.08 13 -5 -3 7.66 2.37 13 -5 -3 4.52 1.98 13 5 -2 603.92 23.96 -13 5 2 631.48 25.43 13 5 -2 608.48 23.92 13 -5 -2 615.56 25.31 13 -5 -2 630.72 24.04 13 5 -1 36.52 4.31 -13 5 1 42.02 5.08 13 5 -1 40.75 4.43 13 -5 -1 29.16 4.35 13 -5 -1 39.63 4.4 13 5 0 384.04 16.72 -13 5 0 392.25 18 13 5 0 397.91 16.83 13 -5 0 381.29 17.84 13 -5 0 367.95 16.05 13 5 1 112.24 7.58 -13 5 -1 112.83 8.24 13 5 1 133.07 8 13 -5 1 109.39 7.43 13 -5 1 121.21 8.53 -13 5 -2 46.38 4.96 13 5 2 46.15 4.42 13 -5 2 45.66 5.07 -13 5 -3 238.6 11.97 13 5 3 230.29 10.98 13 -5 3 232.88 12.12 13 5 4 172.21 8.67 13 -5 4 167.85 9.64 -13 5 -5 27.88 4.11 13 -5 5 32.51 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11.33 14 -1 5 171.5 11.37 14 1 5 165.54 10.8 14 1 5 150.36 10.82 14 1 6 6.28 2.47 14 -1 6 4.6 2.55 14 1 6 4.87 2.15 14 -1 6 3.85 2.08 14 1 6 6.25 2.68 14 -1 7 1009.07 38.28 14 1 7 1007.28 37.22 14 -1 7 1055.02 38.04 14 1 7 1014.79 37.74 14 -1 8 41.05 5.4 14 1 8 37.12 4.83 14 -1 8 45.57 5.44 14 1 8 44.94 5.31 14 -1 9 751.11 29.66 14 1 9 759.11 29.12 14 -1 9 768.92 29.3 14 1 9 765.86 29.26 14 -1 10 67.84 6.4 14 1 10 75.36 6.41 14 -1 10 68.73 6.21 14 1 10 71.78 6.28 14 1 11 348.07 16.41 14 -1 11 354.27 16.85 14 1 11 414.06 17.16 14 -1 11 391.3 16.89 14 1 11 402.72 17.02 14 1 12 49.41 4.74 14 1 12 51.43 4.83 14 -1 12 56.7 4.96 14 1 12 51.76 4.72 14 1 13 23.12 3.02 14 1 13 23.51 3.09 14 1 13 16.38 2.64 14 -1 13 19.6 2.89 14 1 14 69.19 4.82 14 -1 14 69.25 5.02 14 1 14 66.9 4.79 14 -1 14 60 4.53 14 1 14 62.96 4.61 14 2 -15 19.19 2.61 14 -2 -15 22.64 3.08 14 2 -14 10.55 2.22 14 -2 -14 7.34 2 14 2 -13 65.6 5.69 14 -2 -13 71.47 5.59 14 -2 -13 65.11 5.84 14 2 -12 182.9 10.62 14 -2 -12 166.75 9.64 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165.66 10.99 14 -2 -4 178.85 12.23 14 2 -3 5 2.13 14 -2 -3 7.19 2.89 14 -2 -3 1.95 1.88 14 -2 -3 2.41 1.78 14 2 -3 3.14 1.93 14 -2 -3 3.79 2.09 14 2 -2 408.65 18.39 14 -2 -2 433.74 20.91 14 -2 -2 415.36 19.52 14 -2 -2 349.22 18.6 14 2 -2 406.14 19.02 14 -2 -2 390.53 20.09 14 2 -1 28.62 4.06 14 -2 -1 29.1 4.93 14 -2 -1 23.72 4.09 14 -2 -1 28.89 4.44 14 2 -1 33.08 4.61 14 -2 -1 24.71 4.46 14 2 0 898.47 36.62 14 2 0 887.04 33.38 14 -2 0 988.27 36.53 14 2 0 922.41 35.97 14 -2 0 946.8 37.23 14 -2 0 937.23 35.28 14 2 0 997.78 35.81 14 -2 0 980.79 37.06 14 2 1 75.85 7.61 14 -2 1 75.93 7.32 14 2 1 59.26 6.59 14 -2 1 67.59 7.25 14 -2 1 69.98 6.67 14 2 1 67.72 6.74 14 -2 1 73.52 7.42 14 -2 2 617.35 25.84 14 2 2 570.1 25.25 14 -2 2 637.44 27.11 14 -2 2 578.8 23.99 14 2 2 595.1 24.97 14 -2 2 606.84 26.2 14 -2 3 140.62 10.12 14 2 3 147.08 10.25 14 -2 3 139.59 10.67 14 2 3 140.41 9.8 14 -2 3 144.03 10.46 14 -2 4 22.47 4.32 14 -2 4 24.66 4.14 14 2 4 17.76 3.71 14 2 4 20.68 3.72 14 -2 4 26.4 4.46 14 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1001.6 35.9 14 -3 -9 