#============================================================================= data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 16 _journal_issue 4 _journal_year 2025 _journal_page_first 370 _journal_page_last 378 #============================================================================= data_cu_HAKAN_SALIH_2024_0m_a _audit_creation_date 2025-10-03 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _shelxl_version_number 2013-4 _audit_contact_author_address ; Department of Chemistry, Faculty of Science, Mersin University, Mersin, TR 33343, Turkey ; _audit_contact_author_email ; hakan.arslan@mersin.edu.tr ; _audit_contact_author_name ; Hakan Arslan ; _audit_contact_author_phone ; +90.532.7073122 ; _publ_contact_author_id_orcid ; https://orcid.org/0000-0002-3697-577X ; _publ_contact_author_name ; Ummuhan Solmaz ; _publ_contact_author_address ; Department of Chemistry, Faculty of Science, Mersin University, Mersin, TR 33343, Turkey ; _publ_contact_author_email ; ummuhansolmaz@mersin.edu.tr ; _publ_contact_author_fax ; +903243610047 ; _publ_contact_author_phone ; +905392183364 ; _publ_requested_journal ; European Journal of Chemistry ; _publ_section_title ; Crystal structure and supramolecular features of O-ethyl pivaloylcarbamothioate: Insights from Hirshfeld surface and energy framework analyses ; _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ; O-ethyl pivaloylcarbamothioate ; _chemical_name_systematic ; O-ethyl pivaloylcarbamothioate ; _chemical_formula_moiety 'C8 H15 N O2 S' _chemical_formula_sum 'C8 H15 N O2 S' _chemical_formula_weight 189.27 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 61 _space_group_name_H-M_alt 'P b c a' _space_group_name_Hall '-P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 10.144(9) _cell_length_b 10.230(6) _cell_length_c 19.934(19) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2069(3) _cell_formula_units_Z 8 _cell_measurement_reflns_used 6036 _cell_measurement_temperature 298.15(2) _cell_measurement_theta_max 76.369 _cell_measurement_theta_min 4.427 _shelx_estimated_absorpt_T_max 0.746 _shelx_estimated_absorpt_T_min 0.583 _exptl_absorpt_coefficient_mu 2.506 _exptl_absorpt_correction_T_max 0.7543 _exptl_absorpt_correction_T_min 0.5089 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1419 before and 0.1125 after correction. The Ratio of minimum to maximum transmission is 0.6747. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.216 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 816 _exptl_crystal_size_max 0.241 _exptl_crystal_size_mid 0.217 _exptl_crystal_size_min 0.124 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.1349 _diffrn_reflns_av_unetI/netI 0.0658 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 25062 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 79.836 _diffrn_reflns_theta_min 4.436 _diffrn_ambient_temperature 298.15(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source 