European Journal of Chemistry

An efficient and facile ring closure of 2’-hydroxychalcones under irradiation of tungsten light

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Published: Jun 30, 2012
DOI: https://doi.org/10.5155/eurjchem.3.2.208-210.581
Keywords:
2-Pyrazolines, Tungsten light, Photocyclisation, Green chemistry, 2-Methoxyethanol, 2’-Hydroxychalcones
Section
Research Article
Issue
Vol. 3 No. 2 (2012): June 2012
Dates
Received 2011-12-27
Accepted 2012-02-20
Published 2012-06-30


Main Article Content

Sainath Zangade
Department of Chemistry, Madhavrao Patil Mahavidyalaya, Palam, Prabhani, Maharashtra, 431720, India
Avinash Shinde
Laboratory of Organic Synthesis, Department of Studies in Chemistry, Yeshwant Mahavidyalaya, Nanded, Maharashtra, 431602, India
Arvind Patil
Laboratory of Organic Synthesis, Department of Studies in Chemistry, Yeshwant Mahavidyalaya, Nanded, Maharashtra, 431602, India
Yeshwant Vibhute
Laboratory of Organic Synthesis, Department of Studies in Chemistry, Yeshwant Mahavidyalaya, Nanded, Maharashtra, 431602, India

Abstract

An efficient, green and facile reaction has been reported between 2’-hydroxychalcones and hydrazine hydrate in 2-methoxyethanol in presence of catalytic amount of acetic acid under irradiation of tungsten light to afford 2-pyrazolines. Present methodology presents several advantages including simple reaction procedure, no need of catalyst/special apparatus and short reaction time giving quantitative yields of product.

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Zangade, S.; Shinde, A.; Patil, A.; Vibhute, Y. An Efficient and Facile Ring Closure of 2’-Hydroxychalcones under Irradiation of Tungsten Light. Eur. J. Chem. 2012, 3, 208-210.

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