1042.55 36.92 14 -3 -9 1045.11 36.29 14 -3 -9 991.51 35.85 14 -3 -9 1013.77 36.16 14 3 -8 35.98 4.94 -14 3 8 33.54 4.48 14 3 -8 32.86 4.36 14 -3 -8 42.89 5.3 14 -3 -8 31.91 4.4 14 -3 -8 31.72 4.26 14 -3 -8 33.5 4.5 14 3 -7 560.34 23.37 -14 3 7 541.54 22.9 14 3 -7 524.61 21.94 14 -3 -7 546.01 23.38 14 -3 -7 487 21.72 14 -3 -7 531.13 22.57 14 3 -6 58.85 6.28 -14 3 6 60.92 6.35 14 3 -6 57.78 5.73 14 -3 -6 64.49 6.69 14 -3 -6 52.01 5.76 14 3 -5 3.35 2.07 -14 3 5 6.64 2.36 14 3 -5 1.96 1.45 14 -3 -5 11.86 3.11 14 -3 -5 6.04 2.2 14 -3 -5 4.22 1.94 14 -3 -5 6.16 2.3 14 3 -4 23.29 4.22 14 3 -4 23.35 3.76 14 -3 -4 17.18 3.81 14 -3 -4 18.22 3.46 14 -3 -4 15.36 3.23 14 -3 -4 19.21 3.66 14 3 -3 357.46 18.01 14 3 -3 346.35 16.46 14 -3 -3 362.55 18.49 14 -3 -3 382.38 17.67 14 -3 -3 323.37 16.65 14 -3 -3 359.02 17.54 14 3 -2 1.96 1.97 -14 3 2 3.55 1.96 14 3 -2 1.87 1.61 14 -3 -2 3.62 2.38 14 -3 -2 4.65 2.11 14 -3 -2 1.67 1.61 14 -3 -2 5.4 2.24 14 3 -1 641.96 26.78 14 3 -1 611.25 24.29 14 -3 -1 630.21 27.02 14 -3 -1 638.5 25.38 14 -3 -1 612.38 25.02 14 -3 -1 617.13 25.73 14 3 0 55.14 6.14 14 3 0 50.83 5.09 14 -3 0 50.93 6.2 14 -3 0 57.74 5.75 14 -3 0 55.45 5.67 14 -3 0 55.53 5.92 14 3 1 659.26 26.49 14 3 1 593.59 23.17 14 -3 1 613.98 24.24 14 -3 1 601.01 25.16 14 3 2 242.95 13.55 14 -3 2 216.32 11.6 14 -3 2 234.45 12.97 14 3 3 197.97 11.94 14 -3 3 188.08 11.3 14 3 4 325.33 15.76 14 -3 4 290.35 13.97 14 3 4 290.57 14.01 14 -3 4 295.6 15.73 14 -3 4 293.98 14.73 14 3 5 15.34 3.16 14 -3 5 9.71 2.89 14 -3 5 12.3 2.43 14 3 5 12.35 2.39 14 -3 5 13.55 2.9 14 3 6 100.1 7.68 14 -3 6 95.37 6.75 14 3 6 109.57 7.15 14 -3 6 109.02 8.28 14 -3 6 102.68 7.38 14 3 7 438.7 18.52 -14 3 -7 399.17 17.52 14 -3 7 417.64 16.96 14 -3 7 433.29 18.99 14 -3 7 450.7 18.05 -14 3 -8 12.49 2.55 14 3 8 8.31 2.27 14 -3 8 12.33 2.71 14 -3 8 16.15 2.7 14 3 9 367.19 15.19 14 -3 9 347.28 15.46 14 -3 9 343.01 14.4 14 3 10 4.36 1.48 14 -3 10 4.93 1.65 14 -3 10 4.32 1.4 14 -3 11 373.32 14.77 14 4 -11 4.25 1.5 14 4 -10 538.97 20.69 14 -4 -10 543.42 20.91 14 4 -9 19.65 3.1 14 -4 -9 20.68 3.21 14 -4 -9 23.95 3.12 14 4 -8 851.22 30.36 -14 4 8 873.5 30.28 14 -4 -8 883.34 30.96 14 -4 -8 881.62 30.09 14 -4 -8 852.61 29.74 14 -4 -8 758.91 27.94 14 4 -7 263.35 13.05 -14 4 7 289.13 13.41 14 4 -7 273.16 12.64 14 -4 -7 272.07 13.55 14 4 -6 238.66 12.37 14 4 -6 248.08 11.94 14 -4 -6 217.86 12.47 14 -4 -6 248.65 12.24 14 -4 -6 220.29 11.71 14 -4 -6 212.51 10.73 14 4 -5 205.52 11.39 14 4 -5 217.33 10.97 14 -4 -5 206.24 11.13 14 -4 -5 212.01 11.15 14 -4 -5 194.11 10 14 4 -4 12.84 2.84 -14 4 4 12.02 2.87 14 4 -4 10.96 2.48 14 -4 -4 10.86 2.54 14 -4 -4 11.22 2.44 14 -4 -4 7.95 2.09 14 4 -3 181.94 10.5 -14 4 3 167.03 10.51 14 4 -3 150.51 9.11 14 -4 -3 188.25 10.27 14 -4 -3 156.74 9.46 14 -4 -3 139.75 8.58 14 4 -2 447.55 19.04 -14 4 2 418.98 