'sealed tube' _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1452 _reflns_number_total 2246 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT V8.38A (Bruker, 2018)' _computing_data_collection ? _computing_data_reduction 'SAINT V8.38A (Bruker, 2018)' _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2013/4 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _refine_diff_density_max 0.280 _refine_diff_density_min -0.377 _refine_diff_density_rms 0.067 _refine_ls_extinction_coef 0.0077(12) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.024 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 118 _refine_ls_number_reflns 2246 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1261 _refine_ls_R_factor_gt 0.0942 _refine_ls_restrained_S_all 1.024 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0607P)^2^+5.8114P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2259 _refine_ls_wR_factor_ref 0.2485 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C7(H7A,H7B) 2.b Idealised Me refined as rotating group: C4(H4A,H4B,H4C), C5(H5A,H5B,H5C), C6(H6A,H6B,H6C), C8(H8A,H8B,H8C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.54294(16) 0.84457(15) 0.54008(8) 0.0818(6) Uani 1 1 d . . . . . O1 O 0.7112(3) 0.4928(3) 0.6459(2) 0.0711(11) Uani 1 1 d . . . . . O2 O 0.5054(3) 0.6080(3) 0.58975(18) 0.0670(10) Uani 1 1 d . . . . . N1 N 0.6902(4) 0.7093(4) 0.6226(2) 0.0597(10) Uani 1 1 d . . . . . H1 H 0.732(6) 0.794(6) 0.632(3) 0.095(19) Uiso 1 1 d . . . . . C1 C 0.7531(4) 0.6027(4) 0.6521(2) 0.0526(10) Uani 1 1 d . . . . . C2 C 0.5768(5) 0.7145(5) 0.5838(2) 0.0580(12) Uani 1 1 d . . . . . C3 C 0.8755(5) 0.6357(4) 0.6926(2) 0.0557(11) Uani 1 1 d . . . . . C4 C 0.9748(5) 0.7108(6) 0.6489(3) 0.0817(17) Uani 1 1 d . . . . . H4A H 0.9970 0.6591 0.6103 0.122 Uiso 1 1 calc R U . . . H4B H 1.0531 0.7282 0.6744 0.122 Uiso 1 1 calc R U . . . H4C H 0.9364 0.7919 0.6346 0.122 Uiso 1 1 calc R U . . . C5 C 0.8354(6) 0.7201(5) 0.7526(3) 0.0782(16) Uani 1 1 d . . . . . H5A H 0.7966 0.8000 0.7368 0.117 Uiso 1 1 calc R U . . . H5B H 0.9118 0.7397 0.7791 0.117 Uiso 1 1 calc R U . . . H5C H 0.7724 0.6735 0.7794 0.117 Uiso 1 1 calc R U . . . C6 C 0.9392(6) 0.5105(5) 0.7175(3) 0.0809(17) Uani 1 1 d . . . . . H6A H 0.8782 0.4641 0.7456 0.121 Uiso 1 1 calc R U . . . H6B H 1.0170 0.5314 0.7428 0.121 Uiso 1 1 calc R U . . . H6C H 0.9628 0.4569 0.6798 0.121 Uiso 1 1 calc R U . . . C7 C 0.3803(5) 0.6029(6) 0.5532(3) 0.0786(16) Uani 1 1 d . . . . . H7A H 0.3961 0.6060 0.5052 0.094 Uiso 1 1 calc R U . . . H7B H 0.3252 0.6766 0.5654 0.094 Uiso 1 1 calc R U . . . C8 C 0.3147(6) 0.4780(6) 0.5717(4) 0.095(2) Uani 1 1 d . . . . . H8A H 0.2325 0.4708 0.5482 0.142 Uiso 1 1 calc R U . . . H8B H 0.2987 0.4766 0.6191 0.142 Uiso 1 1 calc R U . . . H8C H 0.3706 0.4060 0.5597 0.142 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0881(11) 0.0704(9) 0.0869(10) 0.0188(7) -0.0168(8) 