Pyridazine and its related compounds: Part 33. Synthesis of some disperse dyes derived from 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine and their color assessment on polyester fabric

Ali AbdelHamid Deeb; Mamdoh Bahgat El‐Hossami; Ahmed Awad Mohammed Abdelgawad

doi:10.5155/eurjchem.6.1.57-62.1145

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Published: Mar 31, 2015

DOI: https://doi.org/10.5155/eurjchem.6.1.57-62.1145

Keywords:

Pyridazine, Color assessment, Dyeing properties, Fastness properties, Heterarylazo disperse dyes, Absorption spectral characteristics

Section

Research Article

Issue

Vol. 6 No. 1 (2015): March 2015

Dates

Received 2014-09-06
Accepted 2014-10-18
Published 2015-03-31

Ali AbdelHamid Deeb

Department of Chemistry, Faculty of Science, Zagazig University, Zagazig, 44519, Egypt

Mamdoh Bahgat El‐Hossami

Printing, Dyeing and Finishing Department, Faculty of Applied Arts, Helwan University, Giza, 12311, Egypt

Ahmed Awad Mohammed Abdelgawad

Medicinal and Aromatic Plants Department, Desert Research Center, Cairo, 11753, Egypt

Abstract

Active methylene compound such as ethyl acetoacetate was coupled with diazotized arylamines to give ethyl arylazoacetoacetates. When the obtained compounds refluxed with 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine in the presence of ethanol yielded 1-(4, 5-Diphenyl-1H-pyrazolo[3, 4-c]pyridazin-3-yl)-3-methyl-4-(2-phenylhydrazono)-1H-pyrazol-5(4H)-one derivatives. The dyes were applied to polyester fabric, and their absorption spectral characteristics, fastness properties and color assessment measured.

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Deeb, A. A.; El‐Hossami, M. B.; Abdelgawad, A. A. M. Pyridazine and Its Related Compounds: Part 33. Synthesis of Some Disperse Dyes Derived from 3-Hydrazinyl-4,5-Diphenyl-1H-pyrazolo[3,4-c]pyridazine and Their Color Assessment on Polyester Fabric. Eur. J. Chem. 2015, 6, 57-62.

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