19.14 14 4 -2 443.83 17.93 14 -4 -2 388.53 18.91 14 -4 -2 446.17 18.39 14 -4 -2 427.65 18.06 14 -4 -2 406.82 17.13 14 4 -1 15.03 2.93 -14 4 1 13.17 3.07 14 4 -1 17.39 2.84 14 -4 -1 17.39 3.4 14 -4 -1 16.62 2.96 14 -4 -1 14.47 2.81 14 -4 -1 12.73 2.42 14 4 0 600.96 23.85 -14 4 0 611.99 24.55 14 4 0 582.69 22.23 14 -4 0 613.88 24.81 14 -4 0 609.25 22.87 14 -4 0 584.69 22.47 14 4 1 59.56 5.57 -14 4 -1 58.21 5.79 14 4 1 50.49 4.57 14 -4 1 59 5.89 14 -4 1 58.67 5.01 14 4 2 317.11 14.61 -14 4 -2 302.68 14.83 14 4 2 289.25 12.69 14 -4 2 328.52 15.55 14 4 3 100.22 7.12 -14 4 -3 103.56 7.42 14 -4 3 102.52 7.65 14 4 4 22.79 3.22 -14 4 -4 23.96 3.38 14 -4 4 22.88 3.59 14 4 5 117.74 7.18 -14 4 -5 102.49 6.69 14 -4 5 111.79 7.58 14 4 6 150.33 8.06 -14 4 -6 151.02 8.86 14 -4 6 137.1 8.41 -14 4 -7 8.28 2.12 14 -4 7 10.88 2.15 -14 4 -8 526.03 18.83 14 -4 8 486.94 18.39 14 -5 -7 411.76 16.07 14 5 -6 233.36 10.52 14 -5 -6 262.8 11.51 14 5 -5 29.95 3.15 14 -5 -5 28.78 3.38 14 5 -4 196.01 9.35 14 -5 -4 202.82 10.15 -14 5 3 183.39 9.65 14 5 -3 178.76 8.93 14 -5 -3 205.23 10.05 -14 5 2 23.04 3.18 14 5 -2 28.37 3.04 14 -5 -2 28.31 3.46 -14 5 1 447.39 17.71 14 5 -1 469.09 16.91 14 -5 -1 434.36 17.71 -14 5 0 38.55 3.85 14 5 0 39.16 3.4 14 -5 0 45.55 4.17 -14 5 -1 466.08 17.4 14 -5 1 454.02 17.61 -14 5 -2 126.62 7.8 14 -5 2 123.65 6.93 -14 5 -3 122.49 7.49 -14 5 -4 206.92 10.12 -14 5 -5 13.6 2.2 15 0 -13 85.6 5.74 15 0 -12 -0.28 1.21 15 0 -11 113.18 7.56 15 0 -10 1.05 1.41 15 0 -9 850.6 29.97 15 0 -9 926.4 32.61 15 0 -8 2.67 1.59 15 0 -8 1.61 1.95 15 0 -7 1853.61 59.57 15 0 -7 1888.65 61.54 15 0 -6 3.17 2.04 15 0 -6 1.75 2.17 15 0 -5 1270.53 43.4 15 0 -5 1265.06 44.76 15 0 -4 0.39 1.44 15 0 -4 0.91 1.9 15 0 -3 27.73 4.14 15 0 -3 24.05 4.18 15 0 -2 2.46 1.58 15 0 -2 -1.12 1.45 15 0 -2 2.32 1.86 15 0 -1 293.42 15.1 15 0 -1 319 15.15 15 0 -1 286.84 15.53 15 0 0 0.42 1.47 15 0 0 1.57 1.64 15 0 0 5.05 2.28 15 0 1 960.62 34.71 15 0 1 854.93 34.63 15 0 1 961.92 34.33 15 0 1 949.52 35.21 15 0 2 2.88 1.83 15 0 2 1.58 1.77 15 0 2 5.82 2.23 15 0 2 2.21 1.97 15 0 3 1044.17 36.03 15 0 3 1024.6 36.61 15 0 4 1.15 1.54 15 0 4 2.1 2.03 15 0 4 1.66 1.85 15 0 5 407.55 19.11 15 0 5 432.59 19.01 15 0 6 1.43 1.49 15 0 6 0.38 1.63 15 0 7 66.84 5.95 15 0 7 67.88 5.85 15 0 8 1.27 1.62 15 0 8 1.64 1.26 15 0 9 623.92 24.29 15 0 9 700.89 24.69 15 0 10 2.08 1.33 15 0 10 -0.53 1.14 15 0 11 757.26 26.37 15 0 11 782.45 26.38 15 -1 -13 2.2 1.19 15 -1 -12 5.99 1.89 15 1 -11 5.14 1.57 15 1 -11 2.28 1.3 15 -1 -11 2.89 1.52 15 1 -10 230.19 11.3 15 1 -10 239.5 11.6 15 -1 -10 234.14 12.19 15 1 -9 3.83 1.63 -15 1 9 2.6 1.33 15 -1 -9 3.48 1.78 15 1 -9 4.17 1.72 15 -1 -9 6.06 2.31 15 1 -8 887.03 32.09 -15 1 8 882.75 31.39 15 -1 -8 888.51 32.49 15 1 -8 908.95 32.11 15 -1 -8 887.35 33.02 15 1 -7 69.88 6.27 -15 1 7 69.59 6.11 15 -1 -7 71.64 5.89 15 1 -7 68.85 6.22 15 -1 -7 70.9 6.62 15 1 -6 859.34 31.87 -15 1 6 858 31.75 15 -1 -6 856.38 31.08 15 -1 -6 856.06 31.84 15 1 -6 875.02 31.82 15 -1 -6 826.73 32.17 15 1 -5 46.91 5.31 15 -1 -5 48.8 5.16 15 -1 -5 41.77 4.99 15 1 -5 39.07 4.79 15 -1 -5 42.31 5.3 15 1 -4 148.72 9.91 15 -1 -4 145.75 9.46 15 -1 -4 125.85 8.98 15 1 -4 131.77 9.23 15 -1 -4 122.99 9.41 15 -1 -3 58.68 5.36 15 1 -3 74.9 6.8 15 -1 -3 62.69 6.18 15 -1 -3 57.42 5.82 15 1 -3 63.28 6.21 15 -1 -3 61.94 6.52 15 -1 -2 86.83 6.72 15 1 -2 102.12 8.07 15 -1 -2 90.53 7.59 15 -1 -2 98.35 7.59 15 1 -2 97.63 7.81 15 -1 -2 85.71 7.69 15 -1 -1 10.53 2.52 15 1 -1 10.12 2.87 15 -1 -1 11.56 2.87 15 -1 -1 9.11 2.52 15 1 -1 9.64 2.53 15 -1 0 833.81 30.94 15 1 0 905.14 33.18 15 -1 0 858.64 32.67 15 -1 0 866.17 31.42 15 1 0 859.6 32.34 15 -1 1 51.67 5.28 15 1 1 59.88 6.24 15 -1 1 59.88 6.13 15 1 1 50.47 5.75 15 -1 1 54.64 5.91 15 1 1 54.18 5.62 15 -1 2 1081.81 38.05 15 1 2 1120.45 39.67 15 -1 2 1074.62 39.37 15 1 2 1081.17 39.58 15 -1 2 1132.78 39.74 15 1 2 1126.24 39.28 15 1 3 29.52 4.37 15 -1 3 28.97 3.89 15 1 3 31.33 4.38 15 -1 3 28.37 4.31 15 1 3 33.11 3.98 15 -1 3 24.73 3.9 15 1 3 26.94 4.11 15 -1 4 825 31.11 15 1 4 859.46 31.35 15 -1 4 847.15 31.33 15 1 4 799.44 29.44 15 1 4 812.45 30.57 15 -1 5 3.13 1.9 15 1 5 3.08 1.57 15 -1 5 1.14 1.58 15 1 5 2.27 1.57 15 1 5 0.72 1.45 15 -1 6 92.35 7.09 15 1 6 84.61 6.79 15 -1 6 104.69 7.64 15 1 6 87.31 6.45 15 1 6 102.39 7.23 15 -1 7 1.76 1.75 15 1 7 1.69 1.13 15 -1 7 2.33 1.57 15 1 7 3.32 1.88 15 1 7 1.59 1.32 15 -1 8 460.91 18.72 15 1 8 458.66 18.62 15 -1 8 446.4 18.86 15 1 8 472.85 18.15 15 -1 9 14.81 2.72 15 1 9 13.65 2.29 15 -1 9 12.13 2.45 15 1 9 13.76 2.59 15 -1 10 808.36 27.78 15 1 10 789.82 27.66 15 -1 10 836.71 28.28 15 1 10 774.61 26.99 15 1 10 822.76 27.59 15 -1 10 832.61 28.09 15 -1 11 42.54 3.68 15 1 11 44.28 3.72 15 -1 11 44.04 3.9 15 -1 11 43.51 3.79 15 -2 -12 198.89 9.6 15 2 -11 45.27 4.16 15 -2 -11 49.17 4.47 15 2 -10 76.45 5.68 15 -2 -10 75.69 5.79 15 2 -9 462.21 18.58 -15 2 9 405.52 17.11 15 -2 -9 457.04 17.74 15 -2 -9 453.15 18.34 15 -2 -9 456.64 18.71 15 2 -8 5.83 1.95 -15 2 8 7.5 2.14 15 -2 -8 4.6 1.81 15 -2 -8 5.64 1.92 15 -2 -8 3.17 1.76 15 2 -7 928.62 33.31 -15 2 7 899.9 32.51 15 -2 -7 948.03 32.89 15 -2 -7 906.68 33.28 15 2 -6 21.09 3.5 -15 2 6 14.92 3.17 15 -2 -6 14.5 2.97 15 -2 -6 15.54 3.07 15 -2 -6 16.59 3.19 15 2 -5 541.96 22.78 -15 2 5 525.78 22.49 15 -2 -5 558.85 22.76 15 -2 -5 570.39 22.59 15 -2 -5 566.23 23.04 15 2 -4 126.28 8.9 -15 2 4 116.81 8.62 15 -2 -4 130.7 8.93 15 -2 -4 118.02 8.28 15 -2 -4 120.84 8.74 15 -2 -3 19.3 3.48 15 -2 -3 17.84 3.15 15 2 -3 15.13 2.77 15 -2 -3 17.65 3.45 15 -2 -2 42.7 5.15 15 -2 -2 45.36 4.93 15 2 -2 53.58 4.98 15 -2 -1 201.63 11.77 15 -2 -1 189.54 10.65 15 2 -1 187.02 10.32 15 -2 -1 