0.0075(7) O1 0.066(2) 0.0458(17) 0.102(3) 0.0036(17) -0.0193(19) -0.0046(15) O2 0.0574(19) 0.067(2) 0.076(2) 0.0050(17) -0.0176(17) -0.0053(16) N1 0.055(2) 0.047(2) 0.078(3) 0.0049(18) -0.0148(19) -0.0005(17) C1 0.051(2) 0.041(2) 0.065(3) 0.0027(19) -0.003(2) 0.0018(18) C2 0.056(3) 0.057(3) 0.060(3) -0.001(2) -0.004(2) 0.002(2) C3 0.053(2) 0.051(2) 0.063(3) 0.003(2) -0.004(2) 0.0004(19) C4 0.056(3) 0.095(4) 0.095(4) 0.022(3) 0.004(3) -0.004(3) C5 0.086(4) 0.077(3) 0.072(3) -0.008(3) -0.011(3) 0.003(3) C6 0.079(4) 0.062(3) 0.101(4) 0.009(3) -0.030(3) 0.009(3) C7 0.059(3) 0.086(4) 0.090(4) 0.000(3) -0.023(3) 0.001(3) C8 0.070(4) 0.096(5) 0.119(5) 0.002(4) -0.023(4) -0.020(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C2 1.628(5) . ? O1 C1 1.208(5) . ? O2 C2 1.314(6) . ? O2 C7 1.464(6) . ? N1 H1 0.98(6) . ? N1 C1 1.394(5) . ? N1 C2 1.386(6) . ? C1 C3 1.520(6) . ? C3 C4 1.537(7) . ? C3 C5 1.530(7) . ? C3 C6 1.518(6) . ? C4 H4A 0.9600 . ? C4 H4B 0.9600 . ? C4 H4C 0.9600 . ? C5 H5A 0.9600 . ? C5 H5B 0.9600 . ? C5 H5C 0.9600 . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 C8 1.487(8) . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O2 C7 117.5(4) . . ? C1 N1 H1 114(4) . . ? C2 N1 H1 116(4) . . ? C2 N1 C1 130.1(4) . . ? O1 C1 N1 121.6(4) . . ? O1 C1 C3 123.3(4) . . ? N1 C1 C3 115.1(4) . . ? O2 C2 S1 127.6(4) . . ? O2 C2 N1 112.1(4) . . ? N1 C2 S1 120.3(4) . . ? C1 C3 C4 110.2(4) . . ? C1 C3 C5 108.9(4) . . ? C5 C3 C4 109.6(5) . . ? C6 C3 C1 109.5(4) . . ? C6 C3 C4 109.1(4) . . ? C6 C3 C5 109.5(4) . . ? C3 C4 H4A 109.5 . . ? C3 C4 H4B 109.5 . . ? C3 C4 H4C 109.5 . . ? H4A C4 H4B 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C3 C6 H6A 109.5 . . ? C3 C6 H6B 109.5 . . ? C3 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? O2 C7 H7A 110.3 . . ? O2 C7 H7B 110.3 . . ? O2 C7 C8 107.1(5) . . ? H7A C7 H7B 108.5 . . ? C8 C7 H7A 110.3 . . ? C8 C7 H7B 110.3 . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C3 C4 124.8(5) . . . . ? O1 C1 C3 C5 -114.9(5) . . . . ? O1 C1 C3 C6 4.8(7) . . . . ? N1 C1 C3 C4 -55.9(6) . . . . ? N1 C1 C3 C5 64.4(5) . . . . ? N1 C1 C3 C6 -175.9(4) . . . . ? C1 N1 C2 S1 -164.9(4) . . . . ? C1 N1 C2 O2 17.1(7) . . . . ? C2 O2 C7 C8 -176.1(5) . . . . ? C2 N1 C1 O1 0.5(8) . . . . ? C2 N1 C1 C3 -178.8(5) . . . . ? C7 O2 C2 S1 0.1(7) . . . . ? C7 O2 C2 N1 177.9(4) . . . . ? _shelx_res_file ; TITL cu_HAKAN_SALIH_2024_0m_a.res in Pbca REM Old TITL cu_HAKAN_SALIH_0m in P1 REM SHELXT solution in Pbca REM R1 0.213, Rweak 0.017, Alpha 0.024, Orientation as input REM Formula found by SHELXT: C8 N O2 S CELL 1.54178 10.1436 10.2296 19.9345 90 90 90 ZERR 8 0.0085 0.0056 0.0191 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O S UNIT 64 120 8 16 8 L.S. 10 PLAN 1 SIZE 0.124 0.217 0.241 TEMP 25.00(2) CONF BOND $H LIST 4 MORE -1 fmap 2 acta REM REM REM WGHT 0.060700 5.811400 EXTI 0.007720 FVAR 0.95325 S1 5 0.542944 0.844570 0.540075 11.00000 