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A new potentiometric sensor based on molecularly imprinted polymer for analysis of a veterinary drug imidocarb dipropionate
Mohammed Rizk (1,*)
, Safaa Shafik Toubar (2) , Hossam Ezz El-Din Sayour (3) , Dalia Mohamed (4) , Rehab Moussa Touny (5) (1) Analytical Chemistry Department, Faculty of Pharmacy-Helwan University, Ein Helwan, 11795, Cairo, Egypt
(2) Analytical Chemistry Department, Faculty of Pharmacy-Helwan University, Ein Helwan, 11795, Cairo, Egypt
(3) Analytical Chemistry Department, Animal Health Research Institute, Dokki, 12311, Giza, Egypt
(4) Analytical Chemistry Department, Faculty of Pharmacy-Helwan University, Ein Helwan, 11795, Cairo, Egypt
(5) Quality Control Department, Chemical Industries Development Company, El-Haram, 12111, Giza, Egypt
(*) Corresponding Author
Received: 13 Jul 2013 | Revised: 11 Aug 2013 | Accepted: 11 Aug 2013 | Published: 31 Mar 2014 | Issue Date: March 2014
Abstract
A new potentiometric sensor based on molecularly imprinted polymer (MIP) was fabricated for the recognition and determination of imidocarb dipropionate. The MIP was synthesized using imidocarb as the template material, methacrylic acid as a functional monomer, and ethylene glycol dimethacrylate as a cross linking agent. The sensor showed a high selectivity and a sensitive response to the template molecule in aqueous solution. The MIP-electrode exhibited a near-Nernstian response in a wide concentration range 10-5 - 10-2 M with a lower detection limit of 2×10-6 M. The potentiometric conditions were carefully studied and all measuring parameters were optimized including pH, buffer type, plasticizer type, response time and stability. The applicability of the sensor was tested through potentiometric determination of imidocarb dipropionate in pure drug as well as in pharmaceutical formulation. The proposed method was statistically compared with a reported one showing no significant difference regarding accuracy and precision, which assured a good reliable novel sensor for imidocarb estimation.
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DOI: 10.5155/eurjchem.5.1.18-23.876
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Citations
[1]. Abbas J. Kadhem, Guillermina J. Gentile, Maria M. Fidalgo de Cortalezzi
Molecularly Imprinted Polymers (MIPs) in Sensors for Environmental and Biomedical Applications: A Review
Molecules 26(20), 6233, 2021
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[2]. Ayman H. Kamel, Somaia G. Mohammad, Nasser S. Awwad, Yomna Y. Mohammed
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International Journal of Electrochemical Science 14(2), 2085, 2019
DOI: 10.20964/2019.02.23
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New Miniaturized Disposable Screen-Printed Microchip Integrated with Molecularly Imprinted Polymer for Metronidazole Benzoate Drug Detection
Micromachines 13(12), 2107, 2022
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Validated Stability Indicating Chromatographic Methods for Quantification of Imidocarb Dipropionate; Application for the Determination of Its Residues in Bovine Meat and Milk Samples
Journal of AOAC INTERNATIONAL 103(4), 980, 2020
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[6]. Nesrine Abdelrehim El Gohary, Adel Madbouly, Rasha Mohamed El Nashar, Boris Mizaikoff
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European Polymer Journal 179, 111582, 2022
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DOI Link: https://doi.org/10.5155/eurjchem.5.1.18-23.876
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