180.19 11.18 15 -2 0 27.18 3.67 15 -2 0 26.15 4.17 15 2 0 27.31 3.59 15 -2 0 35.61 4.44 15 2 1 1134.71 41.05 15 -2 1 1287.51 42.3 15 -2 1 1096.47 38.9 15 2 1 1190.71 39.74 15 -2 1 1246.35 41.68 15 2 2 3.96 2.16 15 -2 2 2.88 2 15 2 2 1.84 1.71 15 -2 2 2.71 1.67 15 2 3 848.72 31.54 15 -2 3 847.34 31.75 15 2 3 830.87 29.7 15 -2 3 859.78 31.26 15 2 4 59.45 5.71 15 -2 4 50.14 4.88 15 2 4 51 4.88 15 -2 4 48.13 5.29 15 2 4 48.09 4.54 15 -2 4 55.87 5.42 15 2 5 247.91 12.59 15 -2 5 237.03 11.89 15 2 5 253.63 12.15 15 -2 5 258.36 13.1 15 2 5 245.55 11.48 15 -2 5 232.54 12.21 15 2 6 203.86 10.73 15 -2 6 185.19 9.85 15 2 6 193.48 9.98 15 -2 6 200.06 10.83 15 2 6 169.26 9.13 15 -2 6 207.1 10.64 15 2 7 5.11 1.77 15 -2 7 2.86 1.45 15 2 7 4.68 1.64 15 2 7 3.79 1.41 15 -2 7 2.3 1.36 15 2 8 202.1 10.18 15 -2 8 197.68 9.55 15 2 8 201.56 9.65 15 -2 8 217.42 10.27 15 2 9 506.61 18.75 15 -2 9 484.49 18.31 15 2 10 42.37 3.68 15 -2 10 50.16 4.09 15 -3 -9 65.51 4.98 15 -3 -9 69.13 4.94 -15 3 8 553.04 20.92 15 -3 -8 601.52 21.67 15 -3 -8 570.4 21.01 -15 3 7 0.28 1.13 15 -3 -7 0.9 1.3 15 -3 -7 0.27 1.23 15 3 -6 928.17 31.98 -15 3 6 835.03 31.08 15 -3 -6 929.85 31.93 15 -3 -6 909.29 31.27 15 -3 -6 875.01 30.89 15 3 -5 84.12 6.67 -15 3 5 91.25 6.82 15 3 -5 89.35 6.11 15 -3 -5 97.65 7.14 15 -3 -5 95.35 6.67 15 -3 -5 97.37 6.74 15 3 -4 256.23 12.82 15 3 -4 240.54 11.4 15 -3 -4 253.13 12.96 15 -3 -4 275.59 12.61 15 -3 -4 255.54 12.33 15 3 -3 69.82 6.09 15 3 -3 69.45 5.12 15 -3 -3 69.89 6.19 15 -3 -3 67.74 5.55 15 -3 -3 65.06 5.53 15 3 -2 6.66 2.25 -15 3 2 6.13 2.09 15 3 -2 5.29 1.73 15 -3 -2 5.54 2.02 15 -3 -2 4.67 1.67 15 -3 -2 11.19 2.38 15 3 -1 55.79 5.36 -15 3 1 53.15 5.37 15 3 -1 40.98 3.77 15 -3 -1 55.65 5.59 15 -3 -1 56.17 4.84 15 -3 -1 56.45 5.06 15 3 0 502.13 20.2 -15 3 0 461.06 20 15 -3 0 462.3 20.2 15 -3 0 505.32 19.55 15 3 1 3.34 1.82 -15 3 -1 4.18 1.86 15 -3 1 1.81 1.56 15 -3 1 2.94 1.46 15 3 2 794.04 28.2 -15 3 -2 728.61 27.88 15 -3 2 778.87 27.33 15 3 3 64.21 5.42 -15 3 -3 66.73 5.63 15 -3 3 57.08 4.94 15 3 4 514.93 19.44 -15 3 -4 489.64 19.13 15 -3 4 460.06 18.23 15 3 5 208.78 10.01 -15 3 -5 191.02 9.47 15 -3 5 197.97 10.25 15 -3 5 171.71 8.86 15 3 6 14.9 2.46 15 -3 6 15.22 2.62 15 3 7 216.41 9.68 15 -3 7 204.03 9.91 15 4 -6 74.69 5.02 -15 4 6 70.98 4.95 15 -4 -6 76.38 5.28 15 4 -5 471.46 17.42 15 -4 -5 452.17 17.75 15 4 -4 476.46 17.15 -15 4 4 453.46 17.23 15 4 -3 30.96 3.32 -15 4 3 28.07 3.3 15 4 -2 411.5 15.77 -15 4 2 384.29 15.92 15 4 -1 146.71 7.84 -15 4 1 150.39 8.24 15 -4 -1 150.39 8.42 15 4 0 129.6 7.03 -15 4 0 117.71 7.06 15 -4 0 124.93 7.46 15 4 1 608.31 21.02 -15 4 -1 554.64 21.12 15 -4 1 622.6 21.93 15 -4 2 4.8 1.54 -15 4 -3 456.94 17.69 15 -4 3 481.37 17.63 16 0 -9 1.27 1.08 16 0 -8 504.73 18.88 16 0 -7 1.05 1.24 16 0 -6 1412.77 45.69 -16 0 5 1.2 1.49 16 0 -5 1.77 1.57 