0.08813 0.07043 = 0.08690 0.01880 -0.01678 0.00752 O1 4 0.711168 0.492791 0.645880 11.00000 0.06560 0.04584 = 0.10173 0.00362 -0.01933 -0.00458 O2 4 0.505415 0.607986 0.589750 11.00000 0.05736 0.06741 = 0.07608 0.00503 -0.01759 -0.00532 N1 3 0.690206 0.709343 0.622555 11.00000 0.05471 0.04682 = 0.07765 0.00488 -0.01484 -0.00052 H1 2 0.732264 0.793566 0.631566 11.00000 0.09524 C1 1 0.753052 0.602723 0.652062 11.00000 0.05143 0.04100 = 0.06527 0.00271 -0.00347 0.00179 C2 1 0.576828 0.714501 0.583847 11.00000 0.05616 0.05738 = 0.06035 -0.00108 -0.00401 0.00185 C3 1 0.875531 0.635743 0.692596 11.00000 0.05298 0.05073 = 0.06331 0.00337 -0.00403 0.00037 C4 1 0.974817 0.710777 0.648875 11.00000 0.05582 0.09461 = 0.09456 0.02203 0.00373 -0.00364 AFIX 137 H4A 2 0.997016 0.659144 0.610280 11.00000 -1.50000 H4B 2 1.053085 0.728159 0.674438 11.00000 -1.50000 H4C 2 0.936354 0.791886 0.634602 11.00000 -1.50000 AFIX 0 C5 1 0.835360 0.720068 0.752574 11.00000 0.08614 0.07688 = 0.07168 -0.00850 -0.01122 0.00308 AFIX 137 H5A 2 0.796625 0.799988 0.736804 11.00000 -1.50000 H5B 2 0.911817 0.739660 0.779116 11.00000 -1.50000 H5C 2 0.772425 0.673478 0.779445 11.00000 -1.50000 AFIX 0 C6 1 0.939219 0.510539 0.717470 11.00000 0.07947 0.06207 = 0.10102 0.00889 -0.02955 0.00909 AFIX 137 H6A 2 0.878214 0.464145 0.745555 11.00000 -1.50000 H6B 2 1.016960 0.531430 0.742757 11.00000 -1.50000 H6C 2 0.962767 0.456852 0.679833 11.00000 -1.50000 AFIX 0 C7 1 0.380339 0.602929 0.553160 11.00000 0.05925 0.08628 = 0.09031 -0.00002 -0.02278 0.00104 AFIX 23 H7A 2 0.396123 0.606048 0.505194 11.00000 -1.20000 H7B 2 0.325173 0.676603 0.565423 11.00000 -1.20000 AFIX 0 C8 1 0.314725 0.478005 0.571683 11.00000 0.06996 0.09555 = 0.11864 0.00175 -0.02324 -0.01970 AFIX 137 H8A 2 0.232458 0.470837 0.548161 11.00000 -1.50000 H8B 2 0.298736 0.476576 0.619143 11.00000 -1.50000 H8C 2 0.370632 0.405975 0.559700 11.00000 -1.50000 AFIX 0 HKLF 4 REM cu_HAKAN_SALIH_2024_0m_a.res in Pbca REM R1 = 0.0942 for 1452 Fo > 4sig(Fo) and 0.1261 for all 2246 data REM 118 parameters refined using 0 restraints END WGHT 0.0646 5.5989 REM Highest difference peak 0.280, deepest hole -0.377, 1-sigma level 0.067 Q1 1 0.4622 0.9422 0.5124 11.00000 0.05 0.28 ; _shelx_res_checksum 59750 _shelx_hkl_file ; 1 0 0 1.00 0.60 -1 0 0 2.00 0.80 2 0 0 3471.25 336.37 -2 0 0 2834.02 336.27 -3 0 0 4.90 3.10 3 0 0 -0.50 1.70 4 0 0 4634.54 470.35 -4 0 0 4177.68 470.35 6 0 0 288.47 35.10 6 0 0 297.47 33.60 7 0 0 -7.80 15.50 7 0 0 52.99 21.50 8 0 0 91.89 24.20 9 0 0 25.10 19.70 9 0 0 24.00 17.60 9 0 0 -12.70 11.80 9 0 0 -23.60 23.90 10 0 0 16.50 16.90 10 0 0 18.20 10.80 -10 0 0 -15.00 12.00 11 0 0 10.90 9.70 -11 0 0 -0.30 11.20 11 0 0 -9.00 12.10 11 0 0 1.20 9.30 -12 0 0 22.00 10.60 12 0 0 37.90 13.30 0 1 0 0.00 1.60 0 -1 0 1.30 0.70 0 1 0 -0.80 0.60 0 1 0 0.20 0.70 -1 1 0 0.70 1.70 1 1 0 0.50 1.10 -2 1 0 8.00 2.80 -2 1 0 5.40 1.60 3 1 0 -2.50 1.90 -3 1 0 -1.00 