European Journal of Chemistry

Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide

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Published: Sep 30, 2014
DOI: https://doi.org/10.5155/eurjchem.5.3.394-396.1043
Keywords:
IR, NMR, Furfural, Crystal structure, Acylhydrazone, p-Chlorobenzhydrazide
Section
Research Article
Issue
Vol. 5 No. 3 (2014): September 2014
Dates
Received 2014-03-06
Accepted 2014-03-07
Published 2014-09-30


Main Article Content

Riya Datta
Department of Chemistry, Christ University, Bangalore-560029, India
Ramya Vittalacharya
Department of Chemistry, Christ University, Bangalore-560029, India
Bubbly Shivappa Gudennavar
Department of Physics, Christ University, Bangalore-560029, India

Abstract

A new compound, N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide was synthesized. Elemental analysis, IR spectrum, 1H NMR and X-ray crystal structure studies were carried out to determine the compositions and molecular structure of the compound. It crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 11.3142(4) Å, b = 7.5526(2) Å and c = 22.9030(9) Å. The crystal structure studies reveal intermolecular N-H···O hydrogen bonding interactions in the solid state.


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Datta, R.; Vittalacharya, R.; Gudennavar, B. S. Synthesis, Characterization and Crystal Structure of N’-[(E)-Furan-2-ylmethylidene]furan-2-Carbohydrazide. Eur. J. Chem. 2014, 5, 394-396.

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Supporting Agencies

Centre for Research, Christ University, Bangalore, India, Indian Institute of Technology, Madras, IISC
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