16 0 -4 1086.74 36.38 16 0 -4 1190.91 38.4 16 0 -3 0.96 1.04 16 0 -3 2.18 1.55 16 0 -2 225.95 10.55 16 0 -2 205.18 10.94 16 0 -1 2.34 1.29 16 0 -1 2.83 1.49 16 0 0 14.17 2.49 16 0 0 13.38 2.64 16 0 1 0.79 0.97 16 0 1 0.91 1.31 16 0 2 519.94 19.15 16 0 2 462.19 18.17 16 0 2 514.42 19.67 16 0 3 0.5 1.04 16 0 3 2.71 1.33 16 0 3 0.57 1.26 16 0 4 897.01 30.03 16 0 4 873.6 29.5 16 0 4 900.03 30.53 16 0 5 0.9 1.06 16 0 5 0.41 0.77 16 0 5 0.5 1.14 16 0 6 222.65 9.83 16 0 6 216.67 10.05 16 0 7 0.2 0.84 16 -1 -9 9.99 1.89 16 -1 -8 10.21 2.04 16 -1 -7 643.91 23.41 16 1 -6 2.07 1.33 -16 1 6 1.78 1.29 16 1 -6 0.44 1.1 16 -1 -6 1.69 1.4 16 1 -5 1026.93 33.9 -16 1 5 1054.57 34.1 16 1 -5 963.91 33.46 16 -1 -5 1032.38 34.75 16 1 -4 53.09 4.7 -16 1 4 55.38 4.85 16 1 -4 53.34 4.58 16 -1 -4 63.15 5.32 16 1 -3 743.41 27.22 -16 1 3 762.8 27.66 16 -1 -3 777.91 26.64 16 1 -3 808.34 27.23 16 -1 -3 774.31 27.97 16 1 -2 18.75 2.93 16 -1 -2 19.37 2.75 16 1 -2 17.66 2.75 16 -1 -2 17.76 2.95 16 1 -1 68.73 5.48 16 -1 -1 69.12 5.36 16 1 -1 72.92 5.47 16 -1 -1 66.24 5.59 16 1 0 101.7 6.77 16 -1 0 106.41 6.75 16 1 0 95.85 6.41 16 1 1 295.63 13.54 16 -1 1 304.55 13.45 16 1 1 323.89 13.5 16 1 2 136.35 7.93 16 -1 2 132.23 7.71 16 1 2 125.08 7.37 16 1 3 703.44 25.63 16 -1 3 738.75 25.7 16 1 3 729.07 25.25 16 1 4 29.45 3.37 16 -1 4 36.15 3.64 16 1 4 33.46 3.38 16 1 5 564.66 20.09 16 -1 5 549.97 19.93 16 1 5 521.81 19.27 16 1 6 13.01 2.13 16 -1 6 12.56 2.04 16 -2 -7 80.93 5.31 16 2 -6 556.64 20.64 16 -2 -6 602.96 21.03 16 2 -5 6.92 1.73 -16 2 5 6.62 1.73 16 -2 -5 6.06 1.78 16 2 -4 738.78 25.04 16 -2 -4 694.34 24.26 16 -2 -4 735.3 25.03 16 2 -3 9.59 2.17 -16 2 3 3.94 1.56 16 -2 -3 6.53 1.79 16 -2 -3 7.98 1.91 16 2 -2 283.9 12.63 -16 2 2 271.65 12.58 16 -2 -2 277 12.4 16 -2 -2 297.43 12.72 16 -2 -1 9.28 2.04 16 -2 -1 7.24 1.86 -16 2 0 154.62 8.67 16 -2 0 156.27 8.52 16 -2 0 163.73 8.61 -16 2 -1 20.57 2.97 16 -2 1 26.8 3.18 16 -2 1 21.49 2.89 -16 2 -2 610.88 23.25 16 -2 2 677.25 23.66 16 -2 2 678.46 23.36 16 2 3 2.34 1.33 -16 2 -3 1.65 1.09 16 -2 3 1.68 1.17 16 -2 3 0.22 1.07 16 2 4 809.5 27.51 16 -2 4 824.23 27.7 _iucr_refine_instructions_details ; TITL pbbmor_2_a.res in P2(1)/n pbbmor_2.res created by SHELXL-2018/3 at 09:52:35 on 02-Sep-2021 REM Old TITL REM SHELXT solution in P2(1)/n REM R1 0.078, Rweak 0.004, Alpha 0.031, Orientation as input REM Formula found by SHELXT: C24 N4 O4 Cl2 I CELL 1.54184 13.3922 7.9755 23.3368 90 92.582 90 ZERR 4 0.0002 0.0001 0.0003 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O Pb S UNIT 96 104 16 16 4 8 L.S. 15 PLAN 2 SIZE 0.22 0.2 0.16 CONF BOND $H list 4 MORE -1 fmap 2 acta OMIT 4 0 2 OMIT 1 0 1 OMIT 3 2 1 OMIT 7 0 9 OMIT 2 0 0 OMIT -10 1 21 OMIT 6 4 8 OMIT 3 6 1 OMIT 3 8 1 OMIT 3 4 1 OMIT 3 1 5 OMIT 7 2 9 OMIT 0 0 2 OMIT 2 4 0 OMIT 3 3 5 REM REM REM WGHT 