3.30 4 1 0 1621.74 174.98 -4 1 0 1644.74 175.18 -5 -1 0 -4.40 6.70 5 1 0 2.60 3.60 5 1 0 -3.10 6.20 -5 1 0 1.70 7.40 6 1 0 3188.78 326.47 6 1 0 2888.91 325.57 7 -1 0 29.50 14.80 7 1 0 -1.70 12.30 7 1 0 37.30 14.60 7 -1 0 -10.60 14.40 7 -1 0 45.50 23.50 7 1 0 -4.10 18.30 7 1 0 2.50 8.40 8 1 0 -24.10 19.00 8 1 0 4.30 21.30 8 1 0 50.59 16.30 8 -1 0 16.70 12.70 9 1 0 -17.80 11.70 9 -1 0 -5.00 19.10 9 1 0 -5.80 16.50 9 1 0 20.80 25.50 9 -1 0 3.70 11.30 9 -1 0 33.60 13.00 9 1 0 28.50 17.30 9 -1 0 15.80 24.70 10 1 0 127.29 21.70 10 1 0 81.29 18.00 -10 -1 0 71.29 19.10 10 1 0 97.29 20.50 10 -1 0 119.59 24.30 -10 1 0 104.39 21.30 10 -1 0 95.29 17.20 10 1 0 149.88 26.30 11 -1 0 -12.00 10.10 -11 -1 0 -3.60 10.50 11 1 0 -7.00 10.40 -11 1 0 13.10 12.40 11 1 0 -11.20 13.00 11 1 0 -9.10 9.10 11 -1 0 26.80 14.70 11 -1 0 -12.80 8.10 12 -1 0 -2.40 8.40 -12 -1 0 10.80 8.50 -12 1 0 5.30 10.00 12 1 0 24.10 11.40 12 -1 0 -2.80 11.10 0 2 0 700.63 83.19 0 -2 0 851.81 82.99 1 2 0 0.60 1.40 1 2 0 1.00 1.60 -1 2 0 -4.30 2.90 -2 2 0 3796.92 398.36 2 2 0 3725.83 397.96 2 2 0 3663.53 398.06 3 2 0 0.30 2.40 3 2 0 2.50 3.20 -3 2 0 5.70 4.20 -4 2 0 241.38 29.00 4 2 0 257.87 28.90 4 2 0 255.97 28.30 5 2 0 -5.90 6.50 -5 2 0 10.20 8.90 6 2 0 145.89 17.70 6 2 0 106.19 19.90 8 -2 0 79.69 18.10 8 -2 0 130.59 23.60 8 2 0 89.59 24.90 9 2 0 -14.30 13.00 9 -2 0 -32.40 22.50 9 -2 0 -16.70 10.60 9 -2 0 -3.50 12.10 9 2 0 -12.40 13.10 9 -2 0 -38.20 30.00 9 2 0 10.40 30.10 9 2 0 -18.00 16.40 9 2 0 -11.50 15.10 -10 -2 0 17.10 13.00 10 2 0 13.30 13.80 10 2 0 57.29 17.20 10 -2 0 -5.60 19.00 -10 2 0 20.30 15.80 10 -2 0 16.80 10.50 10 -2 0 20.70 11.30 10 2 0 32.00 13.80 10 2 0 22.40 15.80 11 -2 0 12.20 8.80 11 -2 0 -15.00 14.20 11 2 0 -2.20 13.00 11 2 0 11.20 9.90 -11 -2 0 -4.80 9.50 -11 2 0 26.50 13.80 -12 -2 0 14.00 12.50 -12 2 0 0.50 21.10 12 -2 0 12.80 12.50 12 -2 0 4.00 8.90 -12 -2 0 5.70 7.20 12 2 0 7.80 12.00 0 3 0 1.10 2.00 0 -3 0 -0.10 1.80 -1 3 0 0.80 2.10 -1 3 0 -4.00 3.90 1 3 0 0.70 2.20 1 3 0 -0.30 2.00 2 3 0 480.25 52.39 -2 3 0 486.15 52.99 2 3 0 476.35 51.99 -3 3 0 -0.10 5.80 3 3 0 -1.40 3.10 3 3 0 0.00 3.00 4 3 0 62.09 12.90 4 3 0 59.19 10.10 -4 3 0 53.89 12.50 5 3 0 -3.40 4.80 -5 3 0 -9.60 11.90 5 3 0 1.90 7.50 6 3 0 386.46 44.00 6 3 0 285.87 49.60 6 3 0 286.77 45.10 6 3 0 405.46 40.80 7 3 0 36.50 12.80 7 -3 0 -2.90 25.10 7 3 0 -1.10 16.20 7 3 0 19.30 9.70 8 -3 0 467.35 56.69 8 -3 0 474.25 62.49 8 3 0 550.54 57.49 8 3 0 426.76 65.19 8 -3 0 481.85 57.69 8 3 0 514.95 59.19 8 -3 0 452.75 64.99 9 3 0 10.20 13.30 9 3 0 -15.00 11.40 9 3 0 -11.90 16.30 9 3 0 -3.70 11.70 -9 3 0 -5.90 18.80 9 -3 0 -12.70 10.60 9 -3 0 -16.00 25.30 10 3 0 29.80 15.90 -10 -3 0 -16.00 12.70 10 3 0 -7.50 13.00 10 -3 0 78.79 33.80 10 -3 0 16.30 10.80 10 3 0 27.10 21.30 10 -3 0 10.00 10.90 -10 3 0 -13.90 18.50 11 3 0 -0.50 13.30 11 -3 0 5.80 7.30 -11 -3 0 5.70 9.90 11 -3 0 -16.70 17.30 11 -3 0 3.30 7.60 12 -3 0 0.20 7.20 -12 -3 0 -5.10 