European Journal of Chemistry

The effect of dispersing agent on the dyeing of polyester fabrics with disperse dyes derived from 1,4-diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

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Published: Sep 30, 2013
DOI: https://doi.org/10.5155/eurjchem.4.3.240-244.834
Keywords:
Disperse dyes, Polyester fabrics, Fastness properties, Dispersing agent, Sodium lignin sulfonate, X-ray crystal structure determinations
Section
Research Article
Issue
Vol. 4 No. 3 (2013): September 2013
Dates
Received 2013-05-20
Accepted 2013-06-04
Published 2013-09-30


Main Article Content

Alya Al-Etaibi
Natural Science Department, College of Health Science, Public Authority for Applied Education and Training, Fayha, 72853, Kuwait
Morsy Ahmed El-Apasery
Dyeing, Printing and Textile Auxiliaries Department, Textile Research Division, National Research Centre, 12622, Dokki, Giza, Egypt
Nouria Al-Awadi
Department of Chemistry, Faculty of Science, Kuwait University, Safat, 13060, Kuwait

Abstract

1,4-Diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile (8), is synthesized by reacting ethyl cyanoacetate with ethyl amine to produce the amide 4, which when reacted with methyl propionylacetate, afforded compound 8. Compound 8 is then coupled with aromatic diazonium salts to give the corresponding arylhydrazono-1,4-diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile disperse dyes, 11a-d, whose structures were elucidated by using X-ray crystal structure determinations. A high temperature dyeing method was employed to apply these dyes for polyester fabrics. The relationship between dyeing properties and the concentration of dispersing agent present in a dye bath is evaluated.

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Al-Etaibi, A.; El-Apasery, M. A.; Al-Awadi, N. The Effect of Dispersing Agent on the Dyeing of Polyester Fabrics With Disperse Dyes Derived from 1,4-Diethyl-2,6-Dioxo-1,2,5,6-Tetrahydropyridine-3-Carbonitrile. Eur. J. Chem. 2013, 4, 240-244.

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