0.007900 15.181309 FVAR 0.24277 PB1 5 0.107003 0.017641 0.444109 11.00000 0.01146 0.00988 = 0.00953 -0.00052 0.00278 -0.00126 S2 6 0.053384 0.297383 0.498310 11.00000 0.00897 0.01185 = 0.01373 -0.00048 0.00018 0.00185 S1 6 0.304688 0.067577 0.456739 11.00000 0.01190 0.01616 = 0.00962 0.00258 0.00203 0.00205 O3 4 0.622405 0.031171 0.348736 11.00000 0.01189 0.03608 = 0.02010 -0.00215 0.00439 -0.00122 O4 4 0.393263 0.615962 0.511864 11.00000 0.01643 0.01593 = 0.02173 0.00305 0.00217 -0.00391 O2 4 0.143049 -0.045404 0.545772 11.00000 0.02233 0.01230 = 0.00941 0.00044 0.00353 -0.00054 O1 4 0.133597 0.201624 0.362632 11.00000 0.01238 0.01515 = 0.01455 0.00318 0.00138 -0.00097 N1 3 0.303264 0.244333 0.356874 11.00000 0.01291 0.01489 = 0.01523 0.00558 0.00484 0.00222 N3 3 0.415612 0.029382 0.365881 11.00000 0.00990 0.02055 = 0.01066 0.00244 0.00138 0.00414 N2 3 0.170010 0.208631 0.591974 11.00000 0.01520 0.01354 = 0.00955 0.00112 0.00113 -0.00198 N4 3 0.218960 0.440734 0.543691 11.00000 0.01572 0.00945 = 0.01121 0.00208 0.00094 -0.00053 C14 1 0.150889 0.045617 0.590098 11.00000 0.00637 0.01375 = 0.01515 0.00107 0.00190 0.00226 C23 1 0.399835 0.483002 0.552800 11.00000 0.01583 0.01567 = 0.02121 0.00205 0.00138 0.00044 H23A 2 0.460171 0.516216 0.579956 11.00000 0.00988 H23B 2 0.417887 0.376226 0.534636 11.00000 0.02357 C15 1 0.142898 -0.041047 0.646641 11.00000 0.00664 0.01893 = 0.01081 0.00310 0.00365 0.00251 C9 1 0.483079 -0.083520 0.398977 11.00000 0.01418 0.01441 = 0.01423 0.00149 0.00256 0.00496 H9A 2 0.485627 -0.190304 0.377960 11.00000 0.01488 H9B 2 0.463703 -0.107941 0.436436 11.00000 0.01347 C10 1 0.585534 -0.004100 0.404204 11.00000 0.01350 0.02673 = 0.01690 -0.00301 -0.00186 0.00222 H10A 2 0.576777 0.108085 0.425860 11.00000 0.03236 H10B 2 0.636841 -0.076722 0.425681 11.00000 0.02179 C22 1 0.313689 0.581550 0.470742 11.00000 0.01748 0.01451 = 0.01582 0.00182 0.00285 -0.00144 H22A 2 0.327591 0.485164 0.447291 11.00000 0.01065 H22B 2 0.307774 0.681240 0.442705 11.00000 0.01833 C17 1 0.119223 -0.294529 0.700561 11.00000 0.02224 0.01800 = 0.02461 0.00819 -0.00175 -0.00376 H17 2 0.108855 -0.398981 0.699695 11.00000 0.01781 C13 1 0.156254 0.312166 0.546844 11.00000 0.00930 0.01256 = 0.01153 -0.00283 0.00450 0.00256 C3 1 0.189936 0.472212 0.338389 11.00000 0.01587 0.01039 = 0.01155 0.00087 -0.00455 0.00117 C8 1 0.097315 0.543170 0.348670 11.00000 0.01688 0.01973 = 0.00956 0.00103 -0.00301 0.00332 H8 2 0.049207 0.474181 0.364177 11.00000 0.01916 C12 1 0.453730 0.069349 0.309393 11.00000 0.01376 0.02450 = 0.01201 0.00360 0.00271 0.00550 H12A 2 0.414574 0.138100 0.290615 11.00000 0.02254 H12B 2 0.456234 -0.041690 0.284436 11.00000 0.02478 C20 1 0.157951 0.047810 0.698013 11.00000 0.01747 0.01904 = 0.01349 0.00170 0.00309 0.00316 H20 2 0.176830 0.159531 0.698774 11.00000 