12.60 12 3 0 -13.30 12.10 -12 -3 0 -6.50 9.90 12 -3 0 -0.40 16.10 0 4 0 38.50 6.70 1 4 0 -1.20 3.00 2 4 0 4812.12 510.05 2 4 0 4958.00 509.35 -2 4 0 4549.34 509.35 -3 4 0 2.40 3.60 -3 4 0 0.10 8.50 3 4 0 -1.70 4.20 3 4 0 -1.30 3.90 4 4 0 39.10 8.10 4 4 0 28.20 7.40 5 4 0 6.10 6.40 5 4 0 9.30 8.50 6 -4 0 23.20 29.20 6 4 0 -5.40 13.60 6 4 0 4.10 7.70 6 4 0 16.40 13.70 6 4 0 3.20 11.70 6 -4 0 -43.90 41.10 6 -4 0 13.80 14.30 7 4 0 71.89 22.80 7 -4 0 39.60 26.20 7 -4 0 83.49 23.40 8 4 0 1299.87 146.99 8 -4 0 1351.96 146.99 8 -4 0 1266.77 153.08 8 4 0 1393.56 148.09 8 -4 0 1495.05 153.98 8 4 0 1477.75 149.69 8 4 0 1170.98 155.78 8 4 0 1295.27 149.49 9 4 0 -7.20 17.10 9 4 0 8.60 11.70 9 -4 0 -1.10 10.90 -9 -4 0 -2.00 13.70 9 -4 0 1.70 10.50 9 4 0 9.20 13.50 9 -4 0 19.10 26.70 -10 -4 0 58.09 15.50 10 4 0 76.69 26.50 10 -4 0 90.19 16.20 10 4 0 29.50 12.20 10 -4 0 70.39 25.00 10 4 0 54.29 15.00 11 -4 0 33.20 18.40 -11 -4 0 -5.30 9.50 11 -4 0 2.00 6.90 11 -4 0 -7.40 7.30 -12 -4 0 6.80 7.00 12 -4 0 -4.00 17.90 -12 -4 0 -0.80 6.70 0 5 0 -4.30 4.30 -1 5 0 -1.20 4.00 1 5 0 1.70 6.50 2 5 0 3.20 4.90 -2 5 0 9.00 4.50 3 5 0 2.30 5.10 3 5 0 11.00 6.50 -3 5 0 14.40 5.70 4 5 0 1348.86 139.29 4 5 0 1219.18 138.79 5 5 0 -18.10 16.60 5 5 0 -37.10 29.00 -5 5 0 26.90 14.40 5 5 0 8.20 8.10 5 5 0 8.30 14.30 5 5 0 0.40 14.00 5 -5 0 -15.20 12.60 6 -5 0 1157.48 134.79 6 5 0 1181.18 133.29 6 5 0 1312.77 133.09 6 -5 0 1092.39 133.09 6 5 0 1222.88 138.19 6 5 0 1304.67 132.99 6 -5 0 1227.88 143.29 7 5 0 24.30 12.70 7 5 0 0.90 14.40 7 -5 0 16.00 27.50 8 -5 0 231.48 51.89 8 5 0 292.37 36.80 8 5 0 237.08 45.00 8 5 0 309.77 35.70 8 -5 0 296.27 36.10 9 -5 0 -7.80 10.30 -9 -5 0 8.60 15.80 9 5 0 -17.70 17.90 9 -5 0 -2.70 9.60 9 5 0 1.60 12.00 9 5 0 10.50 13.00 -10 -5 0 0.50 12.10 10 5 0 3.20 15.40 10 -5 0 4.40 8.00 10 5 0 6.10 9.00 10 -5 0 52.59 27.30 10 -5 0 11.50 8.50 -11 -5 0 -5.00 10.40 11 -5 0 8.50 6.90 11 -5 0 19.70 25.50 11 -5 0 -2.10 5.80 0 6 0 2301.17 247.18 -1 6 0 2.10 6.40 1 6 0 -2.60 5.60 -2 6 0 208.98 23.40 2 6 0 159.18 23.70 3 6 0 -4.70 6.70 4 6 0 209.28 28.40 4 6 0 234.88 32.60 -4 6 0 194.78 32.00 4 6 0 233.38 38.20 4 -6 0 359.06 55.19 4 6 0 185.18 47.30 5 6 0 41.70 17.70 5 6 0 32.70 10.60 5 -6 0 74.39 27.70 6 -6 0 132.29 34.30 6 6 0 74.49 35.00 7 -6 0 18.40 26.50 7 -6 0 -4.80 14.00 7 6 0 -14.80 13.00 -7 -6 0 36.60 23.30 7 6 0 34.50 21.70 7 6 0 -9.10 18.00 8 6 0 508.95 56.29 8 -6 0 464.75 56.39 8 6 0 463.75 62.39 -8 -6 0 503.55 63.89 8 6 0 495.45 57.09 9 -6 0 18.10 9.70 9 6 0 13.00 11.80 9 6 0 1.30 8.50 9 -6 0 13.40 9.60 9 6 0 -12.30 18.10 -9 -6 0 -0.20 14.80 9 -6 0 17.90 36.60 10 -6 0 2.00 6.80 10 -6 0 -5.70 6.60 -10 -6 0 -17.30 13.30 10 -6 0 53.99 30.60 10 6 0 2.20 19.60 -11 -6 0 -7.80 6.00 11 -6 0 -4.50 5.50 11 6 0 7.20 12.10 11 -6 0 -1.80 6.10 0 7 0 5.40 15.30 0 7 0 -0.10 8.30 0 7 0 7.80 15.50 0 7 0 -25.50 23.30 -1 7 0 -8.60 16.10 1 7 0 -2.50 13.80 -1 7 0 14.80 13.50 -1 7 0 34.00 22.30 1 7 0 18.30 25.20 -1 7 0 17.80 15.80 -1 7 0 8.10 8.30 1 7 0 -9.00 8.40 -2 7 0 434.46 47.50 -2 7 0 292.37 49.10 2 7 0 404.66 57.19 2 7 0 392.76 46.10 2 7 0 394.16 51.99 2 7 0 365.86 46.90 3 7 0 44.00 22.90 -3 7 0 73.59 19.60 -3 7 0 50.99 15.80 4 7 0 -18.90 24.90 -4 7 0 3.70 15.60 4 7 0 19.90 23.80 -4 7 0 20.30 18.30 5 7 0 -9.10 14.10 -5 7 0 10.90 21.70 5 7 0 45.70 17.40 5 7 0 31.40 24.50 6 7 0 4.50 18.60 6 7 0 59.79 22.80 6 -7 0 -17.50 24.60 6 7 0 23.20 15.70 6 7 0 28.00 11.20 -6 7 0 30.00 24.70 7 7 0 -7.90 8.90 7 7 0 -4.50 12.70 7 -7 0 -14.40 12.00 8 7 0 14.60 9.70 8 7 0 12.60 20.10 9 -7 0 -7.60 7.40 -9 7 0 2.60 10.10 9 7 0 -7.00 8.70 9 -7 0 -13.50 7.60 10 -7 0 5.70 6.30 10 -7 0 -6.10 6.70 -10 -7 0 -1.90 7.60 10 7 0 -5.40 11.80 0 8 0 1074.99 112.79 0 8 0 957.90 112.59 -1 8 0 71.29 14.90 1 8 0 52.19 14.30 -1 8 0 40.10 15.90 1 8 0 33.70 13.80 2 8 0 71.19 15.90 -2 8 0 77.39 20.80 -3 8 0 24.20 14.70 3 8 0 54.19 22.80 3 8 0 32.30 12.90 4 -8 0 6.90 22.20 4 8 0 21.30 11.30 4 8 0 46.50 20.90 -4 8 0 6.50 14.10 -4 8 0 37.50 18.80 4 8 0 -14.40 17.80 -4 8 0 19.20 16.50 5 8 0 35.10 22.40 5 8 0 -6.20 26.80 -5 8 0 25.20 15.00 5 -8 0 10.50 22.40 -5 8 0 13.10 19.10 5 8 0 4.40 10.50 6 8 0 -19.80 20.90 6 8 0 31.70 16.10 6 -8 0 -4.10 23.90 6 -8 0 9.40 12.30 6 8 0 10.10 9.30 6 8 0 27.70 16.40 -6 8 0 -4.80 19.00 -7 8 0 13.60 20.40 7 -8 0 18.50 16.00 8 -8 0 -0.40 7.70 8 8 0 4.40 9.00 9 -8 0 0.60 6.40 -9 -8 0 -1.80 7.70 -9 8 0 -5.20 8.40 9 -8 0 -1.20 6.60 -10 -8 0 2.90 8.10 10 8 0 -0.80 8.70 0 9 0 -16.40 11.80 0 9 0 10.60 12.70 1 9 0 1.70 13.10 2 9 0 47.10 21.90 -2 9 0 30.60 14.00 2 9 0 56.39 23.20 2 9 0 3.70 12.30 -2 9 0 6.70 14.40 2 9 0 19.10 13.90 3 9 0 0.60 11.30 -3 9 0 -6.70 12.80 3 9 0 27.20 42.40 3 -9 0 17.90 19.80 3 9 0 -5.70 12.90 -3 9 0 -6.80 16.20 -3 9 0 5.00 13.30 4 -9 0 61.99 23.10 -4 9 0 74.49 20.20 4 9 0 91.99 16.80 -4 9 0 90.99 18.40 4 9 0 47.70 17.30 -4 9 0 80.89 17.80 4 9 0 54.19 14.10 5 9 0 13.20 10.70 5 -9 0 -12.00 37.20 5 9 0 -5.60 13.40 -5 9 0 6.10 12.00 5 9 0 -4.50 18.70 -5 9 0 -8.80 16.20 6 9 0 7.10 9.50 6 9 0 3.40 12.70 6 9 0 26.40 16.50 6 -9 0 20.50 11.80 -6 9 0 41.60 15.90 -6 -9 0 -5.10 13.40 7 9 0 2.20 8.30 7 -9 0 2.60 7.50 7 9 0 -6.80 12.60 -7 9 0 16.50 20.40 -7 -9 0 3.20 9.90 -8 -9 0 0.40 10.10 8 -9 0 19.10 6.60 -8 9 0 12.00 8.80 8 9 0 17.30 8.00 9 -9 0 -0.60 5.30 9 9 0 -11.50 10.20 -9 9 0 -4.10 7.60 9 -9 0 3.00 4.30 0 10 0 347.27 40.90 0 10 0 335.47 43.90 0 10 0 305.17 42.20 -1 10 0 28.20 12.80 -1 10 0 1.60 11.50 -1 10 0 -7.40 20.20 1 10 0 -12.00 10.30 1 10 0 1.10 18.20 1 10 0 -2.40 12.60 -1 10 0 -2.50 14.90 -2 10 0 317.37 40.70 -2 10 0 348.37 38.80 2 -10 0 339.67 45.80 2 10 0 267.87 44.50 -2 10 0 302.77 40.60 2 10 0 275.17 37.50 -3 10 0 -16.00 11.00 3 10 0 30.60 16.20 3 10 0 13.10 11.50 3 10 0 9.00 11.30 -3 10 0 -3.50 12.30 -3 10 0 -11.70 14.20 -4 10 0 16.20 15.00 4 10 0 29.50 15.10 4 -10 0 44.80 18.90 -4 10 0 41.00 19.90 4 10 0 28.10 12.30 4 10 0 58.79 19.20 4 10 0 12.80 11.00 5 10 0 -16.40 10.00 5 10 0 7.20 8.00 -5 10 0 7.50 11.90 5 10 0 -12.00 15.90 6 10 0 -2.70 7.70 6 10 0 14.40 14.50 6 10 0 -1.00 9.70 -6 10 0 0.90 8.30 -6 10 0 -5.70 12.40 6 -10 0 5.80 7.50 7 -10 0 1.10 6.10 -7 10 0 2.60 7.00 7 10 0 3.00 6.90 7 10 0 -13.60 12.90 8 -10 0 4.50 4.40 8 10 0 -2.10 9.30 8 -10 0 -0.20 4.80 -8 10 0 -5.00 5.00 0 11 0 -14.70 13.80 0 11 0 -11.40 11.70 0 11 0 -3.30 8.00 0 11 0 -4.80 10.40 1 11 0 12.70 10.30 1 -11 0 -2.20 12.50 -1 11 0 3.20 9.60 -1 11 0 1.90 8.20 1 11 0 -15.20 11.60 1 11 0 -6.30 15.80 1 11 0 -7.70 8.50 2 11 0 9.90 11.70 2 11 0 17.70 10.30 -2 11 0 21.90 11.40 2 11 0 33.30 17.90 -2 11 0 -5.50 8.40 -2 11 0 8.50 14.90 2 11 0 -2.00 8.30 -2 11 0 16.30 12.10 -2 11 0 13.10 10.10 2 -11 0 21.80 14.80 3 11 0 12.50 11.80 -3 11 0 4.70 9.60 3 11 0 11.20 9.20 -3 11 0 -0.30 8.60 -3 11 0 -6.00 10.20 3 11 0 47.50 19.40 3 11 0 -7.60 7.70 -3 11 0 11.10 11.70 3 -11 0 19.90 17.10 -3 11 0 5.30 11.50 -4 11 0 71.19 15.70 4 11 0 84.29 14.40 4 11 0 43.40 15.40 -4 -11 0 35.30 19.30 -4 11 0 111.29 20.50 -4 11 0 38.80 16.80 -4 11 0 77.49 15.90 5 11 0 -13.40 7.50 -5 11 0 2.50 7.40 -5 11 0 -1.20 9.00 5 -11 0 -6.40 6.30 -5 -11 0 17.30 15.60 5 11 0 4.40 7.40 5 11 0 -0.70 21.30 6 11 0 28.60 12.50 -6 11 0 5.40 7.10 6 -11 0 13.10 6.00 6 11 0 17.50 9.00 -6 -11 0 19.10 11.60 -6 11 0 13.50 9.80 0 -12 0 11.00 16.80 0 12 0 2.70 6.50 0 12 0 -7.70 7.90 0 12 0 1.90 9.10 0 12 0 -0.80 9.90 1 12 0 1.00 5.50 1 12 0 6.90 10.20 -1 12 0 -5.40 8.60 -1 12 0 -3.40 6.90 1 12 0 5.30 7.60 -1 12 0 -6.60 8.40 -1 12 0 7.80 7.90 1 -12 0 18.30 13.50 -2 12 0 -4.50 8.70 2 12 0 7.50 6.10 2 12 0 17.60 9.50 2 12 0 4.00 7.70 -2 12 0 2.40 7.80 -2 12 0 9.50 8.20 -2 12 0 -4.00 9.50 -3 12 0 0.10 7.40 -3 12 0 -7.40 8.30 3 12 0 6.90 8.50 -3 12 0 12.00 10.50 3 12 0 7.80 5.90 3 12 0 -3.00 10.40 -4 12 0 11.90 7.00 4 12 0 8.40 6.00 0 13 0 0.70 6.20 0 13 0 -1.70 4.10 1 13 0 -9.80 7.30 0 0 -1 1.10 0.80 1 0 -1 1.90 1.20 1 0 -1 1.20 0.80 1 0 1 0.50 0.60 2 0 -1 1.20 1.30 2 0 1 3.70 1.50 -2 0 1 0.00 1.30 -3 0 1 7.60 2.70 -3 0 -1 5.90 3.50 -4 0 -1 2.20 4.90 4 0 1 -0.20 2.40 -4 0 1 3.10 5.20 4 0 -1 5.50 2.80 5 0 -1 -5.00 5.20 5 0 -1 -0.50 3.60 5 0 1 6.50 3.70 -5 0 -1 0.40 7.60 6 0 1 -0.10 5.50 6 0 -1 4.10 7.00 6 0 -1 -5.40 5.60 7 0 1 50.39 23.50 7 0 -1 52.39 15.80 7 0 1 13.50 15.40 8 0 1 50.79 19.10 8 0 1 24.90 23.20 8 0 1 11.00 15.50 8 0 1 61.79 31.20 8 0 -1 -0.20 18.00 8 0 1 29.90 19.10 8 0 -1 -0.90 13.00 9 0 -1 -16.80 16.90 9 0 1 -13.00 18.40 9 0 1 -15.30 12.80 9 0 -1 7.40 12.80 9 0 1 -22.00 11.30 9 0 -1 32.20 20.00 9 0 1 -19.50 19.50 9 0 1 -13.30 25.20 9 0 -1 -7.80 23.60 10 0 -1 31.40 21.30 10 0 1 6.60 10.60 -10 0 -1 2.60 13.20 10 0 -1 11.10 10.70 11 0 1 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3.20 0 2 -25 -1.60 5.30 1 2 -25 0.20 5.70 1 2 -25 4.10 3.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 73502 _olex2_submission_special_instructions 'No special instructions were received'