0.01378 C1 1 0.339649 0.115728 0.387417 11.00000 0.01004 0.01278 = 0.01261 -0.00080 -0.00078 -0.00192 C4 1 0.263268 0.571134 0.314404 11.00000 0.01818 0.01818 = 0.01332 0.00098 0.00023 -0.00048 H4 2 0.308814 0.523864 0.303616 11.00000 0.04432 C11 1 0.558012 0.142185 0.317544 11.00000 0.02269 0.02198 = 0.01788 0.00065 0.00963 -0.00253 H11A 2 0.585966 0.152791 0.280880 11.00000 0.00502 H11B 2 0.557723 0.258563 0.337372 11.00000 0.03437 C7 1 0.078469 0.710108 0.335794 11.00000 0.02980 0.01816 = 0.01420 -0.00355 -0.00483 0.01067 H7 2 0.008643 0.759081 0.343456 11.00000 0.02135 C5 1 0.243548 0.737227 0.300847 11.00000 0.03438 0.01542 = 0.01412 0.00286 -0.00488 -0.00893 H5 2 0.290437 0.803437 0.284708 11.00000 0.03456 C24 1 0.303792 0.467396 0.584858 11.00000 0.01703 0.01274 = 0.01415 -0.00029 -0.00110 -0.00239 H24A 2 0.305326 0.379931 0.610341 11.00000 0.01052 H24B 2 0.291345 0.570286 0.604606 11.00000 0.00585 C18 1 0.134771 -0.206713 0.751466 11.00000 0.01953 0.02942 = 0.01408 0.01122 0.00024 -0.00019 H18 2 0.133803 -0.268879 0.785621 11.00000 0.03467 C2 1 0.208022 0.292975 0.354828 11.00000 0.01533 0.01349 = 0.00687 -0.00050 0.00181 0.00117 C16 1 0.122677 -0.211174 0.648323 11.00000 0.01360 0.01776 = 0.01343 0.00236 -0.00052 -0.00188 H16 2 0.110639 -0.267920 0.615165 11.00000 0.01899 C19 1 0.153806 -0.036942 0.750238 11.00000 0.02405 0.02604 = 0.01073 0.00070 0.00261 0.00394 H19 2 0.166347 0.024912 0.787610 11.00000 0.03703 C6 1 0.151631 0.807721 0.311501 11.00000 0.04620 0.01143 = 0.01403 -0.00407 -0.00930 0.00243 H6 2 0.136502 0.937302 0.306975 11.00000 0.02324 C21 1 0.213729 0.571551 0.498989 11.00000 0.01644 0.00724 = 0.01607 0.00397 -0.00179 -0.00020 H21A 2 0.200422 0.674569 0.513958 11.00000 0.01665 H21B 2 0.159893 0.543494 0.470471 11.00000 0.00948 HKLF 4 REM pbbmor_2_a.res in P2(1)/n REM wR2 = 0.0585, GooF = S = 1.161, Restrained GooF = 1.161 for all data REM R1 = 0.0239 for 4957 Fo > 4sig(Fo) and 0.0241 for all 5001 data REM 420 parameters refined using 0 restraints END WGHT 0.0111 13.5152 REM Highest difference peak 1.330, deepest hole -1.778, 1-sigma level 0.132 Q1 1 0.0894 0.4848 0.4619 11.00000 0.05 1.33 Q2 1 0.1281 0.4848 0.4282 11.00000 0.05 1.25 REM The information below was added by Olex2. REM REM R1 = 0.0239 for 4957 Fo > 4sig(Fo) and 0.0241 for all 31297 data REM 420 parameters refined using n/a restraints REM Highest difference peak 1.33, deepest hole -1.78 REM Mean Shift 0, Max Shift 0.002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0241 REM R1_gt = 0.0239 REM wR_ref = 0.0585 REM GOOF = 1.161 REM Shift_max = 0.002 REM Shift_mean = 0 REM Reflections_all = 31297 REM Reflections_gt = 4957 REM Parameters = 420 REM Hole = -1.78 REM Peak = 1.33 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.569 _oxdiff_exptl_absorpt_